^Volume I.— , ILViS’mATKD BY NUMEKOUd L.VGUA VINOS. ^rt of ®Iag0=l^toU)(ng> insthuctions I FOR SliKtNO THB CHEMICAL AND Pk^LOSOPlIlCAL INS'lRUMENTS A ^ ^A1^.^,^^ «M«-»- f%4-^»-^Y f^*’ •' **' CiMtk V. ^ VA "K.^ ?r '•A*-' "V , #• (K* V\ \jry“U '^. \ ‘•■'TX^ 'u H TH^ ART OP GLASS-BLOWING, OE PLAIN INSTRUCTIONS FOR MAKING THE CHEMICAL AND PHILOSOPHICAL INSTRUMENTS WHICH ARE FORMED OF GLASS; BAROMETERS, THERMOMETERS, HYDROMETERS, Hour-Glasses, Funnels, Sypho7is, TUBE VESSELS FOR CHEMICAL EXPERIMENTS, TOYS FOR RECREATIVE PHILOSOPHY, &C. BY A FRENCH ARTIST. ILLUSTRATED BY ENGRAVINGS. CoKi TP 0,1- O) LONDON : PUBLISHED BY BUMPUS AND GRIFFIN, 3, 8KINNER-STRE ET J AND RICHARD GRIFFIN AND CO. GLASGOW : SOLD ALSO BY SULLIES, BROTHERS, EDINBURGH. 1831. POLYTE CHNIC L IBRARY. The design of the Publishers of the Polytechnic Library in ^ Series of highly-instructive Works, which the Public may be tempted to buy, because they will be cheap, be induced to redd, because they will be brief —be competent to understand, because they will be clearly writ- ten,— and be able to profit by, because they will be works OF PRACTICAL UTILITY. Every volume, therefore, will contain a complete Treatise relating to one of the useful arts or sciences, or the chemical or mechanical trades. JUST PUBLISHED, PRICE HALF-A-CROWN, VOL. I. OP THE POLYTECHNIC LIBRARY, Neail;, printed in 18mo. and bound in Cloth, containing THE ART OF GLASS-BLOWING, Or Plain Instructions for Making the CHEMICAL <5f PHILOSOPHICAL INSTRUMENTS WHICH ARE FORMED OP GLASS; Such as barometers, thermometers, hydrometers, Hour-Glasses, Funnels, Syphons, TUBE-VESSELS FOR CHEMICAL EXPERIMENTS, toys fob RECREATIVE PHILOSOPHY, &C. BY A FRENCH ARTIST. illustrated by upwards op one hundred figures Elegantly engraved on Copperplates. ’ Science, will tod ,M. Of their Apparatus' their leisure hours ’in nw willingly occupy Glass and Enamels with working deterred by the anticinated have hitherto been ginary difficulties of^the the ima- plesJmosTexSit^^ are taught herein the sim- of working Glass into ever^^var^^ I UBLISHED BY BUMPUS & GRIFFIN, SKINNER-STREET, LONDON; R. GRIFFIN AND CO. GLASGOW; AND STILLIES, BROTHERS, EDINBURGH. THE FOLLOWING WORKS, INTENDED TO FORM PART OF THE POLYTECHNIC LIBRARY, Are nearly ready fur Publication. THE DOMESTIC CHEMIST; Comprising Instructions for THE DETECTION OF ADULTERATIONS In numerous Articles employed in DOMESTIC ECONOMY - tion of this instrument consists in dividing a piece of metal, wood, or ivory, into inches and parts of inches. The divided rod is then em- ployed to measure the height of the mercury in the tube. As the rule is moveable, the opera;- tion presents no sort of difficulty ; all that is necessary is to make the zero of the scale coin- cide with the inferior level of the mercury ; the point which corresponds with the superior level of the mercury, seen in the tube, indicates the height of the barometric column. It is in this manner that the cistern barometer is graduated. But if the barometer is one of those in which the surface of the mercury is variable, such as the barometer of Gay-Lussac, it is necessary to have recourse to a different process of gra- duation. If the two branches of the instru- ment are very regular, and of equal diameter, you first measure with precision the height of the column of mercury, then divide it in the middle, and fix the scale, which must be gradu- ated in such a manner that the mark of fitteen inches corresponds exactly with the middle point. This mode of graduation serves to in- dicate merely the apparent height of the baro- metric column. If you desire that the scale should innnediately indicate the real height, you 104 THE ART OF GLASS-BLOWING. must fix the zero at the middle of the column, and then double the figure which marks each degree. When you do not wish to write the real height, you make two divisions, of which one proceeds upwards, the other downwards. You do not, in this case, double the value of each division, but in observations made with such a barometer scale you add the degree marked by the two surfaces, in order to find the real height. It is in an analogous manner that you gra- duate the gauges or short barometers which are employed to measure the density of air under the recipient of the air-pump. You take the height of the mercury in the gage, and fix at the middle of the column the zero of a double scale, of which one division proceeds upwards, the other downwards ; or, instead of this, if you choose to have only one scale, and that an ascending scale, you double the value of every degree. The zero of the barometric scale can be fixed below the inferior surface of the mercury ; but then, to have the real height, it is necessary to measure precisely the height of the mercury in the two branches of the instrument, and to deduct the smaller from the larger. Dial (or Wheel) Harometer . — The dispo- sition which should be given to this instrument is precisely the same as that of the Dial Ther- 7nometer, described in a preceding section. You make a small iron weight float on the in- ferior surface of the mercury, and fix to this weight a silk thread, which is stretched by a the art of glass-blowing. 105 counterpoise, and rolls over a very moveable pulley. The axis of this pulley carries a needle, which turns backwards or forwards according as the column of mercury augments or di- minishes. You arrrange the whole in such a manner that the extreme variations of this co- lumn cannot make the needle describe more than one circumference; with this view you give the pulley a diameter of nearly an inch. The dial barometer being rather an object of luxury than an instrument of precision, you gra- duate it by inscribing the following words, at full length, on the scale. In pi. 4, fig. 16, for example, you write. At the point a b ... c d ... e Fine Weather. ... f ••• g You write nothing at the inferior division. Graduation of the Manometer. — The graduation of this instrument consists in dividing the tube where the air is to be com- pressed, into a given number of parts of equal capacity ; but as, in general, such tubes are employed as are nearly capillary and very regu- lar, the operation is reduced to a linear division, where every degree occupies an equal space. Graduation of Thermometers. Construc- tion of Standard Thermometers. — Having 106 THE ART OF GLASS-BLOWING. constructed your instrument with a very regix- lar tube, or one which has been divided into parts of equal capacity, and having filled it with the proper liquid, according to the instructions given in a preceding section, the graduation is to be effected as follows. Procure very pure ice, break it into small pieces, and fill a vessel with it. When the ice begins to melt, plunge the thermometer into the middle of it, in such a manner that, without touching the sides of the vessel, the whole thermometer, or at least that part of it which contains the liquid, may be covered with ice. Allow the instru- ment to remain in this state until, in spite of the gradual melting of the ice, the surface of the column of liquid remains at a fixed point, and neither falls nor rises. Mark this point very carefully on the stalk of the thermometer, either with a thread or a little drop of sealing- wax, or with the trace of a diamond or a flint. This is freezing point, the zero of the cen- tigrade scale, the thirty-second degree of Fahrenheit’s scale. As for the second fixed point, it is marked during an experiment with boiling water, per- formed as follows : — You employ a vessel of tin plate sufficiently high to enclose the xvhole thermometer ; you pour into this vessel distilled water, till it is about an inch deep, and then you heat it. The vessel is surmounted by a cover pierced with two holes, one of which is intended to receive the stalk of the thermo- meter, the other to allow the steam to escape. When, on continuing the ebullition, you ob- THE ART OF GLASS-BLOWING. 107 serve that the mercury ceases to rise in the tube, you mark the point at which it has stopped, just as you marked the first point. The last mark indicates the boiling point ; the one hun- dredth degree of the centigrade scale, the two hundred and twelfth degree of Fahrenheit’s scale. You transfer to paper the distance which is found between the first point and the second point determined, and you divide this distance into one hundred equal parts, or de- grees, for the centigrade thermometer, into eighty parts for the thermometer of Reaumur, and into one hundred and eighty for that of Fahrenheit. If the tube of the instrument is very regular in the bore, the degrees should be equal in length ; if, on the contrary, you have been obliged to divide it into parts of equal capacity, you find how many of these parts or little spaces it is necessary to take to consti- tute one of the above degrees. You find this by dividing their whole number by 100, or 80, or 180, according to the degrees of the scale which you intend to make use of. Thus, if you find between the two points fixed by melt- ing ice and boiling water, three hundred divi- sions of equal capacity, it is necessary to in- clude three of these divisions in every degree of the centigrade scale. The vessel employed to take the boiling point must be of metal, and its surface should be perfectly clean and well polished, and have no rough points. If sand, or other matters, were permitted to repose on the vessel, and to 108 THE ART OF GLASS-BLOWING. form asperities, the water would enter into ebullition at an inferior temperature. This operation should, moreover, be per- formed under an atmospherical pressure, which is indicated by the barometer when the mercury stands at twenty-nine inches and a half. But as this pressure is different according to the elevation of the place of operation, and, indeed, suffers continual variations even in the same place, it follows that the temperature of boiling water is subject to continual changes, and that, in the graduation of the thermometer, it is in- dispensably necessary to take notice of the height of the barometer at the very moment that the point denoting the degree of boiling- water is fixed upon. You succeed in making the necessary corrections by the help of the following table, which is founded on the ex- periments of Sir G. Shuckburg and of the ■Gommittee of the Royal Society. £See the Table on the opposite page.] Common Thermometers. — Having, by the method which we have just described, obtained a Standard Thermometer, you may procure with facility as many ordinary thermometers as you desire. It is proper to employ the most regular tubes which you can obtain, and when the instruments are ready to be graduated, you must bring them into comparison with your standard thermometer. You place them toge- ther into a liquid of which you gradually raise the temperature, and you mark several points on the scale of the new thermometer, the inter- THE ART OF GLASS-BLOWING, 109 Height of the Barometer in Inches. Correction in When the boiling When the boiling lOOOths of the point is found point is found interval between by immersing by immersing the freezing the Instrument the Instrument and boiling points in Steam. in Water. of Water. 30.60 10' ... 30.50 9 & 30.71 30.41 8 -ti 30.50 30.29 7 1 s 30.48 30.18 6 30.37 30.07 5 V & 30.25 30.95 4 ^ i ^ 30.14 30.84 3 3 ^ 30.03 30.73 2 ^ bo 29.91 30.61 1 29.80 30.50 oj t >* ca fc. 29.69 29.58 29.39 29.28 n 2 s 3 ai 29.47 29.17 3