IP V- V. :i (Qatnell UttiuetBUy Siibrary CHEMISTRY LIBRARY _ Cornell University Library TP 10.C77 1879 ¥.2 Cyclopaedia of practical receipts and co Nhininiii iiiin mil mil inn mil mil mi „.. 3 1924 004 067 058 Cornell University Library The original of tiiis book is in tine Cornell University Library. There are no known copyright restrictions in the United States on the use of the text. http://www.archive.org/details/cu31924004067058 COOLETS CYCLOPEDIA PEACTICAL EECEIPT8 COLLATERAL INFORMATION IN THE ARTS, MANUFACTURES, PROFESSIONS, AND TRADES, INCLDDINO MEDICINE, PHARMACY, AND DOMESTIC ECONOMY; DESiaNED A3 A COMPEEHENSIVE SUPPLEMENT TO THE PHARMACOPCEU AND GENERAL BOOK OP REFERE^fCE FOR THE MANUFACTURER, TRADESMAN, AMATEUR, AND HEADS OF FAMILIES. SIXTH EDITIOIf, REVISED AND PARTLY REWRITTEN BT RICHARD V. TUSON, M.I.C., F.C.S., London and Berlin, FBOFESSOB OF OUmUSTDY AND TOXIOOLOOT IK TUB BOTAL TBTEKIHART COLLBOi; rOBMEMLT LIOnTRBB ON OIXBXIBTBT AT THB OQABINO OB033 HOSPITAL. VOL. IT. NEW YORK : D. APPLETON AND COMPANY, 1, 3, AND 6 BOND STREET. 1880. /f- /^//^ UNIVERSITYI LmRARV ^^TD/ y3/3 A CYCLOPEDIA PRACTICAL RECEIPTS, &c. VOLUME II Ink, LitllogTapli'ic. Prep. 1. Mastic (in tCHrs), 8 oz. ; shell-lnc, 12 oz. ; Venice tur- pentine, 1 oz. J melt together, add, of wax, 1 lb. I tallow, 6 oz. ; when dissolved, further odd of httrd tallow soap (in shavings), 6 oz. ; and when the whole is perfectly combined add of lampblack, 4 oz. j lastly, mix well, cool a little, and then pour it into moulds, or upon a slab, and when cold cut it into square pieces. 2. (I-asteyrie.) Dry tallow soap, mastic (in tears), and common soda (in fine powder), of c;ich 30 parts; shell-lac, 150 parts; lamp- black, 12 parts ; mix as last. Both the above are used for writing on lithographic stones. 3. (Atjtogbaphio.)— o. Take of white wax, 8 oz., and white soap, 2 to 3 oz. ; melt, and when well combined, add of lampblack, 1 oz. ; mix well, heat it strongly, and then add of shell-lac, 2 oz. ; again heat it strongly, stir well together, cool a little, and pour it out as bel'ore. With this ink lines may be drawn of the finest to the fullest class, without danger of its spreading, and the copy may be kept for J ears before being transferred. b. From wliito soap and white wax, of each 10 oz. ; mutton suet, 3 oz. ; shell-lao and mastic, of each 6 oz. ; lampblack, Si oz. ; mix as above. Both the above are used for writing on lithographic paper. When the last is em- ployed, the transfer must be made withinaweek. Ohs. The above inks are rubbed down with n little water in a small cup or saucer for use, in the same way as common water-colour cakes or Indian ink. In winter the operation should be performed near the fire, or the saucer should be placed over a basin contain- ing a little tepid water. Either a steel pen or a camel-hair pencil may be employed with the ink. See Lithoqbapht. Ink, Mark'ing. Syn. Indelible ink. Peb- MANENT I. Ot this there are several varieties, of which the following are the most valuable and commonly used : — 1. Nitrate of silver, i oz. ; hot distilled water, 7 fl. dr. ; dissolve, add of mucilage, i oz. ; previously rubbid with sap green or syrup of bui'kthorn, q. s. to colour. The linen must be first moistened with ' liquid pounce,' or ' the preparation,' as it is commonly called, and when it has again become dry, written on with a clean quill pen. The ink will bear dilution if the writing is not required very black. The POCNCE or pbefabation. A solution of carbonate of soda, 1} oz. ; in water, 1 pint, slightly coloured with a little sap green or syrnp of buckthorn, to enable the spots welted with it to be alterwards known. 2. (Without pbefabation.) Take of ni. Irate of silver, i oz. ; water, J oz. ; dissolve, add as much of the strongest liquor of am- monia as will dissolve the precipitaie formed on its first addition, then further add of mu- cilage, 11 dr., and a little sap green, syrnp of buckthorn, or finely pondered indigo, to colour. Writing oxicnted with this ink turns black on being passed over a hot Italian iron, or held near the fire. 3. Tercbloride of gold, li dr.; water, 7 fl. dr.; mucilage, 2 dr.; sap green, q. s. to colour. To be written with on a ground pre- pared with a weak solution of protochloride of tin, and dried. Dark pui*ple. 4. (Uev. J. B. Reade.) Nitrate of silver, 1 oz., tartaric acid (pure), 3 dr., ate tritu- rated together in a mortar in the dry state; a little water is then added, by which crystals of tartrate of silver are formed, and the nitric acid set free ; the latter is then saturated with liquor of ammonia, sufiicient being added to dissolve all the newly -formed tartrate of silver, avoiding unnecessary excess; lastly, a little gum and colouring matter is added. 6. (Rev. J. B. Reade.) To the last is added an ammoniacal solutitm of a salt of gold. Mr Ke.ule has used for this purpose the " purple of Cassius,' the byposulphate, tliearamonio-iodido, the ammonio-periodide of gold, but any other compound of gold which is soluble in ammonia will do as well. This ink is unacted on by nearly all those reagents which remove writing executed with solutions of the salts of silver alone, as cyanide of potassium, the chlorides of lime and soda, tec, 6. (Redwood.) Nitrate of silver and pure bitartrate of potassa, of each 1 oz. (or 4 parts), are rubbed together in a glass or Wedgwood- ware mortar, and after a short time liquor of ammonia, 4 oz. (16 parts, or q. s.), is added ; when the solution i-s complete, archil, 4 dr. (or 2 parts) ; white sugar, 6 dr. (or 3 paits) ; and powdered gum, 10 dr. (or 5 parts), are dissolved in the liquor, after which sufiicient water is added to make the whole measure exactly 6 fi. oz., when it is ready to be bottled for use. The last three are used in the same manner as No. 2. 7. (Dr Smellie.) From sulphate of iron, 1 dr. ; vermilion, 4 dr. ; boiled linseed oil, 1 57 898 INKS oz.j triturated together until perfectly «mootli. Used with type. 8. (Soubeiian.) Nitrate of copper, 3 parts ; carbonate of soda, 4 parts ; nitrate of silver, 8 parts; mix, and dissolve in liquor of am- monia, 100 parts. Used lilje No. 2. 9. (Ure.) A strong solution of chloride of platinum, with a little potassa, and sugar apd gum, to thidteu. 10. The fluid contained between the kernel and shell of the cashew nut. On linen and cotton it turns gradually black, and is very durable. This has been called anaoaedium or CASHEW-KUT INK. 11. Sulphate of manganese, 2 parts ; lamp- black, 1 part J sugar, 4 parts ; all in fine powder, and triturated to a paste with a little water. Used with types or stencil-plates; the part, when dry, being well rinsed in water. Brown. 12. Black oxide of manganese and hydrate of potassa are mixed, heated to redness in a crucible, and then triturated with an equal weight of pure white clay, and water, q. s. to pfive it due consistence. Used like the last. (Brown.) 13. (Aniline Black Marking Ink.) This ink is prepared by means of two solutions, one cf copper, the other of aniline, prepared as follows : — (1.) COPPBB SOLTTTION. 8'52 grams of crystallised chloride of copper, 10'65 grains of chlorate of soda, and 5'35 grams of chloride of ammonium are dissolved in 60 grams of water. (2.) Anilinb solution. 20 grams of hy- drochlorate of aniline are dissolved in 30 grams of distilled water, and to this are added 20 grams of solution of gum Arabic (1 part of gum to 2 of water) and 10 grams of glycerin. By mixing in the cold 4 parts of the aniline solution, with 1 part of the copper solution, a greenish liquid is obtained which can be em- ployed directly for the marking; but as this liquid can only be preserved for a few days without decomposition, it is advisable to keep the solution separately, until the ink is re- quired for use. The ink may be used either with a pen, or a stencil plate and brush ; if it do not flow freely from the pen it may be diluted with a little water without fear of weakening the in- tensity of the colour. At first the writing appears of a p.ale green colour, but after expo- sure to the air it becomes black, or it may be changed to a black colour immediately, by passing a hot iron over the back of the fabric, or heating it over the flame of a spirit lamp. As, however, a dry heat is apt to make the fibre siiturated with the ink, brittle, it is pre- ferable to hold the marked fabric over a vessel, contuining water in full ebullition ; the heat of the vapour is sufficient to determine almost immediately, the reaction by which aniline black is formed. After the steaming, the writ- ing sliould be washed in hot soapsuds, which gives the ink a fine blue shade. The ink is not acted upon by acids or alkalies, and if care be taken that the fibres are well saturated with it, there is no danger of its being removed by washing. (' Dingler's Journal.') 14. In addition to the above formulse, the following of M. Henry may he worthy of at- tention in large establishments where economy is an object z-^Take 1 oz. of iron filings and 3 oz. of vinegar, or diluted acetic acid. Mix the filings with half the vinegar, and agitate •■ them continually till the mixture becomes thick, then add the rest of the vinegar and 1 oz. of water. Apply heat to assist the action, and when the iron is dissolved, add 3 oz. of sulphate of iron, and 1 oz. of gum previously dissolved in 4 oz. of water; and mix the whole with a gentle heat. To be used with brush and stencil plates. 15. (Crimson Marking Ink.) Dissolve 1 oz. of nitrate of silver, and IJ oz. of carbonate of soda in crystals, separately in distilled water, mix the solutions, collect and wash the preci- pitate on a filter, introduce the washed pre- cipitate still moist into a Wedgwood mortar, and add to it tartaric acid 2 dr. and 40 gr., rubbing together till effervescence has ceased ; dissolve carmine 6 grains, in liquor ammonia (882) 6 oz., and add to it tne tartrate of silver, then mix in white sugar, 6 dr., and powdered gum Arabic, 10 dr., and add as much distilled water as will make 6 oz. (' Fharm. Journal.') Obs. The products of the first two of the above formulae constitute the marking ink of the shops. They have, however, no claim to the title of ' INDELIBLE INK,' " which no art can extract without injuring the fabric " — as is generally represented. On the contrary, they may be discharged with almost as much facility as common iron-moulds. This may be easily and cheaply effected hy means of ammonia, cyanide of potassium, the chlorides of lime and soda, and some of the hyposul- phites, without in the least injuring the tex- ture of the fabric to which they may be applied. The only precaution required is that of rinsing the part in clean water imme- diately after the operation. The 'markingink without preparation' is more easily extracted than that ' with pi-eparatiou.' The" former has also the disadvantage of not keeping so well as the latter, and of depositing a portion of fulminating silver, under some circumstances, which renders its use dangerous. The thinner inks, when intended to be used with type or plates, are thickened by adding a little more gum, or some sugar. Ink, Mark'ing. S^/n. Paokbe's ink. Ink bottoms. Used by packer's for marking bales, boxes, &o. Ink, Perpet'ual, Frep. 1. Pitch, 3 lbs.; melt over the fire, and add of lampblack, | lb. ; mix well. 2. Trinidad asphaltum and oil of turpentine, equal parts. Used in a melted state to fill in INK POWDERS— INOCULATION 899 the Icttfrs on tombstones, mnrblts, ic. With- out actunl violence, it will endure aa long as the stone itself. Ink, Print'or's. See Pbintiito Ink. Ink, Pur'ple. 1. A strong decoction of log- wood, to which a little alum or chloride of tin lias been added, 2. (Normandy.) To 12 lbs. of Campenchy wood add as many giiUons of boiling water, pour the solution through a funnel with a strainer made of coarse flannel, or 1 lb. of hy- drate, or acetate of deutoxlde of copper finely powdered (having at the bottom of the funnel a piece of sponge) ; then add immediately 14 lbs. of almn, and for every 340 galls, of liquid add 80 lbs. of gum Arabic or gum Senegal. Let these remain for three or four days and a beautiful pm-ple colour will be produced. Ink, Ked. Prep. 1. Brazil wood (ground), 4 oz. ; white-wine vinegar (hot), li pint; digest in glass or a well-tinned copper or ena- mel sanccp.in, until tho next day, then gently simmer for half an hour, adding towiirds the end gum Arabic and alum, of each \ oz, 2. Ground Brazil wood, 10 oz. ; white vinegar, 10 pints; macerate for 4 or 5 days; then boil as before to one half, and add of roach alum, 4} oz. ; gum, 5 oz. ; and when dissolved, bottle for use. 3. As the last, but using water or beer instead of vinegar. 4. Cochineal (iu powder), 1 oz. ; hot water, ) pint ; digest, and when quite cold, add of spirit of hartshorn, i pint (or liquor of am- monia, 1 oz., diluted with 3 or 4 oz. of water) ; macerate for u few days longer, and then decant the clear. Very fine. 5. (Buchner.) Pure carmine, 20 gr.; liquor of ammonia, 3 fl. oz. ; dissolve, then add of powdered gum, 18 gr. Half a drachm of pow- dered drop lake may be substituted for the carmine where expense is an object. Colour superb. 6. (Henzeler.) Brazil wood, 2 oz. ; alum and cream of tartar, of each j oz. ; rain water, 16 fl. oz. ; boil to one half, strain, add of gum (dissolved), J oz. ; and when cold, f urtlier add a tincture made by digesting powdered cochi- neal, 1^ dr., in rectified spirit, li fl. oz. 7. (liedwood.) Guarancine and liquor of ammonia, of each 1 oz. ; distilled water (cold), 1 pint; Iritur.ite together in a mortar, filter, and dissolve ia the solution, gum Arabic \ oz. Ink, Se'pia. Sie Sepia. Ink, Sil'ver. From silver leaf or powdered silver, as gold ink. Ink. Sympathet'io. Syn. Diplomatio ink. Invisible i. Fluids which, when used for writing, remain invisible until the paper is heated, or acted on by some other chemical agent. Sympathetic inks have been frequently employed as the instruments of secret corre- spondence, and have often escaped detection; but by he.iting the paper befoi-e the fire until it begins to grow discoloured by the heat, the whole of them may be rendered visible. The following are the most common and amusing sympathetic inks: — 1. Sulphate of copper and sal ammoniac, equal parts, dissolved in water; writes colourless, but turns yellow when heated. — 2. Onion juice ; like the last. — 3. A weak infusion of galls ; turus black when moistened with weak copperas water : — 4. A weak solution of sulphate of iron j turns BLUE when moistened with a weak solution of prussi.ite of potas.sa, and black when moist- ened with infusion uf galls. — 5. The diluted solutioHs of nitrate of silver and of tcrchloride of gold; become respectively dabk BBOWS and PCEPLB when exposed to the sunlight. — 6. Aqua fortis, spirits of salts, oil of vitriol, common salt, or saltpetre, dissolved in a large quantity of water; turus ybllovt or brown when heated. — 7. Solution of chloride or nitm- muriate of cobalt ; turns obekh when heated, and disappears a^'ain on cooling. If tho salt is pure, the marks turn blue. — 8. Solution of acetate of cobalt, to which a little nitre has been added ; becomes eosb colouiied when heated, and disappears on cooling. — 9. A weak solution of the mixed chlorides of cobalt ond nickel ; turns QUEEN. The last three are about the best of our sympathetic inks. — 10. Solution of acetate of lead; turns bbownish- black when exposed to the fumes of sul- phuretted hydrogen. — H. A weak solution of nitrate of mercury ; turned black hy heat and sulphuretted fumes. — 12. Itice water or decoction of starch ; turned blue by a solu- tion of iodine in weak spirit, and by the fumes of iodine, if the paper is first slightly moistened by exposun^ to steaoi or damp uir. Ink, Vi'olet. The same as pukple ink, but weaker. Ink, Yel'low, 1. From gamboge (in coarse powder), 1 oz. ; hot water, 5 oz. ; dissolve, and when cold, add of spirit, J oz. 2. Boil French berries, i lb., and alum, 1 oz., iu rain water, 1 quart, for half an hour, or longer, then strain and dissolve in the hot liquor gum Arabic, 1 oz. Ink, Zinc Labels, to write on. >'.y». HoK- TICULTDBAL INK. 1. Dissolve 100 gr. of tetrachloride of platinum in a pint of water. A little mucilage and lamp black may be added. 2. Sal ammoniac 1 dr. ; verdigris, 1 dr. ; lampblack, i dr. ; water, 10 dr.; mix. INK POWDERS. Prep. 1. Aleppo galls, 4 oz. ; sulphate of iron, IJ oz. ; gum Arabic, 1 oz. ; lump sugar, J oz. ; (all quite dry and in powder) ; mix, and divide into 3 packets. A pint of boiling water poured over one of them produces, in a few hours, a piut of excellent ink. 2. Aleppo galls, 3 lbs.; copperas, 1 lb. ; gum Arabic, i lb. ; white sugar, \ lb. ; all in pow- der ; mix, and divide into two-ounce packets, to be used as the last. Ink powders are very useful in travelling. INK STAINS, to remove. See Spots. INOCULA'TION. Syn. Inocdlatio, L. In medicine and surc/ery, the application of poi- 900 INOSINIC ACID— INTEMPERANCE Eonous or infections matter to any part of the body for the purpo-e of propagiiting a milder form of disease, and thus preventing or les- sening the virulence of future attacks. In this country the term is generally restricted to the artifii'ial propagation of smallpox,' See Vaccination, INOSIiJ'IC ACID. An acid said by Liebig tn exist in the juice of the flesh of animals, after it has deposited its kreatine. IN'OSITE. A species of unfermentahle sugar, discovered by Scherer in the juice of flesh. It forms beautiful crystals, IN'SECTS. Sy». Insecta, L, A class of invertebrate animals belonging to the sub- kingdom Annuloso. The true insect is defined as an articulated animal, having six legs, 2 antennae, 2 compound eyes; a small brain at the anterii>r extremity of a doube medullary cord ; its circulation is effected by a pulsating dorsal vessel, provided with numerous valves; its respiration by tracheae, which foim 2 lateral trunk?, and ramify through the body. The generiition of insects is oviparous. There are two distinct sexes. The adult state is attained through a series of metamorphoses. In general, every insect possesses 2 pairs of wings; the trunk in the adult animal is usually composed of 3 chief parts — the head, thorax, and abdomen. The trunk of an insect may also be described as consisting of 13 seg- ments, of which 1 constitutes the head, 3 constitute the thorax, and 9 the abdomen. Insects are arranged in the following orders: — 1. Hymenoptera, including bees, wasps, ich- neumon-flies, &c. — 2. Coleoptera, including all those kinds commonly called beetles. — 3. Nenroptera, dia'.?>in-flies, ephemerae, white ants, &c. — 4. Strepsijitera, the stylups, &c. — 5. Lepido]itera, the butterflies and moths. — 6. Diptera, the house-fly and other 2-winged insects. — 7. Orthopteia, crickets, grasshoppers, locusts, earwigs, &c. — 8. Hemiptera, bugs, frog-hoppers, aphides, &c. — 9. Aptej'a, fleas, &c. There are several animals belonging to the classes mteiopoda and arachnida which are commonly but erroneously called 'insects.* Of these the centipedes, spiders, and acarides, or mites, are well-known examples. Several useful products, as silk, wax, honkx, cochi- neal, lac, canthakides, &c., are supplied by insects. The class includes numerous creatures which are extremely destructive, and others which are regarded as domestic pests. In the articles devoted to tliese offensive insects various methods of exterminating them are noticed. A powder for destroying insects has recently bien introduced into this country, and has been found peculiarly efficacious. This powder, which is known under various names (iNSEOTS-DESIEOYINa POWDIK, IHJ- mont's INSECTICIDE, &c.), is produced by the Pyrethrum roseum Cancaslcum, a composite flower growincj wild in the Caucasus. The' central or tubular florets of the disc are alone employed, and when ground, furnish the powder of commerce. This powder, though so destructive to insect life, has no injurious effect upon man or domestic animals. See AcAKi, Ant, Bee, Bug, Bites and Stings, Canthaeides, Cochineal, Lao, Pedicitii, Silk, &c. IMSECT'ICIDE POWDER. See Insects. INTEM'PEKANCE. Under this head we refer to habitual indulgence in the use of spirituous or fermented liquors,whether accom- panied or not by fits of intoxication or drunk- enness. The pernicious influence of intoxicating liquors upon individuals and upon society has been so often and ably exposed by the clergy, judges, and magistrates, and by philanthro- pists of every kind, that it would be folly to do more than refer to it here. Fully one half of the dark or disreputable deeds of those who fill our gaols, and fully an equal proportion of the poverty and wretchedness which pauperises our population and crowds our workhouses, are traceable to this damning vice of the Anglo- Saxon race — intemperance. To cure habitual dbunkbsness various means have been proposed, most of which are more ingenious than useful. The following, however, deserves respectful notice: — Dr Kain, an eminent American physician, recommends tiirtar emetic, given in alterative and slightly nauseating doses, for the cure of habitual drunkenness. " Possessing," he ob- serves, " no positive taste itself, it communi- cates a disgusting quality to those fluids in which it is dissolved. These liquors, with the addition of a very small quantity of emetic tartar, instead of relieving, increase the sen- sation of loathing of food, and quickly pro- duce in the patient an indomitable repug- nance to the vehicle of its administration. My method of prescribing it has varied according to the habits, age, and constitution of the patient. A convenient preparation of the medicine is 8 gr., dissolved in 4 oz. of boiling water ; J an oz. (say a table-spoonful) of the solution to be pnt into half a pint, pint, or quart of the patient's favorite liquor, and to be taken daily in divided portions. If vomit- ing and purging ensue" (which is seldom the case), " I should direct laudanum to allay the irritation, and diminish the dose. In some (■ases the change suddenly produced in the patient's habits has brought on considerable lassitude and debility, which, however, were of short duration. In a majority of cases no other effect has been perceptible than slight nausea, some diarrhoea, and a gradual but very uniform distaste to the menstruum." Dr W. Marcet has described the more or less disordered state of the brain, nerves, muscles, and stomach, brought on by the continual use of alcohol, even without in- toxication being produced. The symptoms of this state, which he terms cheonio alco- holism, are quite distinct from those of de- LIBIUM TEEMENS, which is au acute and vio- INTERMITTENT FEVER— INULIN 901 lent diaturbance of the nervous system. From oxporimeiits on a large number of patients, l>r Marcet has arrived at tlie importHnt con- clusion, that oxide of zinc is the true antidote in cases of slow alcoholic poisouing. It sefms to act ai u strong tonic on the nerves, being at the same time a powerful sedative and anli- Bpasniodic' The symptoms of actual intoxication, or the disordered condition of tlie intellectual func- tions and volition, produced by taking exces- sive quantities of alcoholic liquors, need not be described. Among the remedies employed to remove the 'tit of drunkenness,' the prepii rations of ammonia, and the vegetitble acids, are the most common and important. About 2 or 3 fl. dr. of arom.itic spirits of ammonia (spirits of sal volatile), or a like quantity of solution of acetate of ammonia (niindererus spirit), mixed with a wine-glassful of water, will in general neutralise or preatly lessen the action of in- toxicating liquors. In some cases these fluids produced vomiting, which is, however, a good symptom, as nothing tends to restore an ine- briated person so soon as the removal of the liquor from the stomach. Hence tickling the fauces with the finger or a (eatlier, until sick- ness comes on, is a method very commonly adopted by drunkards to restore themselves to a sober state. Tlie use of aromatic water of ammonia was first suggested by Mr Bromly. With a like intention, some persons have recourse to soda water, wliicli acts by the free carbonic acid it contains, and also as a dilueut and, from its coldness, as a tonic on the coats of the stomach. The carbonates and bicarbon- ates of soda and potassa are also favourite re- medies with habitual drunkards. Among the vegetable acids, acetic acid is the one that appears to possess the greatest power of re- moving intoxication ; and after this follow the citric, tartaric, malie, and carbonic acids. These substances are commonly taken by sol- diers before going to parade. The usual dose of vinegar is a small teacupful. lu the West Indies lime juice and lemon juice are bad re- course to. Both these juices act from the citric acid they contain. The use of bitter almonds, as a means of lesseninc: or retarding the effects of fermented liquors was known to antiquity, and is still common among heavy drinkers at the present day. Even small doses of medicinal prussic acid have been foolishly taken with a like intention. See Abstinence, Alcohol, bffects of, Delieiusi tkemens, &c. INTERMIT'TENT FEVER. St/n. AG0B. A disease consisting of paroxysms or periods of fever with perfect intermissions or periods without fever. Marsh miasmata, or the effluvia arising from stagnant water or marshy ground, when acted upon by beat, are the most frequent causes of this malady. For ' ■ On Cliroaic AlcoUolic latoxicatioa." By W. Mucet, U.O., Ib6:!. the prevention of ague in situations where it prevails endemically, small doses of quinine should be taken t«o or three times a day, and flannel clothing should be constantly worn. Symp. Each febrile paroxysm is of three periods or stages — the cold, the hot, and the sweating stage, and these occur in regular suc- cession. The cold stage commences with great languor and aversion to motion ; a sense of coldness down the back soon follows ; then the extremities become cold, the tingi-rs shrunken, and the nails blue; the skin assumes that peculiar conditii>n which is commonly known as 'goose-skin;' the patient shivers, his ttith chatter, and he is glad to draw close to the tire or envelop himself in blankets. After this state of things has continued for a greater or less time, the heat of the surface begins to return, the patient has flushinps and becomes warmer and warmer, and ultimately the whole surface isof adry burrdngbeat; intense thirst, restlessness, severe headache, and sometimes delirium, charaeteri-e this second orhotsta;;e. After this staLce has continued for some time, another change comes over the patient ; mois- ture appears on the face and forehead, the harsh and hot =kin becomes soft, and at last a copious sweat breaks out over the whole sur- face. This is the third orsweatin:.' stage, and after it has passed, the several functions of tiio system return to their ordinary condition. The paroxism may return daily {QroTiDiAN aoue); or every other day (tbktian a.) ; or every fourth day, including that of the first attack (qfautan a.). IVeatm. During the cold stage everything should he done to bring on the hoc ; tlie patient should be placed in a warm bed, with warm pans or bottles of water; he may be allowed the fi'ce use of warm diluent drinks. In the liot stage the opposite course should be adopted; the coverings must be diminished and lemonade and other cooling drink adminis- tered. In the sweating stage there is no occasion for any treatment beyond care to avoid checking the perspiration by premature exposure. During the intermission the dis- ease must be fought with the tonics, Peruvian bark, or its chief alkaloid, quinine. The most effective form of this remedy is the sulphate, which may be given in doses of fiom 2 to 4 jir. every three hours, the rlo-e being greater for a quartan than tor a quotidian. See Aqce-caee, Fbvee, &c. INTOXICA'TIOS. See Intemperance. IN'UIiIN. Syn. IxuLiNK, Alantine, Dah- LINE. A peculiar starch-like substance, first obtained by Rose from the root of Inula Se- lenium or elecampane. It has been found in several other vegetables. Prep. From the rasped root, by the same method that is adopted (or arrow-root or potato farina ; or by boiling the sliced root in 7 or 8 times its weight of water, and after filtration. 902 lODATE— IODINE whilst hot, allowing tlie decoction to repose for a short time. Prop., dj'c. Only very slightly soluble in cold water ; very soluble in boiling water, but is nearly all deposited as the solution cools; it is precipitated by alcohol. In ulin is distinguished from starch by giving a yellow or yellowish-brown instead of a blue colour with iodine; in the decoction not being precipitated by either acetate of lead or infu- sion of galls ; and by the precipitate formed in the cold decoction by an infusion of gall-nuts not disappearing until the liquid is heated to above 212°, whilst tlie precipitate from starch redissolves at 122° Pahr. It appears to be a substance intermediate between starch and gum. I'ODATE'. Spn. lOBAS, L. A salt of iodic acid. The iodates closely resemble the chlo- rates of the corresponding metals. They are recognised by the development of free iodine when their solutions are treated with reducing agents; thus, sulphuretted hydrogen passed into a solution of iodate of potassium reduces this salt to an iodide, iodine being liberated and sulphuric acid and water formed. They deflagrate like the chlorates when heated with combustibles. They are all of sparing solubility, and mimy are quite insoluble in water. They may be made by adding iodine to soluble hy- drates or carbonates, and crystallising the sparingly soluble iodate from the very so- luble iodide. See Iodic acid, Iodine, and Potassium. lODHY'DKIC ACID. See Htdeiodic acid. lOD'XCACID. HIO3. Si/n. Aoidttm iodi- CUM, L. Prep. 1. Iodate of sodium is dissolved in sulphuric acid in considerable excess, the solu- tion boiled for 15 minutes, and then set aside to crystalWse. 2. Decompose iodate of barium by dilute sulphuric acid, 3. (Boursen.) Iodine, 1 part; nitric acid (sp. gr. 1'5), 40 parts; mix, keep them at nearly the boiling temperature for several hours, or until the iodine is dissolved, then evaporate to dryness, and leave the residuum in the open air at a temperature of about 59° Fahr. ; when, by attracting moi^ture, it has acquired the consistence of a syrup, put it into a place where the temperature is higher and the air drier, when in a few days very fine white crystals of a rhomboidal shape will form. <■ Prep., Sfc. Iodic acid is n crystalline solid, white or yellowish-white; it is decomposed into oxygen and iodine by a heat of about 450° to 500° Fahr — a property of which we avail oui'selves for the conversion of the salts of this acid (iodates) into iodiries. It is very soluble in water, and is rapidly decomposed wlien heated with inflammable bodies. Iodic acid is used as a test for morphia and sulphur- ous acid. It has been employed as a tonic, stimulant, and alterative, in catarrhal hoarse- ness, strumous cases, incipient phthisis, &o. — Dose, 3 to 6 gr. Vest. When iodic acid is mixed with an equal quantity of an alkaloid (preferably qui- nine), on a capsule or watch-glass, and a drop or two of water added, several distinct explo- sions occur, accompanied by the copioiis evo- lution of gas. No other substance exhibits a similar reaction. See lODATE. I'ODIDE. Sl/n. lODtlBET*, Htdbiodate*, lODIDUM, lODrKETUM, HtDEIODAS, L. A compound of iodine with a metal or other basic radical. The iodides belong to the same class of bodies as the bromides and chlorides, and may be, for the most part, made in the same manner. All the principal iodides are noticed under the names of their respective bases. See Iodine, &c. rODINE. I. Syn. Iodum, B.P.; Iodinium (Ph. L. & D.), lODlNETJM (Ph. E.), L. ; Iode, Fr. ; loD, Ger. An elementary substance accidentally discovered in 1812, by De Cour- tois, a saltpetre manufacturer at Paris. It was first examined and described by M. Clement, in 1813, and its precise nature was soon after- wards determined by Sir H. Davy and M. Gay-Lussac. In 1819, some six years after its discovery, iodine was first employed in pharmacy. The merit of the introduction of this powerful curative agent into medicine is due to Dr Ooindet, a physician of Geneva, who in that year commenced a series of ex- periments upon it as a remedy for bronchoeelo or goitre. It is found in each of the three kingdoms of nature, but exists in greatest abundance in the vegetable family Alga (Seaweeds). Prep, Iodine is principally manufactured in the neighbourhood of Ghisgow, from the mother-waters of kelp known as iodine lye. 1. Kelp, the half vitrified ashes of seaweed, is exhausted with water, and the solution filtered; the liquid is then concentrated by evaporation until it is reduced to a very small volume, the chloride of sodium, carbonate of sodium, chlo- ride of potassium, and othersalts,beingremoved as they successively assume the crystalline form ; oil of vitriol is now added, in excess, to the residual dark-brown mothei -liquor (iodine- lye), and the evolved gases are either kindled or allowed to escape by a flue; the liquid, after standing some time, is decanted or filtered, heated to about 140° Fahr., and mixed with as much binoxide of manganese as there was oil of vitriol employed; the whole is then introduced into a cylindrical leaden still, furnished with a very short head and connected with 2 or 3 large globular glass receivers, and heat is applied, when fumes of iodine are evolved and condensed in the re- ceivers. During the distillation very great care is taken to watch the process, and prevent the nook of the still becoming choked with condensed iodine. For this purpose the head of the still is usually furnished with a movablo stopper, by which the process may be watched. IODINE 903 and addUiont of mnn^nncsc or aulphnric acid made, if required. To render tlie product pure, it should be pressed between blutling paper, and tlien resublimed in gluss or stone- ware. 2. A solution of sulphate of copper, 4 parts, and protosulphate of iron, 9 parts, are added to the mother-liquid of the soda-works, as long as a white precipitate is thrown down ; this preeipitiite (iodide of copper) is collected, dried, and mixed with its own weight of finely powdered black oxide of manganese, and dis- tilled by a strong heat in a retort, wlien dry iodine pu«ses over. By the addition of sul- phuric acid with the manganese, a le^s heat is required, but the [iroduct is wet with water, like that of the lust formula. 3. The residual liquor of the manufacture of soap from kelp (or other iodine Ive), of the sp. gr. of 1-374, is heated to 236° Fahr., vyith sulphuric acid diluted with half its weight of water, after which the liquor is allowed to cool, and is e tlier decanted or filtered; to every 12 fl. oz. of the filtrate 1000 gr. of black oxide of manganese, in powder, are added; the mixture is put into a glass globe or matrass with a wide neck, over which is inverted another glass globe, and heat is ap- plied by means of a charcoal chauffa-, when iodine sublimes very copiously, and condenses in the upper vessel j as soon as the latter is warm, it is replaced by another, and the two globes are thus applied in succession, as long as violet fumes are evolved. The iodine is washed out of the globes with a little cold water. A thin disc of wood, having a hole in its centre, is placed over the shoulder of the nnitrass, to prevent the heat from acting on the globular receiver. On the large scale, a leaden still, as before described, may be em- ployed, and receivers of either stoneware or glass ; and the addition of the sulphuric acid is made in a basin or trough of stoneware or xvood. Prod. 12 oz. yifld 80 to 100 gr. 4. Another method of preparing iodine has been patented by a Mr Stanford, which con- sists of compressing the wet weed, drying in an oven, and distilling at a high temperature. The inventor claims that double the usual amount of iodine is obtained besides other useful products. 5. Considerable quantities of iodine are now obtained from the mother-liquor of Chilian saltpetre or nitre (nitrate of soda). In 1873, a nitre refinery in Peru which separates the iodine in combination with copper, as cuprous iodide, by means of bisulphide of soda and sulphate of copper, produ( od 15,000 kilos of cupi-ous iodide, corresponding to bOOO kilos of iodine. Other methods of obtaining it from Chilian nitre consist in treating the mother-liquors left after the salt has been crystallised out with sulphurous acid, until the separated iodine l)CL;in8 to redissolve. Nitrous acid has also beeu substituted tor sulphurous. The iodine so procured is purified by snblimation, whilst that which remains in the residual saline matter is removed by treatment « ith chlorine. Prop. Iodine is usually met with under the form of semi-crystalline lumps having a sen i- metallic lustre, or in micaceous, friable scales, somewhat resembling plumbago or gunpowder. By carefully conducted sublimation, or by the slow evaporation of its solution in hydriodic acid, it may be obtained in rhombic plates an inch long. It has a greyish-black colour, a hot acrid taste, and a di-agreeable odonr not much unlike that of chlorine. It fusis at -25^ into a deep-brown liquid, volatilises slowly at ordinary temperatures, boils at 347 , forn.ing a maguiticent violet-coloured vapour, when mixed with water it rapidly lises with the steam at 212° Fahr. It dissolves in about 7000 parts of water, and freely in alcohol, ether, solutions of the iodides, liquiil was known and commonly employed, where strength was required, nearly 3000 yenrs ago. Kust of iron and scales of iron were used as medicines at a period equiilly remote. Sources. Iron in a metallic state (native iron) is of very rare occurrence; but it invariably enters into the composition of meteorites. Combined with oxygen and other elements, as iron ores, it occurs in nearly eviry part of the eartli. These ores may be divided into the oxides and the carbonates. The oxides may be again divided into four distinct classes, viz. — (1) Magnetic iron ore, consisting ofSlJ prot- oxide and 69§ sesquioxide, with an insignifi- cant proportion of silica ; (2) specular iron, or iron glance, composed of the sesquioxide, with a small admixture of ma)i:netic oxide ; (3) red hiomatite, consisting of the sesquioxide nearly ill a state uf purity; and (4) brown lieemntite, the hyclrated sesquioxide of iron. Tlie car- bonutes are principally two, viz. — (5) spathose iron, tlie protocarbonate of iron in a sparry condition, and (6) cliiy ironstone or black band ironstone, wliich consists of the protocar- bonates associated with clay and carbonaceous matter. Swedish iron is made almost entirely from No. 1, wlilch occurs in massive beds at Aren- dahl and Duniiemora, in Sweden. This iron is (if great purity, being perfectly free from sulphur and phosphorus. The titaniferous iron sand found at Taruniiki, in New Zealand, con- sists almost entirely of No. 1 and the metal titaniuin. No. 2 found principally in the islsnd of Elba, in the form of rhombohedral crystals. The micaceous iron ore found in small quantities in Wales and Lancasliire has nearly the same composition, but crystallises in brilliant plates. No. 3 occurs in radiated fibrous masses in different parts of the world. It is found in hirge quantities in Wales and Lan- casliire, some of the specimens from tlie latter locality containing nearly 99-!} "^ '''^ sesqui- oxide. It makes excellent iron. No. 4 occurs in reddish-brown masses of a botryoidal form. It is a valuable ore, and is found in England, Wales, and Scotland. No. 5 is found chiefly at Siegen, in Prussia. No. 6 is the principal ore of the Staffordshire and Scotch iron districts, where it occurs in great abundance, associated with the fuel and the flux required for smelt- ing it. Iron is contained in plants, and forms an essential component of the blood of the higher animals. ' Prep., Sec. Iron is only prepai-ed on the large scale, and an account of tlie manufacture would be out of plice here. Those requiring detailed information must consult the elabo- rate works of Peiiy, Hunt, Fairbairn, Phillips, and other metallurgists. Pure iron may be prepared by introducing fine iron wire, cut small, 4 parts, and black oxide of iron, 1 part, into a Hessian crucible ; covering with a mixture of white sand, lime, and carbonate of potassium (in the proportions used for glass- making); and, after applying a closely fitting cover, exposing the crucible to a very high degree of heat. A button of pure metal is thus obtained, the traces of carbon and silicon present in the wire having been removed by the oxygen of tlie bkck oxiile. Prop., S(c.- The properties and uses of iron are too well known to require description. Its applications are almost universal. It is remarliably ductile, and possesses great tena- city, but is less malleable than many of the other metals. Its sp. gr. is 7"8ii. It is the hardest of all the malleable and ductile metals, and when combined with carbon (steel) admits of being tempered to almost any degree of hardness or elasticity. In dry air it does not oxidise at common temperatures ; but at a red heat it soon becomes covered with >• scaly coating of black oxide, ami at an intense white heat burns brilliantly with the produc- tion of the same substance. Pure water, free from air or carbonic acid, does not tarnish the surface of polislied iron, but the combined action of air and moisture, especially when u little acid vapour is present, causes its surface to be soon covered with rust, which is hydrated sesquioxide of ii on (ferric hydrate). Neiirlyall acids att'iek iron ; dilute sulphuric and hydro- chloric acid do so with considerable eneri;y and the evolution of hydrogen gas. At a red heat iron decomposes water rapidly, liydr>>geu being evolved, and the black oxide of iron formed. Iron is magnetic up to a dull-red iieat, at which point it loses all traces of that property. It melts at about 3300° Pahr. With oxygen, chlorine, iodine, tlie acids, &c., it forms numerous important compounds. As a remedial agent, when properly exhibited, iron acts as a genial stimulant and tonic, and generally proves beneficial in cases of chronic debility, unaccompanied with orgnnic conges- tion or intl.immation. The carbonate (ferrous carbonate), as it exists in mineral waters, held in solution by carbonic acid in excess, appears to be the form most congenial to the human body ; and from its state of dilution is rapidly absorbed by the lacteals, and speedily imparts a ruddy hue to the wan countenance. Iron is undoubtedly one of the most valuable articles of the materia medica, and appeirs from tlio antiquity of its introduction into medicine, and the number of its preparations, to have been deservedly appreciated. Tests. Iron forms two classes of salts, namely, ferrous or proto salts, in which iron exhibits a power of combining with two atoms of any monad element, and the ferric or persalts in which iron has a capacity of uniting with three atoms of any monad element. The ferrous or proto salts have gei-crally a greenish colour, but yield nearly colourless 903 IRON solutions, except when concentrated. Their solutions are Itnown by the following re- actions : — They are not precipitated by hydro- sulphuric acid when acid, and but incom- pletely when neutral. Sulphide of ammonium produces a black precipitate, becoming brown on exposure to the air, insoluble in alkalies, but easily soluble in the mineral acids. Am- monia and potassa give a greenish-white precipitate, gradually becoming green and then brown in the air. This precipitate occasionally is of a bluish-black if excess of potassa is used. The presence of ammoniacal salts interferes with the action of these tests. Ferrocyanide of potassium gives a nearly white precipitate, becoming gradually blue in the air, and im- mediately so on the addition of a little weak nitric acid or chlorine water. Perricyanide of potassium produces a rich deep-blue precipi- tate, insoluble in hydrochloric acid. In highly dilute solutions the effect is only a deep bluish- green coloration. Phosphate of sodium pro- duces a white precipitate, which after a time becomes green. The ferric salts, which are also called the sequi or persalts of iron, have for the most part a reddish-yellow colour, yielding deep- coloured solutions, which exhibit the following reactions : — They redden litmus paper. Hy- drosulphuric acid in acid solutions reduces ferric to ferrous salt«, giving a white or yellow precipitate of sulphur only. In alkaline solu- tions it yields a blackish precipitate, consisting of sulphur and ferrous sulphide. Sulphide of ammonium gives similar reaction. Ammonia and potassa produce bulky reddish-brown pre cipitates insoluble in excess. Ferrocyanide of potassium gives a rich blue precipitate, in soluble in hydrochloric acid, and readily de^ composed by potassa. Ferricyanide of potas- sium deepens the colour, but does not give a blue precipitate, as it does with ferrous salts (proto salts). Sulphocyanide of potassium gives an intense ruby-red colour to neutral or acid solutions. Tincture and infusion of galls strike a black colour. Phosphate of sodium gives a white precipitate, which becomes brown, and finally dissolves on the addition of ammonia. Estim. The iron may be thrown down in the state of ferric hydrate or hydrated sesqui- oxide, washed, dried, ignited, and weighed. The weight, in grains, multiplied by "7, in- dicates the weight of metallic iron. Fifty gr. of the ore are reduced to powder, dissolved in aqua regia, with the aid of heat, and the solution filtered in order to separate the silica and a little alumina which sometimes is left in an insoluble state; an excess of am- monia is then added to the filtered liquor, which produces a reddish-brown precipitate of ferric hydrate mixed with alumina which is collected on a filter, washed, and boiled w'ith a solution of potassa, in order to dissolve the alumina ; the whole is next thrown upon a filter, washed, dried, carefully ignited, and weighed. The above is well adapted to de- termine the quantity of iron in clay iron- stone, the most common ferruginous ore in England. The sulphur in cast and wrought iron, and steel, may be estimated by the following process, invented by M. Koppmayer : — 10 grammes of iron, finely produced and sifted, are introduced into a bottle holding from \ to -Jrd litre. The stopper has three holes. Through one of these passes a funnel with a ground- glass tap, its neck reaching to the bottom of the bottle. Through the second passes the tube at right angles, fitted with a tap and reaching also to the bottom of the bottle. Through the third hole passes a delivery tube, connecting the bottle to the condensing apparatus. This latter consists of a series of bulbs ar- ranged like a staircase, so as to permit the gas to come into the greatest possible contact with the standard solution of ioJine in iodide of potassium, with which the condenseris filled, this solution ought not to be exposed to light. When the apparatus is arranged as above, the atmospheric air is fir-^t driven out of the bottle by means of a current of hydrogen gas, introduced by the tnbe bent at right angles. When it is considered that the air is entirely expelled, the tap of this tube is closed. The funnel is now filled with hydrochloric acid, its tap is opened, and by means of the application of heat the acid is allowed to run down upon the iron without allowing any common air to enter. Hydrogen and sulphuretted hydrogen are formed which pass into the condenser. Acid is thus added until all disengagement of gas ceases. The bottle is then heated till its contents boil, a little water having been first added by means of the funnel. After these operations, hydrogen is allowed to enter anew to sweep out all remaining gases. The iodised solution is then poured out, care being taken to rinse the bulb-tube thoroughly, and titrated with hyposulphite of soda, so as to find the remaining proportion of free iodine. The difi'erence between the original amount of free iodine present in the solution, and the amount thus found, shows the proportion of iodine which has been converted into hydriodic acid, and which is proportional to the sulphur contained in the sample under examination. Iron, Preparations of: — Ferric Acetate. Fe2(CjH302)e. Syn. Pee- ACETATE OP IRON J FeRKI SESCIUIACETAS, L. Prep. Ferric carbonate, 1 part; acetic acid, 6 parts ; digest three days and filter. A dark brownish-red, uncrystallisable liquid, very soluble and powerfully astringent. The cal- cined sesqnioxide of iron of the shops, com- monly sold as carbonate of iron, does not answer well for this or any of tlie sesqui- compounds, owing to its being with difficulty dissolved by acids, especially by the weaker ones. — Dose. (Of the last) 10 to 25 drops, ia water or wine. IRON 909 Ferric AlbTunlnata. Sj/n. Febbi albu- min as, L. Frep. Pmoipitnte a filtered solution of white of egg with aDoth(.T of ferric sulphate or persul- phate of irou, wash the deposit in water, and dissolve it in alcohol holding potassium hydrate in solution. This preparation is highly spoken of by M. Lnssaigne as especially adapted by its nature, on theoretical grounds, lor combining with the tissues of the body. Terric Citrate. Fpj(C5HjO,)j. Si/n. Pee- CITBATB OF IRON, CiTEATE OF SeSQUIOXIDE 01 I., ClTBATE OV I. ; 1<"eEBI OITBAS. Prep, By saturating a solution of citric acid in an equal weight of water with freshly precipitated moist hydrated ferric hydrate, evaporating at 150° Fahr. to the consistence of a syrup, and spreading on glass plates to dry. liy either of the methods adopted for the ammoniocitbatb, merely omitting the addi- tion of tile amiiiunia. It much rexembles the ammonio-citrate, but is only slightly soluble in water, and has a rather less agreeable taste. — Dose, 3 to 6 gr. Ferric and Ammonium Citrate. Syn. Am- MONIO CITKATE OV inON : AmMONIO FEBEIC OITBATB ; FliKBI AMMONIO CITRAS. L. There are several preparations in which the term ' citrate of iron' has been ap- plied. That coiniaonly known umlerthis name is really a double citrate of iron and ammonia, and appears to bo correctly called * ammouio- citrate of iron.' B.l'. Liquor Ferric Pcrsulphntis (B.P.), 8 ; liquor ammonia, 19i ; citric acid (in crystals) 4; distilled water, a sufficiency, mix 14 of the solution ot'nmmoiiia, with 40 of water, and all gradually j tlie solution of ferric sulphate stir constantly and briskly ; let the mixture stand two hours, and put into a calico filter and allow to drain. Wash well the precipitate until it no longer gives a precipitate with barium chloride. Dissolve the citric acid in 8 oz. of the water, and having applied the lieat of a Hater bath add the precipitate of ferric hydrate previously well drained, stir them together until the whole or nearly the whole of the hydrate has dissolved. Let the solution cool, then add 5i of the ammonia, filter through flannel, evaporate to the con- eistency of syrup, and dry it in thin layers on flat porcelain or glass plates at a temperature not exceeding lOU". Prep. (Pli. L.) Ferrous sniphate, 12 oz. ; car- bonate of sodium, l:ii oz.; dissolve each sepa- rately in boiling distilled water, 6 pints ; mix the solutions whilst still hot, and allow the prccipitaie to subside; alter a time decant the supernatant liquor, wash the precipitate frequently with water (drain it), add of citric acid (in "powder), 6 oz., and dissolve by the aid of a gentle heat; when the whole has cooled, add of liquor of ammonia, Ph.L., 9 fl. oz., and gently evaporate to the consistence of a syrup ; in this state spread it very thinly on flat earthenware dishes (or sheets of gla-s), dry by a gentle heat, and when dry keep it in well-stoppered bottles. (Ph. D.) Citric acid, 4 oz. ; distilled water, 16 fl. oz.; hydrated ferric oxide, obtained from the sulphate, 5 oz.; liquor of ammonia, 4 fl. oz., orq. s. (Wholesale.) A mixture of iron filinfrs and citric acid, in powder, with barely sufficient water to cover it, is kept in a warm situation for some days, occasionally stirring the mass, and replacing the water as it evaporates. A saturated solution is next made in distilled water, there being previously added more citric acid (about half the weight of the acid first used), as required; it is then neutralised with liquor of ammonia (about 1} oz. of liquor of ammonia, sp. gr. ■832, to every gallon of the solution of sp. gr. 1025), and the solution is concentrated by evaporation ; the proceas is then completed as in No. 1. The first part of this process produces a salt of the protoxiilo of iron, or ferrous citrate, which is afterwards converted, by exposure to the atmosphere, into a citrate of the magnetic acid, or ferri, ferro. citrate, and, lastly, into citrate of peroxide of iron, or ferric citrate. B.P. Liquor I'erri Persnlphatis 8. Liquor ammonia) 19^. Citric acid (in crystals) 4. Dis- tilled water, a sufficiency. Mix 11 of the solu- tion of ammonia with 40 of water, and add griidually the snlution of ferric sulphate. Stir constantly, let the mixture stand 2 hours, and filter through calico, and allow to drain. Wasli until the washing ceases to precipitate barium chloride, dis-olve the citric acid in 8 of water, add the precipitated ferric hydrate, and heat in a water bath until dissolved. Let the solution cool, add 5i of the ammonia, filter throusjh flannel, evaporate to the consistency of syi up, and dry on flat porcelain plates in thin layers at a temperature below 100° F. Oba. Pharmaceutical writers have been so diS'use in their disquisitions on the preparation of this salt, as would lead to the inference that there is some difiiculty attending it. The con- trary is, however, the case. The only care necessary is to spread the syrup solution very thinly on warm sheets of glass to dry, which it will rapidly do if they are placed in an atmo- sphere of warm dry air, for which purpose a ' drying closet ' is the most convenient. The dry salt may then be easily detached from the glass, and will form thin scales, or lamella!, of great brilliancy and beauty. It is also better to use a little more oxide than the acid will dissolve, as the remainder will be employed in a future operation. Less water may be used, or even a larger quantity than that men- tioned; but in the first case the liquid will become difficult to filter— in the latter it will require more evaporation. Boiling water dis- solves about twice its weight of citric acid, and there remains IJthsof this quantity in solution when cold, and it takes rather more than 910 IRON twice the weight of the citric acid in moist hydrated protoxide of iron to produce satu. ration. Prop., S^c. This heautiful salt is of a rich ruby colour, and forms glistening transparent scales, very soluble in aqueous menstrua, and the resulting solution is less easily decomposed by reagents than the solutions of most of the other salts of iron. It is ' compatible ' with the alkaline of carbonates and bioarbonates, and several other salts, and is nearly tasteless, advantages which have been perhaps overrated hy both prescriber and patient. It is doubtful whether this article has not obtained a larger sale f rom its pleasing appearance than from its medicinal virtues. Several persons who have prepared it in lumps or powder, by the simple evaporation of the solution to dryness, have been unable to sell it under that form, even at a lower price. Am monio- citrate of iron is soluble in water; the solution neither changes the colour of litmus nor turmeric ; nor is it turned blue by ferrocyaniile of potassium ; but either potas- sium byiirate or lime water being added, it throws down ferric hydrate, and ammonia is evolved. From 100 gr. dissolved in water, potassium hydrate precipitates about 34 gr. ,of ferric hydrate. — Dose, 3 to 10 gr., in water, wine, or bitter infusions. Ferric and Strychnine Citrate. (U. S.) Syn. Feebi bt stetchnijj citkas. Prep. Citrate of iron and ammonia, 500 gr. ; stryolinia, 5 gr. ; citric acid, 5 gr. ; distilled water, 9 fl. dr. Dissolve the citrate of iron and ammonia in 1 oz. of the water, aud the strychnia and nitric acid in 1 dr. of distilled water. Mix the two solutions, evaporate the mixture over a water hath, at 140° Fahr., to the thickness of a syrup, and spread on glass plates, so that the salt, when dry, may be obtiiined in scales. Ferric and Magnesium Citrate. Syn. Cixnio OF IKOlf AND MAGNESIA; FeEEI MAGNESIO- CITEAS; FEREI ET MAGlfESI.E CITEAS, L. Prep. As the last, hut using carbonate of magnesium instead of ammonia to neutralise the solution. — Dose, 2 to 10 gr. It has been recommended as a chalybeate in the dyspepsia of gouty and debilitated habits. Ferric and Quinine Citrate. Syn. Citeate OF QUININE AND lEON; FeEEI-QUINIO-CI- TEAS, L. As the ammonio-citrate, but using quinine, recently precipitated, instead of am- monia, to neutralise the acid. B.P. Pure ferric hydrate is prepared from liquor ferri persulphatis, 4J pints, and liquor ammonias, 8 pints, as in the ferric and ammo- nium citrate. Sulphate of quinine 1 is mixed with water 8, and sulphuric acid \\, and when dissolved, ammonia added until the qui- nine is precipitated. The precipitate is col- lected and washed with 30 of water. Citric acid 3 is dissolved in 8 of water by the aid of a water bath, and the ferric hydrate, well drained, added; stir together until dissolved, and add the quinine, stirring well until all is dissolved, and allow to cool ; add li of solution of ammonia diluted with 2 of water, stirring the solution briskly until the quinine at first thrown down by the ammonia is redissolved; filter and evaporate to a syrup, drying in thin layers on Hat porcelain or glass plates at a temperature of 100°. Ferric citrate, 4 parts j citrate of quinine, 1 part; distilled water, q. s.j dissolve, gently evaporate, and proceed as directed for am- monio-citrate of iron. Greenish golden-yellow , scales when prepared by the B. P. process, soluble in 2 parts of water, and somewhat deliquescent; entirely soluble in ether ; taste bitter as well as chalybeate. — Dose, 2 to 6 dr. ; in cases where the use of both iron and quinine is indicated. Ferric and Sodium Citrate. Syn. Feeei soDio-oiTKAS, Feeei et sodje citeas, L. Prep. Prom citric acid, ('arbonate of sodium, and iron or the hydrate, as the ammonio-citrate or potassio-citrate. Ferric Chlo'ride. Fe2Cl6. Syn. Sf.s- QUICHLOEIDE OF lEON, PeECHIOEIDE OF lEON, FEEMUEIATE OF I. ; FEEEI SESQDIOHLO- EIDUM, L. Prep. 1. (Anhydrous.) By pas- sing dry chlorine over heated iron filings. Brown scales. (Hydrated.) Dissolve ferric hydrate in hy- drochloric acid, evaporate to the consistence of a syrup, aud crystallise. Yellow or red scaly crystals. The impure solution of this salt has been greatly used as a sewage deodo- riser. See TiNOTDEE. Ferric and Ammonium Chloride (FcjCle NH4CI. Aq). Syn. Double chloeides of [EON AND AMMONIUM, AMMONIO CHLO- eide of ieon ; Feeei ammonium chlo- kidum. Ferric oxide, 3 oz. ; hydrochloric acid, ^ pint ; digest in a sand bath until dis- solved, then add of ammonium 2 J lbs., dis- solved in water, 3 pints ; filter the liquid, evaporate to dryness, and reduce the mass to coarse powder. Orange-coloured crystalline grains readily soluble in water. Ammonio-chloride of iron is tonic, emmena- gogue, and aperient. — Dose, 5 to 15 gr. ; in glandular swellings, obstructions, &c. Ferric Ferrocy'anide. (Fe4(FeCy6)3 . 18Aq). Syn. Sesquifeeeocyanide of ieon, Peus- siAN BLUE ; Feeei feeeocyanidum, F. bes- QUIFEEKOOYANIDUM, L. Prep. Ferrous sulphate, 4 oz. ; water, 1 pint ; dissolve, add to the solution of nitric acid, 6 fi. dr., in small portions at a time, boiling for a few moments after each addition ; next dissolve ferrocyanide of potassium, 4i oz., in water, 1 pint, and add this last solution, by degrees, to the first liquid, stirring well each time ; lastly, collect the precipitate, wash it with boiling water, drain, and dry it. — Dose, 3 to 5 gr., three or four times daily, as an alterative, tebriluge, and tonic, gradually increasing the quantity until some obvious effect is produced ; in inoN 911 Agnen, epilepay, and neuralgia. See Pbussian BL0S. Ferric Hydrate. Fes(HO),. See under Ferric Oxide. Ferric Iodide. Fc,I,. Si/n. Febbi peeio- DIDUM, L. Prep. Freely expose ii solution of ferrous iodide to the air j or digest iodine, in excess, on iron, under water, gently evaporate, and sublime. A deliquescent, volatile red com- pound, soluble in water and alcohol. It is rarely employed in medicine. Ferric Oxide. FejOj. Syn. Sebquioxide o» IBON, Peboxide ov ieon, RbiJ oxide of 1. ; FSBBI BESQtriOXYDUM, F. PBEOXYDUM, P. OXTDUJI bi;bbuu, L. This substance is found native under several forms, but that employed in the arts is prepared by one or other of the following methods : — From metallic iron. From iron wire or clean iron filings cut into pieces, moistened with wa er, and exposed to tlic uir until com- pletely converted into rust; it is then ground with water, elutriated, and dried, i!i a similar way to that adopted for chalk. For sale, it is usually made up into small conical loaves or lumps. By calcination : — (Bbown-bed COLcothae, Ceocus, Indiak bed, EonaB, Jewellees' e. ; Febei oxtdum eubeum, L.) — C:ilcine ferrous 8ul)jhHtu until the water of crystallisation is expelled, then roast it with a strong fire until acid vapours cease to rise ; cool, wash the residuum with water until the latter ceases to aSect litmus, and dry it. Ferrous sulphate, 100 parts ; common salt, 42 parts; ralcine, wash well with water, drj, and levigate the residuum. This process yields a cheap and bea,utif ul product, which is frequently sold for the ferri sesquioxydum ; but it is less soluble, and therefore unfitted for a substitute for that preparation. By precipitation ; — Feeei sesquioxydum — B. P., Feeei oxtdum: eubeum — Ph. E. L. Uy precipitating a solution of ferric sulphate or chloride with ammonia, in excess, and washing, drving, and igniting in the resulting hydrate. Pure; anhydrous. Ferrous sulphate, 4 lbs. ; sodium car- bonate, 4 lbs. 2 oz. ; dissolve each separately in water, 3 galls.; mix the solution wliiL^t hot, set the mixture aside, that the precipitate may subside, and subsequently wash and dry it as before. Contains water, and a trace of alkali. Feeeic htdeate, Feeei peeoxtdum ht- DEAIDM — (Ph. D., Feeeugo— Ph. E.) — a. (Ph. E ) Ferrous sulphate, 4 oz. ; sulphuric acid, 3i fl. dr.; water, 1 quart; mix, dissolve, boil, and gradually add of nitric acid, 9 fl. dr. ; stirring well and boiling for a minute or two after each addition, until the liquor yields a yellowish-brown precipitate with ammonia ; it mu^t then bo filtered and precipitated with liquor of ammonia (fort.), Sj fl. oz. ; rapidly added and well mixed in; collect the precipi- tate, wash it well with water, drain it on a calico filter, and dry it at a heat not exceeding 180° Fahr. When intended as an antidote for arsenic it should not be dried, but kept in the moist or gelatinous state. Feeeic peboxide, moist (B. P.) Si/n. Feeei peboxidum humidum. Prep. Mix solution of persulpbateof iron (B. P.), 4fl. oz., with 1 pint of distilled wa.ter, and add it f;ra- dually to 33 fl. oz. of solution of soda (B. 1'.), stirring constantly and briskly. Let them stand for two hours, stirring occasionally; then put on a calico filter, and wheu the liquid has drained away, wash the precipitate with distilled water till what passes through ceases to give a precipitate with chloride of barium. Lastly, enclose the precipitate without drying it in a stoppered bottle, or other vessel, from which evaporation cannot take place. Hey hydeate op peboxide of ieon (B. P.). Feeei peboxidum hydbatum. Dry the moist peroxide, 1 II)., at a temperatuid not exceeding 212° Fahr., till it ceases to lose weight. Reduce to a fine powder. — Dose, 5 to 30 grains. Prop. Ferric oxide, prepared by precipi- tation (1, c), is an impalpable powder, o( u brownish-red colour, odourless, insoluble in water, freely soluble in acids, and possessing'a slightly styptic taste, especially when recently prepared. When exposed to heat its colour is brightened, its sp. gr. increased, and it is ren- dered less easily soluble in acids. The oxide prepared by calcination is darker and brighter coloured, le.^s soluble, and quite tastclc s. It lias either a scarlet or purplish cast, according to the heat to which it has been exposed. The finest Indian red, or crocus, usually undergoes a second calcination, in which it is exposed to a very intense heat. It is then known as * purple brown.* The best jeweller's rouge is prepared by calcining the precipitated oxide until it becomes scarlet. The hydrate is of a yellowish-brown colour, and though it can be dried without decomposi- tion, it requires to be kept in a moist i-late. It is best preserved in a well-stoppered bottle, filled with recently distilled or boiled water. Pur. Medicinal ferric oxide or sesquioxide of iron (febei sesquioxydum, Ph. L. & D.) is soluble in dilute hydrochloric acid, scanely effervesciug, and is again thrown down by potassa. Tlie strained liquor is free from colour, and is not dlseolonred by the addition of either sulphuretted hydrogen or ferro- cyanide of potassium. The hydrate (febei peeoxydum htdeatum — Ph. D., FEEEUGO — Ph. E.) is entirely and very easily soluble in hydrochloric acid, with- out effervescence ; if previously dried at ISO' Fahr., a stronger heat drives ofl' about 18|j of water. Uses, J^c. The precipitated oxide is em- ployed in medicine as a tonic and emmeua- gogue, in doses of 10 to 30 gr. ; and as an an- thelmintic and in tic douloureux, in doses of 1 to 4 dr., mixed up with honey. It is also 912 IRON employed to make some preparations of iron. The calcined oxide is employed as a pigment, as an ingredient in a, plaster, &c. The hydrate is used medicinally as a tonic in doses of 10 to 30 gr. ; and in much larger, as an antidote in cases of arsenical poisoning. We are indebted to Bunsen and Berthold for the introduction of this substance as an antRote to arsenic. A table-spoonful of the moist oxide may be given every 5 or 10 minutes, or as olten as the patient can swallow it. ( Pereira.) When this preparation cannot be obtained, rust of iron or even the dry so- called carbonate (sesquioxide) may be given along with water instead. According to Dr Maclagan, 12 parts, and to Devergie, 32 parts, of the hydrate are required to neutralise 1 part of arsenious acid. Fehlingsays that the value of this substance as an antidote to arsenic is materially impaired by age, even when kept in the moist state. The presence of potassium, sodium, ammonium, hydi'ates, sulphates, chlo- rides or carbonates, is not of consequence, and, therefore, in cases of emergency, time need not be lost in washing the precipitate, which, in such cases, need only be drained and squeezed in a calico filter. The magma obtained by precipitating ferrous sulphate with magnesia, in excess, and which contains free magnesia and magnesium sulphate, besides ferric hydrate, precipitates arsenious acid not only more quickly,but in larger quantity, than ferric hydrate does when alone. It will even render inert Fowler's solution, and precipitate both the copper and arsenic from solutions of Schweinfurt green in vinegar, which the pure gelatinous oxide alone will not do. Soluble Saccharated Oxide of Iron. (G.) S^n. Fbeeum oxydatum sacchaeatitm so- LUBiLE. I^rep. Solution or perchloride of ii'ou (sp. gr. 1'480), 2 oz. (by weight) j syrup, 2 oz. (by weight) ; mix, and add gradually, so- lution of caustic soda (sp. gr. 1'330); 4 oz. (by weight); and set aside for 24 hours ; then add to the clear liquid 30 fl. oz. of distilled hot water; agitate and set aside. Pour off the supernatant liquid from the precipitate which will have formed, and pour on fresh dis- tilled water; then collect the precipitate on a filter and wash thoroughly with distilled water. Put the drained precipitate into a porcelain vessel, and mix with it.9 oz. of sugar in pow- der, and evaporate to dryness with constant stirring over a water bath, then mix in enough sugar in powder to make up 10 oz. by weight; reduce to powder and keep in a closed vessel. One hundred parts contain three of metallic iron. Ferric Nitrate. rejfNOj)^. St/m Peoto ni- TEATE OE IKON, NiTEATE OF SESQUIOXIDE OF lEON ; Feeei peeniteas, L. By digesting nitric acid (diluted with about half its weight of water) on iron or ferric hydrate. A deep- red liquid, apt to deposit a basic salt. It is used in dyeing, and has been recommended in dyspepsia, calculous affections, and chronic diarrhcea,— J)o«e, 5 to 10 or 12 drops. Ferric Phosphate. Fe2H3(P04)8. S^». Fee- EIC OETHOPHOSPHATE (Odling) ; FeEEI SES- QTJIPHOSPHAB, PHOSPHAB FEEEICITS, L. A white powder obtained by precipitating ferric chloride by sodium phosphate.— fie* and dose. As the last. Fekeio pteophosphatb. Fe^(P20j)3. A salt containing ferric iron combined with the radical of pyrophosphoric acid. Prep. By precipitating a solution of ferric sulphate with one of pyrophosphate of sodium, taking care to operate at a temperature belovir 59° Fahr. Prop., S(c. A gelatinous precipitate which dissolves with facility in excess of pyrophos- phate of sodium. The citrate of ammonium is the most eligible solvent according to M. Robi- qnet, who first called attention to this salt as a remedial agent. — Dose, 5 to 10 gr. Ferric Sulphate. Pe2(S04)3. Syn. Peksui- PHATE OF lEON, SULPHATE OF SESQUIOXIDE OF IBON; Feeei PEKSXTLPHAS, L. Prep. By adding to a solution of ferrous sulphate ex- actly half as much sulphuric acid as it already contains, raising the liquid to the boiling- point, and then dropping in nitric acid, until the liquid ceases to blacken by such addition. The solution evaporated to dryness furnishes a buff-coloured mass, slowly soluble in water. Prop., S[c. With the sulphates of ammonium and potassium it unites to form compounds to which the name 'iron alums' has been given. It forms the active ingredient in the ' liquor oxysulphatis ferri ' of Mr Tyson, and is said by Dr Osborne to be a constituent of ' Widow Welch's pills.' This salt is also formed when ferrous sulphate is calcined with free exposure to the air. Dissolved in water, it is used as a test for hydrocyanic, gallic, and tannic acids. Ferric Sulphide. Syn. Pbesulphidb op IKON. This compound is prepared in the hydrated state (feeei peesulphueetum htdeatum) by adding, very gradually, a neutral solution of ferric sulphate to a dilute solution of potassium sulphide, and collect- ing, &c., the precipitate, as in the case of the hydrated ferrous sulphide. Proposed by Bouchardat and Sandras as a substitute for ferrous sulphide, to which they say it is pre- ferable. Ferric Tan'nate. Syn. Feeei taiotas, Feeeum tannicum, L. Prep. Prom tnnnin, 1 part ; boiling water, 150 parts ; dissolve, add of freshly precipitated ferric hydrate (dried at 212° Fahr.), 9 parts; evaporate by a gentle heat to one half, filter, add of sugar 1 part, complete the evaporation, and at once put it into bottles. — Dose, 3 to 5 gr., thrice daily ; in chlorosis, internal haemorrhages, &c. Double Ferric and Ammonium Tartrate. Syn. AmMONIO TAETEATE of IKON, DOITEIE TAR- TBATE OF IKON AND AMMONIUM; AMMONIO lEON 913 PEBMC TAETBATE, FbBBI AMMOUIO lAfi- TBATE; Fliuai AMMOSIO TAETBA8. Prep. (Aikin.) Tartaric acid, 1 part ; iron filings, 3 parts ; digest in a sufficient quantity of bnt water to barely cover the mixture for 2 or 3 days, observing to stir it frequently, and to add just enough water to allow the evolved gas to escape freely ; next add ammonia, in slight excess, stir well, dilute with water, de- cant, wash the undissolved portion of iron, filler the mixed liquors, and evaporate to dry- ness; dissolve the residuum in water, add a little more ammonia, filter, and again gently evaporate to dryness, or to the consistence of a thick syrup, when it may be spread upon hot plates of glass or on earthenware dishes, and dried in a stove-room, as directed for the cor- responding citrate. Tartaric acid, 6i oz. ; water, 7 pints ; dis- solve, neutralise the selection with sesquicar- bonate of ammonium, and add 6J oz. more tartaric acid ; to the solution heated in a water batb, further add moist hydrated oxide of iron (obtained from eesquioxide of iron, 53i dr., dissolved in hydrochloric acid, and precipitated by ammonia) ; when dissolved, filter, and eva- porate, &c., as before. Prop., 1(0. Glossy, brittle lamellffl, or irre- gular pieces, of a deep garnet colour, almost black, very soluble in water, and possessing a sweetish and slightly ferruginous taste. By repeated re-solution and evaporation its sweet- ness is increased, probably from the conversion of a part of its acid into sufjar. It contains more iron than a given weight of the sulphate of the same base. It is the most pleasant- tasted of all the preparations of iron except the aramonio-citrate, last noticed. — Dose, 3 to 10 gr. Ferric and Potassium Tartrate, Syn. Tab- TBATB OF POTASaA AND lEON, FEKEO-TAETEATE OP P0TAS3A ; FeEEIO TABIEATB OE P. ; FeEKI TAETAEATITM (B. P.), FeEEI POTASSIO-TAETEAS (Ph. L.), Fbeeum taetaeizatum (Ph. E.), Feeei taetaeitm (Pll. D.), Feeei et po- TASsiE taetbas (Ph. U. S.), L. Prep. (B. P.) Prepare ferric hydrate from 4 fl. oz. of liq. ferri persulphas, B. P., as in making the double citrate, and add it to 2 oz. of the acid tartrate of potassium, dissolved in 30 oz. of water. Digest for 6 hours at 140°, allow to cool, and decant off the clear solution, which is to be evaporated down and dried on glass plates.— (Ph. L.) Ferrous sulphate, 4 oz., is dissolved in water, 1 pint, previously mixed with sulphuric acid, i fl. oz. ; heat is applied to the solution, and nitric acid, 1 fl. oz., gra- dually added ; the solution is boiled to the con- sistence of a svrup, and then diluted with water, 4 galls, (less "the pint already used) ; liquor of ammonia, 10 fl. oz., is next added, and the pre- cipitate washed, and set aside for 24 hours j at the end of this time, the water being decanted, the still moist precipitate is added, gradually, to a mixture of bitartrate of potassium, 2 oz.. and water, \ pint, heated to 140° Fahr. ; after vol,. II. a time the undissolved oxide is separated by a linen cloth, and the clear solution either gently evaporated to dryness or treated iu the same manner as the citrate (lastly, pre- serve it in well-stoppered bottles). The formulie of the Ph. E., D., & U. S., are essentially tfie same. The Ph. D. orders a heat not beyond 150° Fahr. to be applied to the mixture of the oxide and bitartrate, with occasional stirring for 6 hours, and the desiccation to be conducted at the same tempei'ature. Ohs. This preparation is a double salt of potassium and iron ; it is therefore wrongly called ' tartrate of iron' as is commonly heard. It is totally soluble in water ; the solution is neutral to litmus and turmeric, unaffected by ferrocjaiiide of potassium, and not precipitated by acids nor alkalies, nor acted on by the magnet. Heated with potnssa, 100 gr. throws down about 34 gr. of sesquioxido of iron. Entirely soluble in cold water; taste freely chalibi-ate. That of commerce has generally a feebly inky taste, a slight alknline reaction, is slightly deliquescent, dissolves'in 4 parts of water, and is nearly insoluble in alcohol. Potassiotartrute of iron is an excellent fer- ruginous tonic. — Dote, 10 to 20 gr., made into a bolus with aromatics, or dissolved in water or other convenient menstruum. Ferric Valerianate. Syn. Vaibbianate op SESQUIOXIDE OF IBON, VaLEEIATE OP lEON; Fekki valeeianas (Ph. D.), L. Prep. (Ph. D.) By adding a solution of sodium vale- rianate to another of ferric sulphate, and collecting and washing the precipitate, which is to be dried by placing it for some days folded in bibulous paper, on a porous brick ; after which it is to be carefully kept from the air. Prop., S;c. A reddish-brown amorphous powder ; nearly insoluble in water; soluble in rectified spirit, and in the dilute acids with decomposition. Citrate or tai-tnite, fl.ivoured with oil of valerian, is frequently sold for it. — Dose, 1 to 3 gr. ; in anosmia and chlorosis complicated with hysteria. Ferroso-Ferric Hydrate. Fc3(HO)8. Syn. Htdeatbd peeeoso-peeeic oxide, Ht- DEATBD MA0NETIO OXIDE. (B. P.) Liquor ferri persulphas, h\; ferri sulphas, 2; solu- tion of soda, 80 ; distilled water, a sufficiency. Dissolve the ferrous sulphate in 40 of water, add the solution of soda, stirring them well, boil the mixture, let it stand for two hours, put in a calico filter, wash with distilled water until the washing gives no precipitate with barium eliloride, and dry at a temperature not exceeding 120. Ferrous sulphate, 6 oz. ; sulphuric acid, IbO minima ; nitric acid, 4 fl. dr. ; stronger solution of ammonia, 4i fl.oz.; boiling water, 3 pints; dissolve half of the sulphate in half of the water, add the oil of vitriol, boil, add the nitric acid gradually, boiling after each addition for a few minutes ; dissolve the remaining half of the sulphate in the rest of 58 914 IRON the boiling water ; mix the two solutions, add the ammonia, stirring well (and boil for a short time) ; collect the precipitate on a calico filter, wash it with water until it ceases to precipitate a solution of nitrate of barium, artd dry at a heat not exceeding 183° Fahr. The formulas of Gregory and Dr Jephson are similar. Ferrous sulphate, 8 oz., dissolved in a mix- ture of water, 10 fl. oz., and sulphuric acid, 6 fl. dr., is converted by means of nitric acid, 4 fl. dr., diluted with water, 2 fl. oz., into ferric sulphates ; this solution is then added to another, formed by dissolving ferrous sulphate, 4 oz., in water, -^ pirit ; the whole is then mixed with liquor of potassium hydrate, 2| pints, and after being boiled for 5 minutes is collected on a calico filter, and washed, &c., as before ; and is to be preserved in a well-stop- pered bottle. Prop., ^c. The hydriite is a black sand- like substance, consisting of very minute crystals. When pure it is attracted by the magnet, and is entirely soluble in hydrochloric acid; and ammonia added to the solution throws down a black precipitate. The oxide is the chief product of the oxidation of iron at a high temperature in the air and in aqueous vapour. It is more permanent than ferrous oxide, but incapable of forming salts. — Dose, 5 to 20 gr. two or three times a day. Ferroso-ferric Oxide. Fe304. Sy». Ma&- NEiio o. OS I. ; Feeki oxteum nigbum, F. o. MAQNETIOUM (Ph. D.), OXTDTJM TEEEOSO- PEKEiouM, L. This occurs native, but that used in medicine is prepared artificially. From the black scales of iron that fall around the smith's anvil, by washing, drying, detaching them from impurities by means of a magnet, and then treating them by grinding and elutriation, as directed for prepared chalk. The product of this process is in- ferior as a medicine to the hydrate obtained as below, being less easily soluble in the juices of the stomach. Ferroso-ferric Oxide. Fp^Oj. Si/n. Ma&- NEiio OXIDE. See Feeboso-feeeic oxide. Iron, Black Oxide of. ( K. P.) Si/n. Feeei OXYDUM MAGNETICTJM ; FeEEI OXTDUM NI- Geum; Maetial .asTHlOPS. Frep. Dissolve sulphate of iron, 2 oz., in 2 pints of distilled water, and add solution of persulphate of iron (B. P.), 55 fl. oz., then mix with solution of soda, 4 pints (B. P.), stirring well together. Boil the mixture, let It stand for 2 hours, stir- ring occasionally, then put it on a calico filter, and when the liquid has drained away wash the precipitate with distilled w«ter till what passes through ceases to precipitate chloride of barium. Finally, dry the precipitate at a temperature not exceeding 120° Fahr. — Dose, 5 to 10 gr. Ferrous Acetate. F(C2H 302)3. Si/n. Febei AOETAS, L. Frep. 1. From freshly precipi- tated ferrous carbonate dissolved in dilute acetic acid. a. By adding a solution of calcium acetate to another of ferrous sulphate, and evaporating the filtered liquid, out of contact with the air. Small, colourless, or pale-greenish needles or prisms, very soluble and prone to oxida- tion. Ferrous Arsenate. re3(As04)2. St/n. Feeei AESENIAS, L. Prep. 1. From a solution of sodium arseniate, added to a solution of ferrous sulphate, the precipitate being collected, washed in a little cold water, and dried. — Dose, ,15 to -jV gr., made into a pill j in lupus, psoriasis, cancerous affections, &c. Exter- nally, combined with 4 times its weight of ferrous phosphate and a little water, as a paint to destroy the vitality of cancerous for- mations. An ointment (20 to 30 gr. to the oz.) is also used for the same purpose. They are all dangerous remedies in non-professional liands. 2. (B. P-) Prep. Sulphate of iron, 9 oz.; arseniate of soda dried at 300° F., 4 oz. ; ace- tate of soda, 3 oz. Dissolve the arseniate and the acetate of soda in 2 pints, and the sulphate of iron in 3 pints, of boiling distilled water, mix the two solutions, collect the white pre- cipitate which forms on a calico filter, and wash until the washings cease to be affected by a dilute solution of chloride of barium. Squeeze the washed precipitate between folds of strong linen in a screw-press, and dry it on porous bricks in a warm air-chamber whose temperature shall not exceed 100° F. — Dose, -jJjth of a gr. Ferrous Arsenite. re(As02)2. Sy». Feeri AESENis, L. From the pota^slum arsenite, and ferrous sulphate, as the last. A yellowish- brown powder, occasionally used in medicine as a tonic, alterative, and febrifuge. — Dose, Ferrous Bromide. FeB^j. Si/n. Feeei BEOMIDFM, L. Prep. (Moir.) Bromine and iron filings, of each 1 part; water^S parts; mix in a stoppered phial, set it aside, occasion- ally shaking it, for 2 or 3 days, and when tlie colour of the bromine has disappeared, and the liquid becomes greenish, filter and evaporate to dryness. — Dose, 1 to 6 gr., as a tonic, diu- retic, and resolvent, in similar cases to those in which iodide of iron is given. Ferrous Carbonate. Fe(C03). Sgn. Peo- TOCAEBONATE OF lEON; FbEKI CABBONAS, F. SUBCAEBONAS, L. This occurs in nature as BPATHOSE OEE, the chief constituent as of CLAY lEONSlONE, and in many chalybeate WATEES. Prep. (B. P.) Ferrous sulphate (sulphate of iron), 2 ; ammonium carbonate, IJ ; boiling distilled water, 320; refined sugar, 1. Dis- solve the sulphate and ammonium carbonate each in i of the water, and mix; allow to stand for 24 hours and decant, of the clear solution, add the remainder of the water to the precipitate, stir well, allow to settle, and decant off. Collect the deposit in a calico filter, press, rub in the sugar in a IRON 915 porcelain mortnr, and dry at a temperature not exceeding 212° Fabr. Small coherent grey lumps. Precipitate a solution of ferrous eul- phute with a solution of sodium carbonate, well wash the green powder with water which has been boiled, and dry it out of contact with the air. On the slightest exposure to air it is converted into ferrous hydrate or oxide. This change is for the most part prevented by combining it with sugar, as in the following preparation. With sugar: Feeki CABBONiS baooabata, B. P.; 8ACCHABINB C. OJ I.; FEBKUM CAB- BONICUM BACOHABATUM, PEBEI CABBONAS COM BACCHAEO— Ph. L., PBBBI CAEB0N4S 8AC0HABATDM — Ph. E. & D. L. — (Ph. L.) Ferrous sulphate, 4 oz. j sodium carbonate, 4i oz. ; dissolve each separately in quart of boiling water, and mix the solutions whilst hot; after a time collect the precipitate, wash it frequently with water, and add of sugar, 2 oz., previously dissolved in water, 2 fl. oz. ; lastly, evaporate the mixture over a water bath to dryness, and keep it in a well-closed bottle. Prop., S(c. A sweet-tasted greenish mass or powder, consisting cliiefly of carboniite of iron. It is one of the best of tlie chalybeatc-i. — Doxp. 5 to 10 gr. When pure, it should bo tiisily soluble in hydrochloric acid with brisk uH'ur- vescence. Ferrous Chloride. FoClj. Si/n. Protochlo- EIDB OF IRON; MURIATB OF IKOS ; FKBBT CHLOiUDUM, L. Frep. 1. (Anhydrous.) By passing dry hydrochloric acid gas over ignited metallic iron. The chloride sublimes in yel- lowish crystals. 2. (Hydratcd.) Dissolve iron filings or scale in hydrochloric acid, evaporate and crystallise. Soluble green crystals. Forrons Citrate. Pe3(C6H507)j. Syn. Pbo- TOOITBATB IliON, ClTRiTB OF FBOTOXIDE OP iito:*. This snlt is easily formed by digesting iron filings or wire with citric acid, and evapn. rating the solution as quickly as possiljle out of contact with the nir. It presents the appear- ance of a white powder, nearly insoluble in water, and rapidly passing to a higher state of oxidation by exposure to the air. Its taste is very metallic. It is exhibited under the form of pills, mixed with gum or syrup, to prevent it from being prematurely decomposed. Ferrous Ferrlcy'anide. St/n. Fkbridoyakide OF IBON. I'rep. By adding a solution of potassium fcrricyanide (' red prussiate of pot- ash') to a solution of ferrous sulphate (or any other soluble ferrous salt), and collecting and drying and precipitate. A bright-blue powder. (See TuBNUutt's blce.) Ferrous Hydrate. Fe2(HO)j. See under Febbocb oxidb. Ferrous Hydrate, Fe(H0)2. Miy be pre- cipitjitcd from ferrous solutions as a white powder, by alkaline hydrates. It rapidly absorbs oxygen, and turns first green, aud then red, by exposure to the air. Both the oxide and hydrate are very powerful bases, neutralising the acids and forming stable shUs, which, when soluble, have commonly a pale green colour, and a nauseous metallic taste. Ferrous Hypophosphlte. Sun. Febbi htfo- PHOSPnis. From the double decomposition of hypophosphlte of lime and sulphate of iron, as hypophosphito of potash. Ferrons Iodide. Felj. St/n, Protoiodide OF iBON, Iodide of ieon; F. iodidfm, Febbi hydeiodas, F. iodubetum, L. Prep. (B. P.) Fine iron wire, 1; iodine, 2; dis- tilled water, 10. Introduce the iron, iodine, and 8 of water into a flii-k, heat it about ten minutes, and boil until all the red colour is gone. Filter thron^li paper into a polished iron dish, washins with the rest of the water, and boil until a drop of the solution taken out on iron wire solidifies on eoMling. Pour on porcelain and cool. (I'll. L. 183G ) Iodine, 6 oz. ; iron filinijs, 2 oz. ; water, 4J pints; mix, boil in a sand bath until the liquid turns to a pale green, filter, wash the residuum witli .1 little water, evaporate the mixed liquors in an iron vessel at 212° Fahr. to dryness, and immediately put the iodide into well-stoppered bottles. Iodine, 1 oz., and clean iron filings or turn- ings, i oz., are put into a Florence flask witli distilled water, 4 fl. oz., and having applied a gentle heat for 10 minutes, the liquid is boiled until it loses its red colour; it is then at once filtered into a second flask, the filter waslied with water, 1 fl. oz., aud the mixed liquid is boiled down, until it solidifies on cooling. With sugar: Saccharine iodide of iron, Sacchabumferriiodidi, Febriiodidumsac- CHABATUM, L. Irou (in powder), 1 dr. ; water, 5 dr. ; iodine, 4 dr. ; obtain a solution of iodide of iron, as above, and add to it of sugar of milk (in powder), li oz. ; evaporate at a tempera- ture not exceeding 122' Fahr., until the mass has a tenacious consistence, then further add of sugar of milk, 1 oz., reduce the mixture to powder, and preserve it in a well-stoppered bottle. Every 6 gr. contains 1 gr. of iodide of iron. From "syrup of iodide of iron" exposed in a shallow vessel, in a warm place, until it crystal- lises ; the crystals are collected, dried, and powdered. A simpler plan is to gently evapo- rate the whole to dryness, and to powder the residuum. The saccharine iodide may be kept for some time in a corked bottle without un- dergoing decomposition. Obs. The preparation of the above com- pound, like that of the citrates, has formed a fertile subject durin; some years for phar- maceutical amateurs to dilate upon. There is in reality not the least difficulty in the process. As soon as iodine and iron are mixed together under water much heat is evolved, and if too much water be not used the combination is soon complete, and the liquor merely requires 916 IRON to be evaporated to dryness, out of contact with tlie air. at a heat not exceeding 2la° Fahr. This is most cheaply and easily performed by employing a ghiss flask, with a thin broad bottom andva narrow mouth, by which means the evolved stesm excludes air from the vessel. The whole of the uncombined water may be known to be evaporated when vapour ceases to condense on a piece of cold glass held over the mouth of the flask. A piece of moistened starch paper occasionally applied in the same way will indicate whether free iodine is evolved; should such be the case, the heat should be immediately lessened. When the evaporation is completed, the mouth of the flask should be stopped up by laying a piece of sheet india rubber on it, and over that a flat weight ; the flask must be then removed, and when cold broken to pieces, the iodide weighed, and put into dry and warm stoppered wide- mouth glass phials, which must be immediately closed, tied over with bladder, and the stoppers dipped into melted wax. Prop., ^c. Ferrous iodide evolves violet vapours by heat, and ferric oxide remains. When freshly made it is totally soluble in water, and from this solution, when kept in a badly stoppered vessel, ferric hydrate is very soon precipitated; but with iron wire immersed iu it, it may be kept clear in a well-stoppered bottle. — Dgse, 1 to 3 gr., or more, as a tonic, stimulant, and resolvent. It has been given with advantage in anjemia, chlorosis, debility, scrofula, and various glandular affections. Ferrous lactate. Fe {C3\ifi^)^. Si/n. Pko- TOLACTATE OF IKOS; FBBBI lAOTAS, FEEE0M lAOTicuM, L. Prep. Boil iron filings in lactic acid diluted with water, until gas ceases to be evolved, and filter whilst hot into a suitable vessel, which mnst be at once closely stopped ; as the solution cools, crystals will be deposited, which after being washed, first with a little cold water, and then with alcohol, are to be carefully dried. The mother liquor, on being digested, as before, with fresh iron, will yield more crystals. Into sour whey, 2 lbs., sprinkle sugar of milk and iron filings, of each, in fine powder, 1 oz. ; digest at about 100° Fahr., until the sugar of milk is dissolved, then add a second portion, and as soon as a white crystalline powder begins to form, boil the whole gently, and filter into a clean vessel; lastly, collect, wash, and dry the crystals as before. Prop., ^c. Ferrous lactate is a greenish- white salt ; and when pure,forms small acicular or prismatic crystals, which have a sweetish ferruginous taste, and are soluble in about 48 parts of cold and in 12 parts of boiling water. It has been regarded by many high authorities as superior to every other preparation of iron for internal use, as being at once miscible with the lactic acid of the gastric juice, instead of having to be converted into a lactate at the expense of that fluid, as it is asserted is the case with the other preparations of iron. — Dose, 2 to 6 gr., frequently, in any form most convenient. Ferrous Ma'late (Impure). Syn. Fbbei MALAS IMPUEUS, L. Prep. (P. Cod., 1839.) Porphyrised iron filings, 1 part; juice of sour apples, 8 parts ; digest for 3 days in an iron vessel, evaporate to one half, strain through linen whilst hot, further evaporate to the con- sistence of an extract, and preserve it from the air. — Dose, 5 to 20 gr., where the use of iron is indicated. Ferrous Nitrate. (FeNOglo. Sya. Pboto NITEATE OF lEON, NiTBATE OF PEOTOXIDB OP lEON ; Feeei niteas, L. By dissolving fer- rous sulphide in dilute sulphuric acid, in the cold, and evaporating the solution in vacuo. Small green crystals, very soluble, and prone to oxidation. Ferrous Oxalate. (U.S.) Syn. Feeei oxa- LAS. Prep. Sulphate of iron, 2 oz. ; oxalic acid, 396 gr. ; distilled water, q. u. Dissolve the sulphate in 30 oz. (old measure), and the acid in 15 oz. (old measure) of distilled water. Filter the solutions, mix them, shake together, and set .iside until the precipitate is formed. Decant the clear liquid, wash the precipitate thoroughly, and dry it with a gentle heat. Ferrous Oxide. FeO. Syn. Peotoxidb of lEON, Feeei peotoxtdum, L. This substance is almost unknown in a pure state, from its extreme proneness to absorb oxygen and pass into the sesquioxide. Ferrous Phosphate. Syn. Phosphate of lEON, Neuteal p. of peotoxide of ieon, BiMETALIilC FEEBOUS OETHOPHOSPHATE (Od- ling^J; Feeei phosphas (Ph. U. S.), L. A salt formed from ordinary or tribasic phosphoric acid. Prep. (B. P.) Ferrous sulphate, 3 ; sodium phosphate, 2i; sodium acetate, 1; boiling distilled water, 80 ; dissolve the sulphate and sodiuin salts, each in half the water, mix, and stir carefully, filter through calico, wash with hot dis'tilled water until it ceases to give a pre- cipitate with barium chloride, dry at a heat not exceeding 120" Fahr. (Ph. U. S.) Ferrous sulphate, 5 oz.; sodium phosphate, 6 oz. ; dis- solve each separate in 2 quarts of water, mix the- solutions, and after repose for a short time wash and dry the precipitate. Prop.,S^e. A slate-colourod powder; inso- luble in water; soluble in dilute nitric and hydrochloric acid. — Dose, 5 to 10 gr. ; in amenorrhcea, diabetes, dyspepsia, scrofula, &c. ; and externally, as an application to cancerous ulcers. Ferrous Sulphate. FeSO,. 7Aq. Syn. Peo- TOSDLPHATB OF lEOIT, SuLPHATE OF IEON, COP- PEEA3, Geben titeiol, Shoemakee's black ; Feeei sulphas (B. P., Ph. L. E. & D.), Vit- BIOLITM FEEEI. The Crude sulphate of iron or green vitriol of commerce (feeei sttlphas VENALls.Ph. L.)is prepared by exposing heaps of moistened iron pyrites or native bisulphuret of iron to the air for several months, either in its unprepared state or after it has been roasted. IRON 917 VThen decompoBition is sufficiently advanced, the newly formed salt is dissolved out with water, and the solution crystallised by evapora- tion, lu this state it is very impure. The ferrous i^utphate or sulphate i^f iron employed in medicine is prepared as follows : — Prep. (B. P.) Iron wire, 4j sulphuric acid, 4; distilled water, 30. Pour the water on the iron, add' the acid, and when the disengage- ment of gas has nearly ceased, bqil for ten minutes. Filter through paper. Allow to stand twenty -four hours, and collect the crystals. Sulpliuric acid, 1 fl. oz. ; water, 4 pints; mix, and add of commercial sulphate of iron, 4 Ib-i. ; iron wire, 1 oz. ; digest with heat and occasional agitation until the sulphate is dissolved, strain whilst hot, and set aside the liquor that crystals may form; evaporate the mother-liquor for more crystals, and dry the whole. Dissolve the transparent green crystals of the impure sulphale of iron in tlieir osvn weight of water, acidulated with sulphuric acid, and re-crystallise. The formula of the Ph. U. S. is similar. Dried; Fisehi sctu'HAs exsiooata, 13. P.; Fbuei sxtlphas exsiccatum — Ph. E., P. 8. BlOOATtTM — Ph. D. From ferrous sulphate, heated in a shallow porcelnin 6r earthen vessel, not glazed with lend, till it becomes a greenish-grey mass, and then reduced to pow- der. The heat should be that of an oven, or not exceeding 400° Fahr. Five parts of the crystallised sulphate lose very nearly 2 parts by drying. Granulated; Pbbei sulphas geakulata, Ii. (B. P.) A solution of iron wire, 4 oz., in sulphuric acid, 4 fl. oz., diluted with water, li pint, after being boiled for a few minutes, is filtered into a vessel containing rectified spirit, 8 fi. oz., and the whole stirred until cold, when the granular crystals are collected on a filter, washed with rectilied spirit, 2 fl. oz., and dried, first by pressure between bibulous paper, and not beneath a bell-glass over sulphuric acid, after which they are put into a stoppered bottle, to preserve tliem from tlie air. Frop., ifo. Ferrous sulphate forms pale bluish-green rhombic prisms, having an acid, styptic taste, and acid reaction ; it dissolves in two parts of cold and less than one part of boiling water; at a dull- rod heat it suffers decomposition; sp. gr. 1-82. It is perfectly soluble in water ; a piece of iron put into the solution should not be covered with metallic copper. 3y exposure to the air it effloresces slightly, and is partly converted into a basic ferric sulphate. — Dose, i to 4 gr., in pills or solution ; externally, us an astringent or styptic. In the arts, as sulphate of iron (cop- peras), it is extensively used in dyeing, and for various othor purposes. The dried sulphate (ferri sulphus oxsiccatum) is chiefly used to make pills. Crude sulphate of iron is frequently con- taminated with the sulphates of copper, zinc. manganese, aluminium, magnesium, and cal- cium, which, with the exception of the first, are removed with difficulty. It also contains variable proportions of the neutral and basic ferric sulphates. The preparation obtained by direct solution of iron in dilute sul- phuric acid should, therefore, be alone used in medicine. In commerce there are four varieties of crude sulphate of iron or copperas known, — greenish-blue, obtained from acid liquors, — pale green, from neutral liquors, — emerald green, from liquors containing ferric sulphate, — and oohrey brown, which arises from age and exposure of the other varieties to the air. Even the first two of these contain trices of ferric sulphate, and hence give a bluish pre- cipitate with ferrocyanide of potassium ; whereas the pure sulphate gives one which is at first nearly white. Ferrous SiUphide. FeS. Si/n. Sulphitret OP IRON, SuiPniDE OP I., PHOTOSULPniUE o» I.; Feebi suli-hubkxcm; (Ph. E. & D.), L. Prep. (Ph. E. &D.) Expose a bar of iron to a full white heat, and instantly apply a solid mass of sulphur to it, observing to let the melted product fall into water; afterwards separate the sulphide from the sulphur, dry, and preserve it in a closed vessel. From sublimed Bulpbnr, 4 parts; iron filings, 7 parts ; mixed together and beatvd in a common fire till the mixture begins to glow, and then removing the crucible from the heat, and covering it up, until the reaction is at an end, and the whole has become coUI. Hydrated; Feeei peotosulphubetcm ht- BBATITM, L. By adding a solution of ammo- nium sulphide or of potassium sulphide to a neutral solution of ferrous sulphate made with recently distilled or boiled water; the precipi- tate is collected on a filter, washed as quickly as possible with recently boiled water, squeezed in a linen cloth, and preserved in the pasty state, under water, as directed under ferric hydrate. Prop., Sfo. The sulphide prepared in the dry way is a blackish brittle substance, attracted by the magnet. It is largely used in the laboratory as a source of sulphuretted hj drogeu. The hydrated sulphide is a black, insoluble substance, rapidly decomposed by ex- posure to the air. Proposed by Mialhe as an antidote to the salts of arsenic, antimony, bis- muth, lead, mercury, silver, and tin, and to arsenious acid; more especially to white ar- senic and corrosive sublimate. . A gargle con- taining a little hydrated sulphide of iron will instantly remove the metallic taste caused by putting a little corrosive sublimate into the mouth. (Mialhe.) On contact with the latter substance it is instantly converted into ferrous chloride and mercurious sulphide, two com- paratively inert substances. It is administered in the same way as ferrous hydrate. When taken immediately after the ingestion of cor- rosive sublimate, it instantly renders it in- 918 IRON ALUM— lEON, DIALYSED nocuous ; but when the administration is de- layed until 15 or 20 minutes after the pjisun has been swallowed, it is almost useless. Ferrous Tar'trate. Syn. Feeki taeteas, Febei PKOTOTAETEAa, L. Prep. 1. From iron filings, 2 parts; tartaric acid, 1 part; hot water, q. s. ; digest together until reaction ceases, agitate the liquid, pour off the turbid solution, and collect, wash, and dry the pow- der as quiclily as possible, and keep it out of contact with the air. Crystallised potassium tartrate, 132 parts ; ferrous sulphate, 139 parts; dissolve each separately, mix the solutions, and collect the precipitate as before. A nearly insoluble pow- der ; seldom used. Obs. By dissolving the corresponding hy- drates in a solution of tartaric acid, employing the former in slight excess, and evaporating, both the ferrous and ferric tartrate are easily obtained. IRON AL'UM. See Alttms. IRON CEMENT'. See Cements. IRON, DIALYSED. (Paris Pharmaceutical Society.) Syn. Pbeefm dialysatcm. Oxide DE FEB DIALTBE. Prep. Solution of ferric chloride (sp. gr. 1'245), 100 grams ; solution of ammonia (sp. gr. 1'169), 35 grams ; add the ammonia in small quantities to the ferric chlo- ride ; at first the precipitate formed is redis- solved very rapidly, but afterwards disappears more slowly. When the liquor has again be- come transpai'ent, it is introduced into the dialyser ; the distilled water in which the vessel containing the ferruginous solution is placed, must be frequently renewed. After a time the highly coloured solution is no longer precipitated by silver nitrate, and gives no acid reaction. It is then absolutely free from the disagreeable taste of certain ferruginous preparations. A small quantity of hydro- chloric acid always remains in the liquor, which may be shown by precipitating the oxide of iron by a slight excess of ammonia, filter- ing, adding an excess of nitric acid, and then silver nitrate. Ten c.c. are evaporated, and from the residue must be calculated how much distilled water is required to be added to pro- duce at 10 per cent, solution. 2. ('American Journal of Pharmacy.') Take 10 parts of liq. ferri perclilor. (B. P.), pre- cipitate by liquor ammonitB, and wash the pre- cipitate thoroughly. Mix this with 12 parts of liq. ferri perclilor. (B. P.), and place in a dialyser. The dialyser is placed in a suitable vessel with distilled water, the water under it renewed every 24 hours. The operation is continued until no trace of chlorine exists, at which time the preparation is found to be neutral. It usually takqs from twelve to fifteen days to complete the process. The resulting preparation, which should be of a deep dark red colour, contains about 5 per cent, of the oxide of iron, If the solution after completion of the operation should con- tain more than 5 per cent, of iron, it may be diluted with dialysed water till it reaches that point. The above formula is said to furnish an article precisely similar to the original Bravais' dialysed iron. 3. (E. B. Shuttleworth.) Add ammonia to a solution of perchloride of iron as long as the precipitate formed is redissolved. A solution is produced which contains ferric hydrate dis- solved in ferric chloride, with free chloride of ammonium. Either the liquor ferri perchlor. fort. (B. P.), or the liquor ferri chloridi (U. S.), may be conveniently used, and the liquor ammonise, sp. gr. "959 or -960, of either Pharmacopoeia will be found a convenient strength. If the ammonia be added to the strong solution of iron, considerable heat is evolved, and, on cooling, the preparation be- comes gelatinised — often so much so that the vessel containing it may be inverted. It is better to avoid this result, and to such end the solution of perchloride must be diluted until of a sp. gr. of about 1-300. This degree may be nearly enough approached by diluting two measures of the B. P. liquor with one of water; or adding one measure of water to five of the U. S. preparation. This solution will generally remain permanently bright and fluid. The amount of liquor ammonias required will of course vary with the acidity of the per- chloride. The liquor ferri B. P. will sometimes bear as much as an equal volume. A gela- tinised solution, even when made from the un- diluted liquor, will often become fluid when put upon the dialyser, but, as I have said be- fore, it is better to work with bright solutions. 4. (l)rPile.) Dr Pile, noticing the fact that chloride of sodium is one of the most rapid crystalloids to dialyse, used a solution of carbo- nate of sodium to add to the solution of ferric chloride in place of the ammonia so generally recommended, and with great success. The solution of ferric chloride (U. S.) which has been neutralised by a cold solution of carbo- nate of sodium is poured int(9 a fioating dia- lyser. Starting with 1 pint of solution of ferric chloride, which on being treated with the sodium solution and ready to dialyse, had a sp. gr. of 1'175, it had in 5 days increased to 5 pints. The water in which the dialyser floated was changed daily. At the end of five days it had passed through the membrane all the crystalloids. Was free from taste of foreign substances, and owing to increase of bulk had now the sp. gr. of 10295, and on evaporation yielded 5 per cent, dry oxide of iron. Too long dialysation will cause the solution of iron to become gelatinous. Mr Shuttleworth' says that an efficient dialyser may be made out of one of the flat hoops of an ordinary flour barrel, a bell jar, or even an inverted glass funnel. He gives the pre- ference to the former, and limits its diameter to ten or twelve inches; if it exceeds this, the septum is liable to bulge in the centre, • I ' Canadian Pbarmaciutical Journal,' Oct, 1877. IRON FILINGS— IRON LIQUOR 919 and to miike tho layer of Uqnid too deep at lliat. point. The pHFcbment paper employeil for the sep- tum must be entirt-ly free from liolea ; this is an casuntiul coTidition, aud If any should be discovered— by the Kimple process of spong- ing thi' upper surface of the paper with water, and tlii'U carefully examining the under sur- fiice, — they must be stopped by meiins of a little white of egg, applied and coagulated by heat; or by a drop of collodion. The parchment paper is not the Itind ordi- narily known under that name, but a less porous description, which has been niade by previous immersion in dilute sulphuric acid. Well-washed bladder, deprived of its outer coat, also makes a good septum. The septum should be tied around the hoop with twine, but not too tightly, and should be BO arranged that its edges shall be left stand- ing up around the hoop, so as to absorb any liquid escaping from the hoop at its junction with the septum. The dialyscr being ready for use, the liquid intended for dialysis is poured into it to a deptli of not more than half iin inch, and the dialyscr with its coutents is then floated on the surface of some dis- tilled water, contained in a suitable receptacle. The hoop must only be allowed to sink just below the level of tho water ; if it gets below this point, it will be necessary to keep it up by some support or tho other. It is necessary to change the water in the outer vessel daily. For the first two or three days distilled water should ahvnys be used. When this is not obtainable rain water should be enipliiyed. When the water shows the absence of chlorides, and tho preparation ceases to have a ferruginous taste, the operation may be regarded as finished. The process generally occupies one or two weeks. " A pig's bladder, completely filled with the iron solution, securely tied, and immersed in water frequently changed, answers well for making this preparation. Tho process re- quires a longer time than with a carefully re- gulated and properly conducted dialysis, but it entails considerably less trouble. 1 consider it an advantage to procure the bladder perfectly fresh, as it is then easily cleaned by pure water, and alkaline ley need not be used. Great care is necessary in tying the neck carefully. This can be best accomplished by a few turns of iron wire. Above this may be secured a piece of twine, to suspend the blad- der, by means of a stick, or rod, placed on the edge of the vessel containing the water. The bhidder should be perfectly full, and immersed altogether in water. The attraction of the solution for the water is so great, that consi- derable pressure is manifested, and should any parts or holes be in the bladder, the liquid will be forced out, water will take its place, and failure result."' Pretty general consent appears to have fixed I ' Canadian Pharmaceutical Journal,' Oct., 1877. the strength of the solution of dialysed iron at five per cent. Where .it exceeds this, the solution must he diluted with distilled water ; and where it falls short of the amount, it will have to be reduced to the required volume by standing it in a warm and dry situation. The employment of much heat must be par- ticularly avoided as it very frequently leads to the destruction of the compound ; hence every eare should be taken to render the eva- poration of the fluid nnnecssary. There seems little doubt that the so-called " dialysed iron " is an oxychloride of the metal. Prof. Maisch " believes it to be a very basic oxychloride of iron. On the supposition that the oxychloride and chloride of iron are both present in the liquid put into the dialyser, the origin of the oxychloride admits of easy ex- planation : — The chloride being a crystalloid, diffuses through the septum into the outer water, and thus becomes separates from the oxychloride, which being a colloid, and incapa- ble of a passage through the membrane, re- mains in solution in the dialyi^er. The comparative freetlom from taste and easy assimilation of the oxychloride of iron render it a valuable therapeutic agent. The dose of the five per cent, solution is 15 to 50 drops daily, in divided doses. .Svnip forms a pleasant vehicle for its administration. Dialysed iron has been successfully employed in a case of arsenical poisoning. The * Ame- rican .Journal of Pharmacy ' for January, 1878, contains an interesting paper by l)r Mattison detailing a series of experiments, which conclusively prove its value as an anti- dote to arsenic. Dr Mattison recommends the administration of the iron to be imme- diately followed by a teaspoonful or more of common salt. IRON Fr'IiIHGS. Si/n. Febbi kamestta (Ph. L. 1836). Feeei limatuba (Ph. E), Ferbi scobs (Ph. D.). The usual method of preparing iron filings for medieal purposes has been already noticed ; the only way, however, to obtain them pure, is to act on a piece of soft iron with a clean file. The Fr. Cod. orders them to be forcibly beaten in an iron mortar, and to be separated from oxide and dust by means of a fine sieve, and from the grosser parts by means of a coarse hair-sieve. — Dose, 10 to 30 gr., in sugar or honey, as a chalybeate; in larger doses it is an excellent vermifuge, especially for ascarides or the small thread- worm. lEOIT LIftTJOS. Syn. Pteolighite op IKON, Dtee's acetate op I., Black iiquoe. Tab ikon l. ; Febbi acetas vexalis, L. This article, so extensively nsed in dyeing, is a crude mixed acetate of the protoxide and sesquioxide of iron. It is usually prepared by one or other of the following methods : — 1. Old scraps of iron (hoops, worn-out tin- plate, &c.) are left in a cask of pyroligneons acid, occasional agitation being had recourse . ' Ibid., Oct.. 1877. 920 IRON, REDUCED —ISSUE to, until a sufficiently strong solution is ob- tained. By keeping the acid moderately warm in suitable vessels it will become saturated with the iron in a few days. With cold acid, on a large scale, forty days or more are re- quired to complete the process. 2. A solution of pyrolignite or crude acetate of lime, is added to another of green copperas, as long as a precipitate is formed; after re- pose, the clear liquor is decanted. IROir, EEDTTCED. Syn. Qubvenne ibon ; Febeum keeaotum (B. p.), Feeei Pulvis, L. j Fee Eeduii, F. Prep. This preparation, which consistsof metallic iron in a line state of division mixed with ii variable amount of magnetic oxide of iron, is made by passing perfectly dry hydrogen over peroxide of iron heated to red- ness in a gun-barrel. Frop. A greyish-black powder, attracted by the magnet, and exhibiting metallic streaks when rubbed with firm pressure in a mortar. Rapidly absorbs oxygen, and must, therefore, be preserved from the air in well-stoppered bottles. It dissolves in hydrochloric acid with the evolution of hydrogen. 10 grains added to an aqueous solution of 50 gi-ains of iodine and 50 grains of iodide of potassium, and di- gested with them in a small flask at a gentle beat, should leave not" more than 5 grains undissolved, which should be entirely soluble in hydrochloric acid. XTsea. In medicine it is chiefly given to restore the condition of the blood in all anaemic states of the system. There is no pulveru- lent state of iron so convenient as this for children, as it has no taste, and only a very small dose is required. — Dose, 1 to 5 grains (children, i to 1 grain), in powder, pill, or between bread and butter. Iron reduced by Electricity. See Elbo- TEiciTT, Irott reduced by. Iron, to remove Rust from Polished. Rust of iron may be removed from a polished grate by means of emery paper, or by scraping some Bath-brick to a fine powder, mixing it with a little oil and rubbing the spots well with a piece of flannel dipped in tliis mixture; after which some whiting should be applied by diligent friction. This operation requires daily repetition until the rust has disappeared. Steel fire-irons, fenders, &c., when put aside in the summer, should be previously smeared thinly over with a species of paraffin, known to druggists by the name of 'vaseline' or 'cosmoline,' or with grease, mercurial oint- ment, &c. Iron, to remove the Stains of, from Marble. Rub on very cautiously (confining it to the surface only occupied by the spot) some strong hydrochloric acid, removing it directly the spot disappears. Should this cause any diminution in the polish, this may be restored by means of emery paper. IRON WIRE. Syn. Feeeum in pila TEACTUM (Ph. L.), Feuei mlum (Ph. E.), Feebi riLA (Ph. D.), L. This is the only form of metallic iron retained in the Ph. L, It is used to make preparations of iron. ISATINE. CgHjoNA- ■*■ jeHow crystal- line body obtained by the oxidation of indigo. When acted upon by potash it becomes con- verted into aniline. Isatine may l)e formed by heating indigo in a dilute solution of di- chromate of potash and sulphuric acid, or by treating indigo under proper conditions with nitric acid. ISCHU'RIA. In pathology, retention, stop- page, or suppression of the urine. I"SINGLASS. Syn. Ichthtocolia, L. The finest kinds of isinglass are obtained from various species of the genus Acipenser, or sturgeon, that from the great sturgeon being perhaps the most esteemed. It is the air-bag, swimming bl.Tdder, or sound, dried without any other preparation than opening, folding, or twisting it. The picked or cut isinglass of the shops consists of the lamps of staple isin- glass picked in shreds by women and children, or cut by machines. JProp., S(c. Good isinglass is the purest natural gelatin known. Its quality is deter- mined by its whiteness, absence of the least fishy odour, and ready and almost entire solu- bility in boiling water; the solution forming a nearly white, scentless, semi-transparent, solid jelly, when cold. It is soluble in weak acids, and this solution is precipitated by al- kalies. The aqueous solution is not precipi- tated by spirit of the common strengths. 1 part of good isinglass dissolved in 25 parts of hot water forms a rich, tremulous jelly. It is very commonly adulterated. Of the different varieties of isinglass, the Russian is the best and most soluble. See Geiatin. ISOM'ERISM. In c?iemistry, identity of composition, with dissimilarity of properties. Isomeric compounds (isomerides) are such as contain the same elements in the same pro- portions, but which differ from each other in their chemical properties; thus, formate of ethyl and acetate of methyl are isomeric, having precisely the same ultimate composi- tion, though differing in the arrangement of their elements. ISOMORPHISM. In chemistry, the quality possessed by bodies differently composed of assuming the same crystalline form. Isomor- phous substances are found to be closely allied in their chemical nature; and the fact of two bodies crystallising in the same form has often led to the discovery of other points of similarity between them. The alums, for instance, no matter what their component"!, all crystallise in octahedra, and a crystal of potassium-alum, if transferred to a solution of chrome-alum, will continue to increase with perfect regularity from the deposition of the latter salt. IS'SUE. Syn. Fonictjltts, L. In surgery, a small artificial ulcer formed on any part of the body by means of caustic or the lancet, and kept open by daily introducing an ISSUE ISSUE PEAS-IVOHr 921 FBA covered with Fome digestive or stimnlating ointment; die wliole beiug duly secured by au appropriate bBDdage. ISSUE PEAS. Sgn. Piss peo fonticulis, L. Tliose of tlie sliops are ttie iiniuaturc fruit of t)ie orange tree (oBANaE bebbies). Tbey are usually smoothed in a lathe. Issue peas are also 'turned' from orris root.' Tlio fol- lowing compound issue peas are occasionally employed: — 1. Orris root (in powder) and Venice tur- pentine, of each I part; turmeric, 2 parts; beeswax, 3 pai-ts; melted together and made into peas whilst warm. 2. Beeswax, 3 parts; melt, add of Venice turpentine, 1 part; mix, and further add, of turmeric, 2 parts; orris root (in powder), 1 part ; mix well, and form the mass into peas whilst warm. Moro irritating than the common pea. 3. (Dr Gi ay.) Beeswax, 12 parts ; ver- digris and white hellebore, of each 4 parts; orris root, 3 parts; canthnrides, 2 parts; Venice turpentine, q. s. Used to open issues instead of caustic, but their employment requires c»re. ISSUE PLAS'TERS. See Plastebs. ITCH. Si ; and in one case of albuminuria it is nar- rated that a permanent diminution of albumen from 14-40 to 12 grammes followed its use. An alkaloid has been obtained from the piperaceous jaborandi by ParodI, and named by him Jaborandine. Some short time after- wards Mr A. W. Gerrard succeeded in separating the alkaloid from the rutaceons jaborandi, to which, in accordance with Mr Holmes' sug- gestion, and because Fnrodi had anticipated him in the adoption of the previoas title, he gave the name pilocarpine. Mr Gerrard recommends the following process for the preparation of pilocarpine : — "Prepare a soft extract either with leaf or bark, with 50 per cent, alcohol. Digest this with water, filter and wash. Evaporate the filtrate to a short extract, cautiously add ammonia in slight excess, shake well with chloroform, separate the chloroform solution, and allow it to evaporate ; the residue is the alkaloidal pilocarpine with probably a small amount of impurity." Mr Gerrard has also succeeded in preparing a crystalline nitrate and hydroclilorate of the alkiiloid, both of which possess the medicinal powers of the jaborandi. The abridged description of a sample of jaborandi from Pernambuco is from Mr Holmes' paper in the ' Pharmaceutical Journal.'' The cut is from the last edition of Royle's ' Materia Medica.' " The specimens of the plant examined a." 6 11 c Pilocarptu pitinatifoUuj. a, flower; }, flower with tbe petals removed; e, carpels- appear to belong to a shrub about 5 feet high. The root is cylindrical, hardly tapering at all, nearly J inch in diameter for the first 12 inches, and very sparingly branched. Bark of root of a ^ ' Medical Times and Gazette.' pale yellowish brown, abont a line in thickness, and has a short fracture. The root has an odour like a mixture of bruised pea-pods and orange-peel. Its taste is first like that of > Srd series, t, (81. 924 JAGGERY— JALAP. green peas; this eoon disappears, and gives rise to a tingling sensation. The stem is i inch in diameter near the root, narrowing to J inch in the upper branches. The bark is thin, greyish-brown, longitudinnlly striated, and in some specimens sprinkled over with a number of white dots. The wood of the stem is yellowish-white and remarkably fibrous. The leaves (one of which is represented in the drawing) are imparipinnate, about 9 inches long, with from 3 to 5 pairs of opposite leaf- lets, which are articulated to the rachis, and have very short, slightly swollen petlolates. The rachis of the leaf is swollen at the base. The pairs of leaflets are usually about IJ Inch apart, the lowest pair being about 4 inches from the base of the rachis. The leaflets are very variable in size, even on the same leaf. Their general outline is oblong- lanceolate. They are entire, with an emargi- nate or even retuse apex and an unequal base, and texture coriaceous. The veins are promi- nent on both sides of the leaf, and branch from the midrib at an obtuse angle in a pin- nate manner. When held up to the light the leaflets are seen to be densely pellucidly punc- tate. These pellucid dots, which are receptacles of secretion, are not arranged, as in another kind of jaborandi, in lines along the veinlets, but are irregularly scattered all over the leaf, and appear equally numerous in every part. The whole plant is glabrous." Mr Holmes says there appear to be two varieties, if not species, of this Pilocarpus, the one being perfectly smooth in every pstrt, as above described, and the other having the stems, petioles, and under surface of the leaves covered with a dense velvety pubescence composed of simple hairs. JAG'GEEY. Si/n. Pam sbgab. A coarse brown sugar made in India by the evaporation of the juice of several species of palms. The following are the principal varieties of this product : — 1. Cocoa jaggeet. From the juice of the Cocoa-nut palm (Cocos nucifera). 2. Malabar jaggeet. From the juice of the Gumraut palm (Saguerus saccherifer), 3. Mtsokb jaggeky. From th^ juice of the wild Date-palm (Phaeniic sylvesWis) j 17 galls, yields 46 lbs. 4. Paimtea jaggeet. From the juice of the Palmyra palm {Borassus Jlaielliformis) ; 6 pints yield 1 lb. JA'LAP. Si/n. jALAPa; radix, Jalapa, B. P. (Ph. L. & D.) CoNVOLVUM jalap js eadix (Ph. E.), L. The dried tubercles of the JExo- gonium purga, I. jalapa — (Royle.) Jiilap is a powerful stimulant and drastic purgative, producing copious liquid stools; but when ju- diciously administered, both safe and efiica- cious. It appears to be intermediate in its action between aloes and scammony. — Dose, 10 to 30 gr., in powder; in constipation, cere- bral affections, dropsies, obstructed monstrna- tion, worms, &c. Owing to its irritant pro- perties, its use is contra-indicated in inflam- matory affections of the alimentary canal, and after surgical operations connected with the abdomen and pelvis. It is usually adminis- tered in combination with sulphate of potassa or bitartrate of potassa and ginger; with mer- curials, as the case may indicate. The powder is very generally adulterated. Jalap Biscuits. 1. An ounce of jalap mixed with 16 ounces of the materials for ginger- bread or other kind of cake. 2. Pure resin of jalap, 56 grams, powdered sugar and flour, 1000 grams; tincture of va- nilla, 10 grams, white of egg. No. 20, yolk of egg. No. 40. Let the resin be emulsified with the yolks of the egg, add successively the sugar, tinc- ture, and -flour, and mix thoroughly into a paste, with which thorouglily incorporate the whites of eggs, previously beaten up. Let the mass be divided into 144 biscuits, and bake. Jalap, Res'in of. Syn. Besina jalaps, L. Frep. 1. (Ph. E.) See Exteaot op Jalap. 2. (NativfUe.) Jalap root is digested iu boiling water for 24 hours, and after being re- duced to thin slices more water is added, and the whole boiled for 10 minutes, with occa- sional agitation ; the liquid is then expressed in a tincture press, and the boiling and press- ing repeated a second and third time (these decoctions by evaporation yield aqueous ex- teaot op jalap); the pressed root is next treated with rectified spirit, q. s., and boiled fur 10 minutes, and then allowed to cool; the tincture is then pressed' out, and the boiling with fresh alcohol and expression is repeated twice ; a little animal charcoal is added to the mixed tinctures, and, after thorough agitation, the latter are filtered; the liquid is now dis- tilled until nothing passes over, the superna- tant fluid is poured olf the fluid resin, and the latter dried by spreading it over the surface of the capsule, and continuing the heat. The product is a friable and nearly colourless resin, which forms a white powder resembling starch. Prod. Fully 10^ of pure resin. 3. (Planche.) Resinous extract of jalap is dissolved in rectified spirit, the tincture agi- tated with animal charcoal, and after filtration gently evaporated to dryness. Pur. The jalap resin of commerce is gene- rally adulterated with scammony, gum, guaia- cum or resin. When in a state of purity, it does not form an emulsion with milk, like scammony resin, but runs into a solid mass. It is insoluble in fixed oils and turpentine, whilst the common resins are freely soluble in those menstrua. Its alcoholic solution, dropped on a piece of absorbent white paper, and ex- posed to the action of nitrous gas, does not acquire a green or blue colour; if it does, guaiacum resiu is present. 2g of this adul- teration may be thus detected. (Gobley.) It is insoluble in ether; but guaiacum resin, common resin, and some others, are so; the JALAPIC ACID— JAPANNING 92S decanted pllicr shonM not become opalescent wlien mixed witli water, and aljould evaporate without leaving any residuum. Powdered jalap resin plactd in cold water does not dis- solve, but forma n semi-lluid, transparent mass, as if it had been melted. Dissolved in a wntcli-gliiss with a little oil of vitriol, a rich crim-ou-coloured solution is obtained, from which, in a few hours, a brown viscid resin separates. Tliese last two characteristics dis- tinguish it from other resins. Obs. Eiirthenware or well-tinned copper vessels must ahme be used in the above pro- cesses, as ciintiet with copper or iron turns the resin blacic, and this tinge can only be re- moved by redissolving the resin in alcohol, the addition of animal charcoal, and re-evapo- ration. Jalap resin is an energetic cathartic. — Dose, 1 to 5 gr. See Jalapin. Jalap, Factitions Sesin of. Si/n. Re3inx JALAPX PAOTiTiA, L. A substance frequently sold for jalap resin is made by fusing a mixture of pale yellow resin and scammony resin, and adding, when it has cooled a little, but still semi-Huid, a few drops of balsam of Peru or tiilu ; the mixture is then poured into small paper capsules or tin moulds. Its eflects re- semble those of jalap resin, but it iuflaraes less. (Landerer.) Jalap, Soap of. Syn. Sapo jalapjb, Safo JALAriNUS, L. frep, (Ph. Bor.) Kesin of jalap and Castile soap, of each I port ; recti- fied spirit, 2 parts, or q. s. to dissolve the in- gredients softened by a gentle boat ; subse- quently evaporate the mixture by the heat of a water bath until reduced to 4| oz., or it has acquired the consistence of a piil-mass. Prop., ^c. A greyish-brown mass, soluble in rectified spirit. Said to be milder in its action than the resin alone. — Dose, 5 to 15 oz. JALAF'IC ACID. Syn. Odoeous pkin- CIPLE op Jalap. — Pereira. Prep. Add an alcoholic solution of acetate of lend to a similar solution of jalap resin, collect the precipitate (jalapiite of lead), and throw down the lead by means of sulphuretted hydrogen. (See Absinthic acid.) a brownish, soft, greasy sub.itance, smelling strongly of jalap, soluble in alcohol and alkali, and slightly so in ether. Jalap resin contains about 13§ of this sub- stance. JAL'APIN. CsiHsjO,,. Syn. Jalapina. Jalap resin is commonly sold under this name, but pure jalapin is prepared by one or other of the following formulas t — Prep. 1. The liquid filtered from the jala- pate of lead in preparing jalapic acid is a solution of aci tate of jalapin, which, after any trace of lend is removed, by adding a few drops of dilute sulphuric acid, aud filtration, yields the whole of its jalapin, as a precipitate, on the addition of 5 or 6 times its volume of water; this is collected, washed with a little cold distilled, water, and dried by exposure to a current of warm dry air. 2. (Hume.) Coarsely powdered jalap ia digested in strong acetic acid for 14 days, the 'tincture filtered ammonia added in ex- cess, and the whole agitated strongly; the mixture is then filtered, the deposit washed in cold water, redissolved in acetic acid, re- precipitated by ammonia, and again washed and dried. Z. (Kayser.) Pure jalap resin, in powder, is diuested for some time in boiling ether, by which means the jalapic acid is lemoved, and pure jalapin remains undissolved. Prop., S^c. Atransparent, colourless, scent- less, insipid resin, very soluble in alcohol, but insoluble in ether. It is the active purgative principle of crude jalap resin. JAMArciITE. Syn. Jamaicina. A pecu- liar alkaloid obtained by Huttensclimidt from the bark of the Cabbage-tree (Andira in- ermis). Prep. The aqueous solution of cabbnge- tree bark, treated with sulphuretted hydrogen and evaporated. Prop. Yellow crystals soluble in water and, to a limited extent, in alcohol ; fusible, and very bitter tasted. It forms salts with the acids, which, in small doses, produce restless- ness and trembling; and in larger ones, purging It is said to be vormifui;e. JAMES'S POWDER. Sec Powdebs. JAMS. Syn. Pkesbrves. Conserves of frnit with sugar, prep'.ired by boiling. In the latter respect they diU'er from the conserves of the apothecary. Prep. The pulped or bruised fruit is boiled along with i to J of its weight of loaf sugar, until the mixture jellies, when a little is plxced on a cold plate; the semi-fluid mass is then passed through a coarse hair sieve whilst hut, to remove the stones and skins of the fruit, and as soon as it has cooled a little is pouird into pots or glasses. It is usual to tie these over, when cold, with paper which has been dipped in brandy. The pots must then be placed aside in a dry and rather cold situa- tiou. I'he following fruits are those from which jams are commonly prepared : — Apricots, cher- ries (various), cranberries, currants (black, red, and white), gooseberries (ripe and green), mulberries, Orleans plums, raspberries, and strawberries. Red currants are commonly added to the last, to remove insipidity. JAPAM'. See Vaenish, aud below. JAPANHING. The art of covering paper, wood, or metal, with a coating of hard, bril- liant, and durable varnish. The varnishes or lacquers employed for this purpose in Japan, China, and the Indian Archipelago, are resin- ous juices derived from various trees belong- ing to the natural order Anaeardiaceie, espe- cially Stagmaria vemicijlua, Holigama longi- folia, Semecarpus Jnarcardium, and species of Sus (Sumach). For use, they are purified by a defecation and straining, and are afterwards mixed with a little oil, and with colouring 926 JAPONIC ACID— JELLY matter, as required. In this country var- nishes of amber, asphaltum, or copal, or mix- tures of them, pass under the names of 'japan' and 'JAPAN TABNISH.' Proe. The surface is coloured or painted with devices, &c., as desired, next covered witii a highly transparent varnish (amber or copal), then dried at a high temperature (135° to 1,65° Pahr.), and, lastly, polished. Wood and paper are first sized, polished, and varnished. For plain surfaces, asphaltum. Tarnish or japan is used, See Vaenishino. JAPONIC ACID. CijHioOs, When catechn is exposed to the air in contact with caustic alkalies, black solutions (alkaline japonates) are formed ; with carbonated alkalies, red so- lutions (alkaline rubates); the acid of the former may be separated. It is a black pow- der, insoluble in water, soluble in alkalies, and precipitated by acids. Buric acid forms red insoluble compounds with the earths and some other metallic oxides, JAEAVE. The Spanish name for saesa- FAEILLA BEER. See Beekb (in pharmacy). JASPER. Syn. Iaspis, L. A mineral of the quartz family, occurring in rocky masses. It takes various shades of red, yellow, brown, and gi-een, and is occasionally banded, spotted, or variegated. It was formerly used as an amulet against h83morrbages and fluxes. It is now extensively worked up into rings, seals, snuff-boxes, vases, &c., for which it is well cal- culated from its extreme hardness and suscep- tibility of receiving a fine polish. JATRO'PHIC ACID. Syn. Ceotonic AOId, Iateophio a. a peculiar fatty acid disco- vered by Pelletier and Caventon, and originally regarded by them as the cathartic principle of croton oil and croton seeds, but since shown by Redwood and Pereira to be nearly inert. Prep. The oil is saponified by caustic pota«sa, and the resulting soap is decomposed by tar- taric acid ; the fatty matter which fioats on the surface of the liquid is then skimmed off the aqueous portion, and the latter submitted to distillation ; the liquid in the receiver is a solution of jatrophic acid. Prop., S(c. Volatile ; very acid ; has a nau- seous odour ; is solid at 23°, and vaporizes at 3.5° Pahr. It forms salts with the bases, none of which possess any practical importance. JATI'MANGE. Prep. From isinglass, 1 oz.; boiling water, 12 oz. ; dissolve, add of any sweet white wine, 4 pint; the yolks of 2 eggs beaten to a frpth, and the grated yellow peel of two lemons ; mix well, and heat the whole over the fire until sufficiently thickened, stir- ring all the time ; lastly, serve it np or pour it into moulds. JAUN'DICE. Syn. loTBEUS, Moebtts ltt- TBOins, L. A disease characterised by a yel- low colour of the eyes and skin, deep-coloured urine, and pale alvine evacuations. It appears to arise from a disordered action of the brliarj organs. The treatment consists of the admi- nistration of saline aperients, and small doses of blue-pill, followed by tonics and diaphoretics. The action of these remedies should be pro- moted by the copious use of diluents (particu- larly saline water), and exertion in the open air, when possible. When there is much pain and vomiting, anodynes (or opium, morphia, &c.) may be administered. Janndice is not in itself a dangerous disease, but it some- times lays the patient open to attacks of others which are so. Animals. — Jaundice affects cattle, givingrise to a tawny hne of the skin and membranes, Pleuro-pneumonia is frequently followed by jaundice. The best remedies are large doses of Epsom salts combined with ginger; and if these fail to remove the costiveness, a drachm of calomel should be added. If necessary, the above purge must be repeated next day, the action being assisted by giving the animal warm fluids. Tonics and stimulants are also sometimes superadded to the above treatment. JEL'LT. Syn. Gblatina, L. A term now very loosely applied to various substances which are liquid or semi-liquid whilst warm, and be- come gelatinous on cooling. Jellies are coloured by the addition of the usual stains used by confectioners, and are rendered transparent by clarification with white of egg. Jelly, Almond. Syn. Gelatiita amtoda- LAETJM, L. Prep. From rich almond milk, i pint ; thick hartshorn jelly, i pint ; susar, ii oz. ; with 2 or 3 bitter almonds and a little lemon peel, to flavour, heated together, strain ed, and moulded. Jelly, Ar'row-root. Syn. Gelatina m aeantje, L. From arrow-root, \\ oz., to water, 1 pint. Tons les mois jelly is made in the same way. Jelly, Bis'cuit. Prep. From white biscuit (crushed beneath the rolling-pin), 4 oz. ; cold water, 2 quarts ; soak for some hours, boil to one half, strain, evaporate to 1 pint, and add, of white sugar, | lb., red wine, 4 oz., and cinnamon, 1 teaspoonful. In weakness of the stomach, and in dysentery and diarrhea, and in convalescence combined with rich beef gravy or soup. Jelly, Bladder-wrack. (Dr Russell.) Syn. Gelatina fuci. Prep. Bladder-wrack {Fucus vesiculosus), 2 lbs. ; sea water, 2 lbs. ; macerate for 15 days. Applied to glandular tumours. Jelly, Bread, Syn. Panada ; Geiatina PANis, L. Prep. Cut a French roll into slices, toast them on each side, and boil in water, 1 quart, until the whole forms a jelly, adding more water if required ; strain, and add sugar, milk, &c., to palate. It may be made with bnith from which the fat has been skimmed, instead of water. Used as the last. Jelly, Broth. Syn. Soup-jellt. Prom broth or sonp from which the fat has been skimmed, evaporated until it becomes gelatinous on cool- ing. A few shreds of isinglass are commonly added. See Soup (Portable). JELLY 927 Jelly, Calvei' Feet. Prep. For each foot take of water 3 pints, and boil to one half ; cool, ekim off the fat, and again boil for 2 or 3 minutes with the peel of a lemon and a little spice ; remove it from the fire, strain through a jeliy bug (see Filtkatioh), add the juice of u lemon and a glass of wine, and when it has cooled a little put it into glasses or ' forms.' Obt. If this jelly is required to be very transparent it must be treated as follows : — After Ihe fat is removed it should be gently warmed, just enough to melt it, next well beaten with the white of an egg and the sea- soning, and then brought to a boil for a minute or two, when it will be ready for straining, &c. The calves' feet should not be bought ready boiled, but only scalded. Cows' feet (' CO'W HKBLs') make nearly as good jelly as that from calves' feet, and are much more economical. Jelly, Ceylon Moss. Syn. Gblatina gbaoi- lAKlJ?, L. JPrep. (Dr Sigmond.) Boil Ceylon moss (Oranularia liohenoides), i oz. in water, 1 quart, for 25 minutes, or till the liquid jellies on cooling; strain and flavour. Very nutri- tious ; recommended in irritation of the mucous membranes and phthisis. Jelly, Copaiba. (M. Caillot.) Syn. Gbla- TtNA coi'AlBA. Prep, Isinglass, 4 parts ; water, 40 parts ; dissolve in a water bath, and add 20 parts of sugar ; pour the clear liquid jelly into a warm mortar, and add copaiba, 60 parts; triturate, and pour in a vessel to jelly. Flavour with some aromatic essential oil or balsam of tolu. Jelly, Cor'sican Moss. St/n. Gelatina hel- MISTHOOORTI, L. JPrep. (P. Cod.) Corsicaii mi)S3 (Oracilaria Selminthooorton), 1 oz. ; water, q. s. ; boil 1 hour, and strain 8 fl. oz. ; to this add of isinglass (previously soaked in a little water), 1 dr. ; refined suirar, 2 oz. ; white wine, a wine-glassful. Vermifuge. See DECOCTIOIf. Jelly, Fruit. Under this head we include those jellies made from the juices ol fruits. Frep. The strained juice mixed with J to i its weight of refined sugar, uniil it 'jellies' on cooling, observing to carefully remove the scum as it rises. The process should be con- ducted by a gentle heat, and it is preferable not to add the sugar until the juice is some- what concentrated, as by lengthened boiling the quality of the sugar is injured. Oba. Jellies are sold in pots or glasses, like JAMS. Both jams and fruit jellies are refrige- rant and laxative ; they are, however, mostly employed as relishes, especially during fevers and convalescences. The principal fruit jellies are : — Apple, BARnERBT, ohebby (from either Cornelian or Kentish cherries), oubeant (black, white, and red), kldeebbebt, ooosebeebt, PLDM, QUINCE, easpbeeby. See Lemon and Obanqe jelly. Jolly, Glycerin. Syn. Gelatina glyce- BlNi. Mix glycerin to the required consist- ence with compound tragacanth powder. Or take powdered gum Arabic, \ oz. ; syrup, 4 oz. (3 oz. of sugar to 1 oz. of water); the yolks of 3 eggs; olive oil, 4 oz. ; glycerin, 2 oz. Rub the gum and syrup well together, add the yolks, and when mixed add the oil and plvce- rine, previously triturated together. Applied to chapped bauds, abrasions, &c. See Glycb- BIN ov Stabch. Jelly, Gra"vy. By evaporating meat gravies Jelly, Harts'hom. Syn. Gelatina cobnit CEBVi, L. Prep. (P. Cod.) Hartshorn shav- ings, 8 oz. ; wash it in water, then boil in clean water, 3 pints, till reduced to one half; strain, press, add of sugar, 4 oz., the juice 'of one lemon, and the white of an egg beaten up with a little cold water ; mix well, clarify by heat, evaporate till it jellies on cooling, then add the peel of the lemon, and set it in a cool place. It may be flavoured with wine, spices, &c. Very nutritious. Jelly, Iceland Uoss. Syn. Gelatina li- CHENIS, L. Prep. (P. Cod.) Iceland moss, 2 oz. ; soak for 1 or 2 days in cold water, then boil for 1 hour in water, q. s. to yield a strong solution ; stain, decant the clear after repose, apply heat, and dissolve therein of isinglass, 1 dr. ; evaporate the whole to a proper con- sistence, put it into pots, and set them in a cool place. Nutritions. Recommended in phthisis. The jelly of Iceland moss and cin- chona (OELATINA LI0HEN18 CtTM CINCHONA — P. Cod.) is made by adding to the above syrup of cinchona, 6 fl. oz. Jelly, Iceland Moss (Sweetened). (P. C.) Syn. Gelatina liohenis sacchakata. Prep. Saccharatcd Iceland moss (see Iceland moss, SacCHABATEd), 7i oz. ; sugar, 7i oz. ; nut. r, 15 oz. ; orange-flower water, 1 oz. Boil the first three substances and remove the scum which forms, and then let the jelly flow into a vessel which contains the orange-flower water. Jelly, r'rish Moss. Syn. Gelatina chon- DBi, L. Prep. From Irish or carrageen moss. See Decoction. Jelly, I"Binglass. Syn. Confectionkes' JELLY ; Gelatina ichthyocoll^, L. Pr/-p. From isinglass dissolved Hi water by boiling, and evaporated till it ' jellies ' on cooling, adding flavouring, as desired, li oz. of good isinglass makes fully a pint of very strong jelly. See Blancmange, Isinglass, Caltes-fjiKT Jellt, &c. Jelly, Lem'on. From isinglass, 2 oz. ; water, 1 quart; boil, add of sugar 1 lb., clarify, and when nearly cold add the juice of 5 lemons, and the grated yellow rinds of 2 oranges and of 2 lemons ; mix well, strain off the peel, and put it into glasses. Jelly No'yean. As Prircn jellt, but strongly flavoured with bitter almonds. Jelly, Or'ange. From orange juice, 1 pint; let it stand over the grated yellow rind of 3 or4of the oranges for a few hours, then strain, and add, of loaf sugar, J lb., or more, isinglass 928 JEEVINE— JUNIPER BERRIES i oz., dissolved in water, 1 pint ; mix, and put It into glasses before it cools. Jelly, Puncli. From isinglass, 2 oz.j sngar. If lb.; water, 1 pint; dissolve, add of lemon juice, i pint; the peels of 2 lemons and of 2 oranges; rum and brandy, of each i pint; keep it in a covered vessel until cold, then liquefy it by o. very gentle heat, strain, and pour it into moulds, A pleasant and decep- tive way of swallowing alcohol. Jelly, Quince. (E. P., 1744.} St/n. Gbla- TINA OYDONIOEUM. Frep. Juioe of quinces, 3 lbs. ; sugar, lib. ; boil to a jelly. Jelly, Rice. Sj/n. Cbeme de Riz. From rice bdlled in water, sweetened, and flavoured. Jelly, Sago. Prep. Soak sago in cold water for 1 hour, strain, and boil in fresh soft water until it becomes transparet; then add wine, sugar, clear broth, milk, or spices, to flavour. 1 oz. of sugar makes a pint of good jelly. Jelly, Salep. (Soubeiran). S^n. Gelatina SALEPiE. Frep. Ground salep, 4 dr. ; sugar, 4 oz. ; water, a sufiicient quantity. Boil to 12 oz., and flavour to the taste. Jelly, Ta'pioca. As Saoo jellt, but using tapioca in lieu of sago. JEEVINE. CjoHjNjOj An alkaloid dis- covered in 1837, by Simon, in the root of the Veratrum album, and by Mitchell, in 1874, in the root of the Veratrum viride. Dr H. C. Wood, jun., describing the physiological efiects of jervine, says they consist " in general weak- ness, lowering of arterial pressure, a slow pulse, profuse salivation, and finally convul- sions." Jervine was analysed by Will, who ascribed to it the above composition. JES'UIT'S BARK. See ClifCHOlfA. JESUIT'S DROPS. See Dbops. JESUIT'S POWDER. Powdered cinchona bark. JET. A variety of mineral bituminous carbon, very hard, and susceptible of a fine polish. JEWELS. See Diamond, Emebaid, Gems, &c. JEWEL'RY. The gold in articles of jewelry, whether solid or plated, which are not intended to be exposed to very rough usage, is generally ' coloured,' as it is called in the trade. This is done as follows : — 1. (Reb sold ooiouE.) The article, after being coated with the amalgam, is gently heated, and, whilst hot, is covered with gilder's wax ; it is then ' flamed' over a wood fire, and Btrongly heated, during which time it is kept in a state of continual motion, to equalise the action of the fire on the surface. When all the composition has burned away, the piece is plunged into water, cleansed with the 'scratch- brush' and vinegar, and then washed and bur- nished. To bring up the beauty of the colour, the piece is sometimes washed with a strrag solution of verdigris in vinegar, next gently heated, plunged whilst hot into water, and then washed, first in vinegar, or water soured with nitric acid, and then in pure water ; it is, lastly, burnislied, and again washed and dried. 2. (Oe-molit coioue.) This is given by covering the parts with a mixture of powdered hematite, alum, common salt, and vinegar, and applying heat until the coating blackens, when the piece is plunged into cold water, rubbed with a brush dipped in vinegar, or in water strongly soured with nitric acid, again washed in pure water, and dried. During this process, the parts not to be dried in 'or-molu colour' should be carefully protected. The frauds practised in reference to the • fineness' of the metal used in jewelry is noticed under Gold (Jeweller's). See also AssAYiNo, Diamond, Gems, Gildins liquoe, GiLDiNct wax, &c. JEW'S PITCH. See Asphaititm. JOURNAL BOXES, Alloy for. Copper, 24 parts; tin 24 parts; antimony, 8 parts. First melt the copper, then add the tin, and lastly the antimony. JUICE (Spanish). See Extbact and LlQUOEIOE. JU'JUBE. A fruit resembling a small plum, produced by various specie^ of Zizt/phus. Com- bined with sugar, it forms the jujube paste of the shops, when genuine; but that now almost always sold under the name is a mix- ture of gum and sugar, slightly coloured and flavoured. JU'LEP. Syn. Julap ; Julepum, Julepus, Juiapium, L. a term usually regarded as synonymous with 'mixtube'; but according to the best authorities, implying a medicine which is used as a vehicle for other forms of medicine. The word comes through the French, from a Persian expression, which sig- nifies 'sweet drink.' A julep, according to Continental writers, is a drink of little activity, generally composed of distilled waters, infu- sions, and syrups, to which mucilages and acids are sometimes added ; " but never powders or oily substances, which could interfere with its transparency." In England the juleps of old pharmacy are now classed under ' mixtuees.' JU"NiPER BERRIES. Syn. Junipeki BAOO^, J. communis BACOa; (Ph. E.), JUKI- PEEU8 (Ph. L.), L. The fruit of the Juniperus communis, or common juniper tree. In the old Ph. L. & D. both the tops and berries (juni- peki peuotUs ET OACUMINA— Ph. L. 1836; JUNIPEEUS — BACC^, CACUMINA — Ph. D. 1862) were ordered. The berries are stomachic and diuretic, and have been long employed in drop- sies, either alone or combined with foxglove and squills. The tops (summitates) have been highly praised in scurvy and certain cutaneous affections. — Dose, 1 to 2 dr., made into a conserve with sugar, or in the form of infusion or tea. Donath found 100 parts of the berries to contain — Water .... 2944 Volatile oil . . . -91 Formic acid . . . 1-86 JUNKET— KAMALA 929 Broaghl forward . 32-21 Acotic acid ■94 Sralic acid (combined) •21 Oxalic acid traces \Vax-like fatty matter . ■64 Green resin (from ethereal solation) 8-46 Hard brown resin (from nlcoboUc solution) 1-29 Bitter principle (called juniperin) . •37 Pectine . . . . •73 Albuminous substance! . 4-45 Sugar . . . . 29 65 Col hi lone , 1583 Mineral sabstances . 233 9M1 JUN'KET. St/n. DBVONsniBB jonket, CuuD JELLT. Ji'rom warm milk put into a bowl, and then turned with a little rennet ; some scalded cream and sugar are next added, with a sprinkling of cinnamon on the top, without breaking the curd. Much esteemed by holiday folk iji the western counties during the hot weather of summer. Sometimes, very strangely, a little brandy finds its way into these trifles. JUTE. This is the fibre yielded by the Cof chorus eapaularis, a lime tree growing in India and China. It is the material of which sacks, gunny bags, and coarse thread are made. It mixes even with linen or cotton, and hence may not improbably be employed as a sophis- ticant of these substances. The plates on piige 929 exhibit the different microscopic appearances of the three sub- stances. KALEIDOSCOPE. . Syti. Flo-web-olass. A pleasing philosophical toy invented by Sir David Brewster, which presents to the eye a series of symmetrical changing views. It is foi-med as follows : — Two slips of silvered glass, from 6 to 10 inches long, and from 1 to 1 i inch wide, and rather narrower at one end than the other, are joined together lengthwise, by one of their edges, by means of a piece of silk or cloth glued on their backs j they are then placed in a tube of tin or pasteboard, blackened inside, and a little longer than is necessary to contain them, and are fixed by means of small pieces of cork, with their faces at an angle to each other that is an even aliquot part of 4 right angles (as the J, J, -stj, &c.). The other end of the tube is then closed wiih an opaque screen or cover, through which a small eveliole is made in the centre; and the other end is fitted, first with a plate of common glass, and at the distance of about Jth of an inch, with a plain piece of slightly ground glass, parallel to the former; in the inter- mediate place or cell are placed the objects to form the images. These consist of coloured pieces of glass, gla.«s beads, orany other coloured diaphanous bodies, sufiiciently small to move VOL. II. freely in the cell, and to assume new positions when the tube is shaken or turned round. A tube 80 prepared presents an infinite number of changing and symmetrical pictures, no one of which can be exactly reproduced. This toy is so easily constructed, is so very inex- pensive, and at the same time so cap.ible of affording an almost inexhaustible fund of amusement to the young, thot we advise our juvenile friends to try their bands at its con- struction. Any common tube of tin or paste- board may be used, and strips of glass smoked on one side will answer for mirrors. KA'LI. The name formerly applied to a speciesof SoiioiaemployedformakingBARiiLA. It is sometimes used as a designation for the crude alkalies, and is the Qerman synonym for ' potassa.' Kali, Acid'ulated. Syn. Leuon and eaii, LsuoNZATED K. A common preparation of the shops for making a pleasant effervescing drifught. It is sometimes incorrectly styled ' citrate of potash.' Prep. 1. Carbonate of soda and tartaric acid, of each 6 oz. ; lump sugar, 1 lb.; all in the state of fine powder, and separately dried by a very gentle heat, after which they are mixed together, flavoured with essence of lemon, 1 dr., rubbed through a gauze sieve in a warm dry situation, put into bottles, and corked down immediately. 2. Fitiely powdered white sugar, 16 lbs. ; tartaric acid, 4i lbs. ; carbonate of soda, 4 lbs. ; essence of lemon, 1 oz. ; as the last. Keeps well. A dessert-spoouful of either thrown into a glassful of water makes a pleasant effer- vescing draught. KA'LIUM. [L.] Potnssium. KAL'YCOB. A cosmetic lotion ; it resem- bles ' Gowland'b Lotion,' but is got up in a rather more pleasing style. See Lotion. KAUAIiA. A powder consisting of the minute glands obtained from the capsules of the RoUlera tinctoria, a plant belouging to the nat. ord. Euphorbiacea. Kamala is im- ported from India, where it is known under the name of kameela. The rottlera, from which it is obtained, is a tree from 15 to 20 feet in height, indigenous to India and to many of the East Indian Is^lands. Kamala has long been employed in India as a remedy for tapeworm, and within the last few years has been given for the same purpose in this country with very general success. It may be administered in doses of from thirty grains to three drachms, suspended in water, rubbed up with mucilage, or mixed with syrup. In large doses, such as three drachms, it some- times purges violently. After the third or fourth motion the worm is generally evacuated dead. A second dose may be taken in about four hours should the first fail to act ; or in- stead of a second dose, some castor oil may be given. Kamala is also used extcrnnUy by the natives of India in various skin complaints, particularly in scabies. It is also said to have proved useful in herpetic ringworm. 59 JUTE KAOLIN— EERMES 931 Dr ilnderson obtained from the resinous colnuring maiter, which ia the principal con- stituent of kamula, u yellow crystalline sab> ■t«nce, to which he gave the name rottUrin. The existence of rottlerin has since been con- firmed by Mr Groves, who found that it becomes changed by exposure, a circumstance to which hu attributes its non-detection in old specimens of the drug, and to which may very reasonably be attributed Leube's failure to find it. The 'British Pharmacopoeia' ascribes the following ' characters ' to kaniala :— " A fine granular mobile powder, of a brick-red colour; it is with difficulty mixed with water, but when boili-d with alcohol the greater part is dissolved, forming a red solution. Ether dis- eolves most of it, the residue consisting prin- cipally of tufted hairs. It nliould be free from sund or earthy impurities." Karaala forms a very considerable article of export from India, it being a valuable dye. KA'OIiIN'. Syn. China ci,at, Poboblain 0. A fine white clay, derived from the decom- position of the felspar of granitic rocks. The potteries and porcelain works of this country are chiefly supplied with this substance from cxten^iv« tracts of it which occur near St Austie, Cornwall. See Clay. Eisner ' gives the following process for dis- tintcnishing kaolin from ordinary clay : — He agitates it in a test-tube wicli pure strong sulphuric acid till n uniform mixture is pro- duced, decants the acid after subsidence, dilutes it carefully with six volumes of water, and supersaturates tiie cooled solution with ammonia- Kaolin thus treated separates but slowly from the strong acid, and the diluted acid solution gives an immediate white precipitate witii ammonia, whereas ordinary day is but slightly attacked by the acid, separates quickly from it, and the acid after dilution gives but an insishificant precipitate with ammonia. KAFKOMOR. Syn. Capnomor. A colour- less oil obtained from crude kreasote by dis- tillation with potassa. It boils at 360° Fahr., has a peculiar odour, and is insoluble in water, but readily soluble in an alkaline solution of krea>ote. EATAL'TSIS. Syn. Catalysis, Contact ACTION. Terms applied to a class of chemical actions in which the decompositions, and the recombination of the elements of compound bodies, is apparently excited by the mere pre- sence of, or contact witlj, other bodies, which do not tliemselves suffer such a change. KAVA-KAVA. See Ava. KELP. The alkaline ashes obtained by burning various species of sea-weed, formerly much used for the preparaiion of carbonate of soda. The weeds most valued for the purpo>e are the Fucus vesictdosua^odosus, and tfrratus, and the Laminaria ouliosa ani digitala. ' Dingl., 'Pot. Journ.'(WaUB). Of late years the manufacture of kelp, like that of barilla, has been almost abandoned, except as a source of iodine. Mr E. C. C. Stanford, by carefully collecting and com- pressing the weed, and afterwards subraittini; it to dry distillation, doubles the yield of iodine and bromine, and obtains in addition various valuable hydrocarbons. See Babilla, lODiNK, Soda, &c. KEE'MES. Syn. Keemkb gbains, Al- KBBMKS; GeaNCM TINOTORIUM, L. The dried bodies of the female Coccus Ilieu of Linnseus, a small insect of the order Semiptera, which flourishes on the Ilex oak. It has been u«ed as a red and scarlet dye-stuff ever since the time of Moses ; but is now superseded in this country by cochineal, which gives colours of much greater brilliancy. EER'MES MIN'EEAl. Syn. Kebsies MINEBALB, E. MINEBALIS, L. An amorphous tersulphide of antimony, containing a small admixture of teroxide of antimony and sul- phuride of potassium. Frep, 1. Ik the Htr- MID WAY.— o. (P. Cod.) Carbonate of soda (eryst.), 128 parts (say 21 parts), is dissolved in water, 1280 parts (say 210 parts), contained in a cast-iron pan; tersulphide of antimony (in fine powder), 6 parts (say 1 part), is next added, and the whole boiled lor an hour, with constant agitation with a wooden spatula ; the boiling liquid is then filtered into a heated earthen pan containing a small quantity of very hot water, and the solution is allowed to cool as slowly as possible; the red powder which is deposited is collected on a cloth, pn which it is well washed with cold water, and the superfluous water being removed by pres- sure, the powder is dried by a gentle heat, and is, lastly, passed througli a fine silk-gauze sieve, and preserved from light and air. b. (Wholesale.) From black sulphuride of antimony, 4 lbs. ; carbonate of potassa, 1 lb. ; boll in water, 2 galls., for half an hour, filter, &c., as before. The undissolved portion of sesquisulphuret of antimony may be boiled again several times with fresh potassa and water, until the whole is dissolved. Inferior to the last. c. (Clczbll's KEEMES.) Prom tersulphide of antimony, 4 parts j crystallised carbonate of soda, 90 parts; water, 1000 parts; boil, &c., as in 1, a, and dry the powder, folded up in paper, at a heat not exceeding 90° Fahr. 2. In the dey way. — a. (P. Cod.) Car- bonate of potassa, 100 parts; tei-sulphide of antimony, 50 parts; sulphur, 3 parts; mix, fuse in a Hessian crucible, pour tbt melted mass into an iron mortar, and when cold reduce it to powder; next boil it in water, 1000 parts, contained in an iron vessel, filter the solution, and otherwise proceed as before. Product : large, hnt of inferior quality. 4. (Fownes.) From tersulphide of anti- monv, 5 parts; carbonate of soda (dry). 3 parts; water, 80 parts; fuse, &c., as before. Nearly equal to 1, a. 932 KETCHUP e, (Berzelins.) Carbonate of potassa (pure), 3 parts; tersulphide of antimony, 8 parts; water, q. s. Resembles the last. Prop., ^c. An odourless, tasteless powder, insoluble in both water and alcohol, and, when pure and carefully prepared, entirely soluble in hydrosulphate of ammonia. As prepared by the formulas 1, a, and 1, o, it is a very dark crimson powder, of a velvety smoothness ; but that from the other formulae has a brownish- red colour, more or less deep. The secret of preparinj? this compound of a fine and velvety quality, like that imported from the Conti- nent, consists simply in filtering the solution whilst boiling hot, and allowing it to cool very slowly, by placing the vessel in an appropriate situation for that purpose. Another important point, according to Rose, is to employ suffi- cient alkali to keep the whole of the teroxide of antimony in solution as the liquid cools, instead of allowing a part of it to he deposited with the kermes. This is the reason of the superior quality and mildness of that prepared according to the directions of the French Codex. The liquor decanted from the 'kermes mineral' yields the golden sulphide of anti- mony on the addition of an acid, for which purpose the acetic is generally employed. IDose, i gr. to 3 or 4 gr., as a diaphoretic, cathartic, or emetic. It occupies in foreign practice the place of our James's Powder. KETCH'OP. Syn. Catchdp, Catsup, Katoh- UP. The juice of certain vegetables strongly salted and spiced, so as to be used as sauce ; or a simple sauce made without the natural juice as a substitute for the true ketchup. The following are the principal varieties : — Ketchup, Camp. Prep. Take of good old beer, 2 quarts; white wine, 1 quart; anchovies 4 01.; mix, heat it to the boiling-point, re- move it from the fire, and add of peeled shalots, 3 oz.; mace, nutmegs, ginger, and black pepper, of each, bruised, \ oz. ; macerate for 14 .days, with frequent agitation, then allow it to settle, and decant and bottle the clear portion. Ketchup, Cu' cumber. Prep. From ripe cu- cumbers, in the same way as mushroom ketchup. Very luscious. Mixed with cream, or melted butter, it forms an excellent white sauce for fowls, &c. Ketchup, Marine'. Prep. Take of strong old beer, 1 gall.; anchovies, 1^ lb.; peeled shalots (crushed), 1 lb.; bruised mace, mustard seed, . and cloves, of each i oz. ; bruised pepper and ginger, of each J oz. ; mushroom ketchup and vinegar, of each 1 quart; heat the mixture to the boiling point, put it into a bottle, and ma- cerate for 14 days, frequently shaking ; then strain through flannel, and bottle it for use. Excellent with anything ; like the last, it makes good white sauce, and keeps well. Ketchup, Mush'room, Prep. 1. Sprinkle mushroom flaps, gathered in September, with common salt, stir them occasionally tor 2 or 3 days, then lightly squeeze out the juice, and add to each gallon cloves and mustard seed. of each, bruised, } oz.; allspice, black pepper, and ginger, of each, bruised, 1 oz.; gently heat to the boiling-point in a covered vessel, mace- rate for 14 days, and decant or strain. Should it exhibit any indications of change in a few weeks, bring it again to the boiling-point, with a little more spice, and a table- spoonful more salt. 2. Take of mushroom juice, 2 galls.; pi- mento, 2 oz.; cloves, black pepper, mustard seed, and ginger, of each, bruised, 1 oz.; salt, 1 lb. (or to taste); shalots, 3 oz. ; gently simmer for 1 hour in a covered vessel, cool, strain, and bottle. 3. Take of mushroom juice, 100 galls. ; black pepper, 9 lbs. ; allspice, 7 lbs. ; ginger, 5 lbs.; cloves, 1 lb. (all bruised); salt, q. s. ; gently simmer in, a covered tin boiler for 1 hour. Ketchup, Oys'ter. Prep. Pulp the oysters, and to each pint add, of sherry wine, or very strong old ale, 1 pint; salt, 1 oz.; mace, i oz.; black pepper, 1 dr.; simmer very gently for 10 minutes, strain, cool, bottle, and to each bottle add a spoonful or two of brandy, and keep them in a cool situation. Cockle ketch- up and MUSSEL KETCHUP are made in the same way. Used to flavour sauces when the fish are out of season ; excellent with rump steak, &c. Ketchup, Pon'tac. Prep. Take of the juice of elderberries and strong vinegar, of each 1 pint; anchovies, i lb.; shalots and spice, q. s. to flavour ; boil for 5 minutes, cool, strain, and bottle. Used to make fish sauces. Ketchup, Toma'to. Prep. Prepared from tomatoes or love apples, like mushroom ket- chup, except that a little very strong Chili vinegar is commonly added. An admirable relish for * high' or rich flavoured viands. Ketchup, Wal'nnt. Prep. 1. Take of the expressed juice of young walnuts, when tender, 1 gall. ; boil 10 minutes, skim, add of ancho- vies, 2 lbs.; shalots, 1 lb.; cloves and mace, of each 1 oz. ; 1 clove of garlic, sliced ; simmer in a covered vessel for 15 minutes, strain, cool, and bottle, adding a little fresh spice to each bottle, and salt, q. a. Will keep good in a cool place for 20 years. 2. Take of green walnut shells, 16 galls.; salt, 5 lbs. ; mix and beat together for a week, press out the liquor, and to every gallon add, of allspice, 4 oz. ; ginger, 3 oz. ; pepper and cloves, of each 2 oz. ; all bruised; simmer for half an hour, and set aside in a closed vessel and in a cool situation until sufficiently clear. 3. Take of walnut juice, 1 gall.; vinegar, 1 quart; British anchovies (sprats), 3 or 4 lbs.; pimento, 3 oz.;. ginger, i oz.; long pepper, J oz. ; cloves, 1 oz. ; shalots, 2 oz. j boil and bottle, as before. 4. Prom the juice of walnut shells, 30 galls.; salt, 1 bushel ; allspice and shalots, of each 6 lbs. ; ginger, garlic, and horse-radish, of each 3 lbs. ; essence of anchovies, 3 galls. ; as before. KIBES— KINO 933 Ketchnp, Wine. Frep. Take of mnshroom or walnut ketchup, 1 quart; chopped ancho- vies, \ lb.; 20 shalots; scraped horse-radish, 2 oz. ; spice, q. s. ; simmer for 15 minutes, cool, and add of white and red wine, of each 1 pint ; miicerate for 1 week, strain, and bottle. General 'Remarks. In preparing the above articles, vessels of glazed earthenware, or stone- ware, or well-tinned copper pans, shoald alone be used to contain them whilst being boiled or heated, as salt and vegetable juices rapidly corrode copper, and render the ketchnp poi- sonous. Nothing in the shape of copper, lead or pewter should be allowed to touch them. Even a plated copper spoon left in a bottle of ketchnp for some time will render its contents poisonous. Unpleasant and even dangerous fits of vomiting, colic, and diarrhcca have re- sulted from the neglect of this precaution. See Sauce, &c. KIBES. Tlie vulgar name for ulcerated chilbbins. KID'NEYS. Syn. Renes, L. (In anafomy.) The kidneys, as almost every one knows, are abdominal viscera which secrete the urine, and form the great channels by which the effete nitrogenous matter is removed from the blood. They are subject to various affections, both functional and organic, chronic and acute, of which some are imperfectly understood, and others only admit of alleviation, but not of being cured. See Ubinb and Ueinaey af- fections. Kidneys. (In cookery.) Soyer recommends kidneys to be dressed by gently broiling them, having previously split them, " so as nearly to divide tliem, leaving the fat in the middle," and " run a skewer through them, that they may remain open." After being rubbed with a little butter, and seasoned with salt and pepper, "they may be served on toast, or with any sauce." "You may also egg and bread- crumb them." "Five minutes su6fice for a sheep or lamb's kidney of common size." (Soycr.) One or two lamb's kidneys, plainly broiled and served up with the gravy in them, eaten along with a little dry-toasted bread, form a most excellent and appropriate luncheon or dinner for a dyspeptic or conva- lescent. KIESEBITE. A sulphate of magnesia found in the refuse salt (abraumsalz) of Stassfnrt, neur Magdeburg. It forms about 12S of the abraumsalz. It is employed for washing wool and for the manufacture of ' permanent white' by treatment with chloride if barium ; also for the preparation of Glauber salts, and of hypochlorite of magnesia for bleaching linen. See LiifBtr. KING'S CUP. Frep. Yellow peel of 1 lemon ; lump sugar, IJ oz. ; cold water, 1 pint; infuse 8 or 10 hours, and strain. The addition of a tenspoonful of orange-flower water is a great improvement. Used as a diluent in cases where acid liquors are inadmissible. See Lemonade. KING'S EVIL. SeeScROPCLA. KING'S YELLOW. See Yellow pig- ments. KI'NIC ACID. HCyHuOj. Syn. Qttinic ACID, ClNCHONic ACID. A peculiar monobasic acid occurring in the cinchona barks, in which it exists associated with the alkaloids. Kinic acid is somewhat extensively diffused throughoul the vegetable kingdom, being found in the bark of every.species of the true cinchonas, as well as in the leaves of the oak, the elm, the ash, the ivy, the privet, and the coffee plant and berries. It occurs in 'the cinchona barks most probably combined with the alkaloids, which therefore exist in the plant as kinates. It is readily obtained from kinate of lime by the action of dilute sulphuric acid; the filtered solution evaporated to the consis- tence of a syrup, gradually deposits large crystals resembling those of tartaric acid. Henry and Plisson give the following directions for the preparation of kinic acid : — Make a decoction of cinchona bark with water containing some sulphuric acid, and filter whilst hot, and to the filtrate add gradually freshly precipitated oxide of lead, until the liquid becomes neutral, and changes from a red to a pale yellow colour; care must be taken to add sufficient oxide. The filtrate is freed from lead by passing sulphuretted hydrogen through it, and filtered milk of lime is then added to precipitate the quinine and cinchonine; and tlie filtered liquid is evapo- rated to a syrup, which yields on cooling crystalline callic kinate. To separate tBe acid from the calcic salt, Berzelius directs an aqueous solution of the salt to be made and to be precipitated by basic acetate of leadj the washed precipitate, suspended in water, is then decompo-cd by sulphuretted hydrogen, and tlie solution filtered and evaporated. Or the calcium kinate may be decomposed by an aqueous or alcoholic solution of sulphuric acid.* Kinic acid is, in the form of large tubular crystals, fusible at 161° C. These crystals dissolve in two parts of water; they are also soluble in spirits of wine, but scarcely, if at all, in ether. It forms salts called kinates. Kinate of calcium is obtained from an acidulated infu- sion of cinchona bark, by adding an excess of lime, filtering, evaporating to a syrup, and setting the liquid aside to crystallise. These crystals are purified by re-dissolving them, treating the solution with a little animal charcoal, aud crystallising the salt as before. The liquid from which the bark-alkaloids liave been precipitated by hydrate of lime affords an almost inexhaustible supply of this salt. See KiNONE. KI'NO. Syn. Gum kiso ; King (B. P., Ph. L. E. & D.) The juice flowing from the in- cised bark of the Pterooarpus Marsvpium or Indian, hardened in the sun. — Dose, 10 to 30 » Watts. 934 KIRSCHWASSER— KOUSSO gr., in powder; as an astringent in chronic diarrhoea, &c. Kino, Factitions, met with in the shops, is made as follows : — Logwood, 48 lbs.; tormentil root, 16 lbs. ; madder root, 12 lbs. ; exhaust by coetion with water, q. s.; to the liquor add of catechu, 16 lbs. j dissolve, straiii, and evapo- rate to dryness. Frod. 24 lbs. Extract of mahogany is also commonly sold for kino, KIRSCH'WASSER (-vas ser) [Ger.]. Syji. KiESCHEKWABSEB. A spirituous liquor dis- tilled in Germany and Switzerland from bruised cherries. From the rude manner in which it is obtained, and from the distillation of the cherry-stones (which contain prussic acid) with the liquor, it has often a nauseous taste, and is frequently poisonous. When properly made and sweetened, it resembles noyeau. EISH. An artificial graphite occasionally produced in iron-sraelting furnaces. It occurs in brilliant scales, and is said to possess pecu- liar efficacy in certain forms of anaemia and chlorosis. KITCH'EN . The late Alexis Soyer set down as one of the crying favilts of our countrymen the employment of an apartment for the Icitehen which is either too small or inconve- niently situated, and which, in general, is not sufficiently provided with ' kitchen requisites.' '^ As a workman cannot work properly without the requisite tools, or the painter produce the proper shade without the necessary colours, in like manner does every person wishing to eijonoraise his food and to cook it properly re- quire the proper furniture wherewith to do it." The neglect of these matters, which is so general, is, undoubiedly, a mischievous and deceptive economy. KNIVES, to Clean. After being used all knives should be wiped on a coarse cloth, so as to ensure their freedom from grease previous to being cleaned. The practice of dipping the blades in hot water not only fails to remove any grease that may be on them, but is almost sure to loosen the handles. It is very essential to remove any grease from them, since if this remain it will spoil the knife-board. For cleaning knives, a proper knife-cleaning machine, purchased of a good maker, is best. But where this is not used, the knife-board ought to be covered with very thick leather, iipon which emery powder should be placed. The emery gives a good polish to the knives, and does not wear them out so quickly as Bath- brick. When the points of the knives be- come worn very thin, they should be rounded by the knife-grinder. Where the bundles are good it will sometimes be worth while to fit them to new blades. KNOX'S POWDER. iVep. From common salt, 8 parts ; chloride of li\ne, 3 parts ; mixed together. An ounce of it dissolved in a tumblerful of water furnishes a solution which is similar to Labarraque's disinfecting fluid. KffiCHLIN'S LIQUID. Prep. From copper filings, 96 gr. ; liquor of ammonia, 2 fl. oz. ; digested together until it turns of a full blue colour, and then mixed with hydrochloric aciu, 5 fl. dr.; distilled water, 5 lbs.— Co«e, 1 to 2 teaspoonfuls daily ; in scrofula. It is poisonous in large doses. KOOCH'LA NUT. See Nux vomica. EOU'ffllSS. A liquor prepared by the Cal- mucs, by fermenting mare's milk, previously kept until sour, and then skimmed. By dis- tillation it yields a spirit called rack, racky, or araka. 21 lbs. of fermented milk yield about f pint of low wines, and this, by rectification, gives fully J pint of strong alcohol. It has lately come into use as a remedy for phthisis and general debility. The following formula from the Zeitschriff des Oesterr. Apoth. Ver. (1876, 526), for the preparation of so-called KoTTMlBS ExTEACT, is said to be a good one : — Powdered sugar of milk . 100 parts Glucose (prepared from starch) 100 „ Cane sugar .... 300 „ Bicarbonate of potassium . 36 „ Common salt . . . 33 „ Dissolve these ingredients in 600 parts of boiling frcsli whey of milk, allow the solution to cool, then add 100 parts of rectified spirit, and afterwards 100 parts of strained fresh beer yeast. Stir the mixture well and put into bottles containing a quarter of a litre each. The bottles must be well corked and kept in a cool place. For the preparatiori of Koumiss add 5 to 6 tablespoonfuls of this extract to a litre of skimmed, lukewarm milk, contained in a bottle of thick glass; cork well, keep the bottle for half a day in a moderately warm room (at 16° — 20° C), and afterwards in a cool cellar, shaking occasionally. The bottle should he filled to within 3 — 4 centimfetres of the cork. After two days the Koumiss is ready for use. KOUS'SO. Syn. Cusso, Kosso. This sub- stance is the dried flowers of the Brayera an- theVmintica, an Abyssinian tree which grows to the height of about 20 feet, and belongs to the natural order Bosaceaj. It is one of the most effective remedies known for both va- rieties of tapeworm. The dose for an adult is 3 to 5 dr., in powder, mixed with about half a pint of warm water, and allowed to macerate for 15 or 20 minutes. The method prescribed for its successful administration is as follows : — The patient is to he prepared by a purgative or a lavement, and the use of a very slight diet the day before. The next morning, fasting, a little lemon juice is to be swallowed, or a portion of a lemon sucked, followed by the dose of kousso (both liquid and powder), at S or 4 draughts, at short intervals I of each other, each of which is to be washed KEEASOTE 935 down with oold water acidulated with U'raon jaice. The action of the medicine is sabae- (juently promoted by drinl(ing wealc tea with- out either milk or augar, or water flavoured with lemon juice or toasted bread; and if it does not operate in the course of 3 or 4 hours, a done of castor oil or a saline purgative is taken. The flavour of kousso is rattier disagreeable and nauseating. Its operation is speedy and effectual ; but at the same time it is apt to produce, in large doses, great prostration of strength, and other severe symptoms, which unfit it for administration to tlie delicate of both sexes, or during preguancy or affections of the lower viscera. Care should be talcen not to purchase it in powder, as, owing to its high price, it is uniformly adulterated. The powdered kousso of the shops is, in general, nothing more than the root-bark of pomegra- nate, coloured and scented. KBE'ASOTE. S^n. Cbeabote, Creosote, Kbbobotb; Cbeasotuk (B. p.. Ph. L. & D.), CuEAzoTDM (Ph. E.), h. A peculiar substance, discovered by Reichenbach, iind so named on account of its powerful antiseptic property. It is a product of the dry distillation of organic bodies, and is the preservative principle of wood smoke and pyroligneous acid. Prep. Kreasote is manufactured from wood- tar, in which it is sometimes contained to the amount of 20J to 86g, and from crude pyro- ligneous acid and pyroxilic oil. 1. (P. Cod.) Wood-tar is distilled in a wrought-iron retort until white vapours of paraffin appear; the heavy oily matter which forms the lower layer of the product is col- lected, washed with water slightly acidulated with sulphuric acid, and then distilled in a glass retort, rejecting the first portions, which are chiefly eupion ; the distillate is treated with a solution of potassa (sp. gr. 1-12), the mixed liquids being shaken strongly together; after it is settled, the layer of eupion which forms is removed from the surface, and the potash- solution of kreasote exposed to the air until it becomes black ; it is then saturated with dilute sulphuric acid, the water liquid rejected, and tlie remainder (consisting of crude kreasote) submitted to distillation in glass ; the treat- ment by exposure, potassa, sulphuric acid, and distillation is repeated three times or of tener, until the combination of kreasote and pobissa ceases to become coloured by the action of the air J it is, lastly, saturated with concentrated phosphoric acid, and again distilled, rejecting the first portion that comes over. 2. (M. Simon.) A copper still, capable of containing 80 Berlin quarts, is filled to one third with the oil of wood-tar, and heat is applied; first, the more volatile matters pass over ; these do not contain kreasote, and are, therefore, rejected; hut when, by gradually increasing the temperature, there passes over a very acid liquid, which becomes turbid, and at the same time an oil separates from it when mixed with water, the product is collected, and the distillation* continued nntil the operator notices a squirting in the still, when this part of the process is complete ; the distilled pro- duct is then nearly saturated with potassa and returned to the still, which, in the mean- time, has been well cleaned out, and about half filled with water, and the distillation is recom- menced ; at first an oil comes over, which floats on water, and which consists chiefly of eupion, and is, therefore, rejected; as soon, however, as the oil begins to sink in the water which comes over with it, it is charged with kreasote, and is carefully collected ; the distilling aque- ous fluid being reintrodnced from time to time into the still, and the di-tillation con- tinued so long as any oil continues to come over with it; the heavy oily distillate is now agitated with liquor of potassa. sp. gr. ri20; the portion which remains undissolved is eu- pion, and is skimmed off; the potassa-solution of kreasote still, however, contains a consi- derable quantity of eupion, the greater portion of which may be separated by dilution and distillation with an equal quantity, or with at least ^ths of its volume of water, fresh water being added from time to time, as long as any eupion comes over with the distilled liquor; when this has ceased to pass over, sulphuric acid is poured into the still in quantity exactly sufficient to saturate ^rd only of the potassa formerly employed, and the distillation is again renewed; kreasote now distils over, the first portions of which, however, still contain eupion, after which pure kreasote follows; that is to say, " a kreasote which, when mixed with 6 or 8 times its quantity of a solution of pure potassa, furjiishes a mixture which, by the ad- dition of any further quantity whatever of water, does not become turbid.*' The combi- nation of kreasote remaining in the still is now mixed with sulphuric acid in slight excess, and the distillation renewed, the water coming over with it being from time to time returned into the still; and when no further oil passes over with the water, the process is complete. The kreasote thus obtained is redistilled with the water which has passed over with it, whilst the distilled water, as before, is allowed from time to time to run back into the still. The kreasote thus obtained is then colourless ; but it contains a considerable quantity of water in solution, which is separated by distillation iu a glass retort. The water distils firtt, and then kreasote, which, after cleaning the neck of the retort from the water, must be received in another dry receiver. If the kreasote as- sumes a red colour after being exposed for some time to the air, it must be re-distilled, and then it keeps very well. Korne found that tar prepared from turf furnishes much more kreasote than that from fir- wood, &c. 3. (Ure.) In operating upon pyroligneous acid, if we dissolve effloresced sulphate of soda in it to saturation, at the temperature of 267° Fahr., the kreasote separates, and floats upon the surface ; it is then decanted, and left iu 936 KREATIN— KEBNIC ACID repose for some days, during *hich it deposits a fresh portion of salt tind vinegar ; it is next saturated whilst hot with carbonate of potassa, and distilled along with water ; a pale yellow oily liquid passes over, which is rectified with phosphoric acid, &c., like the crude product of kreasote from tar. Frop. Kreasote is a colourless, transparent liquid, heavier than water, of a peculiar un- pleasant penetrating odour resembling that of smoked meat, and a very pungent and caustic taste ; its vapour irritates the eyes ; it boils at 400° Fahr., and is still fluid at— 16-6° Pahr. ; it produces on white filter paper greasy spots, which disappear if exposed to a heat of 212° Fahr. ; dissolves in 80 parts of water, and mixes in all proportions with spirit of wine, the essential and fatty oils, acetic acid, naph- tha, disulphide of carbon, ammonia, and po- tassa ; it dissolves iodine, phosphorus, sulphur, resins, the alkaloids, indigo blue, several salts (especially the acetates and the chlorides of calcium and tin) ; reduces the nitrate and ace- tate of silver ; is resinified by chlorine, and decomposed by the stronger acids. The aque- ous solution is neutral, and precipitates solu- tions of gum and the white of eggs. It kin- dles with difiiculty, and burns with a smoky flame. When quite pure, it is unaltered by exposure to the air. Sp. gr. 1'071, at 68° Fahr. A slip of deal dipped into it, and afterwards in hydrochloric acid, and then allowed to dry in the air, acquires a greenish-blue colour. It turns a ray of polarised light to the right, whereas carbolic acid does not affect polarisa- tion. Pur. The fluid commonly sold in the shops for kreasote is a mixture of kreasote, picamar, and light oil of tar ; in many cases it is little else than impure carbolic acid, with scarcely a trace of kreasote. Pure kreasote is perfectly soluble in both acetic acid and solution of potassa; shaken with an equal volume of water in a narrow test-tube, not more than the l-80th part disappears ; otherwise it contains water, of which kreasote is able to assume 1-lOth without becoming turbid. If it can be dissolved completely in 80 parts by weight of water, at a medium temperature, it then forms a perfectly neutral liquid. An oily residue floating on the surface betrays the presence of other foreign products (eopion, kaphomoe, pioamab), which are obtained at the same time with the kreasote during the dry distillation of organic substances. Kreasote is " devoid of colour, has a pecu- liar odour, and is soluble in acetic acid. When it is dropped on bibulous paper, and a boiling heat is apjilied for a short time, it entirely es- capes, leaving no transparent stain." (Ph. L.) '*' Entirely and easily soluble in its own weight of acetic acid." (Ph. E.) Sp. gr. 1-046 (Ph. L.), 1-066 (Ph. E. & D.). The density and boiling point of absolutely pure kreasote is given above. When prescribed in pills with oxide of silver, the mass will take fire unless the oxide be first mixed with liquorice or other powder. (Squire.) Uses. Kreasote has been recommended in several diseases of the organs of digestion and respiration, in rheumatism, gout, torpid ner- vous fever, spasms, diabetes, tapeworm, &c. ; but its use has not, in genera), been attended with satisfactory results. It is given in the form of pills, emulsion, or an ethereal or spi- rituous solution. Externally it has been em- ployed in various chronic diseases of the skinj sores of different kinds, mortifications, scalds, burns, wounds (as a styptic), caries of the teeth, &c. ; mostly in the form of an aqueous solution (1 to 80) ; or mixed with lard (5 drops to 1 dr.), as an ointment; dissolved in rectified spirit, it forms a useful and a popular remedy for toothache arising from decay or rottenness. In the arts, kreasote is extensively employed to preserve animal substances, either by wash- ing it over them, or by immersing them in its aqueous solution. A few drops in a saucer, or on a piece of spongy paper, if placed in a larder, will effectually drive away insects, and make the meat keep several days longer than it otherwise would. A small quantity added to brine or vinegar is commonly employed to im- part a smoky flavour to meat and fish, and its solution in acetic acid is used to give the fla- vour of whisky to malt spirit. See Carbolic ACID. KRE'ATIN. CjHjNaOj-Aq. Syn. Ceea- TIN. A crystallisable substance obtained from the jnice of the muscular fibre of animals. It was first obtained by Chevreul, but has recently been carefully studied by Liebig. Frep. (Liebig.) Lean flesh is reduced to shreds, and then exhausted with successive portions of cold water, employing pressure ; the mixed liquid is heated to coagulate the albumen and colouring matter of the blood, and is then strained through a cloth; pure baryta water is next added as long as a pre- cipitate forms, the liquid is filtered, and the filtrate is gently evaporated to the consistence of a syrup; after repose for some days in a warm situation, crystals of kreatin are de- posited ; these are purified by redissolving them in water, agitating the solution with animal charcoal, and evaporating, &c., so that crystals may form. Prop., S;c. Brilliant, colourless, prismatic crystals ; readily soluble in boiling water, sparingly so in cold water and in alcohol ; the aqueous solution is neutral, bitter tasted, and soon putrefies. KEEAT'ININ. C4H7N3O. This substance exists in small quantities, both in the juice of flesh and in conjunction with kreatin in urine. It is also produced by the action of the stronger acids on kreatin. It forms colourless prisma- tic crystals, which are soluble in water, andtlie solution has a strongly alkaline reaction. It is a powerful organic base, and produces crys- tallisable salts with the acids. KKE'NIC ACID. See Ceehio acid. KRYSTALLINE— LAC 937 KKYSTAL'UKE. The name flriginally ap- plied by Unverdurben to ANiLlirE. KUSTITIEN'S METAL. Prep. Take of nuille«ble iron, 3 partu ; boat it to whiteness, und add ot antimony, 1 part ; Molucca tin, 72 parts ; mix under charcoal, and cool. Used to C'lut iron and other metals with a surface of tin; it polishes without a blue tint, is hard, »nd has the advantage of being free from lead and arsenic. KTANrZIira. a method of preserving woud and cordage from decay, long known and practised; patented by Mr Kyan many Nears since. It consists in immersing the niHterials in a solution of corrosive sublimate, 1 part, and water, 60 or 60 parts, either uuder strong pressure or the contrary, as the ur- gency of the case or the dimensions of the articles operated on may require. See Uby BOT. KY'AITOL. A substance obtained from coal- tiir oil, and at first thought to be an indepen- dent principle, but since shown to be identical with ANILINB. IiABAEKAQUE'S FLUID. See Solution of Chloiiidk op Soda. LAB'DANUM. Syn. Lasanitu. An odo- rous, resinous substance found on the leaves and twin's of the Oi/ttua creticut, a plant growing in the island uf Candia and in Syria. It was formerly much used for making stimu- lating plasters. The fuUowing compound is often vended for it : — Labdanum, Facti"tions. Prep. Prom gum nniine, resin, Venetian turpentine, and sand, of each 6 parts ; Spanish juice and gum Arabic, of each (dissolved in a little water), 3 parts ; Canada balsam, 2 parts ; ivory black, 1 part ; balsam of Peru, q. s. to give a faint odour. LA'BELS capable of resisting the action of OILS, SPIUITS, WATER, STHUPa, and DILUTE ACIDS, may be obtained as Ibllows : — Lay a coat of strained white of egg over the label (an ordinary paper one), and immediately put the vessel into the upper portion of a common steum-pan, or otherwise expose it to a gentle heat till the albumen coagulates and turns opaque, tlien take it out and dry it before the fire, or in an oven, at a white heat of about 212° Fahr. j the opaque white film will then become hard and transparent. The labels on bottles containing STEONa ACIDS or alkaline SOLUTIONS should be either etched upon the glass by means of hydrofluoric acid, or be written with incorrodible ink. See Etching and Ink. LAB'ORATOKT. Stin. Labobatorium., L. A place titled up for the performance of expe- rimental or manufacturius operations in che- mistry, pharmacy, and pyrotechny. For full information respecting the best mode of fitting up a chemical laboratory, the reader is referred to works especially devoted to chemical mani- pulation.' Almost any well-lighted spare room > Tlie Uteit and beat work ia the ' Handbook of Cbe- may be fitted up as a small laboratory at very little expense. The gas-furnaces and improved lamps introduced of later years have to a cer- tain extent rendered chemists independent of brick furnaces. A strong working bench, fitted with drawers and cupboards, and having gas-pipes at intervals for attaching different kinds of jets, is an indispensable fixture. A close cupboard or closet, which ia connected by a pipe with the chimney or the external air, ia required to receive vessels emitting corrosive or evil-smelling vapours ; the door of this closet should be of glass. A sink, with a copious supply of water, must be at hand, for washing apparatus. A glass, a stoneware barrel, with a tap of the same material, is required for holding distilled water. Shelve*, supports for apparatus, and drawers, should be provided in abundance. The fine balances and other delicate instruments should be kept iu a separate apartment. With regard to appa- ratus, we may state that the articles most fre- quently required in a laboratory are the gas or al(!ohol lamps ; iron pans for sand bath and water bath ; evaporating dishes ; precipitating jars, funnels, and wash-bottles ; retort-^, flasks, and test-tubes ; mortars and pestles ; retort- and filtering stands ; rat-tnil and triangular files, and glass rod and tubing. The principal philosophical instrument- makers sell chests or cabinets filled with appa- ratus and chemicals, under the name of ' P0BT4 BLE labobatoeies.' Those sold by Mr J. J. Griffin and by Messrs Jackson and Townson are, perhaps, the most complete. Tiiey are well adapted for illustrating all the more valuable facts of chemical science, ami performini; all the ordinary operations of qualitative analysis. LABUSNINE. A poisonous alkaloid, found in the unripe seeds of the laburnum plant, associated with another poisonous alkaloid called CytUtine. LAC. Si/n. Lacca, L. a resinous substance combined with much colouring matter, pro- duced by the puncture of the female of a small insect, Cidled the Coccus lacca or ficua, upon the young branches of several tropical trees, especially the Ficua ladica, Ficua religiosa, and Croton iaccifenim. The crude resinous exuda- tion constitutes the stick-lac of commerce. Shbll-lao or shellac is prepared by spread- ing the resin into thin plates after being melted and strained. Seed-lao is the residue obtained after dissolving out most of the colouring matter contaiued in the resin. Shell-lac is the kind most commonly em- ployed in the arts. The palest is the best, and is known as 'orange-lac' The darker varie- ties — 'liver-coloured,' 'ruby,' 'garnet,' &c. — respectively diminish in value in proportion to the depth of their colour. Uses, ^c. Lac was formerly much used in mical Manipniation,' by Greville TN'iHIaras. Faraday's famous w ork on the Baiue subject haa long been out of print. 933 LAC DYE— LACQUER medicine ; its action, if any, is probably that of a very mild diuretic. It is now chiefly used in DENTIFBIOES, TAEBISHES, L4.CQCEES, and BEALING-WAX. Lac, Bleached. Sgn. White lac; Lacca AI.BA, L. By dissolving lac in a boiling lye of pearlash or caustic potassa, iiltering and passing chlorine through the solution until all the lac is precipitated; this is collected, well washed and pulled in hot water, and, finally, ' twisted into sticks, and thrown into cold water to harden. Used to make pale varnishes and the more delicate coloured sealing-wax. LAC DYE. Sgn. Lac, Lac-iakb, Indian COCHINEAL. A colouring substance used to dye scarlet, imported from India. Prep. By dissolving out the colour of ground stick-lac by means of a weak alkaline solution, and then precipitating it along with alumina by adding a solution of alum. Oba. To prepare the lac for dyeing, it is ground and mixed with diluted ' lac spirit,' and the whole allowed to stand for about a week. The ' cloth ' is iirst mordanted with a mixture of tartar and ' lac spirit,' and afterwards kept near the boil for three quarters of an hour, in a bath formed by adding a proportion of the prepared lac dye to the mixture used for mor- danting. Lac dye is only applicable to woollen and silk. The colours it yields are similar to those obtained from cochineal, but less brilliant. lAC SPIRIT. See Tin moedants. LACE. This decorative fabric is made by interweaving threads of linen, cotton, or silk, into various patterns and designs. Although in some instances lace is made by hand, the greater part is now manufactured by machi- nery worked by steam or water. The hand- made lace was called bone, pillow, or bobbin lace, these two latter names having been given it from its having been woven upon a pillow or cushion by means of a bobbin. The manu- factured article is bobbin net. Lace and the machinery by which it is produced is of so complex a nature that Dr Ure says of one par- ticular form of it " it is as much beyond the most curious chronometer in the multiplicity of mechanical device as that is beyond a com- mon roasting jack." Owing to the improvements in machinery in- troduced of liite years,it maybe mentioned that a piece of lace which twenty years since could only be produced at a cost of 3s. 6d. for labour, may now be turned out for Id., and a quantity of the fabric which sold for £17, now real- izes only 7s. A pair of curtains, each four yards long, may be made in one frame in two hours. The following statistics relating to the British lace industry are of interest: — "In 1843 there were 3200 twist net and 800 warp frames, returning £2,740,000 that year; in 1851, 3200 bobbin net and 800 warp, giving a return of £3,846,000; and in 1866,3552 bobbin and 4U0 warp, returning i£5,I30,000. There has since been no actual census, but about the same number is now at work, and the returns and profits arc greatly increased by im- proved quality and patterns of goods produced. The returns of 1872 were certainly f 6,000,000 at least; and from advancing wages and de- mand for Lever's laces, must still rapidly in- crease. Men are now earning by making them from £4 to £6 for 56 hours' weekly labour."i Lace, Gold and Silver, to Clean. Reduce to fine crumbs the interior of a 2-lb. stale loafj and mix with them \ lb. of powder blue. Sprinkle some of this mixture plentifully on the lace, afterwards rubbing it on with a piece of flannel. After brushing ofE the crumbs rub the lace with a piece of crimson velvet. Lace, to Scour. Take a perfectly clean wine bottle; wind the lace smoothly and care- fully round it; then gently sponge it in tepid soap and water; and when clean, and before it becomes dry, pass it through a weak solution of gum and water. Next pick it out and place it in the sun to dry. If it be desired to bleach the lace, it should be rinsed in some very weak solution of chloride of lime, after removal from which it must be rinsed in cold water. Starch and expose it; then boil and starch, and again expose it if it has not become sufficiently white. The following method is also said to whiten lace : — It is first ironed slightly, then folded and sewn into a clean linen bag, which is then placed for 24 hours in pure olive oil. After- wards the bag, with the lace in it, is to be boiled in a solution of soap and water for 15 minutes, then well rinsed in lukewarm water, and finally dipped in water containing a small quantity of starch. The lace is then to be taken from the bag, and stretched on pins to dry. To scour point lace proceed as follows : — " Fix the lace in a prepared tent, draw it tight and straight, make a warm lather of Castile soap, and with a tine brush dipped in rub over the lace gently, and when clean on one side do the same on the other ; then throw some clean water on it, in which a little alum has been dissolved, to take off the suds ; and, having some thin starch, go over with it on the wrong side, and iron it on the same side when dry ; then open with a bodkin and set it in order. To clean the same, if not very dirty, without washing, fix it as before, and go over with fine bread, the crust being pared off', and when done, dust out the crumbs." (Ernest Spon.) Black lace may be cleaned by passing it through warm water containing some ox- gall, rinsing it in cold water, and then passing it through water in which a small quantity of glue has been previously dissolved by means of heat ; it should then be taken out, clapped between the hands, and dried on a frame. LACQUER. A solution o"f shell-lac in alcohol, tinged with saffron, annotta, aloes, or other colouring substances. It is applied to > ' British MaiiufacturiDg Industries.' Stanford. liACTALBUMEN— LACTIC ACID 939 wood and metals to impart a golden colour. See Vaunisii. LACTALBU'UEN. See Caseiit. LACTATE. S^n. Lactab, L. A aalt of lactic iicid. The lactates are characterised by yielding an emirmous quantity of pe-fectly pure carbonic oxide gas when heated with 5 or 6 parts of oil of vitriol. Most of these salts may be directly formed by dissolving the hydrate or carbonate of the metal in the dilute acid. LACTA'TION. See Iitfawct, NuBBiwa, &c. LACTIC ACID. HjC„Hi„Oe. Syn. Acid op UILK; AciDUit LAOTICUM, L. A sour, syrupy liquid, discovered by Scheele in whey. It is also found in some other animal fluids, and in several vegetable juices, especially in that of beet-root, LHctic acid is by no means an unimportant constituent of the human organism. It is contnincd iu the gastric juice, and is fre- quently formed in the sweat. It has also been dctetted in the saliva of persons suffering from diabetes. A modification of the acid, termed siirkolactic acid, occurs in the fluids of the muscular tissue. It is likewise a product of the fermentation of many vegetiible juices, such as turnips, carrots, beet-root, and cabl)nge, which latter vegetable, after undergoing the lactic fermen- tation, liecomes converted into the sauer krnut of the Germans. In the form of calcic lactate it occurs in DUX vomica. Prep. 1. Dissolve lactate of barium in water, precipitate the barium with dilute sul- phuric acid, carefully avoiding excess, and gently eviipnrate to the consistence of a syrup, or until it acquires the density 1'215. Lactate of calcium may be used instead of Iftctate of barium, in which case a solution of oxalic ocid must be employed as the precipitant. Pure. (See No. 5.) 2. Milk (skimmed or stale), 1 gall. ; bicar- bonuto of sodium, i lb. ; dissolve and expose the liquid to the air for some days, until it becomes sour, then saturate the excess of acid with some more bicarbonate of sodium, and again expose it to the air ; repeat this as often as the liquid becomes sour ; next heat the liquid to the boiling point, filter, evaporate to dryness (or nearly), and exhaust the residuum with rectified spirit; filter the alcoholic so- lution, which contains lactate of sodium, add sulphuric acid as long as it causes a preci- pitate to form, again filter, and concentrate the clear liquid by evaporation. 3. (Boutron and Fremy.) Milk, 3 or 4 quarts ; snRar of milk, 200 to 300 gr. ; mix, and expose fur 2 or 3 days in an open vessel at 70° to 80° Kahr., then saturate with bicar- bonate of sodium, again expose at a moderate temperature, saturate with more bicarbonate of sodium, and repeat the process until the whole of the sugar of milk is decomposed ; then coagalate the casein by heat, filter, eva- porate, extract the acid lactate of sodium by alcohol of sp. gr. -810, and decompose it by the cautious addition of dilute sulphuric acid; again filter, distil off the alcohol, and evaporate as before, 4. (Scheele.) Evaporate sour whey to |th of its bulk, saturate with slaked lime, filter, add 3 or 4 times the quantity of water, cau- tiously precipitate the lime with a solution of oxalic acid, filter, and gently evaporate to dryness in a warm bath ; digest the residuum in strong rectified spirit, and again filter and evaporate. 5. ( Wackenroder.) Sugarof lead, 25 parts; finely powdered chalk, 20 parts; skimmed milk, 100 parts; water, 200 part'*; iligested together at about 75" Fahr. In six weeks the chalk will be dissolved ; the whole is then heated, but not to boiling; the cheese ia strained off, pressed, and the decanted liquid is clarified by albumen and evaporated, to let the lactate of calcium crystallise; the salt is re- crystallised and decomposed, either by sul- phuric acid or by the exact quantity of oxalic acid. This is, perhaps, the most etl'ective mode of prepnring lactic acid. 6. (Wholesnle.) — a. Good raw cane-sngar, 7 lbs., is dissolved in milk (skimmed or stale), 2 galls., and cheese (in a moist or putrescent state), i lb., and chalk, 4 lbs., previously rubbed to a cream with water, !( gall., is then added; the mixture is then exposed in a loosely covered jar, at a temperature of 80° to 86° Pahr., with occasional stirring, for 2 or 3 weeks, or until the whole is converted into a semi-solid mass of crystals of lactate of cal- cium; this is purified either by draining otf ond expressing the liquid portion, dissolving the residue in water, and evaporating the solu- tion for crystals ; or the whole is pnt into a stoneware vessel and heated to the boiling- point, by which the casein is coagulated, and the lactate of calcium is dissolved ; the solu- tion filtered whilst hot, furnishes the salt in crystals on cooling ; these crystals are sub- sequently dissolved in water, and the filtered solution decomposed by oxalic acid, as before. 4, Prom Ciiue-sugar, 4 parts ; moist cheese, 1 part ; chalk, 3 parts j water, 20 parts ; as the last. Obs. Lactic acid prepared by any of the used formulto may be rendered quite pure by dilution with water, saturation with baryta, evaporation, crystallisation, resnlution in water, and the careful addition of dilute sul- phuric acid, as in No. 1 ; the liquid is, lastly, again filtered and evaporated. Another plan is to convert the acid into lactate of zinc, by the addition of commercial zinc-white, and to redissolve the new salt in water, and then de- compose the solution with a stream of sul. phuretted hydrogen. In all cases the evapora- tion should be conducted at a very gentle heat, and, when possible, finished o\er sulphuric acid, or in vacuo. For particular purposes 940 LACTIC FERMENTATION— LACTOMETER this last product must be dissolved in ether, filtered, and the ether removed by a very gentle heat. Care must also be taken to remove the solid lactate of calcium at the proper period from tlie fermenting liquid, as otherwise it will gradually redissolve and dis- appear, and on examination the liquid will be found to consist chiefly of a solution of buiy- rate of calcium. Prop. The product of the above formulae is a solution of lactic acid. It may be concen- trated in vacuo over a surface of oil of vitriol until it appears as a, syrupy liquid of sp. gr. 1'215 ; soluble in water, alcohol, and ether ; exhibiting the usual acid properties, and form- ing salts with the metals, called lactates. Heated in a retort to 266° Fahr.; a small por- tion distils over, and the residuum on cooling concretes into a yellowish, solid, fusible mass, lery bitter, and nearly insoluble in water. This is lactic acid, which has lost half (1 equiv.) of its basic water. By long boiling in water this substance is reconverted into lactic acid. Heated to 480° Fahr., it suffers decomposition, lactide (the anhydrons, concrete, or sublimed lactic acid of former writers) and other pro- ducts being formed. This new substance may be purified by pressure between bibulous paper and solution in boiling alcohol from which it separates in dazzling white crystals on cooling. By solution in hot water and evapo- ration to a syrup, it furnishes common lactic acid. Uses. Lactic acid has been given in dyspep- sia, gout, phosphatic urinary deposits, &c. From its being one of the natural constituents of the gastric juice, and from its power of dissolving a considerable quantity of phos- phate of calcium, it appears very probable that it may prove beneficial in the above complaints. — Dose, 1 to 5 gr. ; in the form of lozenges, or solution in sweetened water. LACTIC FERMENTA'TION. The peculiar change by which saccharine matter is con- verted into lactic acid. Nitrogenous sub- stances, which in an advanced state of putre- I'active change act as alcohol-ferments, often possess, at certain periods of their decay, the property of inducing an acid fermentation in sugar, by which that substance is changed into lactic acid. Thus, the nitrogenised matter of malt, when suflered to putrefy in water for a few days only, acquires the power of acidifying the sugar which accompanies it ; whilst in a more advanced state of decomposition it con- verts, under similar circumstances, the sugar into alcohol. Tlie gluten of grain behaves in the same manner. Wheat flour, made into a paste with water, and left for four or five days in a warm situation, becomes a true lactic acid ferment ; but if left a day or two longer, it changes its character, and then acts like common yeast, occasioning the ordinary pa- nary or vinous fermentation. Moist animal membranes, in a slightly decaying condition, often act energetically in developing lactic acid. The rennet employed in the manufac- ture of cheese furnishes a well-known example of this class of substances. In preparing lactic acid from milk, the acid formed, after a time, coagulates and renders insoluble the casein, and the production of the acid ceases. By carefully neutralising the free acid by carbonate of sodium, the caseiu becomes soluble, and resuming its activity, changes a fresh quantity of sugar into lactic acid, which may be also neutralised, and by a sufficient number of repetitions of this pro- cess all the sugar of milk present may, in time, be acidified. This is the rationale of the common process by which lactic aciil is obtained. Cane-sugar (probably by previously btcoming grape-sugar) and the sugar of milk both yield lactic acid; the latter, however, most readily, the grape-sugar having a strong tendency towards the alcoholic fermentation. If the lactic fermentation be allowed to pro- ceed too far, the second stage of the process of transmutation commences, hydrogen gas and carbonic acid gas are evolved, and the butyric fermentation, by which oily acids are formed, is established. Pasteur ascribes the lactic fermentation to the agency of a specific kind of ferment, which occurs in the form of a greyish layer depo- sited upon the surface of the sediment formed during the fermentation of the sugar, casein, and chalk (see Lactic acid, V), in the manufacture of lactic acid. If to a mixture of yeast, or any nitrogenous substance, and water, sugar, and then chalk, be added, and finally a very small quantity of this greyish substance, taken from a portion of a liquid undergoing active lactic fermentation, lactic acid fermentation is almost immediately setup, the chalk disappears owing to the forma- tion of calcic lactate, and the greyish sub- stance is copiously deposited. When placed under the microscope this ferment is seen to be composed of " little globules, or very short artienlations, cither isolated or in threads, constituting irregfular flocculent par- ticles, much smaller than those of beer yeast, and exhibiting a rapid gyratory motion." If these little particles be washed thoroughly in pure water, and then placed in a solution of sugar, lactic acidification immediately com- mences in the saccharine liquid, and goes on steadily until stopped by the excess of free acid. LACTIDE. See Lactic acid. liACTIN. See Suoae of Milk. LACTOMETER. Syn. Galactometee. An instrument for ascertaining the quality of milk. Milk may be roughly tested by placing it in a long graduated tube sold for the purpose, and allowing it to remain until all the cream has separated and measured, then decanting off the clear whey, and taking its specific gravity ; the result of the two operations, when compared with the known quantity of cream and the density of the whey of an average sample of milk, gives the value of the sample tested. See Mile. LACTOSE— LAKE 941 A little instrument called a ' mUk-teater ' is ■old in London at a low price. It is essen- tinlly a liydrometer wbicli sinlsB to a given lonrk on the stem in pure water, and floats at aaotlier murk at tlie opposite end of the scale in pure milk. . The iDtermrdiate space indi- cates the quantity of water (if any) employed to adulterate the article. As the sp. gr. of pure milk varies, the indications of the ' tester' cannot be depended on. LACTOSE. See Suoab o; Mile. LACTUCA. (B.P) Si/n. LErrcCB. The leaves and lioweringtops of the wild iudij^enous plant Lactuia viroga. They are sedative, narcotic, and powerfully diuretic ; also mildly laxative and diaphoretic. Given in dropsy and visceral obstructions. See Lettuce, Extbact OF. LACTXrCA"SIUM. %». Lettttoe opium. Thbidacb; Lactuoabium (Ph. E. Mr G. Bischof writes : — Some eight months ago a tube was passed in my laboratory, which is supplied with water by the New River Com- pany, into the slate cistern so as to act as a syphon to supply some apparatus with water. The external surface of the tube inside the cistern was therefore alternately exposed to the action of air and water, according to the level of water in the cistern. Recently I noticed a white efflorescence on the greater part of the tube inside the cistern. An adjoining cistern of sheet lead, with a lead overflow pipe fixed into the bottom, shows nowhere any such corrosion. On cutting the tube it became evident that it is a composition tube, that is to say, a lead tube, containing some antimony. On analysis it was found to be composed of — Lead Antimony 98-3 1-7 100-0 Although the external diameter of the tube is only half an inch, 0'29 gram of efflorescence was obtained per foot by gentle rubbing. This dried at 100° C. contained 1-02 per cent, of sulphuric acid, corresponding with 41 per cent, of sulphate of lead. The remainder, ex- cept 1-13 per cent, of a residue insoluble in nitric acid, is carbonate of lead. The alternate exposure to air and water appears not essential to the corrosion, as I have observed a similar effect when the same tubing remained constantly under water. The interior of the tube has also been corroded, although of course no permanent efflorescence could be formed, owing to the rapid flow of the water. The frequent practice of plumbers of nsing composition tubing in connection with water supplies is therefore highly reprehensible, being fraught with considerable danger to the health of those using the water for drink- ing or cooking. Mr Louis Siebold detected lead in eight out of ten samples of concentrated solution of acetate of ammonia as well as in a sample of the ordinary solution of the British Pharmacopoeia. In pursuing bis investigations Mr Siebold found that solutions of acetate of ammonium are capable of dissolving lead from glass. He therefore advises that all forms of the solution, more particularly the concen- trated liquor employed by many chemists for making the weaker solutions, should be kept in bottles free from lead. With the acids lead or its oxides form salts, usually white in colour, and in the majority nearly insoluble in water, but readily soluble in acids. Tests. The oxides and salts of lead, mixed ' 'Journiil of the Chemical Society," April, 1867. LEAD 951 witli a little carbonate of soda, and pxposed on a cliaicoKl support to the reducing flaine of tlie blowpipe, readily yield a soft and ductile globule of inetiiUio lead, and the charcoal, »t the same time, becomes covered with a yel- lowish incrustation of oxide of lead. Both metallic lead and its oxides are soluble in nitric acid, furnishing a solutioa which may be examined with ea^e. Solution of lead salts may be recognised by the following reactions : — Sulphuretted hy- drogou, Bulphydrate of iimmonium, and the alkaline sulphides, give black precipitates, in- soluble in the cold dilute acids, alkalies, allia- line sulphides, and cyanide of potassium. Potassium and sodium hydrates give a white precipitate, soluble in excess. Ammonia (ex- cept with the acetate) gives a white precipi- tate, insoluble in excess. The carbonates of potassium, sodium, and ammonium, give a white precipitate, insoluble in excess. Dilute sulphuric acid (in excess), and solutions of the sulphates give a white precipitate, sparingly soluble in dilute acids, but soluble iu a hot boiling solution of potassium carbonate. Chro- mate and bichromate of potassium give yellow precipitates insoluble in dilute nitric acid, and soluble in solution of potassium hydrate. Iodide of potassium gives a yellow precipitate, soluble in great excess by heat, and separating in small, brilliant, golden-yellow scales, as the liquid cools. A piece of polished zinc precipi- tates metallic lead in an arborescent form, hence called tlie lead tree. To prepare for these tests, a solid supposed to contain lead should be digested in nitric acid, when the solution, evaporated to dryness and redissolved in water, may be tested as above. Eatim. This has been already referred to under previous heads. The ores of lead (ga- lena) may be digested in nitric acid, when the solution may be treated with sulphuric acid, and the lead estimated from the weight of the precipitated sulphate. This is called an assay in the wet way. The method adopted by practical mineralogists is an assay in the dry way, and is conducted as follows : — A small but powerful air-furnace, charged with coke, is brought to as high a tempera- ture as possible, and a conical wrought-iron crucible plunged into the midst of it; as soon as the crucible has attained a dull-red heat, 1000 gr. of the galena, reduced to powder, are thrown into it, and stirred gently with a long piece of ttiff iron wire flattened at the one end, in order to expose as large a surface of the powdered ore to the air as possible, observing now and then to withdraw the wire, to prevent it becoming red hot, in which case some of the ore would permanently adhere to it, and bo reduced before the intended time ; ■ the roasting is completed in 3 or 4 minutes, and any portion oi' tlio ore adhering to the stirrer beiiic detached by a knife, and re- turned into the crucible, the latter is covered up, and allowed to attain a full cherry-red heat, when abont 2 or 3 spoonfuls of reducing flux are added, and the whole brought to a full white heat; in 12 to 15 minutes, the portion of metal and scoria adhering to the sides of the crucible are scraped down into the melted mass with a small stick of moist green wood, after which the crucible is again covered, and the heat urged for 2 or 3 minutes longer, so as to keep the mass in a perfectly liquid state duringthe whole time ; the crucible is then removed from the lire with the cru- cible-tongs, and adroitly tilted so as to dis- charge its contents into a small, ingot-mould of brass, observing to rake the scoria from the surface to the sides of the crucible, so as to allow the molten lead to be poured out without it ; the scoria is then reheated in the crucible with about 4 spoonful of flux, and after being cleansed with a piece of green wood, as before, is at once poured into a second mould, which is instantly inverted ; the little button of lead thus obtained is added to the lead in the other mould, and the whole is accurately weighed. The weight, divided by 10, gives the per- centage of lead (including silver, if present) in the ore examined. One half of the lead thus obtained is put into a dry cupel of bone ash, and placed in the cupelling furnace, and treated as described in the article on assaying; the metallic button left on the cupel is then detached and weighed. The weight, divided by 5, gives the per-centage of pure silver. Ohs. The flux commonly employed in the above assay is composed of red argol, 6 parts ; nitre, 4 parts; borax, 2 parts; fluor spar, 1 part ; well pulverised and thorougldy mixed together. When the ore is very refractory, about a spoonful of carbonate of potassium should be added for each 1000 grains of ore, in which case the roasting may be dispensed with. The quantity of silver in argentiferous galena varies from -nrooi! to i part of the whole. Whenever this ore contains above 2 parts of silver in the 1000, it is found to be profitable to extract the latter. Indeed, by Pattison's process it is found that as small a proportion as 1 in 8000 can be extracted with profit. Uses. The uses of lead in the arts are well known. It enters-into the composition of many important alloys (pewter, type-metal, shot- metal, solder, &c.), it furnishes us with several valuable pigments (chrome yellow, &c.), and it is extensively used in dyeing. Some of its preparations are employed in medicine. Ant., ^c. Administer an emetic of sulphate of zinc or sulphate of copper, and, if necessary, tickle the lauces with the finger or a feather, to induce vomiting. Should this not succeed the stomach-pump may be had recourse to. Epsom or Glauber's salts, or alum, dissolved in water, or water acidulated with sulphuric acid, followed by tea, water gruel, or barley water, are the proper antidotes, and should be taken as soon after the poison has been swallowed as 952 LEAD possible. In poisoning by white lead, Dr Alfred Tajlor recommends the administration of a mixture of snlpbate of magnesium and vinegar, as preferable to the sulphate alone. When the symptoms are those of painter's colic, the treatment recommended under that bead should be adopted. In paralysis arising from lead, small doses of strychnine and its preparations may be cautiously ad- ministered. A symptom of poisoning by lead is the formation of a narrow leaden blue line, from -Jijth to -^th of an inch wide, bordering the edges of the gums, attached to the neck of two or more teeth of either jaw. (Dr Burton.) This discoloration may often bo detected or ren- dered more conspicuous by rinsing the mouth out with water holdi^ig a little sulphuretted hydrogen or sulphydrate of ammonium in solution. Chevallier and Rayer recommend the use of sulphurous or heprttic mineral waters, or of artificial solutions of sulphuretted hydrogen or alkaline sulphides in water, both in cases of acute and chronic poisoning by lead ; but the practical success of this plan does not appear to have been in proportion to theoretical autici- pations. The moist and 'freshly precipitated sulphides of iron are said by their advocates to be infallible if taken sufficiently early. Lead in Aerated Water. Some time since Sir Robert Cbristison condemned the use of syphons for lemonade, owing to the ac- tion of free tartaric acid upon lead, and the rapidity with which waters containing any free acid become charged with lead in syphons. According to Professor Miller, 00175 gr. of lead per gallon is not an unusual amount for average cistern water. Mr John S. Thomp- son, however, reports to the Edinburgh Uni- versity Chemical Society that, after such water has been aerated and put into a syphon, the amount of lead dissolved in it begins to rise in a rapid manner. Thus in potash water, drawn from a syphon, 0'0408 grain of lead per gallon was found to be present, being nearly 25 times the quantity found in the same water before it entered the syphon. Pure aerated water again drawn in a similar manner from a syphon gave 00816 gr. of lead per gallon, or exactly double the amount found in the potasb water, showing at once the well-known protective action that salts of the alkalies and alkaline earths have on lead. " Although," says the 'Medical Journal,' " tliese results are suffi- ciently high and alarming; still, when the water is drawn off in small quantities at a time, as is frequently the case with invalids, the results are found to be still higher ; thus, when potash water was so treated, 0'04.55 gr. of lead per gallon was found, while aerated water, drawn off in small quantities, gave 0'0933 gr. of lead per gallon, showing a very marked rise in both cases. The cause of this increase in quantity of the lead appears to be owing, not so much to the lengthened period of contact between the liquid and the metal as to the fact that the nozzle of the syphon, being exposed to the atmosphere in a. moist state, becomes rapidly oxidised or car- bonated, and is left in the most suitable con- dition ibr entering into solution, so that, when merely small portions of the liquid are drawn off each time, a comparatively concentrated solution of lead is obtained. These results," continues the same authority, " compare accu- rately with those which were obtained by Alessra Savoi'y and Moore, in examining the contents of a series of syphons of aerated water for Dr George Owen Rees, F.R.S., whose atten- tion was drawn to the subject by detecting symptoms of lead-poisoning in himself after he had been in the habit for some time of drinking such aerated water." Lead, Acetate of. Pb(CjH303)2. Syn. PltJMBIO ACETATE, SUaAR OV LEAD, PLUMB! A0ETA3. (B. P.) JPrep. Litharge (in fine pow- der) 24 J acetic acid, 40; distilled water, 20; mix the acetic acid and the water, add the litharge, and dissolve with the aid of a gentle heat, filter, evaporate until a pellicle forms, and crystallise. Drain and dry the crystal. Acetic acid (sp. gr. 10843), 23 parts, is gently heated in a copper boiler rendered electro-negative by means of a large flat piece of lead soldered within it, and litharge (pure, and in fine powder), 13 parts, is sprinkled in ; the heat is then continued, with constant stir- ring, until the acid is saturated, when the mother-waters of a former process, if any, are added, and the whole is heated to the boiling point, and allowed to settle until cold; the clear portion is now decanted, and evaporated in a similar vessel until the liquor has the sp. gr. 1'266 or 1'267, when it is run into salt- glazcd stone-ware vessels (the edges of which have been well smeared with candle grease), and allowed to crystallise. The product is 38 to 38^ parts of crystallised sugar of lead. It is found to be advantageous to preserve a very slight excess of acid during the boiling and crystallisation, to prevent the formation of any basic acetate the presence of which impedes the formation of regular crystals. From litharge, 112 lbs. ; acetic acid (sp. gr. 1-057), 128 lbs. Prop. 180 to 184 lbs. Prop. Pure acetate of lead forms colourless,' transparent, prismatic crystals, slightly efflo- rescent in dry air ; it is soluble in 8 parts of alcohol and in IJ part of cold water; the aqueous solution has a sweet astringent taste, and feebly reddens litmus, but turns turmeric and the juice of violets green; when gently heated, it melts in its water of crystallisation; by continuing the heat, the whole of the water is expelled, and the dry acetate obtained ; at a higher temperature the salt suffers decomposi- tion, and acetic acid, acetone, &c., is given off. Commercial acetate of lead is in general a confused crystalline mass, somewhat resembling broken lump sugar. It is powerfully astrin- gent and poisonous. When pure it is completely soluble in dis- tilled water acidulated with acetic acid form- LEAD 953 in;; a tranipnrent ooloarleos solution, "88 gruins diatolvt'cl in wnter require lor complete precipitation 200 grains nioasures of the volu- metric solution of oxalic acid." (B. P.) Uses, ifc. Acetate of lead ia extensively em- ploved in dyeing and calico-printing. Inme- dicine it is used as an astringent, styptic, and liminoatiitic ; in pulmonary, uterine, and intes- tinal hmmiirrhage, colliquative diarrlicea, phthi- sical Biveata, &c. It is usually combined with morphia or opiam, and with acetic acid to pre- vent it passing into the state of the poisonous carbonate in the stomach. — Vote, j gr. to 2 gr. (Collier); 1 to 2 gr. to 8 or 10 gr., twice or thrii-e a day (Pereira) ; 3 gr. to 10 gr., every 6 or 8 hours (A. T. Thomson). Exter- nally, as a coUyrium, 10 gr. to water, 8 fl. oz. (A. T. Thomson) ; as a lotion, 20 gr. (A. T. (Thomson), 1 dr. (Collier) to water, 8 or 10 fl. oz.; as an injection, 40 gr. to rose water, \ pint. The lotion is cooling and sedative, and is commonly used in excoriations, local inflam- mations, &c. Basic Acetates. There are several of these salts, but only one is of any importance. Tribasic Lead Acetate or Doable Plumbic Acetate, and Dioxide. Pb (CjHsOjjj 2 Hb O. 5y». SUBACETAT£ OF LEAD ; UaSIO LEAD CI- THATE ; GoDLARD'S ACETATB OF LEAD; PlUMBI BUDACE IAS ^U. P.). Prep. Litharge, 7 ; acetate ■of Ic.icl, 10; iind distilled wntur, 40; are boiled half an hour, and evaporated down, and allowed to crystallise out of contact with air. Used under the form of " Plumbi subacetas liquor" v. (». P.) Lead, Arse"uiate of. Pby(As04)3. %». Arse- nate OF L. ; Plcmw ausenias, L. Prep. Gradually ndd a solution of acetate of lead to another of araeniate of sodium. A white, in- soluble powder. Proposed as an external application in certain forms of caucor. Lead, Bro'mide of. PbUrj. Syn. Plumbi BKOMIDDM, L. Prep. By precipitating a solu- tion of neutral acetiite or nitrate of lead with a solution of bromide of potassium. A white, crystalline powder, sparingly soluble in water. It fuses by heat into a red liquid, which turns yellow when cold. It has been used in the same cases its iodide of lead. Lead, Car'bonate of. PbCOj. Syn. Plumbi OABBONAS, L. Prep. By precipitating a cold solution of either acetate or nitrate of lead with a solution of an alkiiline carbonate, observing to well WMsh the precipitate aud dry it in the shade. 'This preparation is seldom employed, the commercial carbonate (white lead) being subntituted for it. See White fioments. Lead, Chloride of. PbClg. Syn. Culobide IBAD; Plumbi ohloeidum: (Ph. L. 183H). Prep. (Ph. \i. 1836). Dissolve acetate of lead, 19 oz., in boiling water, 3 pints ; next dissolve chloride of sodium, 6 oz., in bi>iling watjjr, 1 pint ; mix the two solutions, and when cold wash and dry the precipitate. A white, crys- talline ponder. Dissolve finely powdered litharge in boiling dilute hydrochloric acid, and set aside the fil- tered solution to cool. Brilliant colourless needles. Prop. Soluble in 135 parts of cold and in 22 parts of boiling water; it melts when heated, and solidifies on cooling, forming a horn-like substance (horn lead; plumbi corneum). Uses, S(c. In the Ph. L. 1836, chloride of lead was ordered to be employed in the prepa- ration of ' bydrochlorate of morphia.' Mr Tuson highly recommends it in cancerous affec- tions, to allay pain and restrain morbid action, either in the form of a lotion or ointment. Various mixtures of lead chloriies and oxide are employed as a white pigment under the name of ' Pattison's white.' It is prepared by rapidly mixing a boiling solution of lead chloride with an equal volume of lime water. Another similar compound is called 'patent yellow' or 'Turner's jullow.' Lead, Chromate of. PbCrO^. Syn. Lemox yellow, Leifsic yellow, Paris yellow. Prep. By adding a filtered solution of acetate or nitrate of lead to a like solution of chromate of potassium, as long as the precipitate forms, which is collected, washed with water, and dried. For information respecting the manu- facture of this substance on the large scale, as a colouring substance (chrome yellow), see Yellow fiqmbntb. Lead, Dichromate of. Si/n. Chrome oravse, Chbomb red. PbCrO, . PbO. Prep. By add- ing to a solution of nitrate or acetate of lead a solution of chromate of potassium, ti which an equivalent of potassa has been added. This compound is of a splendid scarlet colour. See Hed piqmbnts. Lead, Cy'anide of. PbCy,. Syn. Plumbi OYANIDUM, L. Prep. By adding hydrocyanic acid to a solution of acetate of lead, as long as a precipitate forms, which, after being washed with distilled water, is dried by a very gentle heat, and preserved from the light and air. Sometimes used as a source of medicinal hydrocyanic acid. Lead, Iodide of. Pblj. Syn. Lead iodide ; Plumbi iodiduu (B. P., Ph. L. E D.). Prep, (B. P.) Nitrate of lead, 4; iodide of pot.is- sium, 4; distilled watr, a sufficiency. Dis- solve with the aid of heat the nitrate of lead in 30 of water, and the iodide of poiassium in 10 of water, mix, collect the precipitate, wash, and dry at a gentle heat. Prop., S(c. A rich yellow-coloured powder, soluble in acetic acid, alcohol, and boiling water; when heated, it fu-es and volatili'^es in yellow vapour, but with a higher degree of heat, violet vapours of iodine are evolved, leaving a residuum (lead) which is wholly soluble in nitric acid. — Dose, i gr. to 4 gr. or more, made into a pill ; as a deobstruent and resolvent, in enlargements of the cervical, axillary, aild mesenteric glands, and in scrofu- lous aliections and scirrhous tumours. Lead, Nitrate of. PbCXO,),. Syn. Plumbi NITKAS, L. (B. P., Ph. E. D.) 954 LEAD Frep. (Ph. D.) Litharge (in fine powder), 1 oz.j pure nitric acid, 2 fl. oz., diluted with water, \ pint; mix, apply a sand-hent, and evaporate to dryness, occasionally stiiTing; boil the residuum in water, 2i pints ; filter, acidulate with a few drops of nitric acid, eva- porate to a pellicle, and set the liquid aside to cool; lastly, dry the deposited crystatls on bibulous paper, and preserve them in a well closed bottle. (Commercial.) By dissolving white lead in dilute nitric acid, and crystallising. Vses, S(c. This salt is extensively used in calico printing, and in the preparation of the iodide and otlier salts of lead. It was for- merly much esteemed in asthmas, h£emor- rhages, and epilepsy. It is now often used in an external application in cancer, ulcers, wounds, and various cutaneous affections. It is the basis of Liebert's celebrated 'cosm^- tique infallible,' and of Ledoyen's ' disinfect- ing fluid.' A very weak solution is an excellent application to chapped nipples, lips, hands, &c. — Dose, i to 1 gr. ; in the form of pill or solution, washed down with a table- spoonful of water very slightly acidulated with nitric acid. lead, Nitro-sac'charate of. Syn. PlttmBi KITKOSACCHAKAS, L. Prep. (Dr S. E. Hos- kins.) Nitric acid, 1 part; water, 19 parts; mix ; in this dilute acid saccharate of lead (in fine powder) is to be dissolved, and set aside that crystals may form, which are to be dried by pressure between the folds of bibulous paper. A weak solution of the talt, acidulated with saccharic acid, lias been employed by Dr Hos- kins as a solvent for phosphatic calculi, with apparent success. Lead, Oxide of. PbO. Syn. MouoxiDB OP LEAD, Protoxide or lead. Yellow oxide OE LEAD, Plumbi oxtdum (B. P.) Prep. This substance is obtained perfectly pure by expelling the acid from nitrate of lead, by exposing it to heat in a platinum crucible ; or, still better, by adding ammonia to a cold solution of nitrate of lead until the liquid becomes faintly alkaline, washing the precipi- tate with cold water, drying it, and heating it to moderate redness for 1 hour. Prop., ifc. Pure protoxide of lead has a lemon -yellow colour, and is the best of all the salts of lead. It is very heavy, slightly so- luble in water, and freely so in acids, particu- larly when in the hydrated state ; the aqueuus solution has an alkaline reaction; at a red heat it melts, and assumes a semi-crystalline form on cooling ; in the melted state it ra- pidly attacks and dissolves siliceous matter, with which it unites to form glass (flint glass) ; when heated along with organic sub- stances of any kind, it is easily reduced to the metallic state. On the commercial scale, this oxide is pre- paied by heating the grey film or dross that forms on the surface of melted lead when freely exposed to the air. When the process s arrested, as soon as the oxide acquires a uniform yellow colour, it is called massicot; when the heat is still further increased, until it fuses or partially vitrifies, it forms litharge of which there are several varieties. See Litharge, Massicot. Lead, Red Oxide of. Syn. Red lead. Minium. Prep. This is prepared by exposing anf used pro- toxide of lead to the air for a long time, at a dull red heat. It is a very heavy powder, of a fine red colour, decomposed by a strong heat into protoxide of lead, and oxygen gas, which is evolved. Somewhat uncertain in its com- position, but is generally of the composition Pb304 or Pb022PbO. See Red Pigment. Lead, Dioxide. PbOj. Syn. Bikiodidk op LEAD, Peroxide op lead, Pccb oxide op LEAD. Prep. By digesting red oxide of lead in dilute nitric acid ; or by infusing a mixture of protoxide of lead and chlorate of potassium at a heat a little below redness, and washing the powdered mass in water; or by transmit- ting a current of chlorine gas through a solu- tion of neutral acetate of lead. This oxide gives up half its oxygen at a read heat; acids also decompose it. Its chief use is in chemical analysis, to separate sulphurous acid from certain gaseous ' mixtures, which it converts into sulphuric acid, which it at the same time absorbs, forming sulphate of lead. It has recently been employed as an oxidising agent in the manufacture of the aniline dtes. Lead, Pyrolig'nite of. Sugar of lead made with rough pyroligneous acid. Used in dyeing, chiefly for the preparation of acetate of alumina. Lead, pac'charate of. Syn. Plumbi sao- OHARAB, L. Prep. (Dr S. E. Hoskins.) Nitric acid, 2 parts; water, 10 parts; mix in a porcelain capsule, add of sugar, 1 part ; and apply heat until reaction ceases ; then dilute the liquid with distilled water, neutralise it with powdered chalk, filter, and add to the fil- trate a solution of acetate of lead, as long as a precipitate (saccharate of lead) forma ; lastly, collect the precipitate on a filter, wash and dry it. Used to make nitro-saccharate of lead, and as a source of saccharic acid. Lead, Sul'phate of. PbSOi. Syn. Plumbi sulphas, L. This salt occurs native in trans- parent octohedra (lead vitriol), and is obtained in large quantities as a by-product in the pre- paration of acetate of aluminum for dyeing. Prep. By adding dilute sulphuric acid to a solution of a soluble salt of lead. It is very sparingly soluble in water and in dilute sul- phuric acid, soluble in strong hydrochloric afiid and bitartrate of ammonium. Lead, Sul'phide of. PbS. Syn. Plumbi SULPHIDE. This occurs abundantly in nature in the form of galena. Prep. By fusing metallic lead with sulphur or by passing sulphuretted hydrogen through a solution of a salt of lead. Lead, Tan'nate of. Syn. Plumbi tannas, L. Prep. Precipitate a solution of acetate of LEAD DUST— LEATHEE 955 lend with an infusion of galls, and wash and dry tliu precipitate. Astringent, sedative, and liiL'iniistntic. — Doae, 1 gr. and upwards, uiade into a pill. It h:is been highly recoinmended iu the t'orm of ointment and cntaplasms, in bed-Rores, cliroiiic alcera of the feet, white ■wcUiugs, &c. Lead, Tar'trate of. Syn. Plumbi tabtbas, L. Prep. By precipitating acetate of lead, by tartrate of ammonium, washing and drying. LEAD DUST. Syn. PuLVis PLtJMBi, Plum- bum BiviaUM, li. Prep. By melting new lend, adding bruised charcoal, mixing with violent agitation, which must be continued until the metal ' sets,' and then pounding and washing awiiy the ohiinoal. Used by potters. LEAD, GEANULATED. Prep. By melting new lead, and pouring it in a small stream from an iron ladle with a hole drilled in its bottom, into a pail of water. Used to make solutions and alloys. LEAD, SED. See Bed fiombkts. LEAD, WHITE. See WuirE pigment. LEAD PYROPH'ORUS. See Pibophorus. LEATH'EB. Syn. CoBlUM, CoBius, L. Leather is the skin of animals which has been prepared by one or other of several processes adopted for the purpose, having tlie common object of preventing its spontaneous destruc- tion by putrefaction, besides other objects, which are more or less peculiar to each variety of this useful substance. Leather is only prepared on the large scale, and primarily either by tlie pi-ocess of ' tan- NINO' or ' TAWINO,' in the manner briefly de- scribed under these heads. GuBBiED irEATUEB is leather which has been tanned, and sold to the currier, who, after soaking it in water, and rubbing it to soften it, pares it even with a broad, sharp knife, rubs it with a piece of polished stone or wood, and, whilst still wet, besmears it with oil or grease (dubbing), which gradually penetrates the leather as the moisture evaporates. It next undergoes the operation of ' waxing,' which consists of first rubbing it on the flesh side with a mixture of oil and lamp black ; it is then ' black-sized' with a brush or sponge, and, when dry, is lastly 'tallowed' with a proper cloth, and ' slicked' upon the flesh side with a broad and polished lump of glass. Leather curried on the hair or grain side, termed ' black on the grain,' is blackened by wettincr it with iron liquor, and rubbing it with an iron ' slicker' before applying the oil or grease. The grain is finally raised by the 'pommel' or 'graining board' passed over it in various directions. Leather is dyed or stained by the appli- cation, with an ordinary brush, of any of the strong liquid dyes, in the cold or only gently heated, to the surface of the skin previously stretched on aboard. The surface, when dry, is commonly finished off with white of efff and the pommel or smoothing stick. Bookbinders geoi rally employ copperas water as a black 9t:iin or sprinkle ; a solution of indigo as a blue one ; and a solution of salt of tartar or commou soda, as a brown one. Leather, before being japanned or varnished, as in the preparation of what is called ' eua- mbllbd' and ' patent leatheb,' is carefully freed from grease by the application of ab- 8orl>ent substances or hard pressure between rollers, and the surface is nicely shaved, smoothed, and polished by appropriate tools, the varnish is then applied to the grain siiie for the former, and the flesh side of the skin for the latter, which is previously stretched out tight on a board to receive it. The whole is, lastly, submitted to a gentle stove-heat to harden the varnish ; and the process is re- peated, if necessary. Uses, Sfc. These are well known, and are all but universal. The leather manuacture of Qreat Britain is equU in importance ai^ utility to any other department of our industry, and inferior in point of value and extent only to those of cotton, wool, and iron. " It we look abroad on the instruments of husbandry, on the implements used in most of the metilianic trades, on the structure of a multitude of engines and machines; or if we contemplate at home the necessary parts of our cbithing — breeches, shoes, boots, gloves — or the furni- ture of our houses, the books on our shelves, the harness of our horses, or even the sub- stance of our carriages ; what do we see but instances of human industry exi-iled upon leather p What an aptitude has this single material in a varii-ty of circumstances for the relief of our necessities, and sujiplyintr conve- niences in every state and stage of life ! Without it, or even without it in the plenty we have it, to what difficulties should we be exposed ?" (Dr Campbell.) Leather is a kind of natural felt, but of much closer and firmer texture than that of artificial origin. " The thinner and softer kinds of leather arc some- times used as body-clothing; but its speciiil and proper purpose is the manufacture of coverings for the feet, to protect them from cold and water." (Eras. Wilson.) See Japan- ning, Vabnish, &c. Leather, destmction of, by Gas. It is well-known that the binding of buoks suffer considerable damage, when the books are kept in apartments lighted by coal gas. 'f hat the cause of this deterioration is due, as was be- lieved, to the combustion of the bisulphide of carbon contained in the gas, and its consequent oxidation into sulphuric acid, is exem[>lified by the following interesting communication Irom Professor Church, published in the ' Chemical News ' for October 19th, 1877. He says :— "Vellum seems unaffected; morocco suffers least ; calf is much injured, and rnssia still more so. The disintegration is most rapid with books on the upper shelves of a library, whither the heated products of combustion ascend, and where they are absorbed and con. denscd. 956 LEAVEN— LEECH By comparing specimens of old leather, with specimens of new, it is quite clear that the destructive influence of gas is due mainly to its sulphur. True there are traces of sulphates in the dye and size of new leather bindings, but the quantity is insignificant and theie is practically no free sulphuric acid. That leather may be destroyed by the oil of vitriol produced by the burning of gas in a library is proved by the following observations and analyses. The librarian of one of our public libraries forwarded to me the backs of several volumes, which had been 'shed' by the books on the upper shelves in an apartment lighted by gas. The leather of one of these backs (a volume of the ' ArchsBoIogia ') was carefully scrapeii off so as to avoid any paper or size from underneath. This task of scraping was easy enough, ^or the leather was reduced to the cousisteucy of Scotch snuff. On analysis of the watery extract of this leather, the follow- iug figures were obtained : — — o "o ^ — Free sulphuric acid in decayed leatVier .... Combined 6'21 per cent. 2-21 „ 8-42 IEAVEN. Dough which has become sour or run into a state of incipient putrefaction. When a small quantity of it is added to recent dough, it excites fermentation, but is apt to produce a disiigreeable taste and odour in the bread. It is now superseded by yeast. Both these substances are used in the same way. LEAVES (Medicated). Syn. Folia medi- OATA, L. On the Continent several prepara- tions of this kind are in use. In many cases the leaves of tobacco deprived of nicotin, by soaking them in water, are dried, and then moistened or steeped in a tincture or infusion of the medicinal substance. In this way bel- ladonna, camphor, and henbane, are often administered. Cruveilhier recommends opiated belladonna leaves for smoking in troublesome coughs, phthisis, spasmodic asthmas, &c., to be prepared as follows : — Belladonna leaves, 1 oz., are steeped in an infusion of opium, 10 gr., in water, 1 fl. oz. (or less), and are then care- lully dried in the shade. " MtrsTAED leaves (RiggoUot's) consist of mustard moisfened with water, spread on paper, and dried." (Squire.) See CiGAES (in ;pharmaey), and Vegetables. Leaves, Hovr to Dissect. " For the dissection of leaves,'' sajs Mrs Cussons, " I iind the process of maceration too long and tedious, to say nothing of the uncertainty as to the results. I have therefore adopted the use of alkali in saturated solution, the speci- mens to be inb'oiiuced while the liquid is heated to the boiling point ; the time of im- mersion to be regul:ited by the cliaracter of tlie various leaves and the nature of the epi dermis to be removed. When the specimen is freed from epidermis and cellular tissue, it must be subjected to the action of chlorine to destroy the colouring matter. The intro- duction of peroxide of hydrogen not only serves to render the lace-like specimen purer in colour, but also preserves it. In destroying the colouring matter in ferns this also is in- valuable; added to the chlorine it gives i> solidity to the bleached fronds, and appears to equalise the action of the chlorine. For skeletonising capsules the slow process of maceration by steeping in rain-water is alone available ; a moderate heat may be applied to hasten the process, but alkali is useless. The only known flower which can be dissected is the Hydrangea japonica. The fibi-ous nature of the petals renders it easy to skeletonise in the perfect truss in which it grows. Skele- tonised leaves and capsules appear to gain in the process a toughness and durability not possessed by them in their natural state." LECANOK'IC ACID. See Oesbllinic acid. LEECH. Sj/n. Hieudo (B. P., Ph. L. & D.), L. The ofiicinal leech of the Pharma- copoeias is the Sanguisuga medicindlh {Sirudo medicinalis — Guv.), familiarly kuown as the ' old English' or ' speckled leech.' It is also occasionally called the ' Hamburg grey' or ' Russian leech,' from being imported from those parts. Its characteristics are — Back, greenish or olive- green, sometimes almost black or intense brown, with 6 rusty-red or yellowish longitudinal stripes, which are mostly spotted witli black. — Belly, dirty yellow or liglit olive green, spotted more or less with black. The spots are very variable in size and number ; in some cases few, in otliers so numerous as to form the prevailing tint of the belly. This variety, which is the most valu- able of the commercial leeches, is chiefly im- ported from Hamburg. Another variety of leech, the Sanguiswga officinalis, familiarly known as the ' Hamburg' or ' French green leech,' is imported from Bordeaux, Lisbon, and Hamburgh. Its charac- teristics are — Back, brownish olive-green, with 6 reddish or rusty yellow longitudinal bands. — Belly, light dirty pea-green, or yel- lowish green, free from spots, but exhibiting two lateral stripes. This leech is vastly in- ferior to the preceding variety, and some of those imported from France and Portugal are absolutely useless, from their indisposition to bite, arising from the fraud practised by the collectors and dealers of gorging them with blood to improve their apnearHnce before sending them to market. The above are the species of leech commonly employed in medi- cine in this country, but many''others are noticed by writers on the subject. LeechfS are best preserved in water ob- tained from a pond, and occasionally clianged ; when kept in spring water they soon die. The introduction of a hand to which an ill-flavoured medicine or odour adheres into the water in which they are kept is often LEECHING— LEMON 957 ■nfllcient to poison them. The application of •aline matter to tlie skin of leeches, even in very BrouU quantities, iininediiitely occasions tlie expulsion of the contents of the stomach ; hence a few grains of common salt are fre- quently spriukled over them, to make them d'sgorge the blood which they have swallowed. The frequent changinfT of the water in which leeches are kept is iiijudiciou'. Once a month ill winter, and once a week in summer, is deemed sufficiently often by the large dealers, unless the water becomes discoloured or blooJy, when it should be changed every day, or evei'y other day. When clean pond water cannot be obtained, clean rain water that has been well exposed to the air should alone be employed. Mr J. R. Kenworthy recommends placing in the water a few balls of irregular lamps of pure clay, about 24 inches in dia- meter ; a method which we can recommend as both simple and successful. The plan adopted by M. Fee is as follows : — Place 7 inches of a mixture of moss, turf, and eh»i'conl, in a marble or stone trough, over which sprinkle some small pebbles. At one end of the trough, and about half way up, place a thin shelf of stone or marble, pierced with small holes, on which put first some moss, or por- tions of marsh horse- tail {Equisetum paluttre), and on this a layer of pebbles to keep it down ; then pour in water suiBciently high jnst to moisten the moss and pebbles, put in the leeches, and tie over the mouth of the trough with a cloth. Another plan consists in keep- ing the leeches in a glass tank, or aquarium, pnivided with a pebbly bottom and a few healthy aquatic plants. Propag. According to Dr Wagner, an annual feast on living blood is necessary to render leeches able to grow and propagate. These conditions can only be fulflUed by re- storing to the breeding cisterns those which have been already employed. All artificial methods of feeding them by bladdersor sponges of blood have been found to fail. He recom- mends the employment of two tanks, with the bottom formed of loam, clay, or turf, sur- rounded by an inner border of a similar sub- stance, and an outer one of sand — the one for leeches fit for medical use — and the other for breeding, or for such leeches as have been applied. No leeches are to be taken from the breeding tank until a year has elapsed after their having been applied and fed with human blood; and their removal to the first tank should take place in September, or October, as by this time the breeding season is over. By this plan all leeehes that have been applied are to be carefully restored to the breeding tank, without making them disgorge the blood they have swallowed. LEECH'INQ. This consists in the applica- tion of leeches to any vascular part of the body, for the purpose of withdrawing blood from it, and thus allaying local inflammation, distension of vessels, &c. Leeches are most conveniently applied by means of a common pill-box or a wine glass. The part should be previously washed perfectly clean, and if covered with hair should be closely shaved. Sometimes leeches are indisposed to bite; in such cases, allowing them to crawl over a piece of dry linen or calico, rolling them in porter, moistening the part with a little milk or sweetened milk, or drawing a little blood by a slight puncture or scratch, will usually make them bite freely. To stop the bleeding from leech-bites various plans are adopted, among which the application of nitrate of silver or creasote, or gentle pressure tor some hours with the finger, are the most successful. Of late years a piece of matico leaf or soldier's herb, applied in the same manner as a piece of lint, has been commonly adopted to stop the bleeding of leech-bites. LEEK. Syn. Vo-B.-B.ViS.,'L.'t\\e Allium pomim (Linn.). Its general properties are iiitenueili. lie between those of the onion and garlic. The juice is said to be powerfully diuretic, and capable of dissolving phosphate calculi. LEGU'MIN. Vegetable casein. It is found most abundantly in the seeds of leguminous (podded) plants, e.g. beans, peas, &c., as well as in the sweet and bitter almond. In properties it closely resembles the casein of milk. Legumin may bo obtained from peas or from nliuunds ns follows: — After digesting the crushed seeds for 2 or 3 hours in warm wattr, the undissolved portion is removed by strain- ing through linen, and the strained liquid, after depositing the starch suspended in it, is next filtered and mixed with diluted acetic acid. The white flocculent precipitate which is thus produced, is then collected on a filter and washed. It is afterwards dried, powdered, and digested, first in alcohol, and afterwards in ether. R'lclileder considered that, as thus obtained by Dumas and Cahours, it was not absolutely pure, since as it was not entirely soluble in a cold concentrated solution of potash, he recommeu led the alkaline solution being de- canted from the undissolved portion, and again precipitated by the addition of acetic acid. Legumin as thus prepared was believed by Rochleder to be pure, and was found on analysis to give results analogous to those fur- nished by casein. In the seed, legumin occurs associated with considerable quantities of the phosphates of calcium, magnesium, and potassium. Rennet coagulates it like it does the casein of milk, its similarity to which is exemplified by the manufacture of a kind of cheese from peas and beans by the Cliinese. Dried peas contain about a fourth of their weight of legumin. LEM'ON. Sgn. LiMO, L. The fruit o< the Citrus limonum or lemon tree. The juice 958 LEMON ACID— LEMON PICKLE pjeel, aud essential oil are officinal. See Oil, and below, LEM'ON ACID. See Citbio acid. LEM'ON FLA'VOUfi. See Essence op Lemon. LEM'OIT JUICE. SyM. Limonis Btrccrs (B. P.), Sncona LiitoNtrM (Ph. L. ifc D.), L. The juice of the lemon, obtained by squeezing and straining. When freshly expressed, it is turbid, owing to the presence of macilage and extractive matter. These substances render the juice IJable to decomposition, and various metliods have from time to time been proposed for preserving it. Amongst these may be mentioned the addition to the fresh juice of one per cent, of bisulphite of calcium, or ten per cent, of proof sjiirit. " We have examined the juice expressed from two varieties of lemons, viz. Palermo and Messina, with the following results : Palermo. Messina. " Ounces of juice yielded by 100 lemons . ■ - 108 96 Specific gravity of juice 1014-85 1038-56 Percentage of citric acid 8'12 7'04 Percentage of ash . 0-289 0-301 " 100 parts of the ash of the juice of Palermo lemons gave ; Sulphuric acid . . 10'59 Carbonic acid . . 16-33 Chlorine . . 0-81 Phosphoric acid . 6-74 Ferric phospliate . 1-32 Lime . 8-89 Magnesia . 3-02 Potash . 47-84 Soda . 3-32 Silica . 072 Loss . . . 0-42 100-00 " If lemons are kept n, few months before squeezing, the yield of juice is slightly in- creased, but its specific gravity and percentage of citric acid remains unaltereil. It is erroneous to suppose that the acid of the lemon is, by keeping, changed into sugar. We have kept lemons for 12 mouths, and found that the per- centage of acid was not diminished. A certain proportion of sugar was formed, but at ttie expense of the soluble starch contained in the cell-walls of the lemon. Lemon juice on being kept is found to decrease in density, but thi- amount of acid remains the same." (Hark- ness.) Lemon juice may be preserved by heating it to 150° Fahr., filtering, and setting it aside in bottles completel}' filled. If this process be performed in the winter, the juice, it is said, may be kept perfectly good for 12 months. Fresh lemon juice is prevented from decomposi- tion and rendered fit for exportation by mix- ing it with j'ljth of alcohol. (Schweitzer.) The Merchant Shipping Act of 1867 re- quires that after a. ship has been at sea ten days 1 oz. of lime or lemon juice, mixed with 1 oz. of sugar and J pint of water, sliall be served out to each of the crew between the hours of 12 and 1 in the day. Adult. Lemon juice is frequently adulte- rated, the adulterants being water, sugar, or gum, and sulphuric or acetic acid. The modus operandi is, to dilute the genuine juice with water, and then bring up the density with the sugar or gum, and the percentage of acid with one or other of the above acids. The examina- tion of lemon and lime juice supplied to the navy is now conducted in the Inland Revenue Laboratory, Somerset House, and it speaks well for that department when we say that cases of scurvy on board ships are now of very rare occurrence. No juice is passed un- less it comes up to a certain standard in specific gravity, and percentage of citric acid, and any sample containing any other acid is at once rejected. Prop. Lemon juice is refrigerant and anti- scorbutic, and has long been extensively em- ployed in the preparation of cooling drinks and effervescing draughts, which are justly esteemed as wholesome summer beverages, as well as palliatives in fevers, nausea, &c. In scurvy, there is no remedy equal to fl-eshly expressed lemon juice ; and in acute rheuma- tism and gout, according to the united testi- mony ot Dr Owen Rees, Dr Babington, and numerous Continental practitioners, it has been exhibited with considerable success. In agues, dysentery, English cholera, nausea, and vomit- ing, heartburn, putrid sore-tliroat, hospital gangrene, syphilis, and numerous skin diseases, it has proved most serviceable. See Citeio Acid, Gout, &c. Lemon Juice, Factl"tiouB. Si/n. Soltttio ACIDI OITBICI, SuCCrs LIMONUM PACTITIITS, L. Prep. 1. Citric acid, li oz. ; carbonate of potassa, 45 gr. ; white sugar, 2^ oz. ; cold water, 1 pint ; dissolve, add the yellow peel of a lemon, and in 24 hours strain through a hair sieve or a piece of muslin. 2. As the last, but using 15 or 16 drops of oil of letaon, to flavour instead of the lemon peel. Obs. The above is an excellent substitute for lemon juice, and keeps well in a cool place. Tartaric acid, and even vinegar, are sometimes used instead of citric acid ; but it is evident that it then loses all claim to being considered as an imitation of lemon jnice, and to employ it in lieu of which -would be absurd. lEM'ON PEEL. S^n. Coktex mmonum (B. P., Ph. L.), L. " The fresh outer part of the rind." (B. P.) " The fresh and the dried exterior rind of the fruit ;" the latter dried " in the month of April or May." (Ph. L.) Candied lemon peel (cortex limonum con- DiTUs) is employed as a dessert, and as a fla- vouring ingredient by cooks and confectioners. It is reputed stomachic. See Candyino. LEMOH PIC KLE. See Sauce. LEMONADE— LENS 959 LEKONAOE'. Sgn. Leuon sherbet, EiHo'a CUP ; Liuonaduh, L. ; Limonase, Fr. Prep. 1. Lemona (Hliccd), 2 ia no. ; aug»r, 2^01.; boiling water, li pint; mix, cover up tlie vesecl, and let it stand, witli occasional stirring until cold, then pour oH the clear through a piece of muslia or u clean hair sieve. 2. Juice of 3 lemons; yellow peel of 1 lemon; SHRar, i lb. ; cold water, 1 quart ; digest for 5 or 6 hours, or all night, and decaut or strain us before. 3. Citric acid, 1 to 1) dr. ; essence of lemon, 10 drops ; sugar, 2 oz. ; cold water, 1 pint ; agitato together until dissolved. Ob». Lemonade is a pleasant, cooling sum- mer beverage, and when made as above inny be drauk in large quantities with perTect safety. It also forms an excellent refrigerant and antiseptic drink in fevers and putrid dis- eases generally. Turtaric acid is commonly substituted for citric acid, from being cheaper; it i-, hciwevcr, much inferior, being less whole- some and less agreeable. Lemonade for icing is prepared as above, only u.-ing a little more sugar. Orange slierliet, or orangeade for icing is made in a similar way from orangi'S. Lemonade, Aera'ted. S». The best aerated lemonade nf the London makers is prepared by putting li fl. oz. of rich lemon syrup into each bottle, which is then filled up with aerated water at the bottling iiiaihine. Lemonade, Aiitima"niated. Syn. Likoka- BUM ANTIMONIATOM, L. Prep. By adding tartar emetic, 1 gr., to each pint of ordinary lemonade. — Dose. A wineglassful every ) hour or hour ; as a diaphoretic and expectorant. See Antimonv (Potassio-tartrate). Lemonade, Ape"rient. Syn. Limokadum I»iXATiv0M, L. Prep. 1. Sugar, 1 oz. ; lemon juice, J H. oz. ; sulphate of soda, 3 dr.; water, 8 &. oz.; put them into a soda-water bottle withoat shaking, have the cork ready fitted, add of sesquicarbonate of soda (incryst.), i dr., and instantly cork the bottle, wire it down, and keep it in a cool place, inverted. For a dose. 2. Heavy carbonate of macrnesia, li dr. ; refined sugar, 1 oz. ; essence of lemon, 5 or 6 drops ; water, 8 fl. oz. ; bottle as last, then add of citric acid (cryst.), 3 dr., and in- stantly cork, &c., as before. For a dose. It should be kept for at least 24, hours before being taken. Lemonade, Lactic. Syn. Limonaduv lac- TICUM, L. Prep. ( JIagendie.) Lactic acid, 1 to 4 dr.; syrnp, 2 oz. ,- water, 1 pint; mix. Ilecommended in dyspepsia, &c. Lemonade, Uillc. S^n. Limonasttm lactis, L. Prep, Take of sugar, J lb.; water, 1 pint; dissolve, add the juice of 3 lemons; milk or whey, i pint; stir the whole together and strain through a hair sieve. Some persons add a glassful of sherry. Lemonade, Uln'eral. Si/n. Limonadb mi- nerals, Fr. On the Continent this name is applied to various drinks consisting of w.ttcr acidulated with the mineral acids ;ind sweet- ened with sugar. Thus we have limonade ehloihydrique, nitrique, phosphoriquc, sul- phurique, &c., all of which aie used as cool- ing drinks in fevers, inflammations, skin diseases, &c. Lemonade, Port'able. See Powders. LEMONADE POWDERS. Sec Powders. LEMONATED KALI. See Kali, Potas- SIFM (Citrate), &e. LEN'ITIVES. In medicine, purgatives which act in a gentle manner, and have a soothing effect. See Laxatives. LENS. In optica, a piece of glass or other transparent medium, having one or two curved surfaces, either convex or concave. A descrip- tion of the different kinds of lenses belongs to a work on optics. It may, however, be useful to the chemicar student to remark here that the CoDDiNQTON and Stanhope lenses, which may now be bought at any of the opticians, neatly mounted and of great power, for a few shillings, will be found of the greatest service in examining minute crystals, precipitates, &c. ; and for all ordinary purposes offer a cheap and efficient substitute for more complicated microscopes. An extemporaneous instrument, possessing considerable power, may be made by simply piercing a small circular hole in a slip of metal, and introducing into it a drop of water, which then assumes a spherical form on each side of the metal, while the latter is held ill a horizontal position. The ingenious little TOT microscopes sold about the streets of London, under the form of a perlor.ited pill- box, at one penny each, consist of snch a lens made with Canada balsam iiist culty aroused, and into which he again sinks as soon as the excitement is withdrawn. It frequently arises from plethora, in which case depletion is indicated ; or from the suppression of some usual discharge or secretion, which it should then be our business to re-establish. It also often arises from over mental fatigue and nervous debility, when relaxation from busi- ness, the use of a liberal diet, and ammoniacal stimulants and antispasmodics, are found use- ful. When depending on a determination of blood to the head, cupping may be had re- course to, and all sources of excitement avoided. In all cases the bowels should be moved as soon as possible by means of mild purgatives. IiET'TUCE. Syn. Lactuca, L. The early leaves or head of the Lactuca sativa, or garden lettuce, forms a common and wholesome salad. They are reputed as slightly anodyne, laxative, hypnotic, and antaphrodisaic, and have been recommended to be eaten at supper by those troubled by watchfulness, and in whom there exists no tendency to apoplexy. The leaves and flowering tops of L. virosa are officinal in the B. P., the "flowering herb" (laotitca), in the Ph. L. ; the " inspissated juice," in the Ph. E. ; and the " inspissated juice and leaves," in the Ph. D. The " inspissated juice " pf Lactuca virosa, or strong-scented wild lettuce, is also officinal in the Ph. E. ; and both the "leaves and inspissated juice" of the same variety are ordered in the Ph. D. The last species is more powerful than the cultivated lettuce. See Extract and LAOTUCABitrM. lEUCOREHOE'A. Syn. Whites; Catae- KHrs TAGtiNiE, PLtroE AXBUS, L. The sym- ptoms of this disease are well known to most adult females. The common causes are de- bility, a poor diet, excessive use of hot tea, profuse menstruation or purgation, late hours, immoderate indulgence of the passions, fre- quent miscarriages, protracted or difficult labours, or local relaxation. Occasionally it is symptomatic of other affections. The treat- LEVANT NUT— LIGHT 9G1 ment must bo directed to the restoration of the general health, and imparting tonicity to the parts affected. Tepid or soa bathing, or ■honer baths; bark, chnlybeates, and oiher tonics; with local affusions of cold water, and mild astringent injections, as those of black tea or oak bark, are generally found suceessl'ul in ordinary eases. LEVANT' NUT. See CoccULTJs rsDicrs. LEVIGA'TION. St/n. Levioatio, L. Tlie process of reducing substances to fine powder, by making them into a paste with water, and grinding the mass upon a hard smooth stone or slab, with a conical piece of stune having a flat, smooth, under surface, called a ' muller.' Levigation is resorted to in the preparation of paints on the small scale, and in the elu- triation of powders. The term is also, some- times, incorrectly applied to the lengthened trituration of a substance in a marble or Wedgwood-ware mortar. LEVORACE'MIC ACID. See Kacemic ACID. lEY'DEN JAR. Si/n. Letden phial, Elkoteioal jae. An instrument for the accumulation of the electric fluid. Its sim- plest form is that of a wide-mouthed jar of rather thin glass, coated on both sides with tin-foil, except on the upper portion, which is left uncoated, and having a cover of baked wood, through which passes a brass wire, ter- minating in a metallic knob, and communi' eating with the inner coating. To charge the jar, the outer coating is connected with the earth, and the knob put in contact with the conductor of an electrical machine. The inner and outer surfaces of the glass thus become respectively positive and negative, and the particles of the glass become strongly polarised. On making connection between the two coat- ings with a conducting substance, discharge takes place by a bright spark and a loud snap ; and if any part of the body be interposed in the circuit, a shock is felt. IIBAVIUS'S LIQUOR. See TiK (Tin oblo- bide). LI'CHEN. In pathology, a dry papulous or pimply eruption of the skin, terminating in scurfy exfoliations. " Lichen exhibits great variety in its outward characters in different individuals; in one the pimples are brightly red; in another, of debilitated constitution, they are bluish and livid ; in a third they are developed around the base of hairs; in a fourth they appear as circular groups, and increase by their circumference, while they fade in the centre, forming so many rings of various size; in a fifth, a mndificution of the precedinir, they have the appearance of flex- uous bands; while in a sixth they are remark- able for producing intensity of suffering, or nnasual disorganisation of the skin. They are all occasioned by constitutional disturbance, sometimes referable to the digestive, and some- times to the nervous system. In some in- stances, however, they depend upon a local TOL. II. cause. I have had a crop of lichenous pimples on the backs of my hands from rowing in hot weather; and in hot climates that annoying disorder called prickly heat is a lichen." (Eras. Wilson.) The treatment of this affection is noticed under EiiuPTioss (Papular). LICHENS. Syn. LicnEKES— Juss., Lichen- ALE8 — Lind., L. Indoiany, these arecryptoga- mous plants, which appear under the form of thin, flat crusts, covering rocks and the barks of trees. Some of them, like Iceland moss {Cetraria Islandica), are esculent and medi- cinal and employed either as medicine or food ; and others, when exposed in a moistened state to the action of ammonia, yield purple or blue colouring principles, which, like indigo, do not preexist in the plant. Thus, the Socella tinctoria, the Variolaria orcina, the Lecanora tartarea, fyc, when ground to a paste witti water, mixed with putrid urine or solution of carbonate of ammonia, and left for some time freely exposed to the air, furnish the archil, litmus, and cudbear of commerce, very similar substances, differing chiefly in the details of their prep.iration. From these the colouring matter is easily extracted by water or very dilute solution of ammonia. See Aechii,, CiTDBEAB, and Litmus. LIEBER'S HERBS OF HEALTH— Gesnnde- heitskranter Liebersche — Blankenheimer Thee — Blankenheimer Tea — Herba Galeopsidis Granrtiflora) Concisa (Yellow Hemp Nettle). LIGATURE. In surgery, a small waxed piece of cord or string formed of silk or thread, employed for the purpose of tying arteries, veins, and other parts, to prevent hiBmorrhage, or to cause their extirpation. To be safe and useful they should be round, smooth, and suffi. ciently strong to permit of being tied with security without incurring the danger of breaking or slipping. There are many cases recorded in which emigrants, soldiers, and travellers have lost their lives from the sim- ple inability of those around them to apply a ligature. LIGHT. Syn. Lumbk, Lux, L. Light acts as a vivifying or vital stimulus on organ- ised beings, just as privation of light, or darkness, disposes to inactivity andsleep. " In maladies characterised by imperfect nutrition and sanguinification, as scrofula, rickets, and ana3mia, and in weakly subjects with oede- raatous (dropsical) limbs, &c., free exposure to solar light is sometimes attended with very happy results. Open and elevated situations probably owe part uf their healthy qualities to their position with regard to it." On the contrary, "in diseases of the eye, attended with local vascular or nervnus excitement, in inflammatory conditions of the brain, in fever, and in mental irritation, whether attended or not with vascular excitement, the stimulus of light proves injurious, and, in such cases, dark- ness of the chamber should beenjoined. After parturition, severe wounds, and surgical ope- rations, and in all inflammatory conditions, 61 962 LIGHT, ELECTRIC exclusion of strong light, contributes to the well-d ing of the patient." (Ptreira.) LIGHT, ELECTRIC. We believe we are correct iu stating, that within the lust two or three years some 600 registrations for patents, more or less, have been taken out for elec- tricity applied to the purposes of artificial illumination. Conceding that many, if not the greater part, of these inventions may prove useless, their number is nevertheless an index of the mental activity that has lately been directed to the subject of electric light- ing ; and although we are far from affirming that the problem of the practical application of electricity to the lighting of our streets and dwellings may eventually be successfully thought out, still, we think, looking upon these constant endeavours to accomplish the end in view as links in the chain of that ex- perimental evolution and gradation which has characterised the course of most great dis- coveries, we are justified in regarding them as not altogether improbable auguries and pre- cursors of subsequent success. Shortly after Faraday's discovery in 1830 of electrical induction, or the power of a bar of magnetised steel to set up in a certain direction a current of electricity in a coil of insulated wire when introduced into it, Pixii, reducing the result of Faraday's researches to practice, constructed an instrument, which appears to have been the first dynamic mag- neto-electric machine. By Pixii's contrivance a current of electricity was generated by means of the poles of a permanent horseshoe magnet being made to revolve across those of an electro, or temporary magnet, the induced electricity set up in which in its turn esta- blished in the surrounding helix a current of electricity, which being made to escape by the terminals or ends of the wire coils could be applied to practical use. The dynamic electro-magnetic machines of Saxton and Clarke, which succeeded Pixii's, may be regarded as modifications of this latter, since they differed only in the arrangement of their parts and mode of action. All three machines were chiefly in use in chemical and physical laboratories, whence they have gra- dually been supplanted by the far more useful Euhmkoiff's coil, a very powerful variety of the electro-magnetic instrument. In a small form Clarke's is now chiefly used for medical purposes. That electro-magnetic machines, as cheaper and more convenient sources of electric force, should have been applied to the purposes of telegraphy, will be an obvious inference. Among the most important and effective of the various instruments for attaining this end, it will suffice to mention the magneto-electric machine of Messrs Siemens and Halske, first brought into use in 1854. Except, however, in the case of short dis- tances, or with telegraphs belonging to private persons or commercial firms, these instruments have not met with very general adoption. This is owing to the great tension of the in- duced current, and the consequent difficulty of insulating the wire, particularly for long dis- tances, objections from which the old galvanic apparatus is in a much greater measure free. Mr Henley was the first to use the dynamic magneto-electric machine for working the electric telegraph soon after this instrument had been adopted in England ; but as we have seen, the method, except in the cases quoted, have been in great measure abandoned. A large magneto-electric machine has lately been invented by Wheatstone, the induced spark from which is used for firing mines. The first electro-magnetic machine used for lighting purposes appears to have been one that was the joint invention of MM. Nollet and Vari Malderen, of Brussels, a circumstance to which it probably owes its name of the ' Alliance Machine.' NoUet, who brought out his invention (which is a modification of Clarke's) in 1850, originally designed it for the electrolysis of water, the hydrogen resulting from which it "as proposed to pass through camphine, or some other hydro-carbon illuminant, and to burn as gas. Additionally it was designed to use the hydrogen as a source of motive power by exploding it in a suitably constructed engine. Owing to the improvements, how- ever, effected in the machine by Van Mal- deren, by which it became a powerful gene- rator of magneto-electricity, this purpose was abandoned. ' The Alliance Machine ' consists of a cast-iron frame, on the circumference of which 40 powerful horseshoe magnets, each capable of supporting a weight of 120 to 130 lbs., are fixed, in eight series of 5 magnets each. A number of circular metal discs, around the circumference of which are at- tached sixteen bobbins of insulated wire fixed to a horizontal shelf turned by a pulley, are in such a position with regard to the magnets, that with each revolution of the shaft each bobbin passes sixteen alternate poles of the magnets, and will have had sixteen alternate currents set up or induced in it. Until re- placed by the later and smaller mngneto- electric machine, the * Alliance ' has been the one mostly employed for the production of the electric light in France, and it is still in use in the lighthouses of H6ve and Grisnez, as well as in those of many other places in that country. In 1856 Mr Holmes took out a patent for a machine, which differs from Nollet's in increasing the number of bobbins by arranging them in concentric circles be- tween two brass discs. By this device the bobbins revolve more quickly in succession in front of the poles of the magnets, a plan which ensures the generation of a greater number of currents for every revolution. Like the first application of Nollet's, Holmes' machine was used for lighthouse illu- mination. It was in work from December, LIGHT. ELECTRIC 1858, until Juno, 1862. at the South Foreland lit;litliouae, since which time it has been re- moved to Dungenc88, in the lighthouse of which station it hus been in use ever since. When applied to lighting purposes, both the ' AUIuQce ' and Holmes', and the other machines named, are worked in conjunction with tlie carbon points, which when arranged with proper machinery constitute tlie electric lamp. Wild's and Ladd's are powerful dynamic magneto • electric instruments, capable of yielding large quantities of the electric fluid. Ai'titiclal illumination by means of elec- tricity has, however, been more or less occa- sionally practised for other than lighthouse purpo^e8. For instance, in 1854, during the building of the Napoleon Docks at Rouen, when 800 workmen were engaged nightly for four hours, the electric light was used for several nights with perfect success, the men being able to carry on their work at a distance of more than 100 yards from the source of the light. . In 1862 and 186.3 it was frequently em- ployed in Spain during the night in the con- struction of railways. During the lute Franco- German war in 1870 it was applied to sub- marine illumination, and more lately it has been used in a series of street illumination in St Petersburg. The eli'ctnc light apparatus was placed on the tower of the Admiralty Buildings of th.it city, and by means of it throe of the larger streets were illuminated at night from 7 until 10 o'clock. In this latter case, as well as in that of the Eouen Docks, the lamps were supplied with the electric current generated in batteries. It nitty be said, however, to have been only within the last two years that the question of electric lighting has developed into a burning one, and that the light Itself hus become so much more generally and extensively adopted. Tuis new era in the history of artificial illumination uniy be said to date from the in- troduction of two forms of dynamic magneto- electric apparatus, the one invented by Dr Sieineus, the eminent telegraphic engineer, the other by M. Gramme, of Paris, who, from having been formerly a journeyman carpenter, has now become the head of a manufacture which forms a most important branch of scientific industry. In the apparatus of Gramme and Siemens three marked features and improvements over the older machines liave been achieved : — 1. A great reduction in size, and, conse- quently, in coat, and requisite space for the machiiio. a. The method of generating large quanti- ties of electricity by the mutual action between the different pa'rts of the same machine, and the induction therein set up.' ' Xliia iliscuvery was mudo independently and nearly 3. The production of the electric cnrrent at a much less expenditure of motive power. On this latter point Professor Tyndall, in his report to the elder brethren of the "Trinity House, states that magneto-electric machines of old construction cost ten times more, oc- cupied twenty-five times the space, and weighed fourteen times as much as the recent machines, while they produced only one-fifth of the light with practically the same driving power; which in effect amounts to this— that taking illuminating effect in each case into consideration, the new machines cost one- fiftieth, and are, as regards space occupied, 125 times more advantageous than the earlier forms. In all the older and larger machines the current of electricity, as it was given off from the wire and passed through the carbon paints, was alternate, or first in one direction and then in the opposite — that is, it was a mo- mentary current, first positive and then negative. In Siemens' machine, and in one form of Gramme's, the curreut is direct — that is, it pursues one uniform course in its passage through the carbon points of the lamp, and in its circuit from the terminal of one wire to that of the other. Scientific opinion is somewhat at variance as to the disadvantages of the indirect cur- rent ; many electricians consider that it causes the partial destruction of the contact^, and sets up unnecessary heat in the machine. In magneto-electric machines employed in electro- metuUurgic operations, it is essential the cur- rent should be a direct one. In the Gramme machine the electro-magnet consists of a ring computed of soft iron wire attached to a horizontal spindle or axis, which latter is turned by an end!e-s strap revolving on a pulley. Around this iron ring ore wound a number of coils, each having 300 turns, of insulated copper wire, each coil being bent inside the ring, and ti.rui.cENS, L. ; Looch de Teonohin, Fr. Prep. From oil of almonds, syrup of capillaire, manna and cassia pulp, of each 2 oz. ; pow- dered gum tragacanth, 20 gr. ; orange-flower water, 2 fl. oz. As the last. Tlie above is the quantity for two days, which is as long as it will keep. Linctus of Egg. Syn. Linctus oti ; Lo- HOCH ovi. Prep. Oil of almonds, \ dr.; yolk of 1 egg; syrup of marshmallow, 1 oz. Mix. Linctus, Emonient. Syn. Oily emulsion ; LOHOOH OLEOSUM, E.VIULSIO OLEOSA, L. ; LoooH nuiLEUX, Fr. Prep. (P. Cod) Oil of almonds, powdered gum, and orauge-fljwer water, of each 4 dr. ; syrup of marshmallow, 1 oz. ; water, 3 ft. oz. or q. s. ; for an emulsion. In troublesome coughs, Linctns, Ezpec'torant. Syn. Linctus ex- PECTOEANS, LoHOCH E., L. Prep. 1. Oxymel of squills, confection of hips, syrup of marsh- mallow, and mucilage of gum Arabic (thick), equal parts. Demulcent and expectorant. 2. (Dr Copland.) Oil of almonds and syrup of lemons, of each 1 fl. oz. ; powdered ipeo icu- anha 6 gr. ; confections of hips, 1 oz. com- pound powder of tragacanth, 3 dr. 3. (Ziinetti.) Kermes mineral, 4 gr. ; manna, 6 oz. ; oil of almonds, syrup of squills, and syrup of senega, of each 2 dr. Laxative, de- mulcent, and expectorant. The above are useful in hoarseness, tickling coughs, sore throats, &c. Linctns, Green. Syn. Linctus vibidb; LoHOCH TIEIDE. Prep. Pistachio nuts (or sweet almonds), no. 14; syrup of violets, 1 oz.; oil of almonds, i oz. ; gum tragacanth 15 gr. ; tincture of saffron, 1 scruple; orange- flower water, 2 dr. ; water, 4 oz. Mix. Linctus of Linseed. (E. 1744.) Syn. Linotus lini; Lohoch lini. Prep. Fi-esh drawn linseed oil, 1 oz. ; syrup of tolu, 1 oz. ; sulphur, 2 dr. ; white sugar, 2 dr. Mix. Linctns of Manna. (E. 1744.) Syn. Linctus mann^; Lohoch mannjb. Prep. Equal parts of manna, oil of almonds, and syrup of violets. Mix. Linctns of Naphthalin. (Dupasquier) Syn. Linctus naphthalini; Lohoch naphthal- INI. Prep. To one common lohoch add from 8 gr. to 30 gr. of naphthalin. The latter must be well triturated with the gum. — Dote. One teaspoonful, as an expectorant. Linctus, Pectoral. Syn. Fox lungs ; Linc- tus PECTOBALIS, LorfOCH E PULMONE VUL- PIUM, L. Prep. From spermaceti and Spanish juice, of each 8 oz- ; water, q. s. to soften the liquorice ; make a thin electuary, and add of honey, 3 lbs. ; oil of aniseed, 1 oz. ; mix well. A popular and excellent demulcent in coughs. It formerly contained the herb' fox lun«?, but spermaceti is now substituted for that article Linctns of Poppies. (Th. Hosp.) Syn. Linctus papaveeis. Frep. Compound tinc- ture of camphor, syrup of poppies, and svrup of tolu, of each equal parts. Mix. — Dose, 1 fl.dr. Linctus of Spermaceti. (E. 1744.) Syn. 972 LINEN LllrOTUS CSTACBI; LOHOCH CBTACEI. Frep. Spermaceti, 2 dr. j yolk of egg, q. s.; tritu- rate, and add gradually oil of almonds, i oz. ; syrup of tolu, 1 oz. Mix. Linctus of Syrup of White Poppies. (P. C.) Syn. Linctus steupi papavebis albi; LOHOOH STEUPUS PAPAVBEIS AlBI. Prep. White lohoch, 5 parts ; syrup of poppies (P. C), 1 part. Mix. Linctus, Turpentine. Syn, Linctus btimu- lANa, L. TEEEB1NTHIN.E, LOHOCH ANTHEL- MINTICUM, L. Frep. (Recamier.) Oil of tnrpcntiue, 2 dr. ; honey of roses, 3 oz. ; mix. — Dose. A teaspoonful, night and morning, followed by a draught of any weak liquid; iu worms, more especially tape-worm. Linctus, White. Syn. LiMCTUS AIBUS, mis- tuba ALBA, Lohoch album, L. ; LoocH BLANC, Fr. Frep. (P. Cod.) Jordon almonds, 4J dr. ; hitter almonds, i dr. ; blanch them by steeping them in hot water and removing the skins ; add of white sugar, i oz. ; gum traga- caiith, 20 gr. ; beat to a smooth paste, and further add of oil of almonds and orange- flower water, of each 4 dr. ; pure water, 4 fl. oz. A pleasant demulcent iu tickling coughs. LIS'EJS. Syn. Linteum, L. Linen is a textile fabric made of the libre-flbi'es of the Linum usUaiissimum, or common flax, a plant which from time immemorial has been culti- vated for this purpose. It is remarkable for the smoothness and softness of its texture, and is hence highly esteemed in temperate climates as an elegant and agreeable article of clothing to be worn next the skin. Its fibres are better conductors of heat, more porous, and mijre at- tractive of moisture, than those of cotton, which render it less adapted for body linen in cold weather, as well as in hot weather and hot climates, than calico. The latter, however, lacks the luxurious softness and freshness of linen, whilst the peculiar twisted and jagged character of its fibres render it apt to excite irritation in extremely delicate skins. The common prejudice in favour of old linen and Hax lint lor dressing wounds is thus shown to have reason on its side, and, like many otlier vulgar prejudices, to he supported by the in- vestiijatious of science. Identif. Linen fabrics are commonly sophis- ticated with cotton, which is a much less costly and a more easily wrought material. Various jilans have been proposed to detect this fraud, many of which are too complicated and difficult for practical purposes. The Ibl- Jowitig commend themselves for their sim- plicity and ease of application : — 1. A small strip (a square inch, for instance) of the suspected cloth is immersed for 2 or 3 minutes in a boiling mixture of about equal parts of hydrate of potassium and water, contained in a vessel of silver, porcelain, or hard glass ; after which it is taken out and pressed between the folds of white blotting paper or porous calico. By separating 8 or 10 threads in each direction, their colour may be readily seen. The deep yellow threads are linen, the white or pale yellow ones are COTTON. 2. A small strip of the cloth, after having been repeatedly washed with rain water, boiled in the water, and dried, is immersed for 1 to 2 minutes in sulphuric acid ; it is then withdrawn, carefully pressed under water with the fingers, washed, immersed for a few seconds in ammonia, solution of carbonate of potassium, or solution of carbonate of sodium, again washed with water, and dried between filtering paper. By this treatment the cotton fibres are dissolved, while the linen fibres are merely rendered thinner and more translucent according to the duration of the experiment ; after a shoi*t immersion, the cotton fibres appear transparent, while the iinen fibres re- main white and opaque. 3. Bottger recommends the linen stuffs to he dipped into an alcoholic solution of rosolic acid, then into a concentration solution of sodium carbonate, and finally washed with water. The linen fibre assumes a pink colour, whilst the cotton fibre remains unaltered. 4. (By the micboscope.) The indications afforded by both the previous tests, although quite visible to the naked eye, are rendered still more palpable by the use of a magnifying glass of small power, as the com- mon pocket lens. Under a good microscope the presence of cotton in a linen tissue is very per- ceptible. The fibres of cotton present a distinctly flat and shiivelled ap- pearance, not unlike that of a narrow, twisted rib- bon, with only occasional joints ; whilst those of flax are ronnd, straight, and jointed. The fibres of cotton, after being exposed to the action of strong alkaline lyes, untwist themselves, contract in length, and assume a rounded form, but still continue dis- tinct in appearance from the fibres of linen. The engraving represents a fibre of linen (1) and a fibre of cotton (2), as they appear when magnified 155 diametei's. The difference be- tween the two may be perceived, although less distinctly through a good Stanhope or Cod- dington lens, provided the object be well illuminated. Dyeivg. Linen and cotton, from the simi- larity of their behaviour with dye-stuffs, are treated in nearly the same manner. The affinity of their fibres for colouring matter is very much weaker than that of the fibres of silk and woollen. On this account they are dyed with greater ditTiculty than those sub- stances, and the colours so imparted are, in general, less brilliant and permanent under similar conditions. Linen shows less disposi- tion to take dyes than cotton. The yarn or LINEN 973 cloth, after being aconred and blenched in the unuitl tuuiiner, requires to have an additional tendency given to it, by elieniieal means, to conileuse and retain the inateTials of the dye- bath in its pores. This is effected by steeping the goods in solntions (mordants) which have ut once an affinity for both the fibres of the cloth and the colouring matter. A similar process is employed in dyeing most other sub- stances ; but with cotton and linen, attention to this point is essential to the permanency of | the dye. These matters are more fully ex- plained under the heads CXEiKa and Mos- DANT. The following new process for bleaching linun, having been omitted from our article on "Bleacliiug" is inserted here: — Mr Hodges' process, which is known in Ireland as the " Chemico-Mechanical Pro- cess," owing to tlie patentee turning to account the advantages derivable from the employment of mechanical contrivances driven by steam, combined with the intt'oductlon of a new me- thod of obtaining the hitherto little used hypochlorite of magnesia, may be said to date from the discovery of the substance, known as Kieserite (native sulphate of magnesia), whicli occurs as an essential constituent of the Abraumsalts of Stassf urth. For some time after the introduction of this substance into the market, it was considered of little value except for the production of Bpsom salts; but Mr. Hodges, in the course of some investi- gations in bleaching jute, having had occa- sion to employ large quantities of hypo- chlorite of magnesia, it occurred to him that kieserite might be substituted for the more expensive crude sulphate of magnesia; and the importation into Ireland of the sample for this purpose was tlie first that was ever sent into that country for the manufacture of a bleaching liquor, or, indeed, for any other use. Mr. Hodges on experimenting with the kiese- rite, found that it not only supplied the place of the crude sulphate, but acted as a better precipitant for the lime of the bleaching pow- der, which is employed in the production of the hypochlorite of magnesia ; and that it also pro- duced a stronger and clearer solution. With- out entering into a minute description of the process which is at present successfully car- ried out in a factory erected for the purpose in the neighbourhood of Belfast), the follow- ing outline will be sufBcientto show the nature of the methods adopted. The kieserite, which is imported from Germany in square blocks, on arriving at the works, is conveyed to a house, on the ground-floor of which it is stacked until required, when it is ground to a fine powder, and placed in barrels, is drawn up by means of a crane to a room at the top of the building, at one end of which is a row of three tanks furnished with water taps, agi- tators, and false bottoms. In one of the end tanks a definite quantity of the kieserite pow- der (varying according to its strength, is as- certained by analysis) is placed and dissolved in agiven quantity of water,the solution being assisted by agitators, and on settling the clear liquor is siphoned over into the middle tank. In the third tank bleaching powder (hypochlo- rite of lime), varying in quantity according to the strength of the kieserite solution, is placed. The bleaching powder after being agitated with water is allowed to settle, and the clear solution is siphoned over into the middle tank containing the clear kieserite solution, the agitator being kept in motion, not only during the mixing of the liquids, but for some time after. The mi.\ed liquids are then allowed to remain undisturbed all night, after which the clear hypochlorite of magnesia solution is siphoned into a large settling tank, which is situated in the room below. Prom this vessel it is conducted through wooden pipes (which are so contrived that they can be opened and cleansed at will), into a large cistern standing in the bleaching house. This cistern is fitted with a ball-cock, by which arrangement the liquid can be drawn oSf by a system of wooden pipes as required. The bleaching house in which the cistern is situated is fitted up in an original manner, and covers something more than an acre of ground; whilst the reeling-shed, which is the only part of the works our limits will permit us describe, is 240 feet long by 24 feet broad, and contains ten steeps and twelve reel boxes. Each box is provided with water, a solution of the bleaching agent, and steam pipes, and is capable of reeling at a time about 500 lbs. of yarn. Above the box is a line of rails or pillars. A travelling crane runs along the reels, and carries the reels from one box to another. Attached to this crane is a newly- invented hydraulic pump, by means of which the reels with th^arn on them can be lifted in a few seconds from one box to another. After the yarn has been boiled, washed, and passed through the squeezers in the usual manner, it is put on to a wagon, in which it is carried, by means of a line of rails, down to the first reel box. Here it is placed on to the reels, which are made to revolve by means of steam ; first in one direction and then in ano- ther, through a solution of carbonate of soda, previously heated by means of the steam-pipes before mentioned. The yarn having been sufficiently scalded and so saturated with soda, the reels to which it is attached are raised by the hydraulic pump out of the box, and the yarn allowed to drain for a few minutes, after which the travelling crane carries it on to the next box. Into this box the yarn is again lowered by the pnmp and made to revolve as before, but this time through a solution of the bleaching agent, which immediately re-acting on the carbonate of soda with which the yarn is charged, renders this bleaching agent free from the danger which attends the employ- ment of chlorine, or the ordinary bleading powder used in the older methods of bleaching. 974 LING— LINIMKNT After the yarns liave been brought to the de- sired shade in the solution of Hodges' bleach- ing agent they are either removed as before to a new box, and there washed before being scoured, or they are thrown into one of the steeps filled with water for the night. These operations are repeated with weaker solutions in the remaining reel boxes, cither once or twice according to the shade required. Mr Hodges claims as the chief features of his Invention that it consists, first, in the em- ployment of a bleaching agent which has not hitherto been practically employed, and a cheap method for its production ; second, in the preparation of the yarn prior to being sub- mitted to the action of the bleaching agent, this preparation setting free not only the imprisoned chlorine of the hypochlorite, but also another powerful bleaching agent, oxygen ; third, in new and improved machi- nery, by which the work of bleaching the yarn is greatly shortened ; fourth, in doing away with the tedious and expensive operation of exposing the yarn on the grass ; if this last were the only feature in Mr Hodges' inven- tion, the patentee would have greatly im- proved the process of bleaching, not only, however, does the new process supplant the old long and tedious one, but a great eco- nomy of time is additionally gained in other parts of the process, added to these advan- tages it is stated that a superior finish is given to the yarns, and that in consequence a much greater demand for them has arisen. Mr Hodges contends that the absence of caustic lime from his new bleaching compound gives it great advantages over the old bleach- ing powder, particularly in its application to finely woven fabrics, such as muslins, &c. He also says that fabrics bleached by it receive an increased capacity for iitibibing and retain- ing colouring matter, a fact of considerable importance to the dyer and calico-printer, as they are thus enabled to communicate to the fabrics tints which have heretofore been con- sidered impossible. See Kieberite, The domestic mangement of linen may here receive » few moments' attention. Fruit stains, iron-moulds, and other spots on linen, may, in general, be removed by applying to the part, previously washed clean, a weak solution of chlorine, chloride of lime, spirits of salts, oxalic acid, or salts of lemons, in warm water, and frequently by merely using a little lemon juice. When the stain is removed the part should be thoroughly rinsed in clear warm water (without soap) and dried. Recent iron-moulds or ink spots on starched linen, as the front of a shirt, may be conveniently removed by allowing a drop or two of melted tallow from a common candle to fall upon them before sending the articles to the laundress. The oxide of iron combines with the grease, and the two are washed out together. If the spot is not entirely removed the first time, the process should be repeated. Linen, that has acquired a yellow or bad colour by careless washing may be restored to its former white- ness by working it well in water to which some strained solution of chloride of lime has been added, observing to well rinse it in clean water both before and after the immersion in the bleaching liquor. The attempt to bleach unwashed linen should be avoided, as also using the liquor too strong, as in that case the linen will be rendered rotten. IiING. The Qalus mohta (Linn.), an inferior species of the cod-fish tribe, common in the Northern seas, and used as a coarse article of food by the poor. LDflMENT. Syn. LiNiMENTini, L. A semifluid ointment, or soapy application to painful joints, swellings, burns, &c. The term is also occasionally extended to various spirituous and stimulatmg external apphca- tions. A preparation of a thinner consistence, but similarly employed, is called an ' embko- CATION.' These terms are, however, fre- quently confounded together, and misapplied. Liniments are generally administered by fric- tion with the hand or fingers, or with some substance (as a piece of flannel) capable of producing a certain amount of irritation of the skin. Sometimes a piece of linen rag dipped in them is simply laid on the part. In most cases In which liniments are found beneficial, the advantage obtained from them is attri- butable rather to the friction or local irritation than to any medicinal power in the preparation itself. The greater number of cerates and ointments may he converted into liniments by simply reducing their consistence with almond or olive oil, or oil of turpentine. I/iniment, Ac'id. Sgn. Linimentum aci- DTTM, L. AOIDI STTLPHTTBICI, L. Prep. 1. (Sir B. Brodie.) Salad oil, 3 oz. ; oil of vitriol, i dr. ; mix, then add of oil of turpentine, 1 oz., and agitate the whole well together. As a counter-irritant, in rheumatism, stiff joints, &c. It closely resembles the ' Gulltoniak Embkocation.' 2. (Hosp. P.) Olive oil, 3 oz. ; oil of tur- pentine, 2 oz. ; sulphuric acid, 1 fl. dr. An excellent-alterative, stimulant, diseutient, and counter-irritant, in chronic rheumatism, stiff joints, indolent tumours, and various chronic diseases of the skin. liniment of Albumen. (Dr Chvistison.) Syn. Linimentum albumhhs. Prep. Equal parts of white of egg and rectified spirit, agitated together. In excoriation froUi pressure. Liniment of Am'ber-oil. Syn. LnfnuENTirM snooiNi, L. Prep. 1. From olive oil, 3 parts j oils of amber and cloves, of each 1 part. Re- sembles ' Roche's Embrocation.' 2. (Opiated ; Linimentum succini opia- TUM, L.) From rectified oil of amber and tincture of opium, of each 2 fl. oz. ; lard, 1 oz. Anodyne, antispasmodic, and stimulant. A once popular remedy in cramp, stiff joints, &c. LINIMENT 973 Lioiment of Ainmo"iila. Syn. Ammoniaoal LiNiMBKT, Volatile l., Oil and h abtsuobn ; LlNIMBNTUM AMMONI^B (B. P., Ph. L. E. & D.), L. Prep. 1. (B. P.) Solution of am- munia, 1 ; olive oil, 3 ; mix. 2. (Ph. L. e peculiar character of the substance may indi- cate. This is not done until sliortly before submitting them to the action of the men struum; as, after they are bruised they rapidly lose their aromatic properties by ex- posure to the air. Wlien it is intended to keep them for any time in the divided state they should be preserved in well-corked bottles or jars. The practice of drying the ingredients before pounding them, frequently adopted by ignorarit and lazy workmen for the sake of lessening the labour, is, of course, even more destructive to their most valuable qualities than mere exposure to the air. The length ot time the ingredients should be digested in the spirit should never be less than 5 or 6 days, but a longer period is preferable when distil- lation is not employed. In either case the time may be advatitageously extended to 10 days or a fortnight, and frequent agitation should be had recourse to during the whole period. When essential oils are employed to convey the flavour, they are first di^slilved in a little of the strongest rectified spirit of wine, in the manner explained under Essence ; and when added to the spirit, they are mixed up with the whole mass as rapidly and as per- fectly as possible. In managing the still, the fire is proportioned to the ponderosity of the oil or flavouring substance, and the re- ceiver is changed before the faints come over; as these are unfitted to be mixed with the cordial. In many cases the addition of a few pounds of common salt to the liquor in the still facilitates the process and improves the product. Ingredients which are not volatile are, of course, always added after distillation. The stronger spirit is reduced to the desired strength by means of either clear soft water or the clarified syrup used for sweetening. ' The sugar employed should be of the finest quality, and is preferably made into capil- laire or syrup before adding it to the aro- matised spirit; and not until this last has been rendered perfectly ' fine ' or transparent, by infiltration or clarification, as the case may demand. Some spirits or infusions, as those of aniseed, caraway, &c., more particularly require this treatment, which is best performed by running them through a clean wine bag, made of rather fine cloth, having previously mixed them with a spoonful or two of mag- nesia; but in all cases clarification by simple repose should be preferred. Under proper management, liqueurs or cordials prepared of good materials will be found perfectly ' clear ' or ' bright ' as soon as made, or will become so after being allowed a few days for defecation ; but in the hands of the inexperienced operator, and when the spirit employed is insufficient in strength or quantity, it often happens that they turn out 'foul' or 'milky.' When this is the case, the liquid may be ' fined down ' with the whites of 12 to 20 eggs per hogshead; or a little alum, either alone or followed by a little carbonate of sodium or potassium, both dissolved in water, may be added, in the manner described under Fihinos. An excellent and easy way of manufacturing cordial liquors, especially when it is inconve- nient to keep a large stock on hand, is by simply 'aromatising' and 'colouring,' as cir- cumstances or business may demand, spirit 60 or 64 u. p., kept ready sweetened for the pur- pose. To do this to the best advantage, two descriptions of sweetened spirit should be pro- vided, containing respectively lib. and 31bs. of sugar to the gallon. From these, spirit of any intermediate sweetness may be made, which may be flavoured with any essential oil dissolved in alcohol, or any aromatised spirit or ' infusion ' (see helow), prepared either by digestion or distillation. As a general rule, the concentrated essences, made by dissolving 1 oz. of the essential oil in 1 pint of the strongest rectified spirit of wine, will be found admirably adapted for this purpose. These essences, which should be kept in well-corked bottles, are employed by dropping them cautiously into the sweetened spirit until the desired flavour is produced. During this operation LIQUEUR 985 the UqnoT ahould be frequently and violently (hakon to prodaco complete admlxtare. If by any accidoMt the essence is added in too large a quantity, the resultiug ' milkiness ' or excess of flavour may be removed by the addition of a little more apirit, or by clarifica- tion. In this way the majority of the liqueurs in common use may be produced extempo- nineouoly, of nearly equal quality to those prepared by distillation. For those which are coloured, simple digestion of the ingredients is almost universally adopted. The " process by distillation" should, however, be always employed to impart the flavour and aroma of volatile nromatics to the spirit, when expense, labour, and time are of less importance than the production of a superior article. The French liqueuristes are famed for tlie pre- paration of cordials of superior quality, cri'iiui- like smoothness, and delicaje flavour. Their success chiefly arises from the employment of very pure spirit and sugar (the former in a larger proportion than that adopted by the English compounder), and in the judicious npplicatiim of the flavouring ingredients. They distinguish their cordials as 'eanx' and 'extraits' (waters, extracts), or liqueurs which, though sweetened, are entirely devoid of viscidity ; and ' baumes,' ' crimes,' and Miuiles' (balms, creams, oils), which con- tain sufiicient sugar to impart to them a syrupy consistence. The greatest possible attention is given to the preparation of the aromalised or flavouring essences, in France called ' infusions.' These are generally made by macerating the aromatic ingredients in spirit at about 2 to 4 u. p. (sp. gr. 022 to •925), placed in well-corked glass carboys, or stoneware jars or bottles. The maceration is continued, with occasional agitation, for 3, 4, or even 5 weeks, when thearoinatised spirit is either distilled or Hltered ; generally the former. The outer peel of cedrats, lemons, oranges, limettes, bergaraottes, &c., is alone used by our Continental neighbours, and is obtained either by carefully peeling the fruit with a knife, or by ' oleo-saccharum,' by rub- bing it olf with a lump of hard white sugar. Aroiuiitic seeds andwoodsare bruised bypouud- ing before being submitted to infusion. The substances employed in Prance to colour li- queurs arc, for — blue, soluble Prussian blue, sulphate of indigo (nearly neutralised with chalk), and the juice of blue flowers and ber- ries; — amber, fawn, and brandy coliur, burnt sugar or spirit colouring; — green, spinach or parsley leaves (digested in spirit), and mix- tures of blue and yellow ; — red, powdered cochineal or brazil wood, either alone or mixed with a little alum ; — violet, blue violet petals, litmus, or extract of logwood ; — purple, the same as violet, only deeper ; — yellow, an aque- ous infusion of snfllower or French berries, aud the tinctures of saffron and turmeric. A frequent c.inse of failure in the manufac- ture of liiiueurs and cordials is the addition of too mnch flavouring matter. Persons nn- accustomed to the use of strong aromatic essences and essential oils seldom sufficiently estimate their power, and, consequently, are very apt to add too much of tlieni, by which the liqueur is rendered not only disagreeably high flavoured, but, from the cicess of oil pre- sent, also ' milky,' or ' foul,' either at once, or, what is nearly as bad, on the addition of water. This source of annoyance, arising entirely from bad manipulation, frequently discourages the tyro, and cuts short his career as a manufacturer. From the viscidity of cor- dials they are less readily ' fined down ' than unsweetened liquor, and often give mnch trouble to clumsy and inexperienced opera- tors. The most certain way to prevent dis- appointment in this re-pect is to use too little rather than too much flavouring ; for if the quantity proves insufficient, it is readily 'brought up' at any time, but the contrary is not effected without some trouble and delay, A careful attention to the previous remarks will render this branch of the rectifier's art far more perfect and easy of performance than it is at present, and will, in most case-^, pro- duce at once a satisfactory article, ' fine, sweet, and pleasant.' The cordials of respectable British 'com- pounders ' contain fully 3 lbs. of white lump sugar per gallon, and are of the strength of 60 to 64 u. p. The b.iumes, cremes, and huiles imported from the Continent are richer both in spirit and sugar than ours, and to this may be referred much of their superiority. Mere sweetened or cordialised spirits (eanx, of the Pr.) contain only from 1 to IJ lb. of sugar per gallon. The purity of liqueurs is determined in the manner noticed under Bbandy, Wine, &c. The following list embraces nearly all the cordials aud liqueurs, both native and im- ported, met with in trade in this country : — Absinthe. Si/n. Extbait d'absinthe de Suisse ; Swiss bxtbact of wokmwood. I'rep. From the tops of Absmlhum majus, 4 lbs.; tops of Ahsinthum minus, 2 lbs. ; angelica root. Calamus aromaticua,C\\inese aniseed, and leaves of dittany of Crete, of each 15 gr. ; brandy or spirit at 12 n. p., 4 galls.; macerate for 10 days, then add water, 1 gall. ; distil 4 galls, by a gentle heat, and dissolve in the distilled spirit, of crushed white sugar, 2 lbs. Tonic and stomachic. Alker'mes. This liqueur is highly esteemed in some parts of the South of Europe. Frep. 1. Bay lejives and mace, of each 1 lb. ; nutmegs and cinnami>n, of each 2 oz. ; cloves, 1 oz. (all bruised) ; cognac brandy, SJ palls. ; macerate for 8 weeks, frequently shaking, then distil over 3 galls., and add of clarified spirit of kermes, 18 lbs.; orange-flower water, 1 pint ; mix well, and bottle. This is the ori- ginal formula fur the ' alkermes de Santa jilaria Novella,' which is much valued. 2. Spice, as last j British brandy, 4 galls. LIQUEUR water, 1 gall. ; macerate as before, and draw over 4 galls., to wliich add, of capillaire, 2 galls., and sweet spirit of nitre, i pint. Cassia is often used for cinnamon. Inferior to the last. An'iseed Cordial. Prep. 1. From aniseed, 2 oz. (or essential oil, li dr.), and sugar, 3 lbs. per gall. It should not be weaker than about 45 u. p., as at lower strengths it is impossible to produce a full-flavoured article without its being milky, or liable to become so. 2. (Anisette de Boedeaux.) — a. (Foreign.) Aniseed, 4 oz. ; coriander and sweet fennel seeds, of each 1 oz. (bruised) ; rectified spirit, i gall . ; water, 3 quarts ; macerate for 5 or 6 days, then draw over 7 pints, and add of lump sugar, 2i lbs, i. (English.) Oil of aniseed, 1 5 drops ; oils of cassia and caraway, of each 6 drops ; rub them with a little sugar, and then dissolve it in spirit (45 u. p.), 3 quarts, by well shaking them together ; filter, if necessary, and dis- solve in the clear liquor sugar, li lb. See I'EPPEEMIHT {helovi). Balm of Molucca. Prep. From mace, 1 dr.; cloves, i oz. ; clean spirit (22 u. p.), 1 gall. ; infuse for a week in a well-corked carboy or jar, frequently shaking, colour with burnt sugar q. s., and to the clear tincture add of lump sugar, 4i lbs.; dissolved in pure soft water, i gall. On the Continent this takes the place of the ' cloves ' of the English re- tailer. Bit'ters. These have generally from 1 to li lb. of sugar per gallon.^ Cax'away Cordial. Prep. Generally from the essential oil, with only 2^ lbs. of sugar per gall. 1 fl. dr. of the oil is commonly reckoned equal to i lb. of the seed. The addition of a very little oil of cassia, and about half as much of essence of lemon or of orange, improves it. See Brandt (Caraway). Ce'drat Cordial. Prep. From essence (oil) of cedrat, J oz. ; pure spirit (at proof), 1 gall ; dissolve, add of water, 3 pints, agitate well; distil 3 quarts, and add an equal measure of clarified syrup. A delicious liqueur. See Ceeme and Eau (helow). Cin'namon Cordial. Prep. This is seldom made with cinnamon, owing to its high price, but with either the essential oil or bark of cas- sia, with about 2 lbs. of sugar to the gall. It is preferred coloured, and therefore may be very well prepared by simple digestion. The addition of 5 or 6 drops each of essence of lemon and orange peel, with about a spoonful of essence of cardamoms per gall., improves it. 1 oz. of oil of cassia is considered equal to 8 lbs. of the buds or bark. 1 il. dr. of the oil is enough for 2i galls. It is coloured with burnt sugar. Cit'ron Cordial. Prep. From the oil or peel, with 3 lbs. of sugar per gall., as above. (See below.) CitroJielle. iSi/n. Eatt de Baebabes. Prep. 1 See article Bittkes, I. From fresh orange peel, 2 oz. ; fresh lemon peel, 4 oz. ; cloves, i dr ; corianders and cin- namon, of each 1 dr. ; proof spirit, 4 pints ; digest for 10 days, then add of water, 1 quart, and distil 4 gall. ; to the distilled essence add of white sugar, 2 lbs., dissolved in water, 1 quart. 2. Essence of orange, i dr. ; essence of lemon, 1 dr. ; oil of cloves, and cassia, of each 10 drops J oil of coriander, 20 drops ; spirit (58 0. p.), 5 pints ; agitate until dissolved, then add of distilled or clear soft water, 3 pints; well mix, and filter it through blotting paper, if necessary ; lastly add of sugar (dis- solved), q. B. Clairet. Sgn. Rossams des sin geaines. Prep. From aniseed, fennel seed, coriander seed, caraway seed, dill seed, and seeds of the candy-carrot (Aihamantia cretensis — Linn.), of each (bruised) 1 oz. ; proof spirit J gall. ; digest for a week, strain, and add of loaf sugar, 1 lb., dissolved in water, q. s. Cloves. Syn. Clove coediai.. Prep. Prom bruised cloves, 1 oz., or essential oil, 1 fl. dr., to every 3 galls, of proof spirit. If distilled, some common salt should he added, and it should be drawn over with a pretty quick fire. It requires fully 3 lbs. of sugar per gall., and is generally coloured with poppy flowers or burnt sugar. The addition of 1 dr. of bruised pi- mento, or 5 drops of the oil for every oz. of cloves, improves this cordial. See Balm op Molucca {above). Coriander Cordial. Prep. From corianders, as the last. A few sliced oranges improve it. Creme d'Anis. As aniseed cobdial, only richer. CrSme des Barbades. As citeonelle, adding some of the juice of the oranges, and an addi- tional lb. of sugar per gall. Creme de Cacao. Prep. Infuse roasted caracca-cacao nuts (cut small), 1 lb., and va- nila, \ oz., in brandy, 1 gall., foV 8 days; strain, and add of thick syrup, 3 quarts. Creme de Cedrat. Syn. Huile de Cedbat. Prep. From spirit of citron, 1 pint ; spirit of cedrat, 1 quart; proof spirit, 3 quarts; white sugar, 16 lbs., dissolved in pure soft water, 2 galls. CrSme de ffiacarons. Prep. 1. From cloves, cinnamon, and mace, of each (bruised) 1 dr.; bitter almonds (blanched and beaten to a paste), 7 oz. ; spirit (17 u. p.), 1 gall. ; digest a week, filter, and add of white sugar, 6 lbs., dissolve in pure water, 2 quarts. 2. Clean spirit (at 24 u. p., sp. gr. -945), 2 galls. ; bitter almonds, J lb. ; cloves, cinnamon, and mace, of each in coarse powder, li dr.; infuse for 10 days, filter, and add of white sugar, 8 lbs. ; dissolved in pure water, Igall. ; lastly, give the liqueur a violet tint with infu- sion or tincture of litmus and cochineal. An agreeable, nutty-flavoured cordial, but, from containing so much bitter almonds, should be only drank iu small quantities at a time. The UQUEUB 987 Knglish use only one half the above quantity of uluiunils. Cr6me de Naphe. Prep. Prom sweetened spirit (60 u. p.) containing i\ lbs. of sugar per gull., 7 quarts ; orange-flower water (foreign), 1 quart. Delicious. Crime de Noyeau. See Noyeau. Crime d'Oraoge. Prep, rrora oranges, (sliced), 3 dozen; rectilied spirit, 2 gxlls. ; digest for 14 days ; add, of lump sugar, 28 lbs. (previously dissolved in water, 4i galls.); tincture of s:iffron, \\ fl. oz. ; and orange- flower water, 2 quarts. CrSme de Fortngal. Flavoured with lemon, to wliich a little oil of bitter almonds is added. Curaf ao. Prep. From sweetened spirit (at 56 u. p.), containing 3i lbs. of sugar per gall., flavoured with u tincture made by dige>ting the ' oleo-saccharum ' prepared from Seville oranges, 9 in number ; cinnamon, 1 dr. ; and niacu, J dr., in rectified spirit, 1 pint. It is coloured by digesting in it for a week or 10 days Brazil-wood (in powder), 1 oz., and alter- wards mellowing the colour with burnt sugar, q. 8. Delight of the MandaxlnB. From spirit (22 u. p.), 1 gall. ; pure soft water, \ gall. ; white sugar (crushed small), 4^ lbs. ; Chinese aniseed and ambrette or musk seed, of each (bruised) \ oz. ; saHlower, \ oz. ; digested together in a carboy or stone bottle capable of holding double, and agitated well every day for u fort- night. £aa de Cedrat. Syn. Cidbat wateb. As ciiKME SB obdbat, buC using less sugar. Ean de Chasseurs. See Feffebmint {below). Eau de Vie d'Andaye. Syn. Eau se tie b'Anis; Aniseed liqueub beandt. Prep. From brandy or proof spirit, 1 gall. ; sugar, 1 lb. ; dissolved in aniseed water, 1 pint. Gold Cordial. Prep. From angelica root (sliced), 1 lb. ; raisins, i lb. ; coriander seeds, 2 oz. ; caraway seeds and cassia, of each 1 J oz. ; cloves, \ oz. ; figs and sliced liquorice root, of each 4 oz. ; proof spirit, 8 galls. ; water, 1 gall. ; digest 2 days, and distil 3 gallons by a gentle heat ; to this add, of sugar, 9 lbs., dissolved in rose water and clean soft water, of each 1 quart ; lastly, colour the liquid by steeping in it of hay saffron, 1^ oz. This cordial was once held in much esteem. It derives its name from a small quimtity of gold leaf being for- merly added to it. Huile d'Anis. See Cbeme d'Ams {above). Hnile de Vanille. Flavoured with essence or tincture of vanilla. It is kept in a decanter, and used to flavour liqueurs, grog, &c. Hnile de Venus. Prep. From the flowers of the wild carrot, 2\ oz., and sugar, 3 lbs. to the gall. It is generally coloured by infusing a little powdered cochineal in it. Jargonelle. Syn. Jaeoonelle cobdial. Flavoured with essence of jargoiu'lle pear (ace- tute of amyl). Fine-upple cordial ami liqueui-s from some other fruits are also prepared from the new fruit essences. See EsBEHCB. lem'on Cordial. Prep. Digest fresh ond dried lemon peel, of each 2 oz., and fresh orange peel, 1 oz., in proof spirit, 1 gall., for a week ; strain with expression, add of clear soft water q. s. to reduce it to the desired strength, and lump sngar, 3 lbs. to the gallon The addition of a little orange-flower or rose water improves it. Liqnodilla. Flavoured with oranges and lemons, of each, sliced, 3 in number; with sugar 21 lbs. per gall. Lov'age Cordial. Prep. Prom the fresh roofs of lovage, 1 oz. to the gallon. A fourth of this quantity of the fresh roots of celery and sweet fennel are also commonly added. In some parts a little fresh valerian root and oil of savine are added before distillation. It is much valued by the lower classes in some of the pro- vinces for its stomachic and emmenagogue qualities. Oil of Ce'drat. See Cbeub sb Cedbat {above). Orange Cordial. Like i.emon cobdial or CBEME B'oEANOB, from fresh orange peel, J lb., to the gallon. Farfait Amour. Syn. PeeeectLovb. Prep. Flavoured with the yellow rind of 4 lemons, and a teaspoonful of essence of vanilla to the gallon, with sugar, 3 lbs., and powdered cochineal q. s. to colour. Fep'permint. Syn. Pbppeemint cobdial, SpOBTSMAN's 0., X. MINT; Eau db chas- SEUBB, Fr. This well-known compound is in greater demand in every part of the kingdom than all the other cordials put together. Prep. 1. From peppermint water and gin or plain spirit (22 u. p.), of each 1 pint ; lump sugar, I lb. 2. (Wholesale.) English oil of peppermint, 5 oz., is added to rectified spirits of wine, 3 pints, and the mixture is agitated well toge- ther for some time in a corked bottle capable of holding 4 pints or more ; it is then emptied into a cask having a capacity of upwards of 100 galls., and perfectly white and flavourless proof spirit, 36 galls., is poured in, and the whole well agitated for ten minutes; a solu- tion of the best double refined lump sugar, 2} cwt., in about 35 galls, of pure filtered rain water, is then added, and the contents of the cask well * rummaged up' in the usual manner for at least 15 minutes ; sufficient clear rain water to makeup the whole quantity to exactly 100 gallons, and holding in solution alum, 5 oz., is next added, and the whole is again well agi- tated for at least a quarter of an hour, after which the cask is bunged down, and allowed to repose for a fortnight before it is ' broached' for sale. Obs, The last formula produces a beautiful article provided the ingredients are of good quality. Care on this point is particularly necessary in reference to the essential oil, which should ouly be purchased of some known 983 LIQUEUR DE LA MOTTE— LIQUOE respectable dealer. The sugar should be suffi- ciently pure to dissolve in a wine-glassful of clear soft water without injuriug its trans- parency, and the cask should be a fresh- einptiedgin pipe, or one properly prepared for gin, as. If it gives colour, it will spoil the cor dial. When these particulars are attended to, the product is a bright transparent liquor as soon as made, and does not require fining. Should there be the slightest opacity, the addition of 2 oz. of salt of tartar, dissolved in a quart of hot water, will have the effect of * clearing it down * in the course of a few days. The product is 100 galls, of cordial at 64 u, p. Pimen'to. St/ii. Pimento oobdial, Pimento DEAM. Kather strongly flavoured with allspice or pimento. It has obtained a great repute iti the West Indies in diarrhoea, cholera, and bowel complHints generally. Rasp'berry Cordial. Prep. From raspberry brandy, capillaire, and water, equal parts. A similar article is prepared by flavouring sweet- ened spirit with the new ' raspberry essence.' £at'ifia. The numerous liqueurs bearing this name are noticed in another part of this volume. See Eatifia. Shrub. See the article Shbitb in another part of this work. Sighs of Love. Prep. 1. From proof spirit flavoured with otto of roses and capillaire, equal parts. 2. From sugar, 6 lbs., pure soft water, q. s. to produce a gallon of syrup, to which add, of eau de rose, 1 pint; proof spirit, 7 pints. It is stained of a pale pink by powdered cochineal. A very pleasant cordial. A drop or two (not more) of essence of ambergris or vanilla im- proves it. Tears of the Widow of Malabar. Prep. As BALM OP Molucca, but employing cloves (bruised), i oz., mace (shredded), 1 dr., and a teaspoontul of essence of vanilla for fla- vouring. Some add of orange-flower water, i pint, It is slightly coloured with burnt sugar. Tent. From plain spirit (22 u. p.) and port wine, of each 1 quart; sherry and soft water, of each 1 pint; orange-flower water and lemon juice, of each i pint; essence of ambergris, 2 drops (not more) ; sugar, 2 lbs. See Wine. Us'quebangh. See the article UsQUEBAvan in another part of this work. LIQUEUR DE LA MOTTE. [Fr.] See Deops (Golden) and Tinctube. LldUEUK DOREE. [Fr.] Prep. .Take of cinnamon, bitter orange peel, and Peruvian bark, of each { oz. ; hay saffron, i oz. ; brandy and Malaga wine, of each 3 quarts; digest tor a week, strain, and add of lump sugar, 2 lbs. Tonic, stomacliict and stimulant ; chiefly used as an afjreeable alcoholic dram. LIftUEUR DE PRESSAVIN. [Fr.] Prep. From oxide of mercury (freshly precipitated) and cream of tartar, of each 1 oz. ; hot water, 1 quart ; dissolve and filter. For use 2 spoon- { fuls of this liquor are added to 1 quart of water. — Dose. A wine-glassful 3 or 4 times a day, avoiding the use of common salt. This is simply a solution of potassio-tartrate of mer- cury, and may be taken in the usual cases in which mercury is administered. LIftUODIN'NA. See Liqtjeitb. LIQUIO-AMBAR. Si/n. Cofaibje balsam. A fluid balsamic juice obtained from the Zrijaid- amber styracijlua, an American tree. It cosely resembles liquid bioeax in its properties, and may be applied to the same purposes. See Stteai. LIQ'UOR. 8yn. LlQUOE, L. ; LiQUEUB, Fr. This term is given in the London Phar- macopoeia to those aqueous solutions commonly though improperly called 'watees;' ammo- niae liquor potassfe, &c. It is now more cor- rectly applied to the ' watees ' of the British Piiarmacopceia. See Solution. The term 'liquor' has also, of late years, been applied to certain concentrated prepara- tions, most of which would be more correctly terined 'fluid exteacts,' as they merely dift'er from good extracts in their consistence, and from ordinary extracts in containing less starchy matter, albumen, and gum. There is also usually a little spirit added to them to prevent decomposition. Liquors of this kind may be prepared of the finest quality by the same processes that are required for the pre- paration of good soluble extracts ; observing to stop the evaporation as soon as the consist- ence of treacle is acquired, and when cold, to add l-4th or l-5th part of their weight (after evaporation) in rectified spirit. The addition of 3 or 4 drops of the oils of cloves and mustard seed, dissolved in the spirit, will secure them from any risk of ' moulding ' or fermenting ; in fact, with this addition many of them will keep well without spirit, provided they are evaporated sufliciently, and kept in a cool place. The liquors, which are merely con- centrated infusions or decoctions, and which, in their consistence, do not even approximate to ex tracts, may be made in the manner directed under those heads. Much confusion would be prevented if the terms 'concentrated decoction,' ' concentrated infusion,' &c., were adopted for those vegetable preparations possessing eight times the usual strength; 'liquors' for those of a higher strength, but still sufficiently liquid to be treated as such in dispensing, &c. ; and ' fluid extracts' for those possessing considerable consistence, and approaching the common ex- tracts in their degree of concentration and mode of preparation. See Decoction, In- fusion, Essence, Extbact, Solution, &c. *#* The following formulte present some illustrations of the preparation of this class of medicines. Liquor of Ammonia. Syn. Liquor Ammo- Ni,E. Prep. Strong solution of ammonia, 1 pint ; distilled water, 2 pints; mix and pre- serve in a stoppered bottle. Sp. gr. -gsg. LIQUOR 989 Llqaor of Ammonln, Stronger. Sj/n. Liqcob AuuoniM FOKTIOB. Prep. Mix chloride of Rininoniura in course powder 3 lbs., and slaked lime 41bt., und introdnce the mixture into an iron bottle, placed in a metal pot surrounded by aund. Connect the iron tube which screws air-tight into the bottle in the usual manner, by corks, glass tubes, and caoutchouc collars, with a Woulf's bottle capable of holding a pint ; connect this with a second Woulf's bottle of the same size, the second bottle with a matrnss of the capacity of three pints, in which 22 oi. of distilled water are placed, and the matrass by means of a tube bent twice at right angles, with an ordinary bottle contain- iug distilled water 10 oz. Bottles 1 and 2 are empty, and the latter and the matrass which contains the 22 oz. of distilled water are furnixlied ench with a siphon safety- tube charged with a very short column of mercury. The heat of a fire, which should be very gradually raised, is to be now applied to the metal pot, and continued until bubbles of con- densiblc gas cease to escape from the extremity of the glass tube which dips into the water of the matrass. The process being terminated, the matrass will contain about 43 tl. oz. of strong solution of ammonia. Bottles 1 and 2 will now in- clude the first, about 16, the second, about 10 fl. oz. of a coloured ammoniacal liquid. Place this in a flask closed by a cork, which should be perforated by a siphon safety-tube containing a little mercury, and also by a second safety-tube bent twice at right angles, and made to p iss to the bottom of the terminal bottle used in the preceding process. Apply heat to the flask until the coloured liquid it contains is reduced to three fourths of its original bulk. The product now contained in the terminal bottle will be nearly of the strength of solution of ammonia, and may be made exactly so by the addition of the proper quantity of distilled water, or of strong solution of ammonia. Density "191, contains 32*6 per cent, of ammonia. Antidotes. — Vinegar and water followed by acidulated demulcent drinks. Liquor, Anodyne. See Spirit of Gtheb. Liquor, Antinephritic. Si/n. Liquor akxi- NBPHBiTictJS, L. Prep. (Adams.) Poppy heads, 6 oz. ; water, 1.J pint j boil to one third, strain with pressure, and add of nitrate of potassa, 1 oz. — Dose, 1 to 2 teaspoonf uls night and morning ; in gravel and painful affections of the kidneys and bladder. Liquor, Antipodag'ric (Begnin's). Syn. Hoff- mann's OOrT LIQUID; LlQUOB ANTIPODAG- BI0C8 HoFFMANNll, L. Prep. From Boyle's fuming liqiiir, 1 part; spirit of wine, 3 parts. Sudoritic. — Dose, 20 to 30 drops; or exter- nally, in gout, and other painful affections, either alone or combined with camphor. See AmMONII'M, PERStTLPniDE OF. Liquor Antipsor'ic. S^n. LiQUOE anti- PSOEiorg, LoTio A., L. Prep. (Van Mons.) .Sulphuretof sodium, li dr. j hydrochlorate of ammonia, 75 gr. ; dissolve each separately in water, J pint, mix the solutions, and filter. In. itch and other moist skin diseases. Liquor, Bleaching. See Solution of Chlo- EiDB OF Lime. Liquor, Blistering. B. Sgn. Liquob Kpis- PA8TICU8 LiNIMENTUM CANTHAEIDES. Prep. Mix cantharides in powder, 8 oz. ; and acetic acid, 4 fl. oz. Pack in a percolator, and after 24 hours pass ether slowly through until 20 fl. oz. are obtained. Keep in a stoppered bottle. Liquor, Boyle's Pu"ming. The perhydro- sulphate of ammonia. Liquor of Calum'ba. Sgn. Liquor ca- LUMB^, L. Same as cohoentbatbs ikfusion of oaluhba. Liquor of Cam'phor. See Ebsencb. Liquor of Chiret'ta. Same as Cohcen- TBATED INFUSION OF CHIBBTTA. Liquor of Cincho'na. Si/n. Liquob of BABK ; CONOENTBATKD INFUSION OF BABE, Inspissated i. or b. ; Infusum oinchonjK 8PIS8ATUM (Ph. L), L. Prep. 1. (Ph. L.) Yellow cinchona bark (bruised), 3 lbs., is mace- rated in distilled water, 6 pints, at two suc- cessive operations, as directed under extract of cinchona— Ph. L. ; the mixed infusions are evaporated by the heat of a water bath tg one fourth, and placed aside to settle ; the clear portion is decanted, the remainder strained, and the mixed liquid again evapo- rated until its sp. gr. reaches 1-200; to this, when cold, rectified spirit is dropped in, by degrees, " so that 3 fl. dr. may be added to each fl. oz. of the liquor; " lastly, allow it to repose for 20 days, that the dregs may subside. Ois. It is not at all clear whether the Col- lege means 3 fl. dr. of spirit to be added to each fl. oz. of the liquid before its addition, or that it is to be added so that each fl. oz. of the product shall contain that quantity. We pre- sume the former. 1 9. dr. of this preparation is said to represent fully 4 fl. oz. of the in- fusion OF CINCHONA — Ph. L. ; but it is ob- vious that it must be liable to gi-eat variations in strength. " In a general way I fl. dr. may be considered equal to 3 fl. oz. of the infusion." (Pereira.) As commonly met with, this pre- paration is nearly destitute of the cinchona alkaloids. 2. Yellow cinchona bark, bruised, 56 lbs., and water holding in solution sulphuric acid, 1^ lb., are macerated together, with occasional agi- tation, in a covered earthen vessel, for 48 hours, after which the liquor is expressed, and the residuum or marc is treated with fresh water; the mixed strained liquid is then evaporated as rapidly as possible in earthenware, to exactly 6 lbs.; to this rectified spirit, li lb., is added, and the whole is set aside for a week or 10 days; the clear portion is, lastly, decanted and preserved in well-closed buttles. The pro- 990 LIQUOR duct is very rich in quinine. It is 96 times as strong as the dbooction op oinohona — Ph. L., and 12 times as strong as the above preparation of the Ph. L. This preparation resembles the 'liQFOB cinchona' sold by certain bouses in the trade at 248. per lb., wholesale. 3. Exhaust the bark as above by macera- tion in 3 successive waters without acid, filter, evaporate the mixed liquors to 7 lbs., and pro- ceed as before. Inferior to the last, and less rich in the cinchona alkaloids. Very thick ; scarcely liquid. 4. From palk baek : — (LiQUOE cinchona VATJLTDS ; Infusum cinohon^: spissatum — Fh. ii.) From pale bark, as the last. See Ineubion op Cinchona. Liquor, Disinfect'ing. See Solution (Chlo- rides of Lime, Soda, and Zinc), and DlsiN- FEOTINa COMPOUNDS. Liquor of Er'got. . S^n. Essence of ergot of eye, conoenteated infusion of e. ; Essentia becalis coenuti, Liquoe eboot^, Infusum EE&OTiE concenihatum, L. Frep. Recent ergot of rye (reduced to coarse powder by pounding, or preferably by grinding it in a pepper-mill), li lb., and boiling distilled water, 4 lbs., are digested together in a closed vessel, with frequent agitation until cold, and then put into a wide-mouthed bottle, along with rectified spirit, 2 lbs. j the whole is then allowed to macerate for a week, after which the liquor is expressed and filtered. Obs. 4 fl. dr. of this essence are equal to 1 dr. of ergot in sub stance. It is 8 times the strength of the INFUSION (as usually prepared according to the formula of Pereira and others), and 2i times the strength of the tinctuee of eegot of the London Apothecaries' Hall. This is the only essence of liquoe of eegot known in the wholesale trade. Liquor of Flints. See Solution. Liquor of Gntta Percha. B. Sfftt. Liquoe Gutta peecha. Gntta percha in thin slices, 1 oz. J carbonate of lead in fine powder, 1 oz. ; chloroform, 8 ti. oz. Add the gutta percha to 6 fl. oz. of chloroform in a stoppered bottle, and shake them frequently till solution has been effected. Then add the carbonate of lead previously mixed with the remainder of the chloroform, and having several times shaken the whole together set the mixture aside, and let it remain at rest until the soluble matter has subsided. Lastly, decant the clear liquid and keep in a well-stoppered bottle. Liquor, Libavius'a. Bichloride of tin. Liquor of Mat'ico. Syn. Conoenteated infusion op , MATICO ; LiQUOE MATICONIS, INPUSUM MATICONIS CONCENTEAIUM, L. Frep. From matico leaves, 1 lb.; rectified spirit, i pint; distilled water, 32 fl. oz.j digest 10 davs, express, and filter. 1 fl. dr. added to 7 fl. dr. of water is equal to 1 fl. oz. of the common infusion. Liquor of Myrrh. Si/n. Solution of mteeh ; Liquoe MYEEHiE, Loco liquaminis myb- EHiE, L. JPrep. (Ph. Bor.) Extract of myrrh (Ph. Bor.), 1 oz. ; distilled water, 5 fl. oz. ; mix thoroughly, decant, and strain. It should be of a brownish-yellow colour, and turbid, — Dose, i to 1 fl. dr. Liquor of O'pium. Sgn. Liquoe opii, L. o. concenieatus, L. opiatus, L. See Black DEOP.' 1. (Messrs Smith.) Opium, 4 oz., is made into an extract, and ' denarcotised ' by ether; it is then dissolved in alcohol, filtered, evapo- rated nearly to dryness, and redissolved in water q. s. to furnish 12 oz. of solution ; to this is added, of rectified spirit, 2f oz., with water q. s. to make the whole up to 16 oz. — Dote, 3 to 12 drops. 2. (Acetic; LiQUOE OPll ACETICUS, L.) See Laudanum (Houlton's). 3. (Citric; Liquoe opii citeicus, L.) — a. Powdered opium, IJ oz. ; lemon juice, li pint; evaporate to one half, cool, add of rectified spirit, 5 fl. oz., and the next day decant or filter; same strength as * laudanum.* b. (Liquoe MOEPHiiE citbatis — ^Dr Por- ter.) Opium, 4 oz. ; citric acid, 2 oz. ; tritu- rate, and add of boiling water, 15 fl. oz. ; digest with agitation for 24 hours, and filter. This last has above three times the strength of ' LAUDANUM.' It is sadly misnamed. 4. (Hydrochloric; Solution of Mubiate op Opium ; Liquoe opii hydbochloeicus, L. — Dr Nichol.) Powdered opium, li oz. ; dis- tilled water, 1 pint ; hydrochloric acid, li fl. oz. ; digest a fortnight, and strain with ex- pression. Same strength as 'LAUDANUM.' Ac- cording to Dr Nichol, this is preferable to every other preparation of opium. 5. (Sedative; Battlet's Sedative solu- tion op Opium ; Liquoe opii sedativub, L. — a. Hard aqueous extract of opium (bruised), 3 oz., is boiled in water, li pint, until dis- solved; to the solution, when cold, rectitied spirit, 6 oz. is added, together with water, q. s. to make the whole measure exactly 1 quart; the liquor is, lastly, filtered. b. Prom hard extract oF opium, 22 oz. ; boiling water, 13 pints ; rectified spirit, 3 pints ; as the last. c. From extract of opium — Ph. L., 4} oz.; water, 1 quart; boil till reduced to 34 fl. oz.; cool, fllter, and add of rectified spirit, 5 fl. oz., and water, q. b. to make up exactly 1 quart. Obs. The first two forraulte, which vary only in their quantities, are identical with that em- ployed by Mr Battley. As hard extract of opium is not always at hand, we have intro- duced a formula in which the ordinary extract is ordered. It gives a precisely similar pro- duet to the others, provided the cold aqueous decoction is filtered before adding the spirit. Battley's liquoe opii sedativus is an excel- lent preparation, less exciting than opium or laudanum.— Dose, 10 to 30 drops. Dr Chris- tison states that 20 drops of Battley's solution are equal to 30 drops of the common tincture. ' Under Deops, p. 691. LIQUORICE 991 Llqnor, Pancreatic (Van den Corput). Syn. LiQl'OB I'anohkatini. Pancreatiii and ear- biiiiateof |iolash, of each 10 gr. ; balm water, 2} tl. oz. J ayrup of orange peel, 5 dr. — Doie, i H. oz. to 1 H. oz. Liquor of Fepiin. (Mr Sqaire.) Si/n. Li- (jnott PKP8INI. Prep. 1 drachm of Bou- dault's peiisin in 1 oz. of distilled water. Salt must be added if it is to be preserved. — Dose. A teaxpoonf 111. Liquor of Khn'barb. Sj/n. LiQUOB bhei, Inpuscm hhei conoenthatum, L. Prep. 1. Hhubarb (well bruised), 6} oz. ; water, q. n. ; rectified spirit, i pint ; proceed as for INFDSION OF OALUMBA (conc.) ; to produce a quart. 8 times the usual strength. 2. See iNPDBloir 07 RnVBABB (Concen- trated). 3. See Extract op Rhitbabb (Fluid). Llqnor of Sarsaparil'Ia. Si/n. Fluid ex- tract OP 8AKBAPABILLA ; LlQUOR 8AKZ£, ES- SENTIA 8AB8APABILL.B, L. Prep. Either the simple or the compouud liquor of sarsaparilla may be made from the corresponding decoc- tion, or, preferably, the infusion prepared with water at 125" Fahr., by carefully evaporating it until Bufficiently concentrated, and then straining it through flannel, and adding a little spirit. Jamaica sarsaparilla should be alone employed, as the other varieties, espe- cially the Honduras, not only possess less medicinal virtue, and yield less extract, but are very liable to ferment and get mouldy, unless an undue proportion of spirit is added to them. See Extract op Sabsapabilla (Flnid). Liquor of Sen'na. Si/n. Liqttor SENNiG, L. Both the PLUID extbaot and the concen- trated INPU8I0N OP 8ElfNA are called by this name, but more generally the former. The following are additional formulse : — 1. (Duncan.) Senna, 15 lbs. ; boiling water, B galls, i proceed by the method of displace- ment, evaporate the product to 10 lbs., add of molasses, 6 lbs. (previously concentrated over a water bath until it begins to congeal on cool- ing), dissolve, and further add of rectified spirit, li pint, together with water q. s. to make the whole measure exactly 12 pints. Every fl. oz. represents 1 oz. of senna. 2. (Ur Twoedy.) As the last, but using tincture of ginger (prepared with rectified spirit), 1^ pint, instead of the spirit there ordered. Liquor of Soap. Si/n. Liquor baponis, L. See Tincture. Liquor, Styp'tic. Syn. Liquob bttfticus, L. Prep, (f h. SlevicoHolsat. 1831.) Alum and sulphate of copper, of each 1^ oz. : sul- phuric acid, 1 oz. ; water, 1 lb. ; dissolve, and tilter. Liquor of Tarax'acnm. Si/n. Fluid ex- TltACTOP DANTlKLION; EXTBACTUM TAEAXACI PLUIDUM, LiQCOK TABAXACI, L. Prep. 1. Dandelion roots (dricdl, 28 lb<., are rinsed in clean O.U1 water to remove dirt, and then sliced small, and macerated in enough cold water to cover them for 24 hours j the liquid is next pressed out, and after the fecula has subsided the clear portion is decanted, and heated to 180° or 190f Fahr., to coagulate the albumen; the liquid is then filtered while hot and evaporated by steam, or preferably by a current of warm air, until it is reduced to 22^ lbs. ; to this rectified spirit, 6 lbs., is added, and after thorough agitation the vessel is set aside for a week or a fortnight, after which the clear portion is gently poured from the sediment and preserved in well-closed bottles in a cool place. A very fine article. It represents an equal weight of the root. 2. The expressed j nice of dandelion is heated to near the boiling point, strained, and evapo- rated, as the last, to a proper consistence ; ith or ^tli of rectified spirit is then added, and the liquid is otherwise treated as before. Very odorous and pale coloure<^ . 3. Dried root (coarsely powered), 1 lb. ; water, li pint; rectified spirit, i pint; digest a week, express the liquor, pass it through a hair sieve into a bottle, and in 10 days decant the clear portion. 4. (Ph. Bar.) Extract of dandelion, 3 parts; water, 1 part (or q. s.); triturated together. 5. (W.Procter.) Fresh root, 2 lbs., is sliced and reduced to a pulp, and macerated with ^th of its bulk of rectified spirit for 24 hours; it is then subjected to strong pressure, the marc is treated with water containing a little spirit, 1 pint, and the liquid is again expressed ; the mixed product is evaporated to 12 fi. oz., and when cold, rectified spirit, 4 fl. oz. is added, and the whole filtered. Oba. Liquor of taraxacum has a very large sale. The dose is 1 to 2 fi. dr. tjec Ex- tbaot. Liquor of Valer'ian. See Extbact op Valerian (Fluid). Liquor of Vanil'Uu Si/n. Fluid extbact OP VANILLA; Liquob VANiLLiE, Extkactum T. PLUIDUM, L. Prep. 1. Vanilla ( sliced ), 1 lb.; rectified spirit. 3 pints; prepare a tinc- ture either by displacement or maceration, and reduce it, by distilbition at the lowest possible temperature, to IJ lb. ; put this into a strong bottle whilst hot, add of white sugar (tandy (in powder), i lb., cork down, and agi- tate the whole uufSl it is nearly cold. Very fine. Used chiefly for its odour and flavour. It represents half its weight of vanilla. 2. (W. Procter.) Vanilla (cut into thin transverse slices), 1 oz. ; sugar, 3 oz. ; tritu- rate until reduced to fine powder, put it into a strong pint bottle, along with syrup, i pint : water, 2 oz. ; tie down the cork, and set the bottle for half an hour iq boiling water; cool, straiu, and treat the residue in a like manner with a mixture of water, 6 fl. oz., and rectified spirit, 1 fl. oz. ; lastly, mix the two products. Greatly inferior to the last. LIQ'UO£IC£. Si/n. Stick liquobicb; Li- 992 LISBON DIET DKINK QUOEITIA, GLTCTEBHIZiE EADIX (B. P.), GlT- CTBEHIza) badix.Gltctebhiza (Ph. L. & D.), G. »LABEA (Ph. E), L. " The root or under- ground stem of the Glt/cyrrhiza glabra, fresh and dried, cultivated in Britain." " The recent and the dried root of Chlyet/rrhiza glabra," or common liquorice. "The f'rpsh root is to be kept buried in dried sand for nse." (Ph. L.) It has a sweetish taste, and is slightly aperient, expec- torant, and diuretic. It is a popular demul- cent and pectoral. Its extract and solution are much used as a domestie remedy for cougb. As a masticatory it allays thirst and irritation. Composition of the fresh root of liquorice : Glycjrrbizin . 8-60 Gum 26-60 Matter soluble in alcohol. chieHy resin 0-75 Albumen . , 0-97 Starcli . • 22-91 Woody fibre • 13-36 Moisture 26-81 Ash, 307 per cent — 100-00 (Hassall.) Eoussin asserts that the sweetness of liquor- ice root is not due to glyeyrrhizin, as has been hitherto assumed, but to an ammoniacal com- pound of that substance. Glyeyrrhizin, when purified four successive times by dissolving it in alcohol, and precipitating the foreign matter accompanying it by ether, is a yellowish sub- stance, insoluble in cold water, and almost tasteless. Treated with dilute solution of pot- ash or soda, it rapidly develops a sweet taste. In liquorice root, however, it is not contained in combination with either of these two alka- lies, but appears to exist as an ammoniacal compound, for solutions of potash and soda liberate ammonia, both from the root and the extract. In its compounds with the alkalies glyeyrrhizin plays the part of an aeid, as it forms true salts capable of undergoing decom- position with most of the metallic salts, and also with the salts of the organic alkaloids. With ammonia it forms two compounds, a basic salt, which yields a deep yellow solution, and another containing less ammonia, the solution of which has an amber colour. The former is produced by dissolving glyeyrrhizin in water with an excess of ammonia. Upon evaporating the resulting deep yellow solution to dryness it leaves a yellowish, scaly, shining, brittle, non-hygroscopic residue, which constitutes the second ammoniacal compound. This is readily soluble in cold water, to which it imparts a pale yellow colour and a very sweet taste. The solution turns deep yellow on the addition of a few drops of solution of ammonia, owing to the formation of the basic componnd. The pale yellow solution possesses, in a, marked degree, the taste of liquorice root, which, in- deed, owes its sweetness to this glycyrrhizate of ammonia, or ammoniacal glyeyrrhizin, as the author prefers to call it. One gram of this compound imparts the sweet taste of the root to two litres of water. The author gives the following process for the preparation of the ammoniacal glyeyr- rhizin in the pare state : The carefully-selected roots, freed from all portions presenting a dark fracture, are scraped, and then well pounded, so as to reduce them to a kind of stringy tow. This substance is macerated in cold distilled water for some hours, pressed, and treated a second time in the same manner. The two liquors are mixed aud allowed to stand for some time to deposit the starch. The supernatant liquor is then boiled and fil- tered, to separate the coagulated albumen. After cooling, sulphuric acid diluted with its weight of water is added gradually, with brisk stirring, until a precipitate is no longer formed. The precipitate, at first gelatinous and flocculent, after standing some time, forms a compact semi-solid mass at the bottom of the vessel. The supernatant liquor is rejected, and after roughly washing the precipitate several times with pure water it is finally kneaded repeatedly in distilled water until all trace of acidity has disappeared. The mass is then well drained and agitated in a flask with three times its weight of 90° alcohol until dis- solved, when a similar quantity of 96° to 98° alcohol is added to the syrupy liquid so pro- duced. A little pectic aeid is thua precipi- tated, which is removed by filtration. Ether is then added to the alcoholic liquor as long as a precipitate is formed. After standing twenty-four or even forty-eight hours a black- ish pitchy substance is deposited, which ad- heres to the gliiss, and allows of the dear liquor being decanted. To this clear liquor is added, in small quantities at a time, alcohol of 90° charged with gaseous ammonia, which determines the formation of a yellow, rather heavy, flocculent precipitate of glycyrrhizate of ammonia. This precipitate is washed ra- pidly on a fine cloth with a mixture of equal parts of alcohol and ether, pressed and dried in a current of warm air, or over sulphuric acid. The author suggests the addition of ammo- niacal glyeyrrhizin to pill masses, powders, or mixtures, and states that its power of masking the taste of nauseous medicines is equal to 100 times its weight of sugar. Sulphate of qui- nine, sulphate of magnesia, iodide of potas- sium, and ipecacuanha, lose much of their taste by such an addition. A dose of cod-liver oil or syrup of iodide of iron is rendered more palatable by being pre- ceded by a small dose of the solid ammoniacal glycerin.! Its extract is the common MQtio- EicE, Spanish liquoeice, or Spanish jdice, of the shops. See Exteact, &c. IISBON DIET DRINK. 1. (Foy.) Prep. Guaiacum wood, rasped, 1 oz. ; sarsaparilla, bruised, 3 oz. j mezereon, sliced, i oz. ; crude ' • Journal de Fliarmacie et de Cliimie,' xii 6—11. LIST— LITHIUM 993 antimony (in a rap). 2 oz. ; water, 12 pints, lioil down to 8 pints, and add — red San- ders, rasped, wliite sandal, rasped, of eaci) 8 oz. ; rosewood, rasped sassafras bark, sliicd, of each 1 oz. j liquorice root, sliucd, i oz. Infuse for four hours, strain, and add syrup according to taste. — J)o»e, 1 to 2 pints a day. 2. (Pearson.) Sarsaparilli, bruised, 4 oz.; dried walnut peel, 4 oz. ; guaiacum, rasped, 1} oz. ; crude antimony (in a rag), i oz. ; water, 4 pints. Boil down to 3 pints. LIST, The border or selvage torn off a piece of cluth. It is used by the French polishers and law stationers to form their rubbers, and for numerous other purposes. LITH'ARGG. Syn. Semi-titeified oxide OF lEAD; Plumbi oxtdum (Ph. L.), Plumbi OXTDm SEMIVITBEUM (Ph. D.), LlTHAB&T- BDM (Ph. E.), L. The litharge of commerce is semi-vitrified protoxide of lead, obtained chiefly by scraping oft the drops that form on the surface uf melted lead exposed to a currentof air (dross of lead; plumbum ustum), and heating it to a full red, to melt out any undeoomposed metiil. The fused oxide, in cooling, forms a yellow or reddish semi-crystal- line mass, which readily separates into scales; these, when ground, constitute the ' powdered litharge' of the shops. Litharge is also pre- pared by exposing red lead to a heat suffi- ciently high to fuse it, and 'English litharge' is obtained as a secondary product, by liquefac- tion, from argentiferous lead ore, when it is often called ' silver stone.' Pur. " Entirely, or almost entirely, soluble in dilute nitric »cid. This solution is blucU- cru'd by sulphuretted hydrogen. Potassn throws down a white precipitate, which is re- disxolved by adding the same in excess. If sulpliatK of soda be added to 100 gr. of this oxide dissolved in nitric acid, 135 gr. of sul- phate of lead is precipitated." (Ph. L.) " 50 gr. dissolve entirely, and without effervescence, in Xi fl. oz. of pyroligneous acid, and the solu- tion precipitated by 53 gr. of phosphate of soda remains precipitable by more of the test." (Ph. E.) The solution in both acetic and nitric acid should be colourless. It is of great im- portance to the pharmaceutist to obtain pure litharge, as the slightest impurity will often colour and spoil his lead plaster (emp. plumbi), and solution of diacetate of lead (liq. piumbi DIACETATIS). Utei. Litharge is employed in pharmacy, to make plasters and several other preparation> of lead ; by painters as a ' drier ' for oils ; and for various othoi8onitig, &c., are not taken into tlie calcu- lation. In all cases in which lotions are in- tended for extremely susceptible parts, it is proper to dilute thein with an equal bulk of water. Wlien intended for eye-wat«rs (COL- lyria), they should be diluted with at least 8 to 4 times their bulk of water. See Embuo- CATION, Liniment, Ac. Lotion of Ac'etate of Ammo"ziia. Syn. LOTIO AMMONIJS ACBTATIS, L. Frep. 1. !>alutiou of acetate of ammonia, 1 part j water, 2 parts. 'i. (Hosp. F.) Solution of acetate of am- monia, rectified spirit, and water, eqi\al parts. Discutient and refrigerant. In oriiiuary in- flammaiions. Lotion of Ac'etate of Lead. Syn. Lotio pirMBi AOBTATis, L. Prep. 1. (Collier.) Acetate of lead, 1 dr. ; distilled water, 8 H. oz. Sometimes a little vinegar is added. In ex- coriations, burns, sprains, contusions, &c. See SOLnilON OP DiAOETATE OF LEAD. 2. Acetate of lead, 2 gr. ; distilled water, 1 oz. (Ophthalmic Hospital.) Lotion of Ac'etate of MercuTy. Si/n. Lotio H;DliAU»TRl ACBTATIS, L. Prep. Acetate of mercury, 1 scruple ; distilled water, 1 pint. Mix. Lotion of Ac'etate of Zinc. Si/u. Lotio ziNci AOEi'ATis, L. Prep. 1. (Beral.) Acetate of zinc, li dr. J water, 1 pint. Astringent! siuiilar to lotion of sulphate of zinc. 2. Acetate of zinc, 1 to 2 gr. ; water, 1 oz. An astringent coUjrium in ophthalmia, and as injection in gonorrhoea after the acute stage has passed. Neither tincture nor wine ot opium gives a precipitate with this lotion. Lotion, Acetic. Si/n. Loiio aceti, L. Prep. 1. Vinegar, 1 part ; water, 2 or 3 parts. For bruises, contusions, &c., and as a general refrigerant application to sound parts. 2. Vinegar, 1 fl. oz. ; cold water, \ pint ; as a wash in chronic ophthalmia, &c. lotion. Acid. See Lotions of Acetic, Ni- TGlo, and Pbosphobic acid, &c. Lotion of Acon'itine. Syn. Lotio aconi- TIN^, L. Prep. (Turnbull.) Aconitine, 8 gr. ; rectitied spirit, 2 fl. oz. In neuralgia ; applied by means of a small piece of sponge mounted at the end of a stick. It must never be em- ployed when the skin is broken or abraded; and it would be wise, in most cases, to dilute it with double its volume of proof spirit. Lotion, Al'kaline. Syn. Lotio alk^lina, L. POTASSiB OABBONATIB, L. Prep. (P. Cod.) From salt of tartar, 1 oz. ; water, 1 pint. Stimulant and detergent. Diluted with an equal bulk of water, it forms an excellent cos- metic wash to remove scurf from the hair. Sometimes it is made with almond milk instead of water. Lotion, Almond, Alkaline. (Dr A. T. Thomson). Syn. Solution of potash, 4 fl. oz. ; eumlsion of bitter almonds, 54 fl. oz. To remove the scurf in porrigo furf urans, applied twice a day diluted with warm water. Lotion of Al'nm. Syn. Lotio Aurimns, L. Prep. From alum, li dr. ; distilled or rose water, 1 pint. Astringent. For sore gums, nipples, excoriations, &c. Lotion, Ammonio-Camphorated. Syn. Aqua sedativa, L. Eau bedativb de baspail; Eau, ov lotion ammoniacals oaufub^b. No. 1. Liquor ammonite ('923), 6 parts; cam- phorated spirit, 1 part ; salt, 6 parts ; water, 10 parts. No. 2 contains 8 parts, and No. 3 10 parts of ammonia. Lotion, Ammoui'acal. Syn. Lotio ammo- nia, L. AMMONlACALis, L. Prep. 1. Liquor of ammonia, 3 fl. dr.; cold water, 5 A. oz. As a stimulant to indolent ulcers, and in certain skin diseases. 2. (Swediaur.) Liquor of ammonia, spirit of thyme, and spirit of camphor, equal parts. In headaches; applied to the forehead and temples, and in otiier cases, as a counter- irritant. In most cases it should be used di- luted. 3. (Opiated— Dr Kirkland.) Sal volatile, .3J fl. oz. ; tincture of opium, \ fl. oz. ; water, 4 fl. oz. Anodyne, stimulant, and rt^solvent. Lotion, Antiphlogis'tic. Syn. Lotio anti- PHLOOISTICA, L. Prep. 1. (Copland.) Solu- tion of diacetate of lead, 3 fl. dr. ; solution uf acetate of ammonia, 2 H. oz. ; distilled water, 1 pint. KL^frigerant, sedative, and repellaiit. Used to allay iuHammatiun, &e. 2. (A. T. Thomson.) Opium, 2 dr., dis- tilled vinegar, i pint. Anodyne and refrige- rant; in swelled joints, &c. Lotion of Ar'nica. Syn. LoTio abnic^, L. Prep. 1. Tincture of arnica, 1 11. dr. ; rose water, 2} fl. oz. In contusions, bruises, extra- vasations, &c. 2. (Niemann.) Arnica flowers, \ oz. j hot vinogar, 3 fl. oz. ; boiling water, 5 fl. oz., in- fuse until cold, and strain, in acute hydro- cephalus; or with water, q. s. to measure a pint, as a common lotion. Lotion, Arsenical. Syn. Lotio absknioai.I3, L. acidi aeskniosi, L. Prep. 1. Arse- ninus acid, 5 gr. ; water, 1 pint. In psoriasis, ic. 2. (Compound — M. le Febre.) Araenious acid, 8 gr. ; boiling water, 16 fl. oz. ; dissolve, and add of extract of hemlock, 1 oz. ; solution of diacetate of lead, 3 fl. oz. ; tincture of opium, 1 fl. dr. Every morning, in cancer. Lotion, Astrin'gent. Syn. Lotio asibin- OENS, L. See Lotions of Alum, Sulphate op Zino, &c. Lotion, Barlow's. Prep. From sulpburet of potassium (in powder), 3 dr.; soap (sliced). 1000 LOTION li dr. ; lime water, 7J fl. oz. ; proof spirit, 2 &. oz. In itch, ringworm, &c. lotion, Bateman's. Prep. Prom bichloride of mercury, 2 gr. ; compound spirit of liiveu- der, 1 fl. oz. ; dissolve, aud add of distilled water, 4 fl. oz. In obstinate cutaneous erup- tions, more especially those of a papular character. lotion of Belladon'na. St/a. LoTio eelia- DONN^, L. Prep. (Graefe.) Extract of bel- ladonnii, i dr. ; dilute solution of diacetate of lead, i pint. Applied to tumours and glan- dular enlargements. lotion of Benzoin. Lotio benzoini. Tinc- ture of benzoin, 1 ; rose water, 40. A nice lotion to protect the face from the heat of the sun. Lotion of Biclilo"rlde of Mercury. St/n. Lotio HYDBABaTEi bichloeidi, L. h. chlo- BIDI COEBOSIVI, L. Prep. 1. Corrosive sub- limate, 5 to 10 gr. ; distilled water, 1 pint. The addition of 5 or 6 gr. of hydrochlorate of ammonia, or as many drops of hydrochloric acid, increases the solvent action of the water, and renders the preparation less liable to change. Some persons dissolve the sublimate in 1 or 2 fl. dr. of rectified spirit before adding it to the water; but this is unnecessary. In ob- stinate eruptions, glandular swelling, obstinate sores, &c. ; also as an injection. 2. (Good.) Corrosive sublimate, 1 dr. ; sal ammoniac, 2 dr.; nitre, 4 dr.; water, 6 fl. oz. ; dissolve. In itch, &c. For use, it should be diluted with about 3 times its bulk of water. 3. (Lotio htdeaegtei amtctoalina — St B. Hosp.) Blanched bitter almonds, 1 oz. ; water, 1 pint j make an emulsion, and add o( bichloride of mercury (dissolved in a little rectified spirit), 10 gr. This resembles Gow- land's lotion, and may be used for it. lotion of Bismuth. Lotio Bismuthi. Ni- trate of bismuth, 6 gr. ; corrosive sublimate, i gr. ; spirits of camphor, IJ minim ; water, 1 oz. A soothing lotion in chronic skin affec- tions. lotion, Black. See Lotion, Mbecueial. lotion of Borax. Si/n. Lotio bobacis, L. BOEACICA, L. Prep, 1. (Dr Abercrombie.) Borax, 2i dr. ; distilled vinegar, i pint. In ringworm. 2. (Copland.) Borax (in powder), 1 dr. ; rose water and orange-flower water, of each 3 fl. oz. ; dis.-olve. A fragrant and efiective application to sore gums, sore nipples, exco- riations, &c. 3. (Ur Johnson.) Borax, 2 dr.; precipi- tated chalk, 1 oz. ; rose water and rectified spirit, of Ciich 3 oz. For sore nipples. 4. (Dr Meigs.) Borax, i oz. ; sulphate of morphia, 6 gr. ; rose water, 8 fl. oz. To allay itching and irritation, especially pruritus vulvae. 5. Borax, 1; rose water, 24. Cosmetic. Lotion, Bro'mine. S^n. Lotio beominii. L. Prep. (Dr Glover.) Bromine, 1 dr.; water, 1 pint. As an application to scrofulous ulcers. Lotion for Burns. See Linimekt. Lotion, Camphora'ted. See Lotion, Eta-; POEATINO-. Lotion of Cap'sicnm. St/n. Lotio oapsici, L. Prep. (Griffith.) Tinctures of capsicum and camphor, of each 4 fl. oz. ; liquor of am- monia, 2 fl. oz. A powerful rubefacient and counter-irritHot. Lotion of Carbolic Acid. (Mr Lister.) Si/n. Lotio acidi caebolioi. Prep. 1 part of acid in 20 of water is used to promote the healing of wounds, abscesses, ulcers and burns. A weaker solution of 1 in 40 is in comujon use in the London hospitals. 5 drops to 1 fl. oz. of glycerin forms a good application to eruptions of the skin. Lotion of Car'bonate of So'da. St/ii. Lotio SODJE CAEBONATis, L. Prep, From carbonate of soda, i oz. ; water, 1 pint. To allay itchiug and irritation. See Lotion, Alzaline. Lotion of Cher'iy Laurel.. St/n. Loxio LAUEO-CEBASi, L. Prep. 1. Cherry-laurel water (distilled), li fl. oz. ; di.'^tilled water, J pint. Anodyne; useful to allay irritation, &,c. Some persons with delicate skin employ it as a wash after shaving. 2. Cherry-laurel water (distilled), 4 oz. ; rectified spirit and ether, of each 1 fl. oz.; extract of belladonna, 2 dr. ; agitate well to- gether in the cold. An excellent application in neuralgia, painful tumours, &c. Lotion for Chilblains. See Chilblain, Li- niment, &c. Lotion of CMo"rate of Soda. Si/n. Loiio soxiM chloeatis, L. Prep. (Darling.) Chlo- rate of soda, 5 dr. ; water, J pint. In pru- ritus, &c. Lotion of Chlo'^ride of Ammoninm. Lotio AMMONil ohloeidi. Chloride of ammonium, 1 oz. ; rectified spirit, 1 oz. ; water, 10 oz. To this vinegar is sometimes added. Used as a ilressing for bruises. See also Lotion op Htdeochloeate op Ammonia. Lotion of ChVride of Lead. St/n. Lotio plttmui chloeidi, L. Prep. (Tnson.) Chlo- ride of lead, 1 dr. ; hot distilled water, 1 pint; dissolve. In cancerous ulcerations, painful neuralgic tumours, &c. Lotion of Chloride of Tin. St/n. Lotio STANNI chloeidi, L. Prep. (Nanche.) Chlo- ride of tin, 1 gr.; distilled water, 2 to 3 fl. oz. In cancerous ulcerations. Lotion of Chloride of Zinc. St/n. Lotio ziNCi chloeidi, L. Prep. 1. Chloride of zinc, 10 gr. (or solutiou, i fl. dr.) ; water, 1 pint. Asa disinfeitaut and preventive lotion. 2. (Voght.) Chloride of zinc, 8 gr. ; extract of aloes, 40 gr. ; distilled water, 4 fl. oz. In atonic and foul ulcers. Lotion, Chlorina'ted St/n. Lotio chlo- EINATA, L. Prep. 1. (Lotio calcis chlo- SINAT.E.) — a. From chloride of lime, 3 dr.j LOTION 1001 water, 1 pint ; agitate togrother for some time, and strnin through iuuaUd. b. (Uerheimi.) Chloride of lime, 1 oz. ; water, 1 quart ; triturate and filter. 2. (LoTio boDjB chlobinat«.) From chlo- ride of Boda, aa the lust. They are both ex- celleut waahea for foul ulcera, the itch, &c. ; and, when diluted for the teeth, to sweetftn tlie breath, remove the amell of tobacco smoke, to prevent infection, and for various purposes. When intended for application to very tender or abraded surfaces, they must be largely diluted with water. Lotion of Chlo"rofomi. 8gn. Lotio ohlo- BOFOBMi, L. Prep. Chloroform (pure), li fl. oz. ; rectilied spirit and cold distilled water, of each i pint. Anodyne. A piece of oiled silk should be laid over the rag to prevent evaporation. The lotiou made with water, as comuionly prescribed, is inert. Lotion for Corni. See Cobk. Lotion of Crea'eote. 5y». Lotio cbeasoti, li. Prep. 1. Creasote, 2 fl. dr. ; liquor of potassa, 3 fl. dr. ; water, \ pint. 2. Creasote, 8 fl. dr. ; vinegar and water, of each ^ pint. In bums, itch, phagedenic ulcerations, ringworm, chancre, &c. Lotion of Cy'anide of Fotassinm. Syn. Lotio potassi cyanidi, L. Prep. 1. (Caze- nave.) Cyanide of potnssium, 10 gr. ; emul- sion of bitter almonds, 6 fl. oz. In chronic eruption! and other cases attended with much itching or irritation. 2. (Foy.) Cyanide of potassium, 8 gr. ; dis- tilled water, 1 fl. oz. In neuralgia, acute rheumatism, &c. ; applied by means of com- presses of lineu. Both the above are poisonous if swallowi'd. Lotion of Delphin'ine. 8yn. Lotio dkl- PHlNlJi, Embrocatio d., L. Prep. (l)r Turiibuil.) Delphinine, 20 to60 gr. ; rectified spirit, 2 fl. 07,. Used us lotion of vbeatbia. Lotion of Diac'etate of Lead. Syn. Goc- LABD's LOTION; LOTIO PIUMBI DIACETATIB, L. The dilute liquor of diacetato of lead (liq. plumbi diacetatis dilutus — Ph. L.). ISi'i' SOLCTION. Also Solution of subucetatc of lead (B. P.), 3 minims, with 7 miuims to 1 oz. water. Lotion, Evap'orating. Sy». Lotto etapo- EANS, L. VAP0BAN3, L. BPIIJITUS DILUTI, L. Prep. 1. (Copland.) Sulphuric ether, rectified spirit, and solution of acetate uf ammonia, of each 1} fl. oz. ; rose water, Z\ fl. oz. 2. (Guy's Hosp.) Rectified spirit, 1 part; water, 6 parts. 8. (Erasnms Wilson.) Rectified spirit, 1 part ; water, 4 to 6 parts. 4. (Camphorated — Ware.) Camphor, i dr. ; elder flowers, \ oz. ; rectified spirit, 4 oz. ; digest 24 hours, and strain. Obi. The above are soothing and refrigerant, if allowed to evaporate by free exposure ; stimulant, if the evaporation is prevented by covering the part with the hand, or a piece of oiled silk. They ore useful applicatious in nervous headaches, restlessness, itching and irritability of the skin, Ac. "A little rose water added to the simple water makes an agreeable addition, and sometimes camphor water (julep), or a little Goulard's extract, may be deemed ndvautageous, when a greater degree of calming effect is required." (Eras. Wdson.) Eau de Cologne, diluted with an equal quantity of water, is often used as an evaporating lotion. Lotion of Gall-nnts. Syn. Lotio galls, L. Prep. From gall-nuts (bruised), ) oz. ; boiling water, 1 pint ; infuse until cold, and strain. Astringent. An excellent application to sore nipples, or to strengthen them before suck- ling ; spirit of wine, 3 fl. oz., may be advan- tageously added to the cold infusion, and a like portion of water omitted. Sec Decoction. Lotion of Qlyc'erin. Syn. Lotio oly- ciutiNi, L. OLTCBBIHI.E, L. Prep. 1. Gly- cerin, loz.; water, 1 pint. To allay ilchint;, and remove dryness, iSic., in various skin dis- eases; also in cliaps of the nipples, lips, ami hands. For the latter purpose the addition of 2 to 3 dr. of borax is recommended by some writers. 2. Glycerin, 1 oz. ; thick mucilage, 2 oz. ; lime water, 7 oz. In burns, scalds, chaps, excoriations, &c. 3. (Startin.) Glycerin, 1 oz.; extract of belladonna, 1 dr.; soap linimeut; 3 oz. ; tri- turate together. In bruises, sprains, and swelled joints; gouty, neuralgic, and rheu- matic pains, &c. 4. (Startin.) Trisnitrate of bismuth, \ dr. ; tincture of foxglove and dilute nitric acid, of each 1 fl. dr. ; glycerin, 4 dr. ; rose water, 8i fl. oz. To allay the itching in prurigo, and some other skin diseases. Obs. Varions lotions may be prepared by disi'Olving active medicinal substances in gly- cerin. Lotion, Goulard's. See Lotion of Diacb- TATE of Lead. Lotion, Oont. Syn. Lotio antabthbitica L. Prep. 1. Glycerin, 1 oz. ; extract of belladonna, 3 dr. ; reratrine, 10 gr., dissolved in rectified spirit, 2 fl. oz. ; mix, and further add, of water, 17 fl. oz. It is poisonous if swallowed. 2. (' Scudamobe's g. L.') From camphor mixture, 9 fl. oz. ; rectified spirit, 3 fl. oz. The above are applied on rags or compresses, or are poured on the surface of poultices. Lotion, Gowland's. This celebrated no>trnm is prepared as follows : — I'ake of Jordan al- monds, 1 oz. ; bitter ahnonds, \ oz. ; blanch them, and make an emulsion in soft water, 1 pint; to this add of bichloride of mercury, 15 gr. ; previously dissolved in rectified spirit, 2 fl. dr., together with enough water to make the whole measure 1 pint, and put it into bottles. Obe. This preparation is chiefly used as a cosmetic to improve the complexion ; and also as a wash for obstinate eruptions and minor 1002 LOTION glandular swellings and indurations. As a beautifier of the complexion, it is employed by simply wetting the skin with it, either by means of the corner of a napkin or the fingers dipped into it, after which it is gently wiped o£E with a dry cloth Dr Paris represents this nostrum to contain i dr. of corrosive subli- mate in every pint, which is not the case Lotion, Granville's Conuter-irritant. See LiNiMEifT OF Ammonia (Compound). lotion, Hemlock. Sj/n. LoTii coNli, L. Prep. (Mid. Hosp.) Extract of hemlock, 3 dr.; opium, 1 dr.; boiling water, 1 pint; digest until cold, and strain. Anodyne and resolvent ; in glandular enlargements, painful ulcers, cancer, indarations, rheumatism, neu- ralgia, &c. Lotion, Hooping-cougli. (Struve's.) LoTio ANTIPBHTUSSIOA, L. Prep. (Paris.) Potassio- tartrate of antimony, 1 dr.; tincture of can- tharides, 1 oz. ; water, 2 oz. This is a powerful counter-irritant, and should be used with cau- tion ; as it is apt to induce a troublesome erup- tion on the parts to which it is frequently applied. Lotion of HydrocMo"rate of Ammonia. St/n. LOTIO AMM0NI2E HTDROOHLOEATIS, L. Prep. 1. (Weakeb.) From sal ammoniac, 1 to 4 dr. i water, 1 pint. As a wash in itch, ulcers, tender feet, swelled joints, &c. 2. (Stkongek.) From sal ammoniac, 1 to 2 oz. ; water, 1 pint. In contusions, chronic tumours, extravasations, chilblains, &c., when the skin is not broken. Both are stimulant and resolvent or discutient. Vinegar is often substituted for the whole or part of the water, and sometimes a fifth or sixth part of rectified spirit is adfled. See also Lotion oe Chlobide OP Ammonium. Lotion, HydrociVric. Si/n. LoTio acidi HTDKOCHLOitioI, h. Prep. 1. Hydrochloric acid, 1 fl. oz. ; water, 1 pint. In lepra, and several other skin diseases. 2. (Foy.) Hydrochloric acid, 1 part; water, 16 parts. In chilblains, when the skin is un- broken. Lotion, Hydrocyan'io. Syn. Lotio htdeo- CYANICI, L. AOIDI HYDEOOYANICl, L. Prep. 1. (Magendie.) Medicinal hydrocyanic acid, 1 to 2 fl. dr. ; lettuce water, 1 pint. In he- patic afEections. 2. (Sneider.) Medicinal acid, IJ fl. dr.; rectified spirit and water, of each 6 H. oz. 3. (A. T. Thomson.) Medicinal acid and rectified spirit, of each 2 fl. dr. ; acetate of lead, 16 gr. ; distilled water, 7i fl. oz. In im- pL'tigO, &C. Ohs. Lotions of prussie acid are employed to allay pain and irritation in various chronic skin diseases, especially the scaly and itchy eruptions ; and in cancer, &c., with variable success. See Hydeooyanic aoid. Lotion of Hyposn'lphite of Soda. Syn. Lotio SOD.E HYPOSdLPHiTia, L. Prep. (Startin.) Hyposulphite of soda and alum, of each 1^ dr, ; eau de Cologne, J fl. oz. ; rose water, 7i fl. oz. ; in the advanced stages of acne. Lotion of I'odide of Ar'senic and Mer'cury. St/n. Lotio aesenioi et hydbaeoybi hy- DEIODATIS, L. Prep. Fiom Donovan's solu- tion, 1 part; water, 9 parts. In lepra, psoriasis, and other scaly skin diseases. See Solution. Lotion of Iodide of Fotas'sium. Syn, Loiio- POTASSil lODiDi, L. Prep. 1. From iodide of potassium, 1 to 2 dr. ; water, 1 pint. In the usual ca«es in which ioduretted preparations are employed. 2. (Dr O. Ward.) Iodide of potassium, I dr. ; water, J pint. In itch. (See below.) Lotion of Iodide of Zinc. Syn. Lotio zinci lODtDi, L. Prep. (Boss.) iodine, IJ dr.; zinc filings, 1 dr. ; water, 8 fl. oz. ; digest with heat until the liquid becomes coloured, then filter. In enlarged tonsils. Lotion of I'odine. Syn. Lotto iodikii, L. Prep. From iodine, 2 gr. ; rectified spirit, 1 fl. dr.; dissolve, well agitate the solution viith distilled water, 1 pint, and filter. An ex- cellent wash for scrofulous ulcers, and in chronic ophthalmia, cutaneous scrofula, and several chronic skin disease.s, particularly in highly sensitive habits. Lotion of Iodine Compound. Syn. Lotio lODi COMP., L. Prep. 1. Iodide of potassium, 80 gr. ; iodine, 60 gr. ; water, 1 oz. 2. (Cazenave.) Iodide of potassium and iodide of sulphur, of each 1 dr.; water, 1 pint. In itch ; either alone or diluted with an equal bulk of water. 3. (Dauvergne.) Iodine, 3 dr. ; iodide of potassium, 6 dr. ; water, 3 fl. oz. ; dissolve, and label the bottle No. 1. Sulphuret of potassium, 4 oz. ; water, 8 fl. oz. ; dissolve. For use, a tea- spoonful of No. 1, and a table-spoonful of No, 2, are to be added to about a pint of water. In itch, and several other skin diseases. 4. (Lugol.) Iodine, 1 to 2 gr. ; iodide of potassium, 3 to 6 gr. ; water, 1 pint. In scro- fulous ophthalmia, fistulas, &c. ; and as a wash in numerous skin diseases. 5. (Eighini.) Chloride of lime, 4 dr. ; water, 2\ fl. oz. ; triturate together, filter into a stoppered bottle, and add of tincture of iodine, 1 dr. With a pint of water it forms an effective application in itch. 6. (Soubeiran.) Iodide of potassium, 1 oz.; iodine, \ oz. ; water, 6 oz. ; dissolve. Used as iodine paint ; also as a caustic to touch the ^urfaces of scrofulous ulcers, and the eyelids in scrofulous ophthalmia. 7. Iodide of potassium, J dr. ; iodine, 16 gr. ; water, 1 pint. This is the common and best form of iodine lotion, but for certain purposes it is used much stronger. (See ahove^ Lotion of Iron with Coninm. Lotio feeei CUM CONIO. Sulphate of iron, 8 gr. ; extract of conium, 8 gr. ; water, 1 oz. Lotion, Itch. Syn. Lotio antipsoeioa, L. Prep. (Cazenave.) Sulphuret of potassium, 1 LOTION 1003 dr. ; ioft ioap, 2 dr. j water, 8 fl. oz. ; dissolve. An excellent remedy for the itch. It leaves little smell behind, and does not soil the linen. (See above.) Lotion, Kirkland'i. See LoTloir of Mtbbh. Lotion of Lemon Jnice. Sgn. LoTio aircci LIMONIB, L. Prep. From the freshly ex- pressed juice of lemon, diluted with 4 or 6 times its bulk of water. To render it more agreeable, rose water may be employed, or a few drops of eau . (Iverg.) Unlsam of Peru, 1 dr.; yolk of 1 egg; make an emulsion, nnd add of spirit of wild thyme, 3 fl. oz. For sore nipples ; to be followed, whilst still wet, by a 'dusting' with a powder composed of Peruvian bark, 1 dr. i gum Arabic, 2 dr. Lotion, MercTi"rial. Prep. 1. (Black wash. Black lotion. Mild phagedbnio l. ; Lotio nioba (b.f.), l. htdbaeoyei oinebka, l.h. niob*, l. h. ohlobidi odm calob, l. meb- oubialis n., Aqua phaoed.enipa, mitis, L.) a. (B. p.) From calomel, 3 gr. ; lime water, 1 oz. J well shaken together. i. (Mid. Hosp.) To the last add of thick mucilage, 1 fl. oz. e. (Guy's Hospital.) From calomel, 1 dr., lime water, 8 fl. oz. Obt, Black wash is a favourite application to all kinds of syphilitic and scrofulous sores. The bottle should be well shaken before the lotion is applied. 2. Yellow wash, Y. lotion. Phagedenic L. ; Lotio flava, L. PHAOBDiUNioA, Aqua p., Lotio hyobaroybi flava, L. h. bichlokidi CUM calce, L.) — a. (B. P.) Corrosive subli- mate, 18 gr. ; liine water, 10 oz. ; well shaken togethir. b. (8c B Hosp.) Corrosive sublimate, 20 Br.;llme water, 6 fl. oz. Used as the last, but it is stronger and more active, from con- taining H little undecomposed bichloride. Lotion of Myrrh. St/n. Kibeland's lotion ; Lotio uybbhji, L. Prep. l.(D'r Kirkland. Tincture ol' myrrh and lime water, equal parts. In scorbutic ulcers and gums. 2. (Compnaud; Lotio mybbh^ compo- sita, L. — Ph. Chirur.) Honey of roses and tincture of myrrh, of each 2 fl. dr. ; lime- w»ter, 2| fl. oz. As No. 1 ; also used as a den- tifrite. Lotion of Ni'trate of Bis'mnth. Sgn. Lotio BiSMUiHi nitbatis, L. Prep. (Cutan. Ho.sp.) Subnitrace or trisnitrate of bismuth, i dr. ; corrosive sublimate, 12 gr.; spirit of camphor, i H. dr.; water, 1 pint. In itch, and some other ernptious. Lotion of Nitrate of Sil'ver. Si/n. Lotio aboenti nitbatis, L. Prep. 1. Nitrate of silver, 15 gr. ; nitric acid, 10 drops; distilled water, ^ piut. As a wash for indolent ulcers, sore legs, &c. 2. (Jackson.) Nitrate of silver, 10 gr. ; water, 1 fl. oz. For bed-sores ; applied, at first, twice or thrice a day. 3. (Schreider.) Nitrate of silver, i dr. ; nitric acid, 10 drops j water, li fl. oz. In chil- blains, soft corns, &c. Lotion of Nitrate of Silver (Strong). Lotio ABOENTI NITBATIS F0BTI8. Nitrate of silver, 60 gr. ; distilled water, 1 oz. Lotion of Nitrate of Sil'ver, Etherial. Loiio ABOENTI NITBATIS .STHEBEA. Nitrate of silver, 20 gr. ; distilled water, 1 dr. ; spirit of nitrous ether, 1 oz. Lotion of Ni'tre. Si/n. Lotio potass* NITBATIS, L. Prep. 1. Nitre, 3 dr.; vinegar, 1 pint ; water, f pint. 2. Nitre, 2 dr. ; sal Ammoniac, 1 dr. ; vine- gar and water, of each J pint. In sprains, contusions, extravasations, tender feet, chil- blains, &c. Diluted with an equal bulk of water, it is a popular application to ' black eyes.* Lotion of Ni'tric Acid. St/n. Lotio acidi, L. ACIDI NITBICI, L. Prep. 1. (C.)llicr.) Nitric acid, J fl. oz. ; water, 1 pint. In lepra, and other scaly skin diseases. 2. (Phcebus.) Nitric acid. 1 fl.dr.; lauda- num, li fl. dr. J rose water, i pint. For vene- real ulcers. Lo'tion of Nitromnriat'ic Acid. Si/n. Lo- tion op aqua beoia. /"re^. (Copland.) Ni- tromuriatic acid, IJdr. ; water, 1 pint. In gangrene and mortification. lotion of Nux Vom'ica. Si/n. Lotio nucis VOMIC.E, L. Prep. 1. Alcoholic extract of nux vomica, 10 gr.; rectified spirit and water, of each 2i fl. oz. In amaurosis. 2. (Radius.) Alcoholic exti-act of nux vomica, 8 gr. ; liquor of ammonia (stronger), i fl. oz. ; rectified spirit, 2 fl, oz. In paralysed limbs. Lotion of O'pinm. Si/n. Lotio opii, L. opi- ATA, L. Prep. 1. (Christisou.) Opium, 40 gr. ; water, i pint ; infuse, add to the filtered liquid a solution of sugar of lead, 40, in water, i pint, and filter. 2. (St B. Hosp.) Opium, IJ dr. ; boiling water, 1 pint; triturate and strain. Ano- dyne ; the first is also refrigerant and dis- cutient. Lotion of Ox'ide of Zinc. 5y». Lotio zinci OXYDI, L. Prep. 1. (Augustin.) Oxide of z nc, 1 dr.; elder-flower water. It fl. oz. In pustular erysipelas. 2. (Hosp. F.) Oxide of zinc, i dr.; muci- lage, 2 fl. dr. ; water, 6 fl. dr. As an astrin- gent and desiccaut, in scrofulous eruptions, excoriations, moist chaps, &c. Lotion, Fhageden'ic. See Mebcubial lo- tion (above). Lotion of Phos'phoric Acid. St/n. Lotio 1004 LOUSE ACiDi PHOSPHOEici, L. Frep. (Pereira.) Di- lute phosphoric acid (Ph. L.), 1 fl. oz. ; water, i pint. In caries and fistula. Lotion of Potas'sa. See LoTio POTASsa:, L. Prep, From liquor of potassa, 1 fl. oz. ; water, 1 pint. Detergent ; in scorbutic erup- tions, and foul ulcers, and to prevent infec- tion. Lotion of Potas'sio-tar'trate of An'timony. Syn. LoTio antimonialis, L. antimonii po- TASSIOTAETKATIS, L. RCBEFACIENS, L. Prep. 1; Tartar emetic, 1 dr. ; tincture of camphor, 2 fl. dr. ; water, 1 pint. As a local stimulant. Diluted with twice or thrice its weight of water, it is employed as a coUyrium in chronic ophthalmia, and in specks on the cornea. 2. (Sir Wm. Blizard.) Tartar emetic, 20 gr. ; boiling water, 1 fl. oz. Used to cleanse foul ulcers, to repress fungous growths and warts, and in ringworm, &c. 3. (Pereira.) Tartar emetic, 1 dr. ; hoiling water, li fl. oz. ; dissolve. Employed as a local irritant instead of the ointment. All the above are rubefacient and counter-irritant. See Antimony. Lotion of Quin'ine. Syn. Lotio QTTiNa;, Embeocatio (J., L. Prep. From disulphate of quinine, 1 dr. ; rectifled spirit, 5 fl. oz. Ap- plied over the spine in intermittents. Lotion, Sapona'ceoua. Syn. Lotio saponis, L. SAPONACEA (Ph. L. 1746), L. Prep. From liquor of carbonate of potassa, \ oz. ; olive oil, 4 oz. ; rose water, 12 oz. ; agitate together. Emollient ; chiefly as a cosmetic. Lotion, Saviard's. Prep. (Foy.) Caustic potassa, 1 dr. ; camphor, 20 gr. ; sugar, 1 oz. ; water, 1 pint. As a wash for indolent ulcers. Lotion, Struve's. See HoopiNGt-couGH lotion. Lotion of Snl'phate of Cop'per. Syn. Lotto CUPEI stTLPHATis, L. Prep. 1. Blue vitriol, 1 dr. ; camphor julep, 1 pint. For phagedenic ulcers, and in itch, &c. 2. (Dr Graves.) Sulphate of copper, 10 gr. ; water, 1 fl. oz. In chilblains, ringworm, &c. 3. (Lloyd.) Sulphate of copper, 1 oz. ; water, 1 pint. In itch j either alone or di- luted. Lotion of Sttl'phate of Iron. Syn. Loxio PEEKI sulphatis. Sulphate of iron, 2 gr. ; water, 1 oz. Lotion of Snl'phate of Zinc. Syn. Lotio ZINCI sulphatis. L Prep. 1. Sulphate of zinc, f dr. ; water, 1 pint. Astringent ; in some chronic skin diseases, as a wash for loose, flabby granulations, and for ulcers that dis- charge profusely, &e. 2. (Collier.) Sulphate of zinc, 2 dr. ; water, 1 pint. As a counter-irritant in pains of the joints, periosteum, old sprains, &c. Lotion of Sulphuret of Sodinm. (Dr Barlow.) Syn. Lotio sodii sulphuekti. Prep. Sulphide of sodium, 2 dr.; white soap, 2i dr. ; rectified spirit, 2 dr. ; lime water, 7 oz. For ringworm. Lotion of Tannin. (Mr Druitt.) Syn. Lotio tannini. Prep. Tannic acid, 5 gr. j distilled water, 1 oz. ; mix. On lint, covered with oil silk, to sore nipples. Lotion of Tar. iS^». Lotio picis liquids, L. Prep. (Saunders.) Quicklime, 6 oz. ; water, 2i pints ; slnke, add of tar, 4 oz., and boil to one half. This liquid may be advantageously employed in various chronic skin diseases, especially those affecting the heads of children. See Infusion op Tab. Lotion of Valer'ian. Syn. Lotio valeeian^, Embeocatio antihtsteeica, E. emmena- ooaA, L. Prep. From tincture of valerian and proof spirit, equal parts. In hysteria, suppressions, &c. Lotion of Vera'trine. St/n. LoTio teea- TEia), L. Prep. (Dr TurnbuU.) Veratrine, 20 to 60 gr. ; rectified spirit, 2 oz. In gout, rheumatism, &c. It is extremely poisonous, and must only be used where the skin is sound, and then with great caution. Lotion of Ver'digris. Syn. Lotio .eeuoinis, L. OUPEI citbatis, L. Prep. From verdigris, 3 dr. ; vinegar, i pint ; water, f pint. As a wash for indolent, scrofulous, and venereal ulcers. Lotion of Vin'egar. See Acetic lotion (above). Lotion, Yellow. See Meecueial lotion {above). LOUSE. Syn. Pediculus. There are several species of this offensive parasite infest- ing the bodies of man and domesticated animals. The three varieties of lice found on the human skin are : — (1) The Pediculus corporis, (2) the P. capitis, (3) the P. pubis. (1.) The P. corporis, the body louse, is of a dirty white colour, and varies from half to two lines in length. Its body is broad and elongated, with the margins divided into lobes, and covered with minute hairs ; but it has a narrow thorax, furnished on each side with three legs, which terminate in claws. This creature produces great irritation of the skin, giving rise to a number of little pimples on it, which frequently discharge a watery fluid. It multiplies with extraordinary rapidity, (2.) The P. capitis, the head louse, is much smaller than the above. It is devoid of hairs, with legs large in proportion to its body. It gives rise to « very troublesome eruption, attended with a watery discharge. It is propagated by means of the ova or nits, which are glued to the hairs of the head. (3.) The P. pubis, the crab louse, is a small, round variety, which attaches itself with con- siderable tenacity to the hairs of the stomach and lower part Of the body more particularly, and, like the preceding parasite, glues its eggs to the hairs- Various applications have been recommended for the destruction of these loathsome parasites; amongst which we may mention sulphur, stavesacre, white precipitate, and cocculus indicus, in the form of ointments j LOZENGE 1005 cnrbolio m-id and perchloride of mercnry lot oi)», niid tobiioco. Benzoic acid lias been found of service in allaying the irritation. Diligent washing witli soup and water should be had recourae to previous to applying any of the above remedies, and should the head be infected, the hnir should he cut short, and frequently combed with a small toothcomb. Pedicnli are sometimes conveyed from Hlthy to cleanly persons by means ol' dirty water- closets, chairs, sheets, brushes and combs, and in various otlier ways. School children frequently obtain tbem in consequence of their heads being brought into too cloae contact with the heads of other children infested by them. LOZ'ENGE S,vn. Tkoohe ; TROOHiactrs, Tabella, L.; Tablette, Fr. A small cake, often medicated, consisting principally of pow- dered sugar, made into a mass with some glu- tinous liquid, without the aid of heat, and dried. Thu form given to lozenges (tboohe tabbl- is, TB0CHI8CI, tableiteb) is generally that of a small round tablet or flattened cylinder j but originally they were exclusively made in the shape of a lozenge or rhomb, from which cir- cumstance their liiniiliar name is derived. Lo- zenges are distinguished from DBOPS OS I'ASTILLES by the non-employment of heat in their preparation ; and from PASTK8, by the latter being formed of vegetable juice or pulp, and having a softer consistence. In the preparation of lozenges the dry ingredients, separately reduced to a very fine powder, are first perfectly mixed together, and then beaten into a stiff paste with the glu- tinous liquid employed to give them form ; the mass is next rolled out to a desired thickness, and cut into pieces of the proper shape by means of a small cylinder or punch of steel or tin-plate, called a ' lozcngo cutter.' The newly formed lozenges are lastly dried by placing them on an inverted sieve or frame covered with paper in a dry, warm, and airy situation, and are frequently turned until they become hard and brittle, due care being taken to pre- serve them from dust and dirt. To prevent the mass adhering to the fingers and utensils during the process of manufacture, a little finely powdered starch, or a very little olive oil, scented with the same aromatic as that con- tained in the Inzenges, may be used. Mucilage of gum Arabic or of gum tragacantb, thin isinglass size, or the strained white of egg, are the substances usually employed to make the pulverulent materials adhere together. A strained decoction of Irish mo«s is now fre- quently used for the same purpose, for infe- rior qualities. The larger the proportion of gum which enters into the composition of lozenges, the slower they dissolve in the mouth ; hcnco powdered gum is frequently added to the other tnuterials to increase their quality in this respect, as m ell as to give an additional solidity to those which, like chalk, for instance, are of a peculiarly dry or crumbly nature. Starch and potato flour are often added to lozenge-masses inlieu of a portion of the nw'znr, and even plaster of Paris is not unfrequeiitly employed to give them weight j frauds which are readily detected in the manner noticed under Gum and Suoab. As a general rule, medicated lozekoes should weigh from 8 to 10 gr. each, and a medium dose of their active ingredient should be distributed through the bulk of 6 to 8 of them, in which case 3 to 5 of them may be safely taken as a dose, or sucked durin? the lapse of 3 or 4 hours. This will be useful in the preparation of those for which no esta- blished proportions are given. In 'sending out' corapoimds of this class containing active medicaments, as moi-phia or opium, the retailer as well as the manufacturer should be careful that the quantity contained in each lozenge is plainly marked on the label. In lozenges intended for mouth cosmetics or to perfume the breath, amberjrris is gene- rally regarded as the most appropriate per- fume; but hard smokers frequently prefer cloves and cinnamon, and some ladies give the preference to roses, orange flowers, and orris or violets. Lozenges are coloured with the same stains as are used for liqueurs and sweetmeats. Lozenges, as well as all othersimilar articles of confectionery, should be preserved in well- closed glass bottles, or jars, or in tin canisters, so as to be perfectly excluded from the air aud damp. • Lozenges, Absorljent. Tkochisoi antacidi, L. JPrep. 1. Take of precipitated chalk, i lb. ; gum Arabic, 2 oz. ; double refined white sugar, 14 oz. ; all in impalpable powder ; oil of nut- meg, i fl. dr.; pass the mixture through a fine sieve, beat it up with mucilage q. s., roll the mass into a thin sheet, and cut it into lo- zen;;e9 ; lastly, dry them by exposing them on a sheet nf white paper to the air, out of con- tact with dust. 2. As the last, but substituting heavy car- bonate of magnesia, 1) oz., for an equal weight of chalk. In diarrhcca, heartburn, acidity, &c. See LozENQES, Chalk, Magnesia, L., Soda, &c. Lozenges, Aca'cia. See Lozenoes, Gr>r. Lozenges, Acid'nlated. St/n. Acidulated LEMON lozenges, TaBTABIO ACID 1. ; TbO- CHisci AciDi tabtabici (Ph. E ), L. Prep. From tartaric acid, 2 dr. ; oil of lemon, 10 drops; while sugar, 8 oz. ; mucilage, q. s. to make a lozenge mass. The same ingredients mixed with heat form acidulated or acid DBOFS. Both are useful in coughs, hoarseness, sore throats, &c. See Lozenges, Cayenne, Citbic acid. Rose, &c. Lozenges, Al'kaline. See Lozenges, Soda, ViCHT, &c. Lozenges, Alum. Si/n. Tbochisci ALU- minis, L. Each lozenge contains IJ gr. of alum. As an astringent. See LozENGBS, AsinrNGENT. 1006 LOZENGE Lozenges, An'iseed. Syn, Tbochisoi anisi, L. Frep. From oil of aniseed, li fl. dr. ; finest white sugar, 1 lb. ; mucilage, q. s. Carmina- tive and stomachic. In colic, griping, &c.j and 93 a pectoral. Lozenges, Anthelmiu'tic. See Lozenges, WOBM. Lozenges, Antimonial. Syn. Tbochisoi an- TIMONIALES, MOESULI STIBII KlTNKELII, L. ; 'I'ABLETTES DE KuNKEL, Fr. Prep. (P. Cod.) Levigated sulphuret of antimony and car- damom seeds, of each 1 oz. ; almonds (blanched), 2 oz. ; cinnamon, i oz. ; sugar, 13 oz. ; mucilage of tragacanth, q. s. ; to be divided into 15-gr. lozenges. As an alterative. Lozenges. Ape"rlent. S^n. Tbochisoi ape- BIENTES, L. Each lozenge contdins 1 gr. each of calomel and scammony, and 2 gr. of jalap ; or, instead of the last, i gr. of jalapine. 2 to 3 for a dose. Lozenges, Astrin'gent. Syn. Teochisci ASTKIHGENTES, L. Each lozenge contains li gr. of alum and 2 gr. of catechu. In spitting of blood, relaxed uvula, sore throat, &c. See Lozenges, Alttm. Lozenges, Bark. S^n. Teochisci cincho- na;, L. Frep. (P. Cod.) Cinchona, 2 oz.; cinnamon, 2 dr. ; white sugac, 14 oz. ; muci- lage of gum tragacanth, q. s. j mi.\, and divide into 16-gr. lozenges. Tonic. Lozenges, Bath. St/n. Dawson's lozenges. From extract of liquorice and gum Arabic, of each li oz. ; sugar, 17 oz. It is both rolled into lozenges aifti formed into pipes. Demul- cent ; in tickling coughs, &c. Lozenges, Benzoic Acid. (Th. Hosp.) Syn. Tkochisci acidi benzoici. Prep. Benzoic add in powder, 175 gr.; tragacanth in powder, 70 gr. ; refined sugar in powder, 280 gr. ; red currant paste, a snflicient quantity to make 1 lb. Divide into 350 lozenges, and dry at a moderate heat in a hot-air chamber. A valu- able stimulant and voice lozenge in nervo- muscular weakness of the throat. Lozenges, Bicarbonate of Soda. Tboohisci soDiE BicAEBONATis. Bicarbonate of soda, in powder, 3600 gr. (8i oz.) ; refined sugar, 25 oz. ; gum acacia, in powder, 1 oz. ; mucilage, 2 oz. ; distilled water, 1 oz. ; mix, and form in 720 lozenges. Each lozenge contains 5 gr. of bicarbonate of soda. — Dose, 1 to 6 lozenges. Lozenges, Bis'muth. St/'n. Tbochisoi bis- MUTHi, L. Prep. 1. (B. P.) Subnitrate of bismuth, 346 gr. ; carbonate of magnesia, 4 oz. ; precipitated chalk, 6 oz. ; sugar, 29 oz. ; gum acacia, 1 oz. ; mucihigey 2 oz. ; rose water, a sufiiciency ; make 720 lozenges. Each lozenge contains 2 gr. of subnitrate of bismuth, — Dose, 1 to 6 lozenges. 2. (Trousseau.) Each lozenge contains 1 gr. of subnitrate of bismuth. Tonic and anti- spasmodic ; in chronic dyspepsia, gastrodynia, nausea, cramp of the stomach, &c. Lozenges, Black Cur'rant. Teochisci eibis NIGBI, L. Frep, From inspissated juice of black currants and sugar, of each, in powder, 1 lb.; tartaric acid, i oz.j mucilage, q. s. In hoarseness, &c. Lozenges, Bo"rax, Syn. Tbochisoi boea- CIS, L. Each lozenge contains 3 gr. of borax. One occasionally in aphthous sore mouth, sore throat, &c. Lozenges, Bromide of Ammonium. Esch lozenge contains 2 gr. of bromide of ammo- nium. — Dose, 1 to 3 lozenges. In hooping- cough. Lozenges, Burnt Sponge. Syn. Tboohisci spoNGia;, T. s. usT.aB, L. Prep. (P. Cod.) Burnt sponge, 4 oz. ; sugar, 12 oz. ; mucilage of tragacanth, q. s. ; divide into 12-gr. lozenges. In scrofula, glandular enlargements, &c. Lozenges, Caca'o. Si/n. Teochisci buttei cacao, L. Each lozent;e contains l-3rd of its weight of pure cacao butter. In habitual con- stipation ; and in phthisis, scrofula, &c., instead of cod-liver oil ; taken ad libitum. They are usually scented with roses. Lozenges, Caffeine. Sgn. Tbochisoi oap- PEIN.E, L. Each lozenge contains i gr. of caffeine and i gr. of citric acid. In hemicrania, hypochondriasis, &c. Lozenges, Cal'omel. Si/n. Woem lozenges ; Teochisci calomelanos, T. hydeaegtbi CHIOEIDI, L. Prep. (P. Cod.) Each lozenge contains 1 gr. of calomel. Alterative, Ac. They afford a simple way of introducing mercury into the system. During their use salt food and acid liquors should be avoided. When given for worms they should be followed, in a few hours, by a purge. Lozenges, Cam'phor. Si/n. Tboohisci cam- PHOEJE, L. Bach lozenge contains } gr. of (finely powdered) camphor. They must be kept in a well-corked bottle. Lozenges of Carbolic Acid. (Tb. Hosp.) Si/n. Tbochisoi acidi cabbolioi. Prep. Carbolic acid, 350 gr. ; gum Arabic, 220 gr. ; refined sugar, 12i oz. ; muciliige, 1 oz. ; dis- tilled water q. s. to make 1 lb. Divide into 350 lozenges, and finish as with benzoic acid lozenges. Lozenges, Car'bonate of Lime. See Lo- zenges, Chalk. Lozenges, Cat'echu. S)/n. Cachotj lozenges; Teochisci cateohu (B. P.), T. de teeea Japonica, L. ; Tablettes de cachoc, Fr. Prep. 1. (Ph. E. 1744.) Catechu, 2 oz. ; tragacanth, j oz. ; white sugar, 12 oz.; rose water, q. s. 2. (P. Cod.) Extract of catechu, 4 oz. ; sugar, 16 oz. ; mucilage of gum tragacanth q. 8. ; for lO-gr. lozenges. 3. (Tbo. catechu et magnesia — P. Cod.) Magnesia, 2 oz. ; powdered catechu, 1 oz. ; sugar, 13 oz. ; mucilnge of gum tragacanth (made with cinnamon water), q. s. to mix. 4. (Pebfumed.) See Cachou aeomatis^ and Pastils. 5. (B. P.) Pale catechu, in powder, 720 gr.; refined sugar, in powder, 25 oz. ; gum LOZENGE 1007 Arabic, in powder, 1 oz. ; mucilage, 2 oz. ; dU- tilled water, a safGciency; divide into 720 lozengea. Kxcb lozenge contains 1 gr. of catecliu. — Dose, 1 to 3 lozengea. Obi. All the above are taken in diarrhoea, in relaxation of the uvula, in irritation of the larvnx, and as cosmetics to fasten the teeth, and di8guise a fetid breath. The one con- taining magnpsia (No. 3) is also sucked in dyspepsia, acidity, and heartburn. Lozenges, Cayenne'. Si/n. Tbochisoi cap- sici, L. I'Mavoured with essence or tincture of capsicum or cayenne, with a very concen- trated Chili vinegar, or a little pure soluble cayenne pepper. 2. (AoiDntATED.) To each lb. add of tar- taric acid, i oz. Both are used in dyspepsia, and to promote digestion and create an appe- tite. They have also been recommended in temporary deafness arising from exposure to cold. They are generally tinged of a light pink or red colour. lozenges. Chalk. Syn. HKABTBtniK JjO- ZENOEB ; TeOCHISCI OKETa; (Ph. E.), T. CAEDI- ALQioi, Tabell£ Cabdialoics, L. Prep. (Ph £.) Prepared chalk, 4 oz. ; gum Arabic, 1 oz. ; nutmeg, 1 dr. ; white sugar, 6 oz. ; rose or orange-flower water, q. s. Antacid and ab- sorbent. 3 or 4 sucked ad libitum; in heart- burn, dyspepsia, dinrrhooa, acidity of the stomach und bowels, &c. lozenges, Char'coal. Si/n. Tbochisci cab- BONIS, L. Frep. 1. (P. Cod.) Prepared cliarcoal, 4 oz. ; white sugar, 12 oz., mucilage, q. s. to mix. In diurrhcea, cholera, dyspepsia, &c. 2. (Tro. oaebonas cum chooolata — M. Chevallier.) Charcoal and white sugar, of each 1 oz. ; chocolate, 3 oz. ; mucilnge of gum tragacanth, q. s. to mix. Nutritious ; used as the last. Lozenges, Cliing's Worm. Frep. 1. (Yel- low.) From sad'ron, J oz. ; boiling water, 1 pint; infuse, strain, add, of calomel, 1 lb.; powdered white sugar, 28 lbs. ; mix well, make a mass with mucilage of tragacnnth.and divide it into 7000 lozenges. Each lozenge contains 1 gr. of calomel. 2. (Beown.) Prom calomel, 7 oz. ; resinous extract of jalap, 34 lbs. ; white sugar, 10 lbs. ; mucilage of tragacanth, q. ». ; mix, and divide into 6125 lozenges. Each lozenge contains i gr. of calomel and 3) gr. of resinous extract of jalap. 1 t.o 6 of the yellow lozenges over night, IIS a vermifuge, followed by an equal number of the brown ones the next morning fasting. Lozenges, Clilo"rate of Fotassa. Sj/n. Tbo- chisci P0TAB8JB CHI.0BATI8, L. Frep. 1. Each lozenge ccmtains IJ gr. of chlorate ol potassa. In phthisis, sore throat, &c. 6 to 12 a day. 2. (B, P.) Chlorate of potash, in powder, 8600 gr. (8i oz.) ; refined sugar, in powder, 25 oz. ; Kun> aniiin, in powder, 1 oz. ; muci- lage, 2 oz., distilled water, 1 oz., or a suffi- ciency ; mix the powders, and add the muci- lage and water to form a proper mass ; divide in 720 lozenges. Ench lozenge contains 5 gr. of chlorate of potash, — I)o*e, 1 to 6 lozenges. Lozenges, Chloride of Ammonium. Each lozenge contains 2 to 3 gr. of chloride of ammonium. Used in bronchitis. — Dote, 2 to 4 lozenges. Lozenges, CUo"ride of Gold. 1. (Tbochisci AUBI CULOEIDI, L.) Each lozenge contains ■^Zj gr. of neutral chloride of gold. 2 to 4 daily ; in scrofula, cancer, &c. 2. (With BODA ; Teochiboi auei bt bodii CHLOBIDI, T. bodii AUBO-CHLORIDI, L. — Chrestien.) Each lozenge contains -^th pr. of soda-chloride of gold. Two daily ; as the last. Lozengea, Chloride of Lime. Syn. Tbo- chisci CALCIS CHLORtDI, T. C. CHLOKINATiE, L. Each lozenge contains i gr. of dry chlo- ride of lime. They are frequently tinged with a little carmine. Used to sweeten the breath and whiten the teeth. They do not keep well. Lozenges of Chlorinated Soda. %n. Tbo- chisci SOD* CHLOBiNAia:. Frep. Solution of chloride of joda, 1 fl. dr ; sugar, 10 dr.; gum Arabic, 2 dr.; mucilage of tragacanth, q. s. (i dr. of camphor may be added). To be lield in the mouth during infection. Lozenges, Choc'olate. St/n. Tbochisci cno- C01AT.E, L. From vanilla chocolate pressed into sheets, and cut into pieces whilst hot. Lozenges, Cincho'na. Si/n. Trochisci cin- cnONM EXTBACTi, L. Each lozenge contains li gr. of dry extract of bark. A little cinna- mon or nutmeg is often added. See Babk Lozenqes. Lozenges, Cin'namon. Si/n. Trochisci cin- NAMONI, L. From cinnamon (in fine powder), 1 oz., or the essential oil, 1 fl. dr., to each lb. of sugar. Carminative and stomachic. Cassia lozenoes are made in the fame way, and are frequently substituted for them. Lozenges, Ci'trate of Iron. Si/n. Tbochisci FEBKi ciTEATis, L. Each lozenge contains l.i gr. of ammonio-citrate of iron. As a mild cluil\be!ite tonic. They are sometimes made witli equal parts of susjar and vanilla choco- late. Lozenges, Citrate of Magne'sia. St/n. Tbo- chisci MAONESliE CITRATIS, L. E.ich 15-gr. lozenge contains 5 gr. of pure citrate of magnesia. Laxative. Lozenges, Cit'ric Acid. Si/n. Tbochisci ACIDI CITEICI, L. Prep. (P. Cod.) Citric acid, 3 dr.; sugar, 16 oz. ; essence of lemon, 16 drops; mucilage of tragacanth, q. s. ; mix, and divide into 12-gr. lozenges. In coughs, hoarseness, &c. Lozenges, Clove. Si/n. Tbochisci caeto- PHILLI. L. From cloves (powdered along with sugar), 2 oz., or essential oil, 1 fl. dr., to each lb. of sugar. They are frequently coloured. Carminative and stomachic; also used as a 1008 LOZENGE restorative after fatigue, added to chocolate to improve its flavour, and BUcked to sweeten the breath. Lozenges, Congli. Syn. Peotobal lozenges, Pttlmonio l. ; Tbochisci anticatabehales, L. Prep. 1. Blackcurrant lozenze-masa, 1 lb. ; ipecacuanha (in very fine powder), 2 dr. For 12-gr. lozenges. 2. To the last add of powdered opium and camphor, 1^ dr. 3. To either No. 1 or 2 add of oil of aniseed, IJ fl. dr. 4. (Tabieites be TEONOHiif.) From pow- dered gum Arabic, 8 oz. ; oil of aniseed, 16 drops; extract of opium, 12 gr. ; kerines mi- neral, 1 dr. ; pure extract of liquorice, 2 oz. ; white sugar, 32 oz. ; water, q. s. ; mix, and divide into lO-gr. lozenges. B. (Tablettes db Vakdammb.) From ben- zoic acid, 1 dr.; orris powder, 2 dr.; gum Arabic (powdered), 1 oz. ; starch, 2 oz. ; sugar, 16 oz. ; water, q. s. ; mix and divide into 15-gr. lozenges. 6. Each lozenge contains i gr. of lactuca- rium, \ gr. of powdered ipecacuanha, and ^ gr. of powdered squills, together with Jrd of their weight of pure extract of liquorice. Ohs. To render the above serviceable in coughs, hoarseness, &c., the bowels should be kept gently open with some mild aperient, and a light diet adopted, with abstinence from stimulating liquors. See LozENftES, Emetine, Ipecacuanha, &c. lozenges, Cro'tonOil. Syn. Tbochisci ceo- TONIB, L. Prep. (Soubeiran.) Croton oil, 5 drops; powdered starch, 40 gr. ; white sugar, 1 dr. ; chocolate, 2 dr. ; divide into 30 lozenges ; 5 or 6 generally prove cathartic. lozenges, Cutebine. Syn. Tbochisci cube- BINI, L. Prep. (Ph. Hamh.) Copaiba and extract of cubebs, of each 6 oz. ; yolks of 3 eggs ; mix, add of powdered marshmallow root, 6 "z. ; make it into pipes of 12 gr. each, and roll them in sugar. In gleet, &c., and in afEec- tions of the mucous membranes of the throat and fauces. Lablonye orders them to be made of sugar, and flavoured with oil of peppermint. lozenges, CuTiehB. Syn. Tbochisci ctj- BEBa;, L, Prep. 1. (Spitta.) Cubebs, 2 dr. ; balsam of tolu, 6 gr. ; mix, and add of extract of liquorice, 1 oz. ; syrup of tolu, 1 dr.; pow- dered gum, q. s. ; divide into 10-gr. lozenges. One of these, allowed to melt gradually in the mouth, is said to alleviate the obstruction in the nose, in coryza. 2. (U. S.) Prep. Oleoresin of cubebs, i fl. oz. 0. m.; oil of sassalras, 1 fl. dr.; extract of liquorice in powder, 4 oz. ; gum Arabic in powder, 3 oz. ; sugar in fine powder, 3 oz. ; syrup of tolu, q. s. Divide into 480 lozenge's. lozenges of Cyanide of Gold. (Chrestien.) Syn. Tbochisci aubi ctanidi. Prep. Cya- nide of gold, 2 gr. ; chocolate paste, 1 oz. Made into 24 lozenges. From 1 to 4 in the day. lozenges, D'Arcet'a. See Lozen&es, Vioht. lozenges, Diges'tive. See Lozen&es, Khxt- BAEB, GiNOEE, CANBT, DIGESTIVE, &C. lozenges, Edinburgh. Prep. From extract of poppies, 2 oz. ; powdered tragacanth, 4 oz. ; sugar, 10 oz.; rose water, q. d. to form a lozenge mass. lozenges, Emet'ine. Syn. Tbochisci eue- TiN^, L. Prep. (Magendie.) — 1. From im- pure or coloured emetine, 32 gr. (or pure erne- tine, 8 gr.); white sugar, 2 oz. ; mucilage, q. s. to mix; divide into 64 lozenges. Emetic. — Dose, 1 for a child, and 4 ibr an adult. They are generally tinged of a pink colour with carmine. 2. From impure or coloured emetine, 32 gr, (or pure emetine, 8 gr.) ; t^ugar, 4 oz. ; muci- lage, q. s. ; divide into 256 lozenges. Pecto- ral. One every hour, or of tener, for an adult. The last are intended to take the place of ipe- cacuanha lozenges, but are rather stronger. lozenges, Escharot'ic. Syn. Tbochisci es- CHAEOTici, L. Prep. (P. Cod.) Corrosive sublimate, 2 dr. ; starch, 4 dr. ; mucilage of tragacanth, q. s. ; mix, and divide into 3-gr. oat-shaped granules. For external use only. See Caustic (Zinc). lozenges, Ferrocy'anide of Iron. Syn. Tbo- chisci EEEBI EEEBOCTANIDI, T. CEBULEI, L. Each lozenge contains If gr. of pure Prussian blue. Alterative, febrifuge, and tonic; in epilepsy, intermittents, diseases of the gan- glionic system, &c. lozenges. Fruit. Prep. From juice of black currants (boiled to the consistence of an extract), 1 lb.; juice of red cuiTants (similarly treated), i lb. ; powdered gum tragacanth, \ lb. ; sugar, 3 lbs. ; raspberry syrup, q. s. ; pear essence, a few drops. Resemble black currant lozenges, but are more agreeable. lozenges, Garana'. See Lozenges, Pattl- MNIA. lozenges, Gin'ger. Syn. Tbochisci zingi- BEEis, L. Prep. From the best unbleached Jamaica ginger and gum Arabic, of each, in very fine powder, \\ oz. ; double refined lump sugar, 1 lb. ; rose water (tinged with saffron), q. s. A still finer quality may be made by using an equivalent proportion of essence of ginger, instead of the powder. Inferior qnali- ties are prepared with coarser sugar to which some starch is of ten added. Ginger lozenges are carminative and stomachic, and are useful in flatulency, loss of appetite, &e. lozenges. Gold. Syn. 'l^ocHisci AUEi, L. Each lozenge contaius -^ gr, of pulverulent gold. lozenges, Gnm. Syn. Teoschisci ACACia: (Ph. E.), T. gummi ababici, T. gummosi, L. Prep. 1. (Ph. E.) Gum Arabic, 4 oz. ; starch, 1 oz. ; white sugar, 12 oz. (all in very fine powder) ; rose water, q. s. 2. (P. Cod.) Gum Arabic, 1 lb. ; sugar, 3 lbs. ; orange-flower water, 2 fl. oz. 3. (Transparent ) From the same materials, LOZEXGES 1009 but emplnyinp a fjentlo lioat. Demulcent; uaeJ to allay tickling coughi. Lozenges, Quaiacum. (lb. llosp.) Syn. Tbocbisci ocaiaci. Prep. Quiiiacum re.-.iu in powder, 700 gr. ; tragacanth, 70 gr. ; sugar, 280 gr. ; black currant paste, q. s. Divide into 350 lozenges, and finish as benzoic acid lozenges. Lozenges, Qum Tra'gacanth. Syn. Tro- CniSCI TBAOACANTIl^S, 'I'. OUMMI T., L. Prep. (Ph. E. 171I-) Compound powder of traga- canth, 3 oz. ; sugar, 12 oz, ; rnse water, 4 fl. oz, llesemlile Uie last, but are more durable in the mouth. Loieuges, Heart'bani, See Lozbnoes, Chalk, &c. Lozenges, Iceland Moss. Syn. Tbochisci LIOHENIS, L. (F. Cod.) Contain half their weight of dried and powdered lichen jelly. Besciuble gum lozenges. Lozenges, Indian Hemp. Syn. Tsocnisoi CANNABIS, D. 0. Indioi, L. (Ebriard.) Each lozenge contaiud -^ gr. of extract of Indian hemp. Lozenges, I'odide of Iron. Syn. Tbochisoi FEBBi lODiDi, L. Eiich lozenge contains \ gr. of dry iodide of iron. 12 to 20 duily ; in amenorrhcea, chlorosis, scrofulous debility, &o. They are generally flavoured with a little nut- meg or cinnamon. Lozenges, Iodide of Fotasslam. Syn Tbo- chisoi PoTASSi lODiDi, L. Each lozenge contains 1 gr. of iodide of potassium, flavoured with nutmeg or cinnamon. 10 to 15 daily ; in scrofula, indurations, &c. One of the best ways of taking iodide of potassium. Lozenges, Ipecacuan'ha. Syn. Tbochisci IPECACUANH.ii;, L, Prep. 1. (B. P.) Mix ipecacuanha in powder, 180 gr. ; refined sugar in powder, 25 oz. ; gum acacia in powder, 1 oz. ; add mucilage of acacia, 2 fl. oz., and distilled water, 1 oz., or sufficient to form a proper mass. Divide into 720 lozenges, and dry in a hot-air chamber with a moderate hcttt. Each lozenge contains i gr. of ipecacu- anha. 2. (P. Cod., Hamb. do., and Ph. U. S.) Each lozenge contains i gr. of ipccacnanha. 3. (Tbo. ipboao. cum CAMPHOBi.) Each lozenge contains \ gr. of camphor, and i gr. of ipecacuanha. 4. (Tho. ipecac, cum chocolatA — P. Cod.) Each lozenge contains 1 gr. of ipecacuanha, and 12 gr. of chocolate cL la vanilla. The above are pectoral and expectorant, and are very useful in tickling and chronic coughs, hoarse- ness, &c. Lozenges, Ipecacnanha and Morphia. Syn. Tbochisci ipecacuanha et MORPHiiE (B.P.). Each lozenge contains -^^ gr. ipecacuanha and I'j gr. hydroclilorate morphia. — Dose, 1 to 6 lozenges. See LozENOES, HoBFHiA and Ipecacuanha. Lozenges, I'ron. Syn. Teoohisci pebbi, T. OBAI.YBEATI, L. 1. Each lozenge contains 1 gr. TOL. II. of Quevenne's iron. See Lozbkoes, Reduced IBON. 2. (Tbo. febei cabbonatis.) K;ich lozenge contains H gr. of saccharine carbonate of iron. They are both mild and excellent clialybentes. See Lozenges, Steei.. Lozenges, Jn'jnbe. See Paste, Jujube. Lozenges, Ker'mes UineTal. Syn. Tbochisci kebmetis, L. Prep. 1. (P. Cod.) Eich lozenge contains \ gr. of kermes miniral, and about J gr. of gum, made up with sugar and orange-flower water. Diaphoretic and expec- torant. 2. (Compound.) As the last, but with the addition of J gr. of opium, J gr. of f quills, and i gr. of ipecacuanha. Anodyne and expec- torant J both are very useful in catarrhs. Lozenges, Lactate of Iron. Syn. Tbochisci FEBBI LACTATis, L. Prep. (Cap.) Each lozenge contains 1 gr. of lactate of iron. Tonic. Useful in debility, accompanied with a diseased state of the organs of digestion. Lozenges, Lac'tic Ac'id. Syn. Tbochisci Acisi LACTici, L. Each lozenge contains 1 gr. of lactic acid to about 12 ^^r. of sugar. They are best flavoured with vanilla or nutmeg. In dyspepsia, &c., especially in gouty subjects. Those prepared by Magendie's formulse contain a larger proportion of acid, but are much too sour for frequent u^e. Lozenges, Lactaca"riiiin. Syn. Tbochisci LACTUOAEii, L.. Prep. (Ph. E.) Prepared with lactucarium in the same manner as the opium lozenges, Ph. E. Each of these lozenges contains from ^ to f gr. of lactucarium. Ano- dyne and demulcent. Used to allay tickling coughs, &,c. Lozenges, Lavender. Syn. Tbochisci la- TANDULjB, L. From J fl. dr. of Mitcham oil of lavender to each lb. of sugar, and tinged red with liquid lake or cjirniine; or violet, with litmus or indigo. Used chiefly to scent the breath. Those of the shops are generally deficient in odour. Lozenges, Lem'on. Syn. Tbochisci limonis, T. limonum, L. Prep. 1. From li fl. dr. of oil of lemon to each lb. of double refined white sugar. 2. (Acidulated.) See Lozenoes, Citbic and Taetabic. Obs, Lemon lozenges and drops are agree- able sweetmeats, and those that are acidulated are often very uf ef ul to promote expectoration in coughs, &c. The lost are also made into drops as well as lozenges, when they form the ' ACIDULATED LEMON DK0P8 ' of the shops. Those that are made of citric acid are by far the most wholesome. Both lemon lozenges and drops are generally coloured with infusion of saffron or turmeric. Lozenges, Lettuce. Syn Tbochisci lao- TUCi, L. Prep. From extract of lettuce, ex- tract of liquorice, gum, and sugar, equal parts. Anodyne and demulcent ; in obstinate cough without expectoration. See LozENasa, Lac- tuoabium. 64 1010 LOZENGES lozenges, Lichen. See LozENfflES, Iceland MOSS. lozenges, Liquorice. Si/n. Black lozenges ; Tbochisci gltcybbhizs, T. &. GLiBua;, T. BECHici NiGRi, L. I'rep. 1. (Ph. E.) Ex- tract of liquorice and gum acacia, of each 6 oz ; white sugar, 12 oz. ; dissolve in water, q. s. ; evaporate into a paste, and form into lozenges. Pectoral and demulcent. Useful to allay ticljling coughs and remove hoarseness. 2. (With OPIUM.) See Lozenges, OpitrM. Lozenges, Magne'sia. Si/n. Heaetfpen loz- BNGKS; TeOCHISCI MAGNESIA (Ph. E.), L. Prep. 1. (Ph. E.) Carbonate of magnesia, 6 oz. ; powdered white sugar, 3 oz. ; oil of nut- meg, 20 drops ; mucilage of tragacanth, q. s. to mix. 2. (Ph. U. S.) Calcined magnesia, 4 oz. ; sugar, 12 oz.; nutmeg, Idr.; mucilage of tra- gacanth, q. ». ; for 10-gr. lozenges. 3. (Wholesale.) Calcined magnesia, 3 oz. ; powdered gum tragacanth, 1 oz.; double refined lump sugar, J lb. ; rose or orange-flower water, q. s. to make a lozenge mass. Obs. Magnesia lozenges are very useful in heartburn, acidity, and indigestion. The con- fectioners generally omit the nutmeg, and make their mucilage with either rose or orange- flower water, or else add the dry gum to tlie mass, and then mix up the powders with one or other of these liquids. It is also an im- provement to use calcined magnesia, which is about twice as strong as the carbonate, and consequently less need be employed. Lozenges, Manna. Si/a. TuocHisci mann.e, L. Prep. (Van Mons.) Powdered tragacanth, 1 dr. ; white sugar, 12 oz. ; manna, 3 oz. ; orange-flower water, q. s. to mix. Demulcent, and in large numbers slightly laxative. Lozenges, Marshmallow. Si/n. Tbochisci ix,TB.MM, L. ; Tablettbs de guimaute, Fr. Prep. (P. Cod.) Marshmallow root (decor- ticated and finely powdered), 2 oz ; sugar, 14 oz. ; mucilage of tragacanth (made with orange-flower water), q. s. Demulcent and expectorant. Useful to allay the irritation in cough, &e. The preparations of marshmallow have always been highly esteemed as pectorals by the vulgar. Lozenges, Jlin'inni. St/n. Tbochisci minii (Ph. E. 1744), L. Prep. Prom red lead, 1 dr. ; corrosive sublimate, 2 dr. ; crumb of bread, 1 oz. ; rose water, q. s. ; to be made up into oat-like grains. For external use only. Lozenges, Morphia. Syn. Tbochisci mob- phis (B.P., Ph.E.), T. M. HYDBOCHLOBATIS, L. Prep. 1. (Ph. E.) Hydrochlorate of morphia, 20 gr. J tincture of tolu, J fl. oz. ; powdered white sugar, 25 oz. ; dissolve the hydrochlorate in a little warm water, mix it with the tincture and the sugar, make a mass with mucilage of gum tragacanth, q. s., and divide it into 15-gr. lozenges. Each lozenge contains about jL gr. of hydrochlorate of morphia. Used as opium lozenges, but are pleasanter. The morphia lozenges of the shops generally contain -j^ gr. of hydrochlorate of morphia. (Pereira.) 2. (With IPECACITANHA, TBOCHISCI MOB- PHI^ ET iPEOACUANHa; — Ph. E.) As the last, adding of ipecacuanha, 1 dr. Each lozenge contains about -J-^ gr. of hydrochlorate of mor- phia, and Jj gr. of ipecacuanha. Anodyne and expectorant ; in tickling coughs, &c., and to allay pain. 3. Hydrochlorate of morphia, 20 gr. ; tinc- ture of tolu, i oz. ; refined sugar, in powder, 24 oz. ; gum Arabic, in powder, 1 oz.; mucilage, 2 oz., or a sufficiency ; boiling distilled water, i oz. Divide the mass into 720 lozenges. Each lozenge contains uV gr. of hydrochlorate of morpliia. — Dose, 1 or 2 occasionally, for cough. Lozenges, Morphia and Ip'ecacnanha. Sgn. Tbochisci morphia et ipecacuanha (B.P.) Hydrochlorate of morphia, 20 gr.; ipecacu- anha, in fine powder, 24 oz. ; tincture of tolu, i oz. ; refined sugar, in powder, 24 oz. ; gum Arabic, in powder, 1 oz. ; mucilage, 2 oz., or a sufficiency ; distilled water, i oz. ; divide the mass into 720 lozenges. Each lozenge con- tains ^5^ gr. of hydrochlorate of morphia and ^ gr. of ipecacuanha. — Dose, 1 or 2 occasion- ally, for cough. Lozenges of Naphthalin. (Dupasquier.) St/n. Tbochisci naphth alini. Prep. Naphthaliii, 5 scroples ; sugar, 20 oz. ; oil of aniseed to flavour ; form a mass with mucilage of traga- canth, and divide into lozenges of 15 gr. each. Expectorant, and may he taken to the extent of 20 a day. Lozenges, Ni'tre. St/n. Tbochisci nitbici, L. Prep. 1. (Ph. E. 1783.) Nitre, 3 oz. ; white sugar, 9 oz. ; mucilage of tragacanth, q. s. to mix. Diuretic; but chiefly sucked, without swallowing, to remove incipient sore throat. 2. Camphorated; Tbochisci nitei cam- PHOEATi, L. — Chaus-ier. Each lozenge con- tains ^ gr. of opi nm, J gr. of camphor, and 1 gr. of nitre. In hoarseness, sore throat, &c. Lozenges, Nut'meg. Si/n. Tbochisci mt- eistic^, L. Prom oil of nutmeg, 1 fl. dr., to each lb. of sugar, and coloured with infusion of saffron. Carminative and stomachic; in colic, &c. Lozenges, O'pinm. St/n. Anodyne lo- zenges ; Tbochisci opii (Ph. E.), T. glycye- BHiziE CUM opio, L. Prep. 1. (B. P., Ph. E.) Opium (strained), 2 dr.; tincture of tola, ^ oz. ; triturate together, add of powdered sugar, 6 oz.; extract of liquorice (soft) and powdered gum acacia, of each 5 oz. ; mix, and divide into 10-gr. lozenges. Each lozenge con- tains 5 to ^ gr. of opium. Used to allay tick- ling cough and irritation of the fauces, and as an anodyne and hypnotic. 2. (Ph. U. S.) Opium (in fine powder), 2 dr. ; extract of liquorice, gum Arabic, and sugar, of each 5 oz. ; oil of aniseed, J fl. dr.; water, q. s. ; divide into 6-gr. lozenges. Each lozenge contains -^ gr. of opium. As the last. LOZENGES 1011 3. Extract of opium, 72 gr.; tinrtura of tola, i oz. ; reflned sugiir (in powder), 2 oz. ; extract of liquorice, 6 oz. ; distilled water, a surticicncy. Divide the mass into 720 lozenges. Each lozenge contains ^ gr, of extract of opium. — Dose, 1 to 2 lozenges. Lozenges, Or'ange. Si/n. Tbocrisci au- BANTii, L. From oil of orange, 1_J fl. dr. to ench lb. of sugar, and infusion of saftron for colonring. By adding nitric or tartaric ncid, 3 dr. 'ACIDULATED OnAHaE I,0ZENO£S' will be formed. Lozenges, Orangeflow'er. Sffn. Tbocbisci AUBANTii PLOBUM, L. Frep. (P. Cod.) Pow- dered sugar, 1 lb. ; neroli, 1 dr. ; orange-flower water, q. s. ; make it into drops (pastllli) ; or, omit the water, and make it into lozenges with mucilage of tragacanth made with orange- flower water. Delightfully fragrant. Lozenges, Or'rii-root. Syn. Tbochibci ibi- DIS, h. Prep. From orris root (in very fine powder), 1 oz. ; sugar, 1 lb. j mucilage of tra- gacanth, q. s. to mix. Used to perlume the breath. Lozenges Ox'alate of Fotassa. Syn. Tbo- CmSCI POTASS* OXAlATia, T. p. bupeb-oxa- LATIB, L. As ACIDCLATED LOZENGES, but using quadraoxalate of potasaa (salt of sorrel) instead of tart^iric acid. (See below.) Lozenges, Oxal'ic Acid. St/n. Trochisoi AOIDI OXALICr, L. A» ACI DULATED LOZENGES, but using oxalic acid instead of tartaric acid. The last two arc refrigerant, but their use is objectionable, especially for patients who la- bour under the oxalic diathesis. In large quantities they are poisonous. Lozenges, Faregor'ic. Si/n. Tnocuisci pa- BEaOKici, L. Medicated with 2 fl. oz. of paregoric and 2 dr. of tartaric acid, to each lb. of s\igar, and tinged of a pink colour with lake or cochineal. As a pectoral in catarrhs, &c. Lozenges, Fanllin'ia. Si/n. Tbochisci paul- I,INI£, T. GUAHAN^, L. Prep. (Dr Gavrelle.) Ench lozpnge contains nearly i gr. of extract of giirim.i or pauUinia, and is flavoured with vanilla. 12 to 20 daily, as an alterative and tonic; in clilDrosis, diarrhoea. Lozenges, Pec'toral. Sj/n. Tbochisci pec- TOBALES, T. BECHICI, L. Prep. 1. (Dr Grunn.) Powdered squills, 4 parts ; extract of lettuce, 8 parts ; ipecacuanha, 18 parts ; manna, 125 parts ; sugar, 250 parts; mucilage of tragaranth. q. s. tn mix. 2. (Magendie.) See Lozenges, Emetine. 3. Black; T. bkchici nigei.) See Lo- zenges, LlQUOKICE. 4. (White; T. dechici albi.) Orris root, 4dr. ; liquoiice powder, 6 dr.; starch, IJ nz. ; sugar, 18 oz. ; muiilage of tragacanth, q. o. to make a l-zenpo-niass. 5. (Yellow; T. bechici ilavi.) Pow- dered orris root, 6 dr. ; siarch, 4 dr. ; liquo- rice pn« dor, 3 dr. ; safl'ron, 2 dr. ; sugar, 8 oz. ; muril;ii,'e of tr.igacanth, q. ». to mix. Obt. All the above are used as demulcents in coughs, colds, &c. Nos. 1 and 2 are ano- dyne as well as demulcent. For other for- mulas see Lozenoxb, Cough, Liquobice, Opium, Fahr. With 14 oi. of the dried mass mix bicarbonate of soda, 13 vz.; citric acid, 6 oz. ; Kutriir, 3 oz. Sprinkle over the mixture enough rectirit'd spirit so as to make it sufficiently moist to be f;ranuluted by rubbing through a tinned iron sieve. d. (Gxtemporaneoua.) Citric ac'd (cryst.), 20 gr. ; carbonate of magnesium, 14i gr. ; mix in a tumbler of cold wattr, and drink the mixture whilst effervescing. A pleasant saline. Oba, A dry white powder, sometimes sold as citrate of magnesia in the shops, is quite a different preparation to the above, and does nut contain a pirticle of citric acid. The following formula is that of a wholesale London drug-house that does largely in this article i — Calcined magnesia, magnesium oxide, li lb. (or ciirbonate, 2 lbs.) ; powdered tartaric acid, li lb, ; bicarbonate of sodium, 1 lb,; dry each article by a gentle heat, then mix them, pass the mixture through a fine sieve in a warm dry room, and keep it in well-corked bottles. A few drops of essence of lemon and 3 lbs. of finely powdered sugar are commonly adiled to the above quantity. This addition renders it more agreeable. Prop., <^o. Citrate of magnesium ia a mild and agreeable laxative ; its secondary efEects resemble those of the carbonate. — Dose. As a purgative, ) to 1 02. The dose of the effer- vescing citrate must depend on the quantity of magnesia present. A solution of this salt in water, sweetened and flavoured with lemon, forms magnesian lemonade. Magnesium, Boro-cit'rate of. Syn. Maonesi^ Bouo-ciTKAS, L. Frep. (Cadet.) Boraeie acid (in powder), 113 gr. ; oxide of magnesium, 80 gr. ; mix in a porcelain capsule, and add enough of a solution of citric aeid, 260 gr., iu Hater, 3^ pints, to form a thin paste; then add the remainder of the citric solution, and gently evaporate, with constant stirring, to dryness. A eooling saline, and, in small doses, emmcnagogue and lithontriptic. — Dose. As an aperient, 3 to 6 dr. Uagnesium, Oxide of. MgO. Syn. Oxide of Maonesidm, Calcined Magnesia, Magnesia (B. P., Ph. L.). Prej>. 1. (B.P.) Magnesium carbonate, heated in a crucible until all the carbonic anhydride is driven off. Prop., Sfc. White heavy powder, scarcely soluble in water, but readily soluble in acids without effervescence. Its solution In hydro- chloric acid, neutralised by a mixed solution of ammonia and ammonium chloride, gives a copious crystalline precipitate when sodium phosphate is added to it. See next prepara- tion. Magnesia levls (B. P. Si/n. Light mag- nesia. Prep. (B. P.) 1. Light carbonate of magnesium heated in a Cornish crucible until all the carbonic anhydride is driven off. A bulky white powder, differing from the magnesia (B. P.) only in its density, the volume occupied by the same weight being 3i to 1. The properties of the two varieties of mag- nesium oxide are identical, and are used iu medicine as antacids, laxatives, and antilithics, and much used in dyspepsia, heartburn, &c. — Dose, 10 to 20 gr. as an antacid and 20 to 60 gr. Hs a purgative. Magnesium, Fhos'phate of. MgHPO,. 6Aq. Si/n. Magnesia phospuas, L. Prep. From the mixed solutions of phosphate of sodium and sulphate of magnesium, allowed to stand for sometime. Small, colourless, prismatic cr\s- tals, which, necording to Graham, are soluble in about 1000 parts of cold water. Phosphate of magnesium exists in the grains of the cereals, and in considerable quantity in beer. It is also found in guano. Magnesium and Anuno"nium, Phosphate of. MgNH^.PO^, 6 Aq. Sj/a. Ammonio rno8- PHATB OP MAGNESIA; MaGNESIJE BT AMMO- NliE fHOSFHAB, L. This compound falls as a white crystalline precipitate whenever am- monia or carbonate of ammonium is added, iu excess, to a solution of a salt of magnesium which has been previously mixed with a solu- ble phosphate, as that of soda. It sulfides immediately from concentrated solutions, but only after some time from very dilute ones. Prop., Sic. Aminonio-phosphate of magne- sium is very slightly soluble iu pure water; when heated, it is resolved into pyrophosphate of magnesium, and is vitrefied at a strong red heat. It is found iu whcaten bran, guano, potatoes, &,c., and occasionally forms one of the varieties of urinary calculi. Magnesium, Silicates of. There ore several native silicates of magnesia, more or less pure, of which, however, none is directly employed in medicine. Meerschaum and steatite or soap- stone are well-known varieties. Serpentine is a compound of silicate and hydrate of mag- nesium. The minerals augite and hornblende are double salts of silicic acid, magnesium, and calcium with some ferrous oxide. The beauti- ful crystallised mineral called chrysolite is a silicate of magnesium, coloured with ferrous oxide. Jade is a double silicate of magne- sium and aluminum, coloured with chromic oxide. Magnesium, Sulphate of. MgS04,7 Aq. Sj/n. Epsom salt, MioNEsiiE sulphas (B. P. Ph. L. E. & D.), Sal Epsomensis, L. This com- pound was originally extracted Irom the saline springs of Epsom, Surrey, by Dr Grew, in 1695. It is now exclusively prepared on the large scale, and from either magnesian lime- stone or the residual liquor of the sea-salt works. Prep. 1. From dolomite or magnesian limestone. — a. The mineral, broken into frag- ments, is heated witli a sufficient quantity of dilute snlphuric acid to convert its carbonates into sulphates; the sulphate of magnesium is washed out of the mass with hot water, and 1020 MAGNESIUM the solution, after defecation, is evaporated and crystallised, b. The ' limestone,' either simply broken into fragments or else calcined (burnt), and its constituents quicklime and oxide magnesium converted into hydrates by sprinkling (^laking} it with water, is treated with a sufficient quan- tity of dilute hydrochloric acid to dissolve out all the calcinum hydrate without touching the magnesium hydrate; the residuum of the latter, after being washed and drained, is dis- solved in dilute sulphuric acid, and crystallised as before. 2. From bittern. — a. The residual liquor or mother-water of si^a-salt is boiled for some hours in the pans which are used during the summer for the concentration of brine; the saline solution is then skimmed and decanted from some common salt which has been depo- sited, after which it is concentrated by evapo- ration, and, finally, run into wooden coolers ; in about 36 hours, l-Sth part of Epsom salt- usually crystallises out. This is called ' singles.' By re-dissolving this in water, and re-crystal- lisation, 'doubles,' or Epsom salts fit for the market, are obtained. A second crop of crys- tals may be procured by adding sulphuric acid to the mother-liquor, and re-concentrating the solution, but this is seldom had recourse to in England. Bittern yields fully 5 parts of sul- phate of magnesia for every 100 part^ of com- mon salt that has been previously obtained from it. b. A concentrated solution of sulphate of sodium is added to bittern, in equivalent pro- portion to that of the chloride of magnesium in it, and the mixed solution is evaporated at the temperature of 122° Fahr. (Ure) ; cubical crystals of common salt are deposited as the evaporation proceeds, a ter which, by further concentration and repose, regular crystals ot sulphate of magnesia are obtained. c. A sufficient quantity of calcined arid slaked magnesian limestone is boiled in bittern to decompose the magnesium salts, and the liquid is evaporated, &c., as before. This is a very economical process. Prop. Small acicnlar crystals, or (by care- ful crystallisation) large tour-sided rhombic prisms ; colourless ; odourless, transparent ; slightly efflorescent; extremely bitter and nauseous ; when heated, it fuses in its water of crvstallisation, the larger poition of which readily passes off, but one equivalent of water is energetically retained; at a high tempera- ture it runs into a species of white enamel ; it dissolves in its own weight of cold water, and in 3-4ths of that quantity of boiling water; it is insoluble in both alcohol and ether. Sp. gr. 1-66. Pur. Sulphate of magnesium is soluble in an equal weight of water at 60° Fahr., by which it may be distinguished fi'om sulphate of sodium, which is much more soluble. An aqueous solution in the cold is not pre- cipitated by oxalate of ammonium. The precipitate given by carbonate of sodium from a solution of 100 gr. should, alter well wash- ing and heating to redness, weigh 16'26 gr, (B. P.) Digested in alcohol, the filtered liquid does not yield a precipitate with nitrate of .silver nor burn with a yellow flame, and evaporates without residue. "Not deliquescent in the air." (Ph. L.) 100 gr. of the pure crystal- lised sulphate yields 16^ gr. of calcined magnesium oxide, (Pereira.) 10 gr., dis- solved in 1 fi. oz. of water, and treated with a solution of carbonate of ammonium, are not entirely precipitated by 280 minims of solu- tion of phosphate of sodium, (Ph, E.) Uses, (^c. Sulphate of magnesium is an ex- cellent cooling purgative, and sometimes proves diuretic and diaphoretic. — Doge, 1 dr. to 1 oz., as a purgative, or an antidote in pois- oning by lead. Large doses should be avoided. Instances are on record of their having proved fatal, Dr Christison mentions the case of a boy 10 years old who swallowed 2 oz. of salts, and died within 10 minutes. The best anti- dote is an emetic. A small quantity of Epsom salts,' largely diluted with water (as a drachm to i pint or f pint), will usually purge as much as the common dose. This increase of power has been shown by Liebig to re- sult rather from the quantity of water than the salt. Pure water is greedily taken up by the absorbents; but water hold- ing in solution saline matter is rejected by tliose vessels, and consequently passes off by the intestines. Obs. Oxalic acid has occasionally been mis- taken for Epsom salt, with fatal results. They may be readily distinguished from each other by the following chaiacteristics : — OxALio Acid, Tastes extremely soar. Volatilises when heat- ed on platiiinra foil. Produces milkiness when dissolved in hard water. Ei'SOM Salt. Tastes extremely bit- ter and nauseous. Does not volatilise when heateil on pla- tinum foil. Does not produce milkiues-' when dissolved in hard water, Hagnesinm, Tar'trate of. Si/n. MAQirEBif TABTKAS, Magnesia tabtaeioa, L. Prep. By saturating a solution of tartaric acid with carbonate of magnesium, and gently evapo- rating to dryness. It is only very slightly soluble in water. — Dose, 20 to 60 gr., or more ; in painful chronic maladies of the spleen. (Pereira, ex Radmacher.) The effer- vescing tartrate of magnesium, commonly sold under the name citrate, has already been noticed. Magnesium and Potas'sium, Tartrate of. Si/n. POTASSIO-TAETEATE op MAGNESIA; MAGNBSI.B POTASSIO-TAETEAS, M. ET POTASS.E TAKTSA8, L. Prep. From acid tartrate of potassium (in powder), 7 parts ; carbonate of magnesium, 2 parts; water, 165 parts; boiled until the MAGNET— MALIC ACID 1021 •olntion ia complete, and then evaporated nnd crystallised. A mild aperient.— Z'ow, 1 to 5 dr. ; in scurvy, &b. MAG'HET. Si/n. Maonzs, L. Besides its application to the londstone, this name was forinnrly given to several compound^ used in medicine. — Ab8Bnical uaqnet (haones AUSENiOALis), a substance once used as a oau»tic, consisted of common antimony, sul- phur, and arscnious acid, fused together until they formed a sort of glass. Maqneb kfilefsls was native cinnabar. UAHOO'ANT. This is the wood of Swietenia Mahogoni (Linn.), a native of the hotier parts of the now world. It is chiefly imported from Honduras and Cuba, The extract is astringent, aud has been used in tanninj^, and as a substitute for cinchona bark. The wood is chiefly employed for furniture and orna- mental purposes, and, occasionally, in ship- building. Imitations of mahogany are made by stain- ing the surface of the inferior woods by one or other of the following methods : 1. Warm the wood by the fire, then wash it over with aquafortis, let it stand 24 hours to dry, and polish it with linseed oil reddened by digesting alkanet root in it; or, instead ofthf hitter, give the wood a coat of varnish, or French polish which has been tinged of a mahogany colour with a little aloes and an- uotta. 2. Socotrine aloes, 1 oz. ; dragon's blood, i oz. ; rectified spirit, 1 pint; dissolve, and apply 2 or 3 coals to tlie suifiiee of the nond, previously well smoothed and polished ; lastly, finish it off with wax or oil tinged with ulkanet root. S. Logwood, 2 oz.; madder, 8 oz. ; fustic, 1 oz. ; water, 1 gall. ; boil 2 hours, and apply it several times to the wood boiling hot ; whin dry, slightly brush it over with a solution of pearlash, 1 oz.; in water, 1 quart; dry, and polish as before. 4. As the last, but using a decoction of log- wood, 1 lb., in water, 5 pints. Tlie tint may be brightened by adding a little vinegar or oxalic acid, and darkened by a few grains of copperas. Stains and apots may be taken out of mahogany furniture with a little aquafortis or oxalic acid and water, by rubbing the part with the liquid by means of a coik till the colour is restored ; observing afterwards to well wash the wood with water, and to dry it and polish it ns before. MAIZE. Syn. Indian coBir. The seeds of Zea Mayt (Linn.). Like the other corn plants, it belongs to the Grass family (Oraminaceai), and has albuminous grains sufficiently large ■ud farinaceous lo be ground into flunr. Maize is extremely nutritious, and although it ia poorer in albumenoid matters than wheat, it is, of all the cereal grains, the richest in fatty oil, of which it contains abont Sjj. (Damns and Payen.) It is remarkable for its fattening quality on animals, but is apt to excite slight diarrbcea in those unaccustomed to its use. Its meol is the ' polenta ' of the shops. The peculiar starch prepared from it is known as ' oouN ploub,' ' maizena,' Ac. In America the young ears are roasted and boiled for food. The centesimal composition of maize is as follows : — Flesh formers (albumenoid bodii s), 9'9; heat and fat formers (starch, dextrin, and fat), 71-2, fibre, 4-0; ash, 1-4; water, 13-5. Letheby says of maize : " The grain is said to cause disease wheu eaten for a long time, and without other meal — the symptoms being a scitly eruption upon the hands, gre:it pros- tration of the vital powers, and death alter a year or so, with extreme emaciation. These effects have been frequently observed amongst the peasants of Italy, who use the meal as their chief food, but I am not aware of any such effects having been seen in Ireland, where it is often the only article of diet for mouths together." Maixena. This is maize deprived of all its albumenoid or flesh-forming constituents, as well as of its fibre and ash, and is therefore simply pure starch. Its food properties are, therefore, the same as those of arrowroot. COBN FLOVB and Oswego are only other names for the same substance. MALAO'HA. In pharmaci/, a poultice or emollient application. MA'LIC ACID. HaCjHjOj. Syn. AciBtrm ualicum, L. This plant exists in the juice of many fruits and plants, either alone or asso- ciated with other acids, or with potassa or lime. In the juice of the garden rhubarb it exists in great abundance, being associated with acid oxalate of potassa. Prep. (Evcritt.) Thestiilksof common gar- den rhubai'b are peeled, and ground or gmttd to a pulp, which is subjected to pressnrc ; the juice is heated to the boiling point, neutralised with carbonate of potassa, mixed with acetate of lime, and the insoluble oxalate of lime which falls is removed by filtration ; to the clear and nearly colourless liquid, solution of acetate of lead is next added as long as a precipitate ('miilate of lead') continues to form ; this is collected on a filter, washed, difi'uscd through water, aud decomposed by sulphnric acid, avoiding excess, the last portion of lead being thrown down by » stream of sulphuretted hydrogen ; the filtered liquid is, lastly, care- fully evaporated to the consistence of a syrup, and left in a dry atmosphere until it becomes converted into a solid and somewhat crystalline mass of malic acid. If perfectly pure malic acid is required, the malate of lead must be crystallised before decomposing it with sul- phuretted hydrogen. Prod. 20,000 gr. of the peeled stalks yield 12,600 gr. of juice, of which one imperial gallon contains 11,1391 S''- o' ^^J malic acid. Obs. By a similar process malic acid may be 1022 MALLEABILITY— MALT prepared from the juice of the berries of the mountain ash (Sorbus aucuparia), just when they commence to ripen, or from the juice of apples, pears, &c. Prop,, . By dissolving the carbonate in hydriodic acid and evaporating the filtered liquid in vacuo or out of contact with air. — Dose, 1 to 3 gr. ; in anaemia, chlorosis, &c., occurring in scrofulous subjects. Manganons Oxide. MnO. Syn. Pbotoxidb OF Manganese. Frep. By passing a current of hydrogen over manganous carbonate heated to whiteness in a porcelain tube. Olive-green powder rapidly oxidising on exposure to air, and soluble in acids forming maugauous salts. There are four other oxides and two oxy- hydrates that may be treated of here, but of which only the peroxide and the manganates and permanganates are of practical import- ance. Manganons manganic Oxide. MnsO^, or MnO, MnjOj. Syn. Bed oxide of manga- nese, Pkotosksquioxidb of manganese. Found nntive as " Hansmanite" It is pro- duced by igniting manganous carbonate, or manganic, oxide, or manganic peroxide. Red- dish-brown, coloured crystals or powder, and communicates an amethyst colour to glass when fused with it. Manganous-manganic Peroxide. Mn^O^ or MnOj.MnjOa, Syn. Intbkmediatb, oxide OF manganese. Found native as " Varvicile," as a black hard crystalline mass. Decomposed when heated into a lower oxide and oxygen. Manganons Phosphate. MnH.FO^-i- 6Aq. Syn. Phosphate of peotoxide op manga- nese ; Manganesii phosphas, L. Prep. By precipitating a solution of manganous sul- phate with a solution of sodium phosphate. It must be preserved from the air. — Dose, 3 to 12 gr. ; in anaemia, rickets, &c. Manganous Snl'phate. MnS04. Syn. Siri,- PHATE OF PEOTOXIDE OF MANGANESE ; MaN- Ganesii SULPHAS, L. Frep. 1. By dissolving manganous carbonate in dilute sulphuric acid, and evaporating the filtered solution so that crystals may form, or at once gently evapo- rating it to dryness. Pure. 2. (Commercial.) By igniting manganic peroxide (pyrolusite) mixed with about 1-lOth of its weight of powdered coal in an iron crucible or gas-retort, and digesting the resi- duum of the calcination in sulphuric acid, with the addition after a time of a little hydro- chloric acid ; the solution of manganous sul- phate thus obtained, after defecation, is evaporated to dryness, and heated to redness as before ; the mass, after ignition, is crushed small, and treated with water ; the solution is nearly pure, the whole of the iron having been reduced into the state of insoluble peroxide. Used by the calico printers. Cloth steeped in the solution, and afterwards passed through a solution of chloride of lime, is dyed of a per- manent brown, Frop., S;e. Pale rose-coloured crystals of the formulae MnS04, 7Aq. j MnS04, 5Aq. ; or MnS04, 4Aq. ; according to the method of crystallising, furnishing a solution of a rich amethystine colour. With sulphate of potassa it forms a double salt (' manganese alum '}.— Dose. As an alterative and tonic, 5 to 10 gr. ; as a cholagogue cathartic, 1 to 2 dr., dissolved in water, either alone or combined with infu- sion of senna. According to Ure, its action is prompt and soon over ; 1 dr. of it occasions, after the lapse of an hour or so, one or more liquid bilious stools. In large doses it occa- sions vomiting, and in excessive doses it de- stroys life by its caustic action on the stomach. (Dr G. C. Mitscherlich.) It has been adminis- tered with manifest advantage in torpor of the liver, gout, jaundice, syphilis, and certain skin diseases; and, combined with iron, in ansmia, chlorosis, rickets, &c. Manganous Tar'trate. MnC4H405. Syn. Manganesii taeteas, L. Frep. By satu- rating a solution of tartaric acid with most manganous carbonate. Alterative and tonic. — Dose, 4 to 12 gr. Manganate of Barium. BaMn04. Green insoluble powder, obtained by fusing barium hydrate, potassium chlorate, and manganic peroxide together, and washing the product. Manganate of Potassium. K^MnOj. Finely powdered manganic peroxide,, potassium chlo- rate, and potassium hydrate, made into a thick paste with water, and heated to dull redness. The fused product is treated with a small quantity of water, and crystallised by evapo- ration in vacuo. Dark green, almost black crystals, readily soluble in water, but decomposed by excess, or by acids into manganic peroxide, and potassium permanganate. Manganate of Sodium. M2Mn04. Prepared on the large scale by heating a mixture of manganic peroxide and sodium hydrate to red- ness in a current of air. Used in strong solu- tion as a disinfectant under the name of " Condy's green fluid." Manganic Acid. H2Mn04. This acid has not yet been obtained free, but some'of its salts are extensively employed as disinfectants, as " green Condy's fluid." The chief com' pounds are the following : — Manganic Hydrate. Mn2(H0)j. Syn. Hy- DEATED BBSQUIOXIDE OF MANGANESE. found native as " manganite," in reddish- brown crystals. Frep. By passing a current of air through recently precipitated and moist MANGANESE 1027 manganous hydrate. Soft dark brown powder converted into the oxide by beat. Hsnganic Oxide. MujOj. Syn. Sesqui- OXIDB OP MANGANEBK. Found native as "Bran- mite," and readily formed by exposing man- ganons hydrate to the action of air, and drying, or by gently igniting the peroxide brown or black powdei- decomposed by heat. Manganic Peroxide. MnO^. St/n. Pes- MANGANIO OXIDE, BiNOXIDE Off MANOAKESE, Peroxide of manganese, Black oxide of MANGANESE, OxiDE OP MANGANESE, MaN- oanebii oxidum niobum (B. p.), Manqa- KEsii binoxtdum (Ph. L.), Mangamese oxydum (Ph. E.). it is the only oxide of manganese that is directly employed in the arts. It is a very plentiful mineral production, and is found in. great abundance in some parts of the West of England. The manganese of the shop is prepared by washing, to remove the earthy matter, and grinding in mills. The blackest samples are esteemed the best. It is chiefly used to supply oxygen gns, and in the manufacture of glass and chlorine ; in dyeing and to form the salts of manganese. It hns been occasion- ally employed in medicine, chiefly externally in itch and porrigo, made into an ointment with lard. It has been highly recommended by Dr Erigeler in scrofula. Others have employed it as an alterative ami tonic with variable success. When slowly introduced into the system during a lengthened period, it is said to produce paralysis of the motor nerves. (Dr Coupar.) — Dose, 3 to 12 gr., or more, thrice daily, made into pills. Pur. Native binoxide of mancrancse (py- rolusite) is usually contaminated with variable proportions of argillaceous matter, calcium carbonate, ferric oxide, silica, and barium sulphate, all of which lower its value as a source of oxygen, and for the preparation of chlorine. Tlie richness of this ore can, there- fore, be only determined by an assay for its principal ingredient. Assay. There are several methods adopted for this purpose, among which the following recommend themselves as being the most ac- curate and convenient. 1. A portion of the mineral being reduced to very fine powder, 50 gr. of it are put into the liitle apparatns employed for the analysis of carbonates described at page 406, together with about i fl. oz. of cold water, and 100 gr. of strong hvdrochloric acid, the latter con- tained in the little tube (b) ; 50 gr. of crystal- lised oxalic acid are then added, the cork carrying the chloride of calcium tube fitted in, and the whole quickly and accurately weighed or counterpoised ; the apparatus is next inclined so tliat the acid contained in the small tube may be mixed with the other contents of the flask, and the reaction of the ingredients is promoted by the application of a gentle heat ; the disengu<;ed chlorine resulting from the mutual decomposition of the hydrochloric acid and the manganic peroxide converts the oxalic acid into carbonic acid gas, which is dried in its passage through the chloride of calcium tube before it escapes into the air. As soon as the reaction is complete, and the residual gas has been driven offby a momentary ebullition, the apparatns is allowed to cool, when it is again carefully and accurately weighed. The loss of weight in grains, if doubled, at once indicates the percentage rich- ness of the mineral examined in manganic peroxide; or, m^re correctly, every grain of carbonic anhydride evolved represent! 1'982 gr. of the peroxide. 2. (Frcsenius and Will.) The apparatus employed is the ' alkalimeter' figured at page 30. The operation is similar to that adopted for the assay of alkalies, and is a modification of the oxalic acid and sulphuric acid test for manganese, originally devised by M. Berthier, The standard weight of manganic peroxide recommended to be taken by Fresenius and Will is 2 91 grammes, along with 6'5 to 7 grammes of neutral potassium oxalate. The process, with quantities altered to adapt it for employment in the laboratories of these coun- tries, is as follows: — Manganic peroxide (in very fine powder), 50 gr. ; neutral potassium oxalate (in powder), 120 gr. ; these are put into the flask A (see engr., p. 31), alona; with sufficient water to about l-4th fill it ; the fla!>k .^ and /i (the latter containing the sulphuric acid) are then corked air-tight, and thus con- nected iu one apparatus, the whole is accu- rately weighed. The opening of the tube i being closed by a small lump of wax, a little sulphuric acid is sucked over from the fl isk B into the fl;vik A ; the disengagement of oxy- gen from the manganese immediately com- mences and this reacting upon the oxalic acid present, converts it into carbonic anhy- dride gas, which passing through the concen- trated sulphuric acid in the flask B, which robs it of moisture, finally escapes from the appa- ratus through the tube d. As soon as the disengagement of carbonic aiid ceases, the operator sucks over a fresh portion of sulphuric acid, and this is repeated at short intervals, until bubbles of gas are no longer disengaged. The little wax stopper is now removed, and suction is applied at h until all the carbonic acid in the apparatus is replaced by common air. When the whole has become cold it is a?ain weighed. The loss of weight, doubled, indicates the amount of pure manganic per- oxide, in the sample, as before. 3. (Otto.) 50 gr. of the sample reduced to very fine powder are mixed in a glass flask, with hydrochloric acid li fl. oz., diluted with i oz. of cold water, and portions of ferrous sulphate, from a weighed sample, immediately added, at first in excess, but afterwards in smaller doses, until the liquid ceases to give a blue precipitate with red prussiate or potash, or to evolve the. odour of chlorine ; heat being employed towards the end of the process. The 1028 MANGE -MANNACROUP quantity of ferrous sulphate consumed is now ascertained by again weighing the sample. If the peroxide examined was pure, tlie loss of weight will be 317 gr. ; hut if otherwise, the percentage of the pure peroxide may be ob- tained by the rule of three. Thus : suppose only 298 gr. of the sulphate were consumed, then 317 : 100 : : 298 : 94, nnd the richness of the sample would be 94§. The percentage value of the oxide for evolving chloiine may be obtained by multiplying the weight of the consumed ferrous sulphate by •2588, which, in the above case, would give 76g of chlorine. For this purpose, as well as )br chlorometry, the ferrous sulphate is best prepared by precipitating it from its aqueous solution with alcohol, and drying it out of contact with air until it loses its alcoholic odour. Obs, Before applying the above processes it is absolutely necessary that we ascertain whether the peroxide examined contains any carbonates, as the presence of these would vitiate the results. This is readily determined by treating it with a little dilute nitric acid : — if effervescence ensues, one or more carbonates are present, and the sample, after being weighed, must he digested for some time in dilute nitric acid in excess, and then carefully collected on ■• filter, washed, and dried. It may then be assayed as before. The loss of weight indicates the quantity of carbonates present, with snffieient accuracy for technical purposes. The determination of this point is the more important, as these contaminations uot merely lessen the richness of the mineral in pure manganic peroxide, but also cause a considerable waste of acid when it is employed in the manufacture of chlorine. Permanganic Acid. HMnOj. Obtained by distilling cautiously potassium permanganate and sulphuric acid. Dark violet — black li quid, green by reflected light, and rapidly absorb- ing water forming a violet solution. Oxidises organic matter with explosive violence. Permanganate of Barium. Ba (MnO)45. Black soluble prisms, formed by decomposing silver permanganate by means of barium chloride, and cautiously evaporating. Permanganate of Potassium. KMn04. Prep. Potassium chlorate, or nitrate, and potassium hydrate are made into a paste with water, and manganic peroxide added j the mass is dried and heated to redness. The residue is boiled with water, filled through asbestos, and eva- porated down and recrystallised. Dark purple, red, almost black anhydrous long prisms, readily soluble in 16 pints of water. Decomposed in presence of acids by most organic matter. Permanganate of Silver. AgMn04. Frep. Precipitate a strong solution of silver nitrate by means of a concentrated solution of potas- sium permanganate. Small black prisms, soluble in 100 parts of water, with a purple colour. Fermanganateof Sodium. KaMnO^. Obtained as a dark purple lic^uid by passing a current of carbonic anhydride through sodium m^nga- nate. Condy's red fluid is chiefly a sodium permanganate dissolved in water. MAHGE. An eruptive disease, correspond- ing to the itch in man, resulting from the burrowing into the skin of minute animalcules (mites or acari), and common to several do- mestic animals, more especially the dog and horse. Like the itch, it is contagious. The causes are confinement, dirt, and bad living. The treatment should consist in the immediate removal of the cause, the frequent use of soft soap and water, followed by frictions with sul- phur ointment, solution of chloride of lime or sporokton, the administration of purgatives, and a change to a restorative diet. Dun states that in India a very efficient remedy for mange is employed by the native farriers, which con- sists of castor oil seeds well bruised, steeped for twelve hours in sour milk, aud rubbed into the skin, previously thoroughly cleansed with soap and water. "The itchiness disappears almost immediately and the acari are speedily destroyed." A dressing consisting of 1 oz. of chloride of zinc (Burnett's disinfectant fluid) and 1 quart of water may also be applied with advantage. MAN"GEL WUE'ZEL. Syn. Mangold- WUEZEL, HTBEID BEET, RoOT OP SCAECITT. The Beta vulgarit, var. campestris, a variety of the common beet. The root abounds in sugar, and has been used in Germany as a sub- stitute for bread in times of scarcity. In these countries it is chiefly cultivated as food for cattle. The young leaves are eaten as spinach. The percentage composition of mangold wur- zel is as follows : — Flesh-formers (albumenoid bodies), 1"54; heat and fat-formers (sugar, &c.) 8-60; indigestible fibre, 1-12; ash, 0-96; 87-78. MAN'HEIM GOLD. A gold-coloured brass. See GoM) (Dutch). MANTJA Si/n. Manna (B. P., Ph. L., E., & D.), L. A concrete exudation from the stem of Fraxinus ornns and F. rotundifolia, ob- tained by incision. (B. P.) "The juice flowing from the incised bark " of " Fraxinu^ rotundifolia and F. orrnis, hardened by the air." (Ph. L.) The finest variety of this drug is known as flake manna, and occurs in pieces varying from 1 to 6 inches long, 1 or 2 inches wide, and ^ to 1 inch thick. It has a yellowish-white or cream colour; an odour somewhat resembling honey, but less pleasant; a sweet, mawkish taste ; and is light, porous, and friable. It is laxative In doses of 1 to 2 oz. Manna Factitious, made of a mixture of sugar, starch, and honey, with a very small quantity of scaramony to give it odour and flavour, and to render it purgative, has been lately very extensively offered in trade, and met with a ready sale. MAH'NACEOUP. A granular preparation MANNITE— MANURES 1029 of wheat deprived of bran, used as an article of food for eliildren and invalids. (Brande.) MAN'NITE. OjHuO,. Syn. Makna buoab, MrsnBOOM s. ; Mannita, L. A sweet, crys- tallisable aubstiinue, found in manna and in several other vegetable productions. It has been formed artiHc-iallv by the action of sodium- amalgnm upon au alkBlinc solution of cane sugar. Prep. 1. Digest manna in boiling rectified spirit, and filter or decant the solution whilst hot; the mannite crystallises ns the liquid cooU in tnfts of slender, colourless needles. 2. (Ruspini.) Maunn, 61b8. ; cold water (in which the white of an egg has been beaten), 8 lbs. ; mix, boil Tor a few minutes, and strain thesyrupthrough linen whilst hot; the strained liquid will form a semi-crystalline mass on ciioling; submit this to strong pressure in a cloth, mix the cake with its own weight of cold water, and again press it; dissolve the cake thus obtained in boiling water, add n little animal charcoal, and filter the mixture into n porcelain dish set over the fire ; lastly, evapo- rate the filtrate to a pellicle, and set the syrup aside to crystallise. L.irge quadrangular prisms ; perfectly white and transparent. Prop., ^c. Mannite has a powerfully sweet and agreeable taste; dissolves in 6 parts of cold water and about half thiit quantity of boiling water; freely soluble in hot, and slightly so in cold alcohol ; fuses by heat with- out loss of weight; with sulphuric acid it combines to form a new acid compound. It is distinguished from the true sugars by its aqueous solution not being susceptible of the vinous fermentation, and not possessing the property of rotary polarisation. When pure, it is perfectly destitute of purgative proper- ties. It is now extensively imported from Italy, and is chiefly used to cover the taste of nauseous medicines, and as a sweetmeat. UANUEES'. Substances added to soils to increase their fertility. The food of vegetables, as far as their organic structure is concerned, consists entirely of inorganic compounds j and no organised body can serve for the nutrition of vegetables until it has been, by the process of decay, resolved into certain inorganic sub- Ftances. These are carbonic acid, water, and ammonia, which are well known to be the final products of putrefaction. But even when theie are applied to vegetables, their growth will not proceed unless certain mineral suhstanaes are likewise furnished in small quantities, eitljer by the soil or the water used to moisten it. Almost every plant, when burned, leaves ashes, which commonly contain silica, potHssa, and phosphate of lime; often, also, magnesia, soda, sulphates, and oxide of iron. Tiiese mineral bodies appear to be es- sential to the existence of the vegetable tis- sues ; so that plants will not grow in soils de Reprinted from Tnson'i ' Veterinary Fliarmacopoeia.' of sulphate of copper, finely powdered, 1 oz. ; ginger, in' powder, 1 oz.; common mass, 6 oz. ; mix. — Use. Tonic for the horse. — Dose, 6 to 8 dr. Uassa Digitalis Composita. Compound MASS of digitalis. Syn, Cough ball. Prep. Take of Barbadoes aloes, in powder, 2 oz. ; digftalis, 1 oz. ; common mass, 13 oz. ; mix. — Use, For the horse in chronic cough. — Dose, 1 oz. once or twice a day. Moasa Ferri Snlphatis. Mass of sulphate op lEON. Syn, Tonic mass. Prep, Take of sulphate of iron, in powder, 2 oz. ; ginger, in powder, 1 oz. ; common mass, 5 oz. ; mix. — Use, Tonic for the horse. — Dose, 6 to 8 dr. Uassa Besinse Composita. Compound mass of kesin. Syn. Diubetic mass. Prep. Take of resin, in powder, nitrate of potash, in pow- der, hard soap, of each equal parts ; mix.— Use. Diuretic for the horse. — Dose, 1 oz. Uassa Zingiberis Composita. Compound MASS OP QiNOEU. Syn, Cordial mass. Prep, Take of ginger, in powder, gentian root, in powder, treacle, of each equal part'', a Hufficiency ; mix so as to form a mass. — Use, Stomachic for the horse. — Dose, 1 oz. UAS'SICOT. Syn. Masticot, Yellow pbot- OXIDE of LEAD; PlUMBI OXTDUM FLAVUM, Cbeussa oitbina, L. The dros-i that forms on melted lend exposed to a current of air, roasted until it acquires a uniform yellow colour. Artists often apply the same name to white lead roasted until it turns yellow. Used as a pigment. UAS'TIC. Syn, Mastich, Gum mastic ; Mastiche, L. The " resin flawing from the incised bark of Pistaeia Lentiscus, var. Chia," (Ph. L.) It occurs in pale yellowish, trans- parent, rounded teara, which soften between the teeth when chewed, and giving out a bitter, aromatic taste. Sp. gr. 107. It is soluble in both rectified spirit and oil of tur- pentine, forming varnishes. It is chiefly used aa a ' masticatory,' to strengthen and preserve the teeth, and perfume the breath. Mastic. Fine mortar or cement u»ed for plastering walls, in which the ingredients, in a pulverulent state, are mixed up, either en- tirely or with a considerable portion of linseed oil. It sets very hard, and is ready to receive paint in a few days. See Cements. MASTICA'IIOi)'. The act of chewing food, by which it not only becomes comminuted, but mixed with the saliva, and reduced to a form fit for swallowing. It has been justly regarded by the highest authorities as the first process of digestion, and one without which the powers of the stomach are over- tasked, and often performed with difficulty. Hence the prevalence of dyspepsia and bowel complaints among persons with bad teeth, or who 'bolt' their food without chewing it. UAS'IICATOBIES. Syn. Masticatobia, L. Substances taken by chewing them. They are employed as intoxicants, cosmetics, and 1034 MASTICOT— MATCHES raedicinals ; generally with the first intention. The principal masticatory used in this country is tobacco. In Turkey, and several otlier Eastern nations, opium is taken in a similar manner. In India, a mixture of areca nut, betel leaf, and lime, performs the same duties ; whilst in some other parts of the world pre- parations of the cacao are employed. As cos- metics, orris root, cassia, cinnamon, and sandal wood are frequently chewed to scent the breath. Among medicinala, mastic and myrrh are frequently chewed to strengthen the teeth and gums ; pellitory, to relieve the toothache; and rhubarb, ginger, and gentian, to relieve dyspepsia and promote tlie appetite. Prep. 1. (Augustin.) Mastic, pellitory (both in powder), and white wax, of each 1 dr. ; mixed by heat and divided into 6 balls. In tootliaclie, loose teeth, &c. 2. (W. Cooley.) Mastic, myrrh, and white wax, of each 1 part; rhubarb, ginger, and extract of gentian, of each 2 parts ; beaten up with tincture of tolu, q, s., and divided into boluses or lozeng'es of 10 gr. each. One or two to be chewed an hour before dinner ; in dyspepsia, defective appetite, &c. 3. (Qnincy.) Mastic, 3 oz. ; pellitory and stavesacre seed, of each 2 dr.; cubebs and nutmegs, of each 1 dr. ; angelica root, i dr. ; melted wax, q. s. to make it into small balls. As a stimulant to the gums, and in toothache. 4. Opium, ginger, rhubarb, mastic, pellitory of Spain, and orris root, of each 1 dr. ; melted spermaceti, q. s. to mix; for 6-gr. pills. As the last, and in toothache and painful gums, MASTICOT. See Massicot. MATCHES (Cooper's). Syn. Sweetenino MATCHES. These are made by dipping sti'ips of coari-e linen or canvas into melted brimstone. For use, the brimstone on one of them is set on fire, and the match is then at once sus- pended in the cask, and the bung loosely set in its place. After the lapse of 2 or 3 hours the match is removed and the cask filled with liquor. Some persons pour a gallon or two of the liquor into the cask before ' matching ' it. The object is to allay excessive fermentation. The operation is commonly adopted in the Western Counties for cider intended for ship- ment, or other long exposure during transport. It is also occasionally employed for inferior and ' doctored ' wines. . MATCHES (Instantaneous light). Of these there are several varieties, of which the one best known, and most extensively used, is the common phosphorus match, known as the ' con- greve ' or ' Inciter.' ' We need not describe ' The origiiwl 'lucifkrs,' or 'i.tbiit-beaeing MAiciiKS,' invented in 1826, conaieted of strips of paste- boiinl, oi- flat splints of wood, tipped first wiih sulphur, aiid,tlifn with a mixture of sulpliide of Hntimony and cliloriite of poUssa, and were ignited hy drawing tliem brtikly through foldeiJ glass-paper. Tliey required a con- Biderahle effort to ignite tlieni, and fhe compusition was opt to be torn off l»y the violi-nce of the friction. Tlie terrn ' lucifer' havinir become familiar, «as applied to tlie simpler and miire effective match afterwards introduced under the names of 'coftcKhVE' and 'co^GEEVE light,' the 'chemical matches,' 'phosphorus bottles,' and ' prometheans,' in use during the early part of the present century, as these are quite obsolete. We will simply sketch the general process of manufacture now in use for phos- phorus matches : \Januf. The wooden splints are cut by steam machinery from the very best quality of pine planks, perfectly dried at a temperature of 400° Fahr, English splints are of two sizes — ' large' and 'minnikins;' the former 2i inches longer, and the latter somewhat shorter. In the manufacture donble-lengths are used, so that each splint may be coated with the igniting composition at both ends, and then cut asunder in the middle to form two matches. In England the splints are usually cut square in form, but in Germany they are cylindrical, being prepared by forcing the wood through circular holes in a steel plate. The ends of the double splints having been slightly charred by contact with a red- hot plate, are coated with sulphur by dipping them to the requisite depth in the melted ma- terial. In some cases the ends are saturated with melted wax or paraffin instead of sulphur. The splints are then arranged in a frame between grooved boards in such a manner that the prepared ends project on each side of the frame. These projecting ends are then tipped with the phosphorus composition, which is spread to a uniform depth of about -I inch on a smooth slab of stone, kept warm by means of steam beneath. Wlien partially dry, the tipped splints are taken from the frames, cnt through the middle, and placed in heaps of 100, ready for ' boxing,' The different compositions for tipping the matches in use in different countries and fac- tories all consist essentially of emulsions of phosphorus in a solution of glue or gum, with or without other matters for increasing the combustibility, for colouring, &c. In England the composition contains a considerable quantity of chlorate of potassa, which imparts ti snapping and flaming quality to the matches tipped with it, and but little phosphorus, on account of the moisture of the climate. In Germany the proportion of phosphorus used is much larger, and nitre, or some metallic per- oxide, replaces chlDrate of potassa. The Ger- man matches light quietly with a uiild lambent flame, and are injured quickly by damp. The following formulffl have been selected: 1. (Enolish.) Fine glue, 2 parts, broken into small pieces, and soaked in water till quite soft, is added to water, 4 parts, and heated by means of a water bath until it is quite fluid, and at a temperature of 200° to 212° Fahr. The vessel is then removed from the fire, and phosphorus, IJ to 2 parts, is gra- dually added, the mixture being agitatid briskly and continually with a ' stirrer ' having wooden pegs or bristles projecting at its lower end. When a uniform emulsion is obtaintd, chlorate of potassa, 4 to 5 parts, powdered MATfi— MATURATION 1035 glass, 3 to 4 p irts, nnd red lead, smnlt, or other f uluuring mutter, ii sulticiciit quantity (all in a stiite of very fiue powder) arc ndilcd, one at 11 time, to prevent accidents, and the stirring contiuuud until the mixture is comparatively cool. Aicordingf to Mr G. Gore, the above propor- tions arc those of the best quality of English composition. The matches tipped with it dellagrate with a snapping noide. {See above.) 2. (German.) — a. (BOttger.) Dissolve gum Arabic, 16 parts, in tlie least possible quiintity of water, add of phosphorus (in powder), 9 parts, and mix by trituration ; then add of uitre, 14 pnrts ; Vermillion or binoxide of man- ganese, 16 parts, and form the whole into a paste, as directed above ; into this tlie matches are to be dipped, and then exposed to dry. As soon as the matches arc quite ilry they are to be dipped into very dilute copal varnish or lac varnish, and again exposed to dry, by which means they are rendered waterproof, or at least less likely to suli'er from exposure in damp weather. b. (Bijttger.) Glue, 6 parts, is soaked in a little cold water for 24 hours, after wliich it is liqnelied by trituration in a hciited mortar; phosphorus, 4 parts, is now added, and rubbed down at a heat not exceeding 150° Fuhr. ; nitre (in iine powder), 10 parts, is next mixed in, and afterwards red ochre, 6 parts, and smalt, 2 parts, are further added, and the whole formed into a uniform paste, into which the matches are dipped, as before. Cheaper than the last. 0. (Diesel.) Phosphorus, 17 parts ; glue, 21 piirts; red lead, 24 parts; nitre, 88 parts. Proceed as above. Obs. Matches tipped with the above (a, h, and o) inflame without fulmination vvlien rubbed against a rough surface, and are hence termed ' noiseless matches ' by tlie makers. 3. (Safety matches.) The latest improve- ment of note in the manufacture of matches is that of Laudstrom.of Jonkoping, in Sweden, adopted by Messrs Bryant and May (Patent). It consists in dividing the ingredient of the match-mixture into two separate compositions, one being placed on the ends of the splints, as usual, and the other, which contains ihe phos- phorus, being spread in a thin layer upon the end or lid of the box. The following are tlie compositions used by the patentee: — a. (For the splints.) Chlorate of potassa, 6 parts; sul- phuret of antimony, 2 to 3 parts ; glue, 1 part. — 4. (Kor the friction surface.) Amorphous phosphorus, 10 parts; sulphuret of antimony or peroxide of manganese, 8 parts; glue, 3 to 6 parts ; spread thinly upon the surface, which has been previously made rough by a coating of glne and sand. By thus dividing the composition the danffcr of Are arising from ignition of the matches by acciilcntal friction ii< avoided, as neither the portion on the splint nor that on the box can be ignited by rubbing against an unpre- pared surface. Again, by using the innocuous red or amorphous pho'pborus, the danger of poisonini,' is entirely prevented. MATE. Syn. Paraguay Tea. This is the dried leaf of a small shrub, the Ilex Para- gaayenaei, or Bnizilian holly, growing in Paraguay and Brazil; by the inhabitants of which places, as well as S'luth America gene- rally, it is largely employed in the form of » beverage as tea. Its active ingredient. Para- guaine, formerly supposed to be a distinct principle, has from further researches into its composition been discovered to be identical with theine and cati'eine — the alkaloids of tea and coffee. Mr Wanklyn ascribes the following compo- sition to mate : — Moisture ... Ash .... Soluble organic matter . Insoluble organic mutter 6-72 5-86 2510 62-32 10000 IIATE"BIA UED'ICA. A collective name of the various substances, natural and arti- ficial, employed as medicines or in the cure of disease. In its more extended sense it includes the science which treats of their sources, pro- perties, classification, and applicHtiuns. The materia medica of the Pharmacopaia is a mere list, with occasional notes, " embracing the animal, vegetable, and chemical substances, whether existing naturally, prepared in offi- cinal chemical preparations, or sold in whole- sale trade, which we (the College) direct to be used either in curing diseases or in preparing medicines." (Ph. L.) MAT'ICO. Syn. Soldikk'shebb ; Mateco (B.P., Ph. D.); Matica, Heeba matice, L. The dried leaves of a Peruvian plant, gene- rally believed to be the Artanihe elongata, one of the Piperaieie. The leaves have been em- ployed. with considerable success as a mecha- nical external styptic; applied to leech-bites, sliglit cuts, and other wounds &c., and pressed on with the fingers, they seldom fail to arrest the bleeding. Matico has also been much lauded as an internal astringent and styptic, in lioemorrhages from the lungs, stomach, bowels, uterus, &c. ; but as it is nearly destitute of astringent properties, its virtues in these cases must have been inferred from its external ac- tion. As an aromatic, bitter stimulant, closely resembling the peppers, it has been proposed as a substitute for cubebs and black pepper, in the treatment of diseases of the mucous membranes, piles, &c. — Dose, i to 2 dr. ; in powder ; or under the form of infusion, tinc- ture, or boluses. MATUEA'TIOIT. Growing ripe. Amongst surgeons this term is applied to the process of suppuration, or that which succeeds inflamma- tion, and by which pus or matter is collected in an abscess. Warmth, irritation, and a liberal diet promote this change; cold, seda- 1036 MEAD— MEASURE tives, and depletion, retard it. The maturation of fermented liquor is noticed under BfiEWiN a, MAtT LiQUOES, Wines, &o. MEAD. Syn. Mellina, L. An old English liquor, made from the combs from which the honey has been drained, by boiling them in water, and fermenting the saccharine solution thus obtained. It is commonly confounded with metheglin. Some persons add 1 oz. of hops to each gallon ; and, after fermentation, a little brandy. It is then called sack mead, See METHEaLiN. JIEAIi. The substance of edible grain ground to powder, without being bolted or sifred. Barley meal and oat meal are the common substances of this cIbss in England. In North America the term is commonly applied to ground Indian corn, whether bolted or not. (Goodrich.) The four resolvent meals of old pharmacy {quatuor farina resolventes) are those of barley, beans, linseed, and rye. HEALS. The "periods of taking food, usually adapted, in conformity with conveni- ence and the recurrences of hunger, are those which are best adapted to the purposes of health ; namely, the morning meal, the midday meal, and the evening meal." " That these are the proper periods for meals is evident from the fact of their maintaining their place amid the changes which fashion is constantly Introducing." " If we look at these periods in another point of view, we shall find an interval of four hours left between them for the act of digestion and subsequent rest of the stomach. Digestion will claim between two and three hours of the interval; the remaining hour is all that the stomach gets of rest, enough, per- haps, but not too much, not to be justly in- fringed." (Eras. Wilson.) HEA'SLES. Syn. Rubeola, Moeeilei, L. This very common disease is characterised by feverishness, chilliness, shivering, head-pains, swelling and inflammation of the eyes, shed- ding of sharp tears, with painful sensibility to light, oppressive cough, difficulty of breath- ing, and sometimes vomiting or diarrhoea. These are followed about the fourth day by a crimson rash upon the skin, in irregular cres- cents or circles, and by small red points or spots, which are perceptible to the touch, and which, after four or five days, go off with des- quamation of the cuticle. The fever, cough, &c., often continue for some time; and unless there have been some considerable evacuations, either by perspiration or vomiting, fcbey fre- quently return with increased violence, and occasion great distress and danger. Treat, When there are no urgent local symptoms, mild aperients, antimonial diapho- retics, and diluents, shonld be had recourse to; but when the Inflammatory symptoms are emergent, and the lungs are weak, especially in plethoric habits, blood may be taken. The cough may he relieved by expectorants, demul- cents, and small doses of opium ; and the diar- rhoea by the administration of the compound powder of chalk and opium ; the looseness of the bowels, however, had better not be inter- fered with, unless it be extreme. Measles are most prevalent in the middle of winter, and though common to individuals of all ages, are most frequent amongst children. The plethoric, and those of a scrofulous habit, or one which has a syphilitic taint, suffer most from them. Like the smallpox, the measles are conta- gious, and seldom attack the same person more than once during life. See Rash MEASURE. Syn. Mehsttka, L. The unit or standard by which we estimate extension, whether of length, superficies, or volume. The following tables represent the values and proportions of the principal measures employed in commerce and the arts :— Table I. English Lineal Measures. Incites. i'eet. Yards. Poles. FuTlongB. Miles. 1- •083 •028 ■00505 •00012626 •0000157828 12- 1- •333 •06060 •00151515 •00018939 36- 3- 1- •1818 •004515 •00056818 198- 16-5 5-5 !• •025 •003125 7920- 660- 220- 40^ !• •125 63360- 5280- 1760- 320^ 8^ 1^ •** The unit of the above table is the yard, of which no legal standard has existed since that established by the statute of 1824 was destroyed by the fire which consumed the two Houses of Farliameut in 1834. MEASURE Taois II. Eaglith Meamira of Superficiet. 1037 Squire Feat. Square Yards. Polci. Kooda. Acre*. 1^ 9- 272-25 10890- 43560- •1111 1- 80-25 1210- 4840- •00367309 •0330579 1- 40- 160- •000091827 •000826448 •025 1^ . 4^ •000022957 •000206612 •00625 •25 1^ TlBlB III. English Measure of Volume. — The Ihpebial Standabd, and the relative value of its divisions, including those used in Medicine, milk their eqcitalehtb «» avoirdupois and troy weight. in «^ f3 0. Oij. c. Minima Eqnivnlentj in or drops. Fluid Drucliiiii. Fluid Ouncea. Pints. Quarts. Gallons. Pecks. Busliels. Quarters. diltlUed tcater, at 62" Fnljr., in Trny Avoird 1- -016g6l!66 -00208333 •00010416 •00006-208 -00001 SOS grains. wtiglit -91146 60- 1- -136 •00626 -003126 -00078125 _ __ 64 f,S75 It. or. 481)- 8- 1- -05 -025 •00026 ^ __ _ 437-6 1 9600- IfiU- 20- 1- -6 -135 -0625 -016626 ■001953125 876(1- 1 4 192()0- »20- 40- 3" 1- ■35 -125 ■03125 -0U391I625 17500- 3 8 76800 15»U- 161)- 8- 4- 1- •6 125 •OI6G25 " 70000- 10 SoOO- ,SJO- 16- 8- 3- 1- •35 -03135 20 1-280- 64- 33- 8- 4- 1- -126 _ 80 512- 256- 64- 3.. 8- 1- — 640 •#• The standard unit of the above table is the gallon, which is declared, by statute, to be capable of " containing ten pounds avoirdupois weight of distilled water, weighed in the air at the temperature of 62° Fahr., the barometer being at 30 inches." The pound avoirdupois contains 7000 grains, and it is declared that a cubic inch of distilled water, under the above conditions, weighs 252-458 grains ; hence the capacity of the imperial gallon and its divisions are as follows : — Imperial gallon = 277-274 cubic inches. „ quarts = 69-3185 „ „ pint = 34-65925 „ Fluid ounce = 1-73296 „ „ drachm ■= -21662 „ t+t The imperial gallon is l-5th larger than the old wine gallon, — l-60th smaller than the old beer gallon, and — l-32nd larger than the old dry-measure gallon. Table IV. French Metrical or Decimal Measures of Length. Names. Eq, in Metres. Equivalents in English Inches, at 32°falit. English Lonf; Measure, at 62° FaLr. Millimetre . . . CeDlimetre . . . D^cim^tre . . . Metre DecumMre . . . Huctometro • • . Kilometre . , . Myrianiitre . . . •001 •01 •1 1^ • 10^ 100^ 1000^ 10000- . . -03937 . . -39371 . . 3-93708 . . 39-37079 .' . 393-70790 . . 3937-07900 . . 39370-79000 . 393707-90000 Miles, l-ur. Ids. Feet. Inch. 1 3-37 10 2 9-7 109 1 1078 4 213 1 10-3 6 1 156 9-17 •«• The standard unit of the above table is the mfetre, which has been determined to be 89-37079 ioclics. at 32° Fahr. (Capt. Kater) ; the English foot is taken at 62" Fahr. The true length of the m^tre, reduced to the latter temperature, is 89-370091 English inches ; a number 1038 MEAT which varies from that in the table only at the fourth decimal figure. It will be perceived that the principle of nomenclature adopted in applying the names, was to prefix the Greek numerals to the decimal maltiples, and the Latin numerals to the decimal subdivisions. Table V. French Mefrical or Decimal Measures of Volume. Names. Eq. in Litre,. ^I' '" ^S '''•''"= Equivalent in Engliaii Measures. GttU. Fiats. 0». Dr. Minims. Millilitre .... ■001 •0610 16-9 Centilitre . •01 •6103 2 49- Decilitre . •1 61028 3 4 10-36 Litre . . 1- 61-028 1 15 1 43-69 Decalitre . 10- . 610-28 2 1 12 1 16-9 Hectolitre 100- . 6102-8 22 1 4 49- Kilolitre . 1000- . 61028- 220 16 6 40- Myrialitre 10000- .610280- 2201 (= 2754 busheh). *,* The standard unit in the above table is the litre, or the cube of the t'j of a mfetre. Tlie French centiare contains 1 square m^tre, — the are, 100 do., — the hectare, 10,000 do. The old Paris piiit is equal to 1-678 English imperial pint. ■^+t The capacity of solids and aeriform fluids is taken in cubic inches, or feet, in England. In France, the stere, or m^ti-e cube, equal to 35-31658 English cubic feet, is the standard unit. Table VI. Miscellaneous Measures and their Equivalents t Tea or coffee spoonful Dessert „ . Table „ . Wine-glassful . Tea-cupful . . Breakfast-cupful Tumblerful . . . Basiuful .... Thimbleful Pinch (of leaves and flowers) Handful „ „ Cubic inch of water, at 62° Fahr, „ foot „ „ Line Barleycorn Hand Chain . (average) = 1 fl. dr. 2 „ 4 „ 2 fl. oz. 5 ,. 8 .. 8 „ 12 „ ifl. dr. Idr. 10 „ 252-458 gr. 62-32106 lb. : inch. = 4 poles or 22 yards. MEAT. The muscular tissue or flesh of the principal animals constituting the food of man may be said to be composed of the same proximate principles, and, given an equal digestibility and power of being assimilated, may be also said to have au equally nutritive value. Since meat, however, is generally eaten with a certain amount of fat, which accompanies it in varying quantity, the capacity of the meat for forming muscle will, of course, be in inverse proportion to the amount of fat it contains; on the contrary, its power of raising the bodily temperature will be in direct pro- portion. Moleschott (quoted by Parkes) gives the following as the mean composition of fresh beef, as determined by all the Conti- nental chemists : — Water . " . . . , 73-4 Soluble albumen and hsematin . 2-25 Insoluble albuminous substances 15-20 Gelatinous substances . . 3'30 Fat 2-87 Extractive matter . . . 1-38 Creatiu 0-068 Ash 1-6 Dr Parkes remarks of the amount of fat given in the above analysis " that it is evi- dently too low. In the above table we recognise in the albu- minous and gelatinous substances the source of the muscular tissue of the human organism. The ash contains the chlorides, carbonates, and phosphates of potassium, sodium, and calcium. From these salts are derived the MEAT 1039 hydrochloric acid of the gastric juice, the so- dium of the bile, and the calcium phosphate and carbonate of the skeleton. Iron is also present, and this finds its way into the blood. The flavour of meat is much inftiienced by the food of tlie animal. The flesh of the Pampas pig is found to be rank and disagree- able when the animal is killed in its wild state ; il', however, the food be changed for the better, the flesh becomes altogether different and quite eatable. The pork of pigs fed on flesh is said to give off a strong odour, the fab at the same time being unusually soft. Soft fat is also said to form in animals that have been fed on oily foods. When meat is roasted, the fire gradually coagulates the albumen of the joint, the coagu- lation commencing at the surface, and spread- ing by degrees to the interior. Unless the roasting be continued long enough, sufficient heat will not reach the parts nearest the centre to eflect their coagulation ; and it' under these circumstances the meat be removed from the fire, the uncoagulated or inner parts will pre- sent the well-known red and juicy appearance known as ' underdone.' Although a certain quantity of the gravy (which consists of the soluble and saline ingredients) escapes in the process, the greater part is retained. The brown agieeably sapid substance formed on the outside of the nio.vt is known as osmozome, and which is concentrated gravy. The melting fat which collects below forms the dripping. The loss in the meat is principally water. The chemical effects of boiling are explained under the article devoted to that sulyect. Meat generally loses from 30 to 40 per cent., and sometimes as much as 60 per cent, in weight, by cooking. Tiie amount of hone varies, being seldom lees than 8 per cent. It amounts in the neck and brisket to about 10 per cent, and from one third to sometimes half the total weight in shins and legs of beef. The most economical parts are the round and thick flank, next to these the brisket and stickiog-piece, and lastly, the leg. In choosing mutton and pork, selection should be made of tlie leg, after this of the shoulder.' " Oxen," says M. Bizet, "yield of best qua- lity beef 57 per cent, of meat, and 43 per cent. \NHste. The waste includes the internal vis- cera, &c. Second quaUty of beef, 54 per cent, meat and 46 per cent, waste; third quality beef, 51 per cent, meat and 49 per cent, waste. In milking-cows, 46 per cent, meat and 54 per cent, waste. Calves yield 60 per cent, meat, and 40 per cent, loss ; and sheep yield 50 per cent, meat, and 50 per cent, loss." Dr Parkes differs from Bizet as to the latter's value of the ment of the calf. He says the flesh of young animals loses from 40 to 50 per cent, in cooking. It seems to be agreed, however, that animals * Letlifby. when slaughtered shonid be neither too young nor too old. The flesh of young animals, although more tender, is less digestible than that of older ones ; it is also poorer in salts, fat, aud an albuminous substance called ayn- tonin. Consumption of Heat. Dr Letheby, writing in 1868, says that in London "the indoor opera- tives eat it to the extent of 14"8 oz. per adult weekly ; 70 per cent, of English farm labourers consume it, and to the extent of 16 oz. per man weekly j 60 per cent, of the Scotch, 30 of the Welsh, and 20 of the Irish also eat it. The Scotch probably have a larger allowance than the English, considering that braxy mutton^ is the perquisite of the Scotch labourer ; but the Welsh have only an average amount of 2 J oz. per adult weekly j and the Irish allowance is still less. It is difficult to obtain accurate returns of the quantity of meat consumed in Loudon; but if the computation of Ur Wynter is correct, it is not less than SOJ oz. per head weekly, or about 4i oz. per day for every man, woman, and child. In Paris, ac- cording to M. Armand Husson, who has carefully collected the octroi returns, " it is rather more than 49 oz. per head weekly, or just 7 oz. a day." Bondin states that through- out France the consumption is about 50 grammes daily, or under If oz. Dr Letheby, in his work ' On Food,' gives the following as the characteristics of good meat : — " 1st. It is neither of a pale pink colour nor of a deep purple tint, for the former is a sign of disease, and the latter indicates that the animal has not been slaughtered, but has died with the blood in it, or has suffered from acute fever. "2nd. It has a marked appearance from the ramifications of little veins of fat among the muscles. " 3rd. It should be firm and elastic to the touch, and should scarcely moisten tlie fingers — bad meat being wet, and sodden and flabby, with the fat looking like jelly or wet parch- ment. " 4th. It should have little or no odour, and the odour should not be disagreeable, for dis- eased meat has a sickly cadaverous smell, and sometimes a smell of physic. Tliis is very dis- coverable when the meat is chopped up and drenched with warm water. "5tli. It shonid not shrink or waste much in cooking. " 6lh. It should not run to water, or become very wet on standing for a day or so, but should, on the contrary, dry upou the surface.^ " 7th. When dried at a tempevature of 212" or thereabout, it should not lose more than from 70 to 74 per cent, of its weight, whereas bad meat will often lose as much as 80 per cent. „ J , " Other properties of a more refined ctia- racter will also serve for the recognition of bad ' See further on. 1040 MEAT meat, as that the juice of the flesh is alkaline or neutral to test-paper, instead o{ being dis- tinctly acid, and the muscular fibre, when ex- amined under the microscope is found to be sodden and ill-defined." Unsound meat — diseased meat. Dr Letheby , in his ' Lectures on Food,' published in 1868, states that the seizure and condemnation, in London, of meat unfit for human food, during a period extending over seven years, amounted to 700 tons per annum, or to about l-750th of the whole quantity consumed. These 700 tons he dissects into lbs. as follows : — " 805,653 lbs. were diseased, 568,375 lbs. were putrid, and 193,782 lbs. were from animals that had not been slaughtered, but had died from accident or disease. It consisted of 6640 sheep and lambs, 1025 calves, 2896 pigs, 9104 quarters of beef, and 21,976 joints of meat." He admits, however, that this amount, owing to the difficulties and Inefficiency of the mode of supervision, bears a very insignificant proportion to the actual quantity which escaped detection, and which was, therefore, partaken of as food. Professor G»mgee says that one fifth of the meat eaten in tlie metropolis is diseased. In 1863 the bodies of an enormous number of animals suffering from rinderpest, as well as from pleuro-pneumonia, were con- sumed in London ; and we know that thou- sands of sheep die every year, in the country, of rot; the inference from which latter fact is that, since the carcases are neither eaten there nor buried on the spot, they are sent up to, and thrown upon, the London markets. The worst specimens find their way to the poorer neigh- bourhoods, where, as might be expected, their low price ensures a ready sale for them. These sales, it is said, mostly take place at night. The above statements, which, if we exclude Professor Gamgee's figures, do not solve the problem as to the quantity of unsound meat con- sumed in London, not unreasonably justify the assumption that it is very considerable ; and this being admitted, we should be prepared to learn that it was a fertile source of disease of a more or less dangerous character. There is, however, such extensive divergence in the various data bearing upon this point, that no satisfactory solution of it can be said to be afforded. Thus, Livingstone states that, when in South Africa, he found that neither Englishmen nor natives could partake of the flesh of animals affected with pleuro-pneumonia without its giving rise to malignant carbuncle, and sometimes, in the case of the natives, to death, and Dr Letheby attributes the in creased number of carbuncles and phlegmons amongst our population to the importation from Holland of cattle suffering from the same disease. On tlie contrary, Dr Parkes says he was informed, on excellent autliority that the CafEres invariably consume the flesl: of their cattle that die of the same epidemic, without tlie prodnction of any ill effects. Ag.iu, there are numerous well-attested cases in which the flesh of sheep which have died from hraxy (a disease that makes great ravages amongst the flocks in Scotland) is con- stantly eaten without injurious results by the Scotch shepherd. The malady causes death in the sheep from the blood coagulating in the vital organs, and the sheep that so dies becomes the property of the shepherd, who, after re- moving the offal, is careful to cut out the dark congealed blood before cooking it.' Sometimes he salts down the carcase. In cases, however, where thorough cooking or an observance of the above precautions have been neglected, very dangerous and disastrous consequences have ensued. During the late siege of Paris large quantities of the flesh of horses with glanders appear to have been eaten with no evil consequences : and Mr Blyth, in his ' Dic- tionary of Hygifene,' quotes a similar case from Tardieu, who states that 300 army horses affected with glanders (morve) were led to St Germain, near Paris, and killed. For several days they served to feed the poor of the town without causing any injury to health. A similar exemption from any evil effect following the consumption of diseased flesh is recorded by Professor Brucke, of Vienna. Not many years since the cattle of a locality in Bohemia, being attacked by rinderpest, were ordered by the Government to be slaughtered, after which they were buried. The poor people dug up the diseased carcases, cooked the meat, and ate it, with no injurious result. Parent Duchitelet cites a case where the flesh of seven cows attacked with rabies was eaten without injury ; and Letheby states that pigs with scarlet fever and spotted typhus have been used for food with equally harmless results. The flesh of sheep with smallpox had been found to produce vomiting and diarrhoea, sometimes accompanied with fever. One obvious suggestion of the immunity from disease recorded in part of the cases above given is that the injurious properties of the flesh had been destroyed by the heat to which it had been subjected in the process of cook- ing, combined with the antiseptic and protec- tive power of tlie gastric juice. The subject, however, has not been sufficiently examined to warrant the conclusion that every kind of unsound meat niny be rendered innocuous by culinary means. But even were this so the idea of partaking of meat which had once been unsound, from whatever cause, and, as in the instances above quoted, with the pustules of smallpox, the spots generated by typhus, and the rash of scarlet fever upon it, becomes unspeakably re- pulsive and revolting. But we must not be misled because of the difficulty of reconciling the contradictory statements above given, nor by the evidence some of them appear to afford as to the innocuous character of diseased meat, since it is just possible that closer and more 1 Letheby. MEAT 1041 prolongpil observation of the facts may have led to diflVi'unt conclusiooa, Tlius, lor ex- aiapte, pork, iiifpsted with that formidable I'lituzouii, the Trichina firalit, had been par- taken of for years, under the impress on that it WHS a perfectly healthy food, until Ur Zencker, of Dresden, diKcovered that the para- site was the cau^e of a frightful disease, which he called Triohinoaia, and which had hitherto baffled all attempts to find out its origin. Dr Lctheby, writing on this subject, says ; " I have often iiad occasion to investigate cases of mys- terious disease, which had undoubtedly been caused by unsound meat. One of these, of more than ordinary interest, occurred in the month of November, 1860. The history of it is this : — A forcquarter of cow-beef was pur- chased in NcH-gate Market by a sausirge- maker who lived in Kingsland, and who im- mediutt'ly converted it into sausage-meat. Sixty-six persons were known to have eaten of that meat, and sixty-four of them were at- tacked with sickness, diarrhoea, and great prostration of vital powers. One of them died ; and at the request of the coroner I made a searching inquiry into the matter, and I ascertained that the meat was diseased, and that it, and it alone, had boeif the cause of all the mischief."' Here are two instances in which but for subsequent investigation the evil effects nar- rated would nut have been debited to dis- eased meat, but to some other cause. One of the principal and by far the most prolific sources of food-poisoning is the sausage, the eating of which, in Germany more pur- ticularly, has caused the death of a numbei' of persona. The sausages in which these poisonous qualities occasionally develop themselves are the largo kinds made in Wurtemburg, in which district alone they have caused the deaths of more than 150 out of 400 persons during the last fifty years. The poisonous character of the sausage is said to develop itself generally in the spring, when it becomes musty, and also soft in the interior. It is then found to be acid to test paper, and to have a very disagreeable and tainted flavour. Should it be eaten when in this state, after from about twelve to twenty-four hours the patient is attacked with severe intestinal irritation in the form of pains in the stomach and bowels by vomitings, and diarrhoea. To these symptoms succeed great depres. Bion, coldness in the limbs, weak and irregular pulse, and frequent fainting fits. •• Should the sufferer be attacked with convulsions, and difficult respiration, the seizure generally ends in dentil. The nature of the poisonous sub- stance that gives rise to these effects in the sausage has not yet been determined. Liebig believed them to be due to the presence in the meat of a particular animal ferment, which he conceived acted on the blood by catalysis, * Letheby, ' Lectures on Food,' LongniAii sad Co. TOL. U. and thus rendered it diseased. Others have surmised that a poisonous orgardc alkaloid may have been produced in the decaying meat; and others again that the effects may have been caused by some deleterious substance of a fatty nature. M. Van den Corput was of opinion that the mischief was due to the pre- sence in the meat of a poisonous fungns, which he calls a aarcina botulina. This hist theory receives support from the fact that a peculiar mouldiness is always to be observed in these dangerous sausages, and that this is coincident with the development of their poi- sonous qualities. Several effects have been produced by other kinds of animal food — as veal, bacon, ham, salt-beef, salt-fish, cheese, &c., and the food has usually been in a decayed and mouldy con- dition. It would be tedious if I were to detail, or even to enumerate the eases recorded by medico-legal writers ; but I may perhaps refer to a few of them. In 1839 there was a popu- lar f^te at Zurich, and abuut 600 persons par- took of a repast of cold roast veal and ham. In a few hours most of them were suffering from pain in the stomach, with vomiting and diarrhoea ; and before a week had elapsed nearly all of them were seriously ill in bed. They complained of shiverings, giddiness, headache and burning fever. In a few cases there was delirium, and when they teiminated fatally there was extreme prostration of the vital powers. Careful inquiry was instituted into the matter, and the only discoverable cause of the mischief was incipient putrefac- tion and slight mouldiness of the meat." A case is recorded by Dr Geisler of eight persons who became ill from eating bacon which was mouldy ; and another by 5l. OUivier of the death of four persons out of eight, all of whom had partaken of partially decomposed mutton. If some of the foregoing statements fail to demonstrate that the act of partaking of diseased meat is a necessary source of danger to health, there can be no such doubt as to the pernicious and perilous consequences which ensue when meat is consumed contain- ing in its tissues the ova and larvse of certain parasitic creatures. If the fleshy part of a piece of measly pork be carefully examined, it will be found to be more or less dotted about with a number of little bladder-like spots, in size about as large as a hemp-seed.^ If now we carefully rupture one of these little bodies or cysts, there will be found in it a minute worm, which under the microscope will be seen to have a head from which pro- ceed a number of little hooks that perform a very disagreeable office should the parasite be taken into the human stomach by any one making a meal oft' measly and undercooked pork. For, then, being liberated from its sac, or nidus, by the action of the gastric juice of the stomach on this latter, the creature passes > See article " Cjsticerci." 66 1042 MEAT into the intestines. To these it attaches itself by means of the booklets on its head, and instantly becomes a tupevvorm.wbicti grows by a succession of jointed segments it is able to develop, and each one of which is capable of becoming a separate and prolific tapeworm filled with countless eggs. These eggs reach the land through the agency of manure (for they are found in the intestines of the horse), and from this source they get into the stomachs of pigs and oxen, where they hatch not into tapeworm, or tenia, but, travelling through the animal's stomach, burrow into its muscular tissue. Here they establish and envelop themselves in the little cyst or small bladder-lilie substance, whose presence, as explained, constitutes the condi- tion called " measly" pork, and here they remain dormant until such time as, taken into the stomach, they may again become tape* worms, to be again expelled and to perpetuate by their ova the round of metamorphosis. From the circumstance of their being met with enclosed in little sacs or cysts, these parasites have been termed Cysticerci. The variety of them we have just been considering as occurring in pork is called the Cystieercus eellulosce, whilst the tapeworm to which it gives rise is known as the Tinea solium: Another variety of Ch/sticercus is met with in the flesh of the ox, the cow, and the calf. In the human body this also develops into a tape- worm called the Tinea mediocanellata: Tape- worm is a very common disease in Bussia and Abyssinia, and its prevalence is no doubt due to the habit of giving the children in those countries raw meat to suck, under the impres- sion that the child is strengthened in conse- quence. From experiments made by Dr Lewis it was found that a temperature of 150° F., maintained for five minutes, was suffi- cient to destroy these cysticerci. Another and more formidable entozoon, communicable by unsound meat, is the JEeii- nococcus hominis,^ which represents one of the metamorphoses of the Tinea echinococcus, the tapeworm of the dog. In Iceland, where a sixth of the population are said to suffer from the ravages of the Echinococcus hominis, it is ■the custom to feed the dogs on the flesh of -slaughtered animals affected witli this parasite, which in the body of the dog develops into a tapeworm. The innumerable eggs which the worm produces are, however, incapableof being "hatched in the dog's intestines. They have to find another and more suitable habitat, and tliisas secured for them as follows : — Segments of the tapeworm, with their countless ova, being voided with dog's excrement, fall into ■the running water, and on to the fields and pastures, whence they gain their entrance into the«tomachs of human beings, oxen, and sheep. Hereithe eggs become hatched, not into tape- worms, ihut into JSlcMnococci hominis, or pro- spective tapeworms. Burrowing through the ' ' See article '• Echinococcus hominis." membranes of the stomach, the echinococcns establishes itself most commonly in the liver, but not unlrequently in the spleen, heart, lungs, and even the bones of man. In the animal economy they enclose themselves in little sacs or cysts, and give rise to the most alarming and painful diseases, which hitherto have proved incurable. They attack the brain in sheep, and are the cause of the disease known as " staggers." Sheep are also infested by another parasite known as the JDistoma hepatica, the ravages of which give rise in the sheep to that devastating disease — " the rot." The creature is also known by the name of the " liver-fluke," since it principally at- tacks this important organ in the animal. The liver-fluke is of constant occurrence in the livers of diseased sheep, and unless destroyed by thorough, cooking will of course pass into the human economy. Tlie embryo fluke gains admission to the sheep's body through the instrumentality of small snails, to the shells of which it attaches itself. In wet weather the snails crawl over the grass of the meadow which forms the pastures of the sheep, and are swallowed by it. Once in the sheep's stomach the embryo becomes a fluke, and commences its depredations on the animal's liver. After this, the reason why the rot attacks sheep after a continuance of wet weather will be evident. The most terrible of all the meat parasites is a minute worm about ^^t^ of an inch long, found in the flesh of pork. This creature, which is named the Trichina spiralis (from the form it assumes when coiled up in the little cyst or capsule which encloses it), when it gets conveyed into the human stomach with impro- perly cooked or underdone pork, soon becomes liberated from its confinement owing to the destruction of its envelope by the gastric juice. Once in the stomach the parasite grows rapidly, giving birth to innumerable young trichincB, which, by first boring through the membranes of the alimentary canal, pierce their way through the different parts of the body into the muscular tissue, where they become encysted, and where they remain until conditions favorable to their liberation again occur. Until such time, however, as they have become enclosed in the cyst, their movements give rise to indescribable torture, and to a disease known as trichinosis, of which it has been estimated more than 50 per cent, of those attacked by it die. The symptoms of trichi- nosis commence with loss of appetite, vomit- ing, and diarrhoea, succeeded after a few days by great fever — resembling, according to Dr Aitken, that of typhoid or typhus. As might be expected the pains in the limbs are extreme. Boils and dropsical swellings are not unusual concomitants of the malady. Hitherto this frightful disease has been mostly confined to Germany, where there have been several outbreaks of it since its discovery MEAT, AUSTRALIAN— MEAT EXTRACTS 1043 in 1860 by Dr Zenckcr. Feidler says that only free triohina ure killed by a temperRture of 155° P.; and that when they are in their cysts a greater heat may be necessary. From what has been said the importance of efficient cooking muat become manifest. There must always be rifk in underdone pork, whether boiled or roasted. In the pig, the trichina, if present, may always be found in the muscles of the eye. In Germany the makers of pork saa^uges are now said to have these muscles subjected toa microscopicexamination previous to using the meat, which, of course, is rejected if the examination has been unfavorable. The tricliinoe, if present in the flesh of pork, may be seen as small round specks by the naked eye, the surrounding flesh itself being rather darker than usual owing to the inflam- mation set up in it. All doubt, however, on this point may be removed by having recourse to the microscope. Dr Parkes says a power of 60 to 100 diameters is sufficient, and that " the best plan is to tiike a thin slice of flesh, put it into liquor potasi^te (1 part to 8 of water), and let it stand for a few minutes till the muscle becoini'S clear; it must not be left too long, otlierwise the trichinsB will be destroyed. Tlie white Specks come out clenrly and the worm will be seen coiled up. If the capsule is too dense to allow tiie worm to be seen, a drop or two of weak hydrochloric acid should be added. If the meat be very fat a little etiier or benzine may be put on it iu the first place." Legislation relative to meat inspection and seizure. — The law recognising the importance of the supply of pure and wholesome meat gives considerable powers to the difl!erent sani- tnry oflicers who are appointed to inspect it. See Food, Inspkctiok of. MEAT, AUSTRALIAN. See Meat pre- SEEVINO. MEAT BISCUITS. Prep. 1. The flour is mixed up with a rich fluid extract of meat, and the dough is cut into pieces and baked in the usual manner. 2. Whoaten flour (or preferably the whole meal), 8 parts ; fresh lean beef or other flesh (minced and pulped), 2 parts; thorouglily in- corporate the two by hand-kneading or ma- chinery, and bake the pieces in a moderately heated oven. Both the above are very nutri- tious ; the last more especially so, 1 oz. makes a pint of good soup. MEAT, COLO, to Stew. Let the cold meat be cut into slices about half an inch thick. Take two large-sized onions, and fry them in a wine- glass of vlnei^arj when done, pour them on to the meat; then place the whole in a stewpan, and pour over sufficient water to cover it. After stewing about half an hour add sufficient flour and butter to thicken the gravy, and also pepper, salt, and ketchup, to flavour ; then let it simmer gently for another lialf an hour. St'rve up with a little boiled rice around it. MEAT EXTRACTS. Some preparations of this nature have been already noticed under the heads Essence and Exteact ; the follow- ing are additional and highly valuable for- mulse: — Prep. 1. (Dr Breslan.) Young ox-flesh (free from fat) is minted small, and well beaten in a marble mortar, at flrat alone, and afterwards with a little cold or lukewarm water; the whole is then submitted to the action of a press, and the solid residuum is treated in the same manner, with a little more cold water; the juice (reddish in colour) is now heated to coagulate the albumen, strained, and finally evaporated in a wiiter b-ith to the consistence of an extract. As ordinary flish contains only 1« of kreatine, while that of the heart, according to Dr Gregory, contains from l'87g to 1'415, this is the part employed by Dr Breslan. The product possesses an agree- able odour and taste ; and is easily soluble in water. 2. (Falkland.) Fresh lean beef (or other flesh), recently killed, is minced very fine, and digested, with agitation, in cold water, 1 pint, to which hydrochloric acid, 6 drop-j, and com- mon salt, 1 dr., Iiave been added ; after about an hour the whnlc is thrown upon a fine huir sieve, and the liquid jiortion allowed to drain oft without pressure, the first portions that pass through being returned until the fluid, at first turbid, becomes quite clear and trans- parent ; when all the liquid has passed through, cold Wiiter, J pint, is gently poured on, in small portions at a time, and allowed to drain throngh into that previou^ly collected. The product is about } pint of cold extract of flesh, having a red colour, and a pleasant, soup-like taste. It is administered cold to the invalid — a teacupf ul at a time, and must on no account be warmed, as the application of ev.n a very slight heat causes its decomposition and the separation of a solid mass of coagulated albu- men. This cold extract of flesli is not only much more nutritious than ordinary beef tea, but also contains a certain quantity of the red colouring matter of blood, in which there is a much larger proportion of the iron req\iisite for the formation of blood-particles. The li\dro- chloric acid also greatly facilitates the process of digestion. This formula is a modification of the one recently roeonimended by Liebig for the preparation of n highly nutritive and restorative food for invalids. 3. (ExTRACTrM Sanqtiinis botib— Dr Mauthner.) Pass fresh blood (caught from the slaughtered animal) through a sieve, evaporate it to dryness in a water bath, and when cold rub it to powder. — Dose, 10 to 20 gr., or more, per diem, in a little water. Obs. The above preparations are intended to supersede the inefficient compounds— beef tea, meat soups, &c. — during sickness and con- valescence. JIM. Bicslau and Mauthner de- scribe their extracts of flesh and blood as being peculi:irly advantageous in scrofulous exhaustion, exhaustion from ansemia, diar- 1044 MEAT rhoea, &c. The extract of Falkland or Liebig is represented as having been employed both in the hospitals and in private practice at Munich with the most extraordinary success. It is said to be capable of assixnilation with the least possible expenditure of the vital force. Meat, Fluid. This preparation consists of lean meat, in which the albumen has been changed so as to be non-coagulable by heat, and the fibrin and gelatin from their normal insoluble condition to one admitting of their being dissolved in water. lu tliis soluble condition, the first stage effected in stomach digestion, the several bodies are known as peptones or albuminose, and the proportion of their simple constituents remains the same as in ordinary fibrin, albumen, and gelatin. The alteration is effected by finely mincing meat and digesting it with peptone, hydro- chloric acid, and water, at a temperature of about 100° Fahr., until dissolved. The solution is then filtered, the bitter prin- ciple, formed during the digestion, removed by the addition of a little pancreatic emulsion, and the liquor, which has been neutralised by the addition of carbonate of soda, evaporated to a thick syrup or extractive consistence. Fluid meat is the only preparation which entirely represents, and yields the amount of nourishment afforded by, lean meat ; it differs altogether from beef tea and extracts of meat, as all these contain only a small portion of the different constituents of meat. A patent has been granted to its inventor, Mr Darby. Meat, Liebig's Extract of. Syn. Extkaot OF Flesh, Exteaotum cakno. This prepa- ration is an aqueous infusion evaporated to the consistence of a thick paste, of those prin- ciples of meat which are soluble in water.' It is chiefly composed of alkaline phosphates and chlorides, a nitrogenous crystalline base known as kreatine, various extractive matters, which it has been surmised may have origi- nated in the decomposition of certain nitro- genous bodies, and possibly of a small quantity of lactic acid, as it contains neither albumen nor fibrin, two of the most important and nutritious ingredients of fiesh ; it must not, therefore, be regarded as a concentrated form of meat. Liebig says that it requires 34 lbs. of meat to yield 1 lb. of this extract — a statement which, as Dr Pavy justly remarks, shows how completely the substance of the meat which constitutes its real nutritive por- tion must be excluded. This absence of direct nutrient power, now admitted by physiologists, whilst disqualifying the extract as a sub- stitute for meat, does not, however, preclude its use in certain cases of indisposition requiring the administration of a stimulant or restora- tive, in which circumstances it has been found a useful and valuable remedy, and has been suggested as a partial substitute for brandy ' " Altered as they te by the Application of Heat." Deane and Brady, ■ Fharmaceutical tfournal,' Oct. 1866. where there is considerable exhaustion or weakness, accompanied with cerebral depres- sion and lowness of spirits. In this latter respect its action seems analogous to strong tea. In the vast pastures of Australia and the pampas of South America are countless herds of oxen and sheep, whose numbers far exceed the food requirements of the comparatively sparse population of those districts. The fat, horns, hoofs, bones, skins, and wool of these cattle, which form the chief part of the wealth of those countries, are exported principally to Europe. Until within a few years, however, no means had been adopted for the utilisation of the superfluous flesh of the animals, beyond employing it as a manure. By manufacturing it, however, into " extract of meat," this waste has been remedied, and immense works for its preparation are now erected both in South America and in Australia. The process fol- lowed by the different makers, although vary- ing in some particulars, is essentially the same, and consists in extracting by water, either hot, cold, or in the form of the steam, those portions of the meat which are soluble in that fluid, and subsequently evaporating the solution so ob- tained until it becomes of a proper consistence to be put into jars. The extract so obtained keeps well (if all the fat and gelatin are, re- moved), and is most conveniently adapted for exportation. It is said that the extract as being obtained from cattle that have had English progenitors possesses a flavour supe- rior to that which comes from South America, where the animals are of a different and inferior bi:eed. The following interesting description of the manufacture of " Liebig's Extract of Meat" is taken from the Buenos Ayres ' Standard * of September, 1867. The establishment, of which it is a description, is at Fray Bentos, on the Uruguay, South America. " The new factory is a building which covers about 20,000 square feet, and is roofed in iron and glass. We first enter a large flagged hall, kept dark, cool, and extremely clean, where the meat is weighed, and passed through apertures to the meat- cutting machines. We next come to the beef- cutting hall, where are four powerful meat- cutters, especially designed by the company's general manager, M. Geibert ; each machine can cut the meat of 200 bullocks per hour. The meat being cut is passed to ' digerators ' made of wrought iron j each one holds about 12,000 lbs. of beef; there are nine of these dig- erators, and three more have to be put up. Here the meat is digerated by high-pressure steam of 75 lbs. per square inch ; from this the liquid which contains the extract and the fat of the meat proceeds iu tubes to a range of ' fat se- parators ' of peculiar construction. Here the fat is separated in the hot state from the extract, as no time can be lost for cool operation, other- wise decomposition would set in in a very short time. MEAT PRESERVING 1045 _ " We proceed downgtaire to an iminense hall, •ixty feet high, where the fat separators are working ; below them is a range of five cast- iron elariflcrs, 1000 gallons each, worked by high-pressure steam through Hallet's tube lystein. " Each clarifier is proWded with a very in- genious steain-tap. In the monstrous clari- fiers the albumen, fibrin, and phosphates are separated. From hence the liquid extract is raised by means of air-pumps, driven by two thirty horse-power engines, up to two vessels about twenty feet above the clarifiersj thence the liquid runs to the other large evaporators. Now we ascend the staircase reaching the hall, where two im- mense sets of lour vacuum apparatus are at work, evaporating the extract by a very low temperature; here the liquid passes several filtering processes before being evaporated in vacuo. \Ve now ascend some steps and enter the ready-making hall, separated by a wire gauze wall, and all the windows, doors, Ac, guarded by the same to exclude flies and dust. The ventilation is maintained by patent fans, and the place is extremely clean. Here are placed five ready-making pans constructed of steel plates, with a xystem of steel discs revolving in the liquid extract. " These five pans, by medium of discs, 100 in each pan, effect in one minnte more than two million square feet evaporating surface. " Here concludes the manufacturing process. The extract is now withdrawn in large cans and deposited f'lr the following day. " Ascending a few steps we enter the decrys- tallising and packing hall, where two large cast-iron tanks are placed, provided with hot water baths under their bottoms; in these tanks the extract is thrown in quantities of 10,000 lbs. at once, and here decrystallising is made a homogeneous mass and of uniform quality. Now samples are taken and analysed by the chemist of the establishment, Dr Seekamp, under whose charge the chemical and technical operations are performed. " It may be mentioned that the company's butcher killed at the rate of 80 oxen per hour; separating by a small double-edged knife the vertebrse, the animal drops down instantaneously on a waggon, and is conducted to a place where ISO men are occupied dress- ing the meat for the factory, cutting each ox into six pieces ; 400 are being worked per day." Mr Tooth at a meeting before the " Food Committee " lield at the Society of Arts in January, 1868, said that he did not claim any difference in the composition of his article (which was made in Australia) as compared with that made by the South American Company. In the annexed table the composition of some of the extracts of meat of commerce is given: — Liebig's Conipaoy. Tooth, Sydney. Frencli Company, South America. While- head. Twenty- man. Water .... Extractive, soluble in al- cohol Extractive, insoluble . Mineral matter 18-56 45-43 18-93 22-08 16-00 53-00 13 00 18-00 17-06 51-28 10-57 21-09 16-50 28-00 46-00 9-50 24-49 22-08 44-17 8-96 20-81 13-37 59-10 6-72 100-00 100-00 100-00 100-00 100-00 ! 10000 The following are the characteristics of ex- tract of meat of good quality. It should always have an acid reaction, its colour sho\ild be a pale yellowish brown, and it should have an agreeable meat-like odour and taste. It should be entirely soluble in cold water, and should be free from albumen, fat, and gelatin. Meat Pie. Stew 2 lbs. of beef steak with one small onion, the gravy from which is to be thickened with flour, and flavoured with pepper and salt. Put it into a baking dish, and cover with a lard crust. It should be baked for one hour. The addition of two kidneys willgreatly improve the pie. Meat (Australian) Pie. Take 2 lbs. of Aus- tralian meal, or IJ lb. of meat and J lb. of kidney. Season to taste, pour in a little water, cover with a lord crusit, and bake not more than half an hour. MEAT PRESERVING. " The Belgian ^fuse'e de I'Industrie notes the following methods of preserving meat; as the most deserving of attention amongst those communicated to the French Academy of Sciences, and published in the Comptes Sendus. 1. M. Bundet's method, by which the meat is kept in water acidulated with carbolic acid in the proportion of 1 to 5 parts of acid per 1000 of water. A series of experiments proved that all kinds of meat could thus be kept fresh for lengthened periods, without acquiring an ill taste or odour. " The meat may be placed in barrels or air- tight tin cpies, filled with acidulated water of the strength above specified, and headed up ; or the pieces may be packed in barrels or cases in alternate layers with charcoal, pounded small, and saturated with water containing ^^j_ of carbolic acid. The charcoal serves as a vehicle for the antiseptic fluid, and as an absorbent of any gaseous matters given ofl" by 1046 MEAT PRESERVING the meat. The latter should he wrapped in thin linen covers to prevent the charcoal work- ing its way into the tissues. "This method, it ia suggested, might be employed in curing pork in place of ' salting,' or of the more lengthy and costly process of 'smoking;' and also tor the preservation of poultry, game, butter, eggs, &e. " 2. In the case of South American meat M. Baudet proposes the use of large sacks of caoutchouc. The meat should be packed in them, with alternate layers of charcoal as above described, and each sack, when fiUed, should be hermetically closed by drawing another empty caoutchouc sack, cap-wise, over it. The caoutchouc, it is supposed, would fetch enough in the market — its low price notwithstanding — to cover expenses of packing and freight, and so permit the meat to be sold in Europe at a very small advance on cost price. If intended for use a second time, the empty bags should be steeped in boiling waterfor a few minutes, to re- move any organic impurities adhering to them. " 3. M. Gorge's method, which is in use in La Plata, consists in washing and drying the meat, and afterwards steeping in successive waters containing hydrochloric acid and sul- phite of soda, and then packing it in air-tight cases holding 1, 5, or 10 kilog. each. Meat thus treated requires to be soaked in warm water for about half an hour before use. " 4. M. Leon Soubeiran has recommended braying and drying, in the fashion adopted by the Chinese and itfougols, as described by M. Simon, French consul in China, in a coinmu- nication made by him to the Soci^te d'Accli- matation. The pemmican of our Arctic voyagers and the charqui of South America are familiar examples of meat preserved by analo- gous processes. The late M. Payen, a distin- guished member of the Academy, insisted upon the great perfection to which this system might be carried by the aid of hot-air stoves and suit- able apparatus." Besides the foregoing, numerous patents have from time to time been taken out, and processes proposed for the preservation of meat ; so as to enable it to be sent from those distant countries, such as South America, Australia, Canada, &c., where it is greatly in excess of the wants of the population, to other lands, in which the supply is as much below the demand, and the meat at such a price as to preclude its being regularly used as an article of food by the body of the people. As the putrefactive changes set up in dead flesh are dependent upon the combined in- fluences of moisture, air, and a certain tempe- rature, it follows that most of the various methods of meat preservation resolve them-, selves into so many different efforts to remove the meat from the operation of one of the con- ditions above specified as necessary for its decomposition. The okarqui or jerked beef of South Ame- rica affords an example of meat preserved by means of being deprived of moisture. It occurs in thongs or strips which have been prepared by placing freshly killed meat between layers of salt and drying them in the sun. Charqui, although it retains its soundness for a great length of time, and is rendered eat- able by soaking in water and prolonged cook- ing, is difficult of digestion and wanting in flavour, and if any fat be associated with it, this is liable to become rancid. Pemmican is meat which, after being dried and powdered, is mixed with sugar and cer- tain spices, both of which assiist to preserve the meat as well as to improve its flavour, and to remove the tendency to rancidity caused by any fat that may be accidentally present. Another process for the preservation of meat by means of desiccation is that of MM. Blu- menthal and Chollet, who, in ISSi, obtained a patent for preparing tablets composed of dried meat and vegetables, which, after being several times dipped into rich soup, were dried in warm air after each immersion. At a meeting of the Food Committee, held at the Society of Arts, in May, 1868, specimens of dried beef and mutton in powder, from Brisbane, were shown by Mr Orr, who said they had been dried on tinned plates by means of steam. Dr A. S. Taylor, P.R.S., who exa- mined the sample, found it perfectly fresh and good. It had been prepared at least six months previously. At a subsequent meeting, the Committee reported that the soup prepared from this desiccated meat, with the addition of «. small quantity of vegetables, was considered very successful, and the Committee were of opinion that meat so preserved was likely to prove a valuable and cheap addition to the food re- sources of the people. The specimen from which the soup was made had been in the Society's possession, and formed part of the contents of a tin opened upwards of two years ago. The preservation was perfect. We have only space briefly to describe some of the more jirominent of the processes which have been devised for the preservation of meat by excluding atmospheric air. Mr Tallerman, a large importer of Aus- tralian meat, stated in evidence before the Pood Committee of the Society of Arts, in May, 1870, that in the preservation of the meat he sent over to this country he had recourse to a very old practice, which was that of packing the joints in fat, the meat being previously salted or cured. Instead of the meat being packed in brine, the casks with the meat are filled up with melted fat. In Mr Warrington's patent, which dates from 1846, it is proposed that animal sub- stances shall be preserved by enveloping them in a layer of glue, gelatin, or concentrated meat gravy, or otherwise by dipping them in warm solutions of such substances, or by wrapping them in waterproof cloth, or by MEAT PRESEUVINO 1047 covering them with caoutchouc, giitta perchR, or varnish, or thin criani of pluxtrr of Paris, which when mt wiis suturuted witli melted suet, wax, or stfiirin. Tlie pu tent of Prof. Ked wood, which resemblpB Mr Warrington's in eeeliing to exclude at- mospheric air by surrounding the meat with an imperviouR substance, claimed tl>e use of p»rai&n for this purpose, the par»ffin being ufternards coated with a mixture of gelatin and treacle, or gelatin and glycerin. The paraffin is easily removed from the meat by plunging this latter into boiling water, whiih dissolves the outer coating of gelatin mixture, and at the same timcmelts the paraffin and liberates the enclosed joint. Messrs .Tunes and Trevethick's patent con- sistcil in exhausting of air the vessel contain- ing the meat, then forcing into it a mixture of nitrogen and sulphurous acids, and subse- quently soldering the apertures. Ur Letheby says meat, fish, and poultry preserved in this manner have been found good after seven or eight years; and specimens of them were exhibited in the London Exhibition of 18(i2. The removal, however, uf atmo^pheric air from the vessels containing the meat it is designed to preserve is now principal^ ac- complished by means of steam. The germ of this idea originated with M. Pierre Antonie Angilbert more than half a century ngo, but the modification of Angilbert's process, which in principle is that generally adopted by the importers of Australian and Snuth American cooked meat, as well as by the l<)nglish preparers of the article, originated with Messrs Goldner and Wertheimer, nearly forty years since, and, briefly, is as follows : — The Ireshly killed meat is placed in tins, with a certain quantity of cold water. The tins and their contents are then securely soldered down, with the ex- ception of a small opening not larger than a pin-hole, which is left in the. lid. The tins are next placed in a bath of chloride of cal- cium, the effect of which is to heat the water in them up to the boiling point, and after a certain time to more or less cook the ment contained in them. When the meat is thought to be sufficiently cooked, and whilst the steam arising from the boiling water is escaping from the aperture, this last is carefully soldered down, the steam not only having driven out all the atmospheric air from the vessel, but in the act of escaping having prevented the in- gress of any from without. To still further guard against the entrance of air, the tins are covered over with a thick coating of paint. Previously to their being allowed to leave the preserving works they are tested by being placed for some time in an apartment in which the temperature is sufKcieutly high to set np putrefactive action in the meat if any air has been left in the tins, the evidence of which would be the bulging out of the tins, owing to the liberation of certain gaseous products of dicomposilion. When no diatensiin from in- side takes place, the result is considered satis- factory, and the vessels are regarded as pro- perly and hermetically sealed. In some eases the vessels, instead of being heated in a bath of chloride of calcium, are exposed to the action of steam. If the operation be success- fully performed, the meat so prepared will keep perfectly good and sound for years. Mr Kichard Jones effects the removal of the air from the vessels containing the meat as follows :— The meat is put into the tins and entirely soldered up, with the exception of a small tube about the size of a quill, which is soldered on the top of the tin. This tube is placed in connection with a vacuum chamber, and the air exhausted from the tin by means of it. In cooking the meat be also employs a chloride of calcium bath. Dr Letheby, in one of his Canton Lectures on Pood, delivered in 1865, speaking on this part of the subject, and on the above method of meat preservation, says : — " To-night, through the kindness of Messrs Crosse and Blackwell, I am able to show you a specimen of preserved mutton which has been in the case forty-four years, and you will perceive that it Is in excil- lent condition. It formed part of the stores supplied by Messrs Dunkin and Gamble, in 1824, to His Majesty's Exploring ship Fury, which was wrecked in Prince Regent's Inlet in 1825, when the cases were landed with the other stores, and left upon the beach. "Eight years afterwards, in August, 1833, they were found by Sir John Ross in the same condition as they were left ; and he wrote to Mr Gamble at the end of that year, saying, ' that the provisions were still in a perfect state of preservation, although an- nually exposed to a temperature of 92° below and 80° above zero.' Some of the cases were left untouched by Sir John Ross ; and after a further interval of sixteen years the place was visited by a party from Her Majesty's ship Investigator, when, according to a letter from the captain. Sir James Ross, ' the pro- visions were in excellent condition, after hav- ing lain upon the beach, exposed to the action of the sun, and all kinds of weather, for a period of nearly a quarter of a century.' Messrs Crosse and Blackwell have placed the original letters in my hands for perusal, andthey show beyond all doubt that meat preserved in this manner will keep good for nearly half a century — in fact, the case of boiled mutton now before you has been preserved for forty- four years." The generality of the samples of preserved meat from Australia are excellent in quality and flavour,' except that in most cases the' meat has been overcooked, which has arisen * The "Food Committee of the Society of Arts, who have CHretnlly and impartially examiaed uumeroua samples of AuBlraliaa and South Aniericsii preserved mrat, say : "It is perlertly sweet and fresh, hut somewhat insipid from overeookinv, and it srema hkely the flavour could he improvrd if the duration of exposure to heat could be shortened without eadangering the preservation." 1048 MEAT PRESERVING from the too prolonged contact of the meat with the steam, which it is judged necessary shall he generated iu such quantities as to en- sure the certainty of the exclusion of the air. Another inconvenience attending the process, viz. the liability of the sides of the tin to collapse, owing to tfte vacuum formed in its interior, has been remedied by the introduc- tion into the vessel of some inert gas, such as carbonic acid, or nitrogen. Preserved meat at the present time forms a very considerable article of export both from Australia and South America. In the former country there are several establishments of a colossal character, where the work of tinning the meat is carried on, in many of which establishments hundreds of cattle are slaugh- tered daily. The, largest establishments of the kind are at Sydney and Melbourne, whence extensive shipments are being constantly made. The following figures are taken from the Board of Trade returns : — Valve of Meat preserved otherwise than ly Salting, ImportB from Total Australia. Imports. 1871 . . £481,093 . £610,228 1872 . . 657,945 . 816,463 1873 . . 557,552 . 733,331 1874 . , 509,698 . 757,001 1875 . . 249,611 . 592,196 Since 1876 tinned meat has been imported from North America. Several methods have been proposed for the preservation of meat by subjecting it to such conditions that the surrounding temperature should be sufficiently low to arrest putrefac- tion. In Mr Harrison's process the reduction of temperature was effected by the application of melting ice and salt, made to run down the outside of the iron chambers containing the meat. It is affirmed that although the joints submitted to this treatment were solidly frozen, no loss of either flavour or immediate decompo- sition of the meat took place. Mr H arrison's ex- periment wfis perfectly successiul in Australia, but broke down during the voyage of a large cargo of meat shipped from Australia in 1873, owing to a defect in the construction of the ice chamber of the vessel and the failure of the supply of ice. Of other forms of refrigeration applied for this purpose we may mention the process of M. Tellier, by which he proposes to place (on ship-board or elsewhere) joints of meat in a chamber through which a current of air charged with ether or other volatile substance may be passed, with a view to reduce the temperature to 30° P. Also that of M. Pog- giale, from whose report to the Paris Aca- demy of Medicine it appears that in cham- bers contrived on principles similar to M. Tellier's, all kinds of butcher's meat and poultry have been hung for ten weeks, at the end of which time they were found perfectly fresh and wholesome. The agent used in the latter case for the production of cold was methylic ether. The process, however, of refrigeration which has proved not only the most, but in every re- spect successful, was first satisfactorily carried out since 1876, in which time large cargoes of dead meat have been constantly sent to our metropolitan markets, as well as to Glasgow, from New York. The following extract from the 'Dundee Advertiser" gives some interesting details of this process : — " As to dead meat, the first sale was held on the 5th of June, when 100 carcases of beef and 72 of mutton were disposed of. Since then there has never been a smaller supply, and on the average about 150 carcases have been sold weekly. Last week 210 carcases were sold, and on Wednesday evening there were no fewer than 33 lorries, each laden with three tons of butcher's meat. The freight paid for carriage to Glasgow, Liverpool, and London, last week amounted to £1900. Altogether, since the importation began, a million and a quarter pounds of dead meat have been sold in Glasgow. The result of this importation has been a reduction in retail price of Id. per lb., ijistead of an increase in price, which must have taken place without the increased supply. " The oxen are collected chiefly in the states of Illinois and Kentucky. They are there reared in enormous numbers on the prairies. Before they reach New York they are driven over railway for fully a thousand miles. Those animals the carcases of which are to be sent to this country are killed the day before the departure of the steamer. As soon as the carcases are dressed they are put into a cool- ing room capable of containing 500, and subject to a constant Current of cold air, sup- plied by means of a 25 horse-power engine. This sets the beef and extracts the animal heat. Each carcase i^ next cut into quarters,and these are sewn up in canvas, and during the night transferred on board the vessel. Six of the Anchor Line mail steamers have been fitted up with refrigeration compartments, constructed on a patented principle specially for the con- veyance of meat. " After the quarters have been bung up in the room the door is hermetically closed. Adjoin- ing the compartment is a chamber filled with ice. Air tubes are connected with the beef room, and through tliem the animal heat as- cends, and by means of a powerful engine it is blown across the ice, and returned to the beef room iu a cold state. A temperature of about 38° is thus maintained in the beef-room. If it were to get so low as 32° — freezing- point — the meat would be seriously injured.' The heat i«, therefore, regulated by a ther- mometer, and when the temperature gets too low, the speed of the engine is slackened, the normal degree of cold being thus maintained ^ Mr Harrison's experimeats make this statement doubtful. MEAT PRESEnVINQ— MECONIC ACID 1049 almost without variation dnrinfi; the voyage. C'atlle killed on Thoisdny in New York are •old that day fortnight in GlnBgow." The firat patent for the preservation offood by means of ico was granted to Mr John Ling in 1845. Lastly, mention mast not be omitted of another method for the preservation of meat, which consists in the application to it of cer- tain antiseptic substances, the action of which in preventing putrefaction is due to their power of destroying minute parasitic organixms of low animal or vegetable life, that would otherwise attack and set up decomposition in the meiit. Our ordinary salted meats owe their immunity from decay, as is well known, to the presence in their tissues of common fait. Meat preserved, however, bv this means is tough, indigestible, and wanting in many of its most important soluble constitu- ents, wliicli, dissolving part of the salt, run off from the meat and are lost. Amongst other agents which have been found serviceuble as antiseptics, and for which from time to time numerous patents have been taken out, are nitrate of potash, acetate and hydrochlorate of ammonia, the sulphates of soda and potash, and bisulphate of lime. The writer remembers purtaking, some years since, of some Canadian turkey, which had been preserved by moans of this latter sub- stance, and the turkey having been killed some two months before being eaten. It was perfectly sound and of excellent flavour. In this instance the bird had been sent from Canada, witli several others, packed in water- proof casks, filled up with a weak solution of bisulphite of lime. In some cases the saline solution is mcnly brushed over the outside of the meat; whilst in others it is injected into the substance of the flesh. Thiebierge's process consists in dipping the joints for five minutes into dilute sulphuric acid, of the strength of about ten of water to one of acid. Tlie me?it after being ttiken out is carefully wiped and dried, and is then hung for keepiu'f. Sulphurous acid also forms the subject of several patents for the preservation of meat. In the process of Laury, for which a patent was taken out in 1854, the gas was introduced into the vessels containing the food. In that of Belford, for which a provisional specifica- tion was granted the same year, the meat was soaked for 24 hours in a solution of sulphurous and hydroi-hloric acids (the latter beins in the proportion of a hundredth of the volume of the former). The addition of the h\ dro- chloric acid was made with the intention of decomposing any alkaline sulphites that might be formed by the combination of the alkaline salts of the meat with the sulphur- ous acid. Dr Dewar's process, which is very similar to the foregoing, proposes, instead of exposing the meat to sulphurous acid fumigation, to immerse it in a solution of the acid of the same strength as that of the British Pharmaco- poeia. On being taken out of the liqnid the meat, or other article, is, as speedily as possible, dried at a temperature not exceeding 140° P., so that the albumen may be preserved simply in a desiccated, and n . Tr. AriiicEe .... Tr. CamphorsB Co. . „ Digitalis . „ Ergotse „ Ferri Perchloridi • ., Opii . „ Seillse „ Valerian. Ammon ' Uug. Cetacei . „ Hydrargyri . „ „ Ox. Rub. „ Siilph. . ,, Zinci Vin. Colrhici „ Ipecac. . Zinci Sulpbatis Desiccated Soup LIta. oz. dr. 8 6 6 4 6 2 3 All pills to he made and marked 5 grains. Fil. Aloes cum Myrrb& . . 2 doz. „ Col. c. Hyoscy . . . 4 „ „ Hydrarg. . , , 3 „ „ Ipecac, cum Scill^ . . 5 „ „ Quiniee . . . . 6 „ ,, Sapon. Co. . . . 6 „ Medical Stores, Lint 10 oz. Tow 1 lb. Adhesive Plaster ... 3 yds. Male Syringe .... 1 „ Glass ... 1 Fcmnle 1 Pliials (assorted) ... 2 doz. Phial corks . . . . 6 „ Sponges 3 Bed-pan 1 Paper of Pins .... 1 Hernia I'rusfi, 36 in., reversible. 1 Paper of Pill Boxes ... 1 Gallipots 6 Leg and Arm Bandages . . 6 Ciilico 3 yds. Flannel Bandages, 7 yds. long, 6 in. wide .... 2 Flnnnel 2 yds. Triangular Bandages, base 48 in., sides 33 in. . . each 2 fMinim Measures +1 oz, t2oz 2 1 1 1 4 yds. 1 ., tSet of Splints . ■j-Waterpi-oof sheeting . toiled Silk t Enema Syringe and Stomach Pump 1 •j-Bnx of Small Scales and Weights 1 ■j-Wedgwood Mortar and Pestle . 1 „ Funnel ... 1 tSpatulas 2 fAuthorised Book of Directions for Medicine Chests ... 1 tBriti^h Pharmacopoeia . . 1 + One set only of these articles reqnired, IrrespectiTe of nutiilier ol paaseni^ers. N.B.— Only one set of inslTumenta required, without regnrd to the numher ot surgcuua, pusaeugerB, or the length ot the voyage. 1052 MEERSCHAUM— MERCURIAL DISEASE 1 Tenaculum. 1 Artery Forceps. 1 Operating ditto. 1 Finger Knife. u 1 Curve Bistoury, Probe Point. 6 1 Curve Bistoury, Spear Point. a; 2 Probes. 1 Silver Director. (S 1 Caustic Case. a 1 Scissors. hH 1 Spatula. 12 Needles. 1 Skein Ligature Silk. 3 Lancets. 1 Amputating Saw. 2 „ Knives. 1 Bone Forceps. 3 Tooth „ Instruments. 1 Skull Forceps. 1 Trephine. 1 Elevator. 1 Hey's Saw. 1 Trephine Brush. 2 Scalpels. 1 Hernia Knife. 2 Trocars and Canulas. 1 Aneurism Needle. 1 Hernia Director. 1 Tourniquet. 2 Silver Catheters (Nos. 4 and 8). 4 Elastic Gum Catheters (Nos. 3, 6, and 7). 1 Clinical Thermometer; 1 Hypodermic Syringe. 1 dozen charged Tubes for Vaccination. 1 Set of Midwifery Instruments. MEER'SCHAUM. Syn. Eoumb de meb, L. A native silicate of magnesia. It has a sp. gr. ranging between 2'6 to 3'4 ; is readily acted on by acids, and fuses before a powerful blow- pipe into a white enamel. The finest quali- ties are found in Greece and Turkey. Its principal a)iplication is to the manufacture of tobacco-pipes. The Germans prepare their pipes for sale by soaking them in tallow, then in white wax, and, finally, by polishing them with shavegrass. Genuine meerschaum pipes are distinguished from mock ones by the beau- tiful brown colour which they assume after being smoked for some time. Of late years some of the pipemakers have produced a com- position clay pipe, which closely resembles meerschaum in appearance, and is '* warranted to colour well." The composition, which is comparatively valueless, is made up into pipes of suitable patterns, which are frequently suld to the ignorant for "meerschaums." See Cements, Htdeaumc. ME'GRIM. /%». Meaoeim:, Hemiobasia, L, A pain affecting one side of the head only, often periodic, like an ague, and generally of a nervous, hysterical, or bilious character. It is clavus when there is a strong pulsation, con- veying the sensation of a nail piercing the part. See Headache. MEG'RXMS. Syn. Meaorims, Veetioo. In veterinary medicine this term is applied to Iiorses which when at work reel, then stand for a minute dull and stupid, or fall to the ground, and lie partially insensible for a few minutes. " Horses subject to this affection should be driven with a breastplate or pipe collar, so as to prevent pressure on the veins carrying the blood from the bead ; the bowels should be kept in good order; an occasional laxative is advisable, and a course, either of arsenic or quinine, or of arsenic and iron." (Dun.) MEI'ANCHOIT. See Hypochohdeiasis and Insanitt. MELIS'SIC ALCOHOL, A substance ob- tained byBrodie from beeswax. By oxidation it yields ' melissic acid.' MELLA'GO. The old name for a medicine having the consistence of honey, with a some- what sweetish taste. Mellago taraxaci is fluid extract of dandelion. MELTING-POINT, The temperature at which solids assume the liquid form. MEN'STRUUM. [L.] A solvent or dis- solvent. The principal meusteua employed in chemistry and pharmacy to extract the active principles of bodies by digestion, de- coction, infusion, or maceration, are water, alcohol, oils, and solutions of the acids and 0.1 K fl IvlPR MERCU"RIAL BAL'SAM. See Ointmbnt OF Nitrate of Meecuet. MERCU"RIAL DISEASE'. Si/n. MOBBTIS IIEEOURIALIS, Hydkaeqteiasis, L. This results from the injudicious or excessive use of mercury, or exposure to the fumes of this metal. The common and leading symptoms are a disagreeable coppery taste ; excessive salivation j sponginess, tumefaction, and ul- ceration of the gums ; swollen tongue ; loosen- ing of the teeth; exfoliation of the jaws; remarkably offensive breath; debility; ema- ciation; ending (when not arrested) in death from exhaustion. Fever, cachexia, violent purging and griping, a species of eczema (ec- zema MEEC0EIALE, lEPEA MEBCTTEIAIIS), and other forms of skin disease, are also phases, of the same affection, the first of which occasion- ally proves fatal under the influence of sudden and violent physical exertion. The treatment, in ordinary cases, may con- sist in free exposure to the open air, aviiiding either heat or cold; the administration of saline aperients, as Epsom salts, phosphate of soda, &c. ; the free use of lemon juice and water as a common drink ; with weak gargles or washes of chloride of soda or chloride of lime to the gums, mouth, and throat. Severe cases often resist every variety of treatment, and instances are recorded in the medical journals in which the use of even small doses of mer- MERCURY 1053 curUla, administered by the faculty, have, owing to tile poi'iiliar idiosynLiusy of the patients, been followed by the most horrible ■ufforinf;!!, terminating in death. MEE'COBY. Hg. 8i/n. QciOKSiLTBB, Hydbaboybum (B. p.. Ph. L. E. and D.) ; Mkbccbs, Vif absent, Fr. ; Quecksilbeb, Cii'r. A remarkable metal, which has been known from a very early period. 'ITie Romans employed it as a medicine externally, as did the Arabs; but tho Hindoos were probably the first to prescribe it internally. Sources. The most important are the mines of Iilriii, in Carniola; Alinaden, in New Cas- tile; and New Almaden, in California, where it exists combined with sulplmr, under the form of cinnabar. From this ore the pure metal is obtained by distilling it with lime or iron filing-', in iron retorts, by which the sul- phur it cuutains is seized and retiiined, while the mercury rises in the state of vapour, and i* condensed in suitable receivers. Quicksilver is commonly imported in cylindrical iron bot- tles, containing i cwt. to 1 cwt. each. It is also imported in smHll quantities from China, contain^! in bamboo bottles holding about 20 lbs. each. Prep. Mercury, as imported, is usually sufficiently pare for medicinal purposes with- out any further preparation. Mere mechanical impurities, as floating dust, dirt, &c., may be got rid of by squeezing the metal through chamois leather or flannel, or by filtering it through a small hole in the apex of an inverted cone of paper. It can be further cleaned by shaking wt-U with a little strong nitric acid, washing with distilled water, and drying by blotting paper, or filtering througli warm chamois leather. Prop., S(e. Mercury, at all common tem- peratures, is a heavy liquid, possessing a nearly vilver-whlte colour, and a brilliant metallic lustre; solidifies (treezes) at — 40° Fahr., and is then ductile, malleable, and tenacious ; boils at 662" Fiihr., and escapes in colonrless trans parent vapour, of gi'eat density ; it also volati liscs slowly at the ordinary temperature of the atmosphere. The presence of minute quan- tities of lead and zinc greatly retard its evapo- ration at its boiling' heat. It unites with oxy- gen, chlorine, iodine, &c., forming numerous compounds. With the metals it unites to form AMALO-AMS. The only acids which act directly on metallic mercury are the sulphuric and nitric, but for this purpose the former must be heated and concentrated. Nitric acid, however, even when dilute and in the cold, dissolves it freely. Pure mercury is un- altenible in the air at ordinary temperatures. 8p. gr. 13-59 at GO" Fahr. j about 14- when in the solid state. Vaes, S(c, .Mercury is applied to various purposes in the arts ; as the amalgamation of golil and silver, ' wash gilding,' the ^silvering of lni>kiiig-glassoa, the manufacture of ba- rometers and thermometers, and the prepara- tion of several very valuable medicines. In its metallic state it appears to be inert when swallowed, unless it meets with much acidity in the alimentary canal, or is in a state of minute division ; its compounds are, however, all of them more or less poisonous. Mercury has been employed in one or other of its forms in almost all diseases ; but each of its numerous preparations is supposed to have some peculiarity of action of its own, com- bined with that common to all the compounds of this metal. The mercurials form, indeed, one of tho most important classes of the materia medica. Teats. 1. Metallic mercurt/ is detected by its liquid condition and volatility ; and, when in a finely divided or pulverulent state, by ti.e microscope, or by staining a piece of cupper white when tho two are rubbed together. Mercury, when present iu combination, can be detected as under : When intimately mixed with anhydrous sodium carbonate, and heated in a small test-tube, under a layer of the carbonate, de- composition ensues, and a crust of grey sub- limate form's on the cooler portion of the tube. When examined by a lens this crust is seen to consist of minute metallic globules. By fric- tion with a bright glass or iron rod these are uuited into globules, which are visible to the naked eye. A perfectly clean and bright piece of copper, immersed in a slightly acid solution of mercury, becomes in a short time covered with a grey or whitish stain, which assumes a silvery lustre when gently rubbed with a piece of soft cork or leather, and is removed by the subse- quent application of heat. A single drop of liquid may be tested on a bright copper coin in this way. The plate of copper with the deposit of mercury, obtained as above, after being waslied with a weak solution of ammouia, and in dis- tilled water, and dried by pressure between the folds of bibulous paper, may be cut into small pieces, and heated in a test-tube, in order to obtain metallic globules. When the suspected solution contains organic matter, bright copper filings may be employed, and the process modified so as nearly to resemble Reinsch's test for arsenious acid. According to Orfila, " scraped copper plate" is capable of detecting the presence of twoo"' P"''' <>' ^'^ rosive sublimate in a solution. MM- Trousseau and Reveil state that a plate of yellow copper (brass) is even more susceptible than one of red copper. (Smithson's electrolytic test.) This con- sists in the use of a polished wire or plate of gold or copper round which a strip or thread of zinc or tin is wound in a spiral direction. The suspected liquid is acidulated with a few drops of hydrochloric acid, and after immersion for a longer or a shorter period (as half an hour to an hour or two), the gold will have become white if any mercury is present. The coil of 1054 MERCURY zinc or tin is then removed from the gold, and the latter, after being washed and dried be- tween the folds of bibnlous paper, is heated in a test-tube, to obtain metallic globules, as before. An ingenious extemporaneous application of the electrolytic test may be made as follows : — Place a drop or two of the suspected liquid on a clean and bright gold or copper coin, and apply a bright key, so that it may at once touch the edge of the coin and the solution. (See engr.) An electric current will then be a. A. g;o1d or copper coin. b. Drop of suspected solution. e. A bnght key. established as before, and a white spot of re- duced mercury will appear on the surfuce of the metal, which may be recognised in the manner already explained. The salts of mercury are divided into two classes — mercurous, where mercury is a monad element, and unites with one atom of chlorine ; and mercuric salts, where it plays the part of a dyad element, or unites with two atoms. The latter of these will be taken first. Mercury, Pure. (Ph. B.) Syn, Htdear- GYBUM PtTRUM. Place commercial mercury, 3 lbs., in a glass retort or iron bottle, and applying heat cause 2J lbs. of the metal to distil over into a flask employed as a receiver. Boil on this for five minutes hydrochloric acid, 3 dr., diluted with distilled water, 9 fi. dr., and having by repeated affusions of distilled water, and decantations, removed every trace of acid, let the mercury be transferred to a porcelain capsule, and dried- first by filtering paper, and finally on a water bath. Mercuric Salts. Tests. Sulphuretted hy- drogen and ammonium sulphide, added in very small quantities, produce on agitation a per- fectly white precipitate, which acquires suc- cessively a yellow, orange, and brownish-red colour, as more of the test is added ; and, nltimately, when the test is added in consider- able excess, an intensely blai-k colour. This precipitate is insoluble in excess of the precipi- tant, potassium hydrate, potassium cyanide, hydrochloric add, or nitric acid, even when boiling ; but it dissolves readily and completely in potassium sulphide and in ' aqua regia' with decomposition. These reactions arc charac- teristic. Ammonia gives a white precipitate. Potassium hydrate gives a reddish precipi- tate, turning yellow when the test is added in excess. The presence of ammonia causes the precipitate to be white, and when the solu- tion contains much acid both reactions are imperfect. Alkaline carbonates give a brick-red preci- pitate. Potassium iodide gives a scarlet precipitate, which is soluble in excess, and in alcohol, and splution of sodium chloride. The alkaline bicarbonates either do not dis- turb the solution, or only cause a slight degree of opalescence. Mercuric Acetate. Hg(C2H302)2. St/n. Peotaoetate op meecuet. JPrep. By dis- solving mercuric oxide in warm' acetic acid. It crystallises in brilliant micaceous lamina, soluble in their own weight of cold water, and somewhat more soluble in boiling water. Ac- cording to Robiqnet, this is the basis of Keysets antivenereal pills, which do not con- tain snbacetate of mercury, as has been asserted. Mercuric Bromide. .HgBrj. Syn. Pkoto- BBOMIDE OP MEKOUEY, HyDEABOYEI EIBBO- MIDUM. Prep. Two equal parts of bromine and mercury and sublime. Soluble reddish mass; resembles the iodide in its actiou. — Dose, ,L to i gr. Mercuric Chloride. HgClj. Si/n. Peoto- OHLOEIDE OP MEECUEY, PeECHIOEIDE OF MEECUEY, BiCHLOEIDE OE MERCCEY, COE- EOSITE SUBLIMATE ; HYDEAEGYEI PEEOHLO- EiDUM (B. P.), Hyeeaeoyei BICHLOBIDUSI (Ph. L.), Sttblimatus coEEOsrvua (Ph. E.), Subiimatum coeeosivom (Ph. D.), Hydeae- OYEI CHLOEIDTTM COEEOSIVTJM (Ph. U. S.), Hydbaeoyei mueias coEEOsivtrs, L. This is the ' corrosive sublimate' of the shops. Prep. 1. (Ph. L.) Mercury, 2 lbs.; sul- phuric acid, 21i fl. oz. ; boil to dryness, and rub the residuum, when cold, with sodium chloride, 1^ lb., in an earthenware mortar; lastly, sublime by a gradually increased heat. 2. (Ph. K.) Mercury, 4 oz.; sulphuric acid, 2 fl. oz. 3 fl. dr. ; pure nitric acid, 4 fl. oz. ; dissolve, add of sodium chloride, 3 oz., and sublime as before. 3. (Ph. D.) ' Persulphate of mercury' (mer- curic sulphate), 2 parts ; dried sodium chlo- ride, 1 part; triturate, &c., as before. 4. (Ph. B.) Reduce sulphate of mercury, 20 oz., and chloride of sodium, dried, 16 oz., each to fine powder, and having mixed them add black oxide of manganese, in fine powder, 1 oz., thoroughly by trituration in a mortar, place the mixture in an apparatus adapted for sublimation, and apply sufficient heat to cause vapours of perchloride of mercury to rise into the less heated part of the apparatus arranged for their condensation. Obs. In preparing corrosive sublimate, as well as calomel, by the common process, the solution of the mercury is usually made in an iron pot, set in a furnace nnder a chimney, to carry off the fumes; and the sublimation is conducted in an earthen alembic placed in a sand bath, or in an iron pot, covered with a semi-spherical earthen head. Corrosive sub- MERCURY 1055 limate may also be maile by the dirnct solution of mercuric oxide in hydrochloric acid, or by bringing its constituents together in the state of vapour. The latter plan was patented by the late Dr A. T. Thomson. Prof. The mercuric chloride of commerce occurs in white, semi-transparent, crystalline masses, of considerable density ; it possesses an intense coppery taste, is soluble in about 16 parts of cold, and in 3 parts of boiling water ; the boiling solution deposits its excess of salt in lonf; white prisms as it cools; soluble in alcohol and ether, in the latter so much so that it has even the property of withdrawing it from its aqueous solutions ; the addition of hydrochloric acid, ammonious chloride or cam- phor, increases its solubility in all these men- strua. It i< decomposed by contact with nearly all metitUic bodies, and in solution by various organic substances, and by exposure to light. Sp. gr. 5 2 (5-14 to 5-42— Liebig). It melts at about 509° Fahr., and boils and volatilises at a higher temperature. Testa. The presence of mercuric chloride may, under most circumstances, be readily de- tccttil by the tests given. To distinguish it from otiier salts, special tests for chlorine or hydrochloric acid must be applied. If on fil- tering the solution, acidulating it with dilute nitric acid, and testing it with silver nitrate, a cloudy white precipitate be formed, which is insoluble in excess of the precipitant, and in nitric acid, but soluble in ammonia water, and blackened by lengthened exposure to light, corrosive suldimate is shown to be present in the substance examined. Calomel, the >mly compound of mercury with chlorine besides corrosive sublimate, is an insoluble powder, which could not, therefore, be found in the filtered liquid. Calomel, or the white precipi- tate formed by the mercurous salt, with hy- drochloric acid and the soluble chlorides, is soluble in excess of the precipitant, and is not only insoluble in liquor of ammonia, but is immediately blackened by it. For the purpose of demonstrating the pre- sence of corrosive sublimate in a highly co- loured liquid, or one loaded with organic matter, it is necessary to agitate it for some minutes with an equal volume of ether. After repose for a short time, the ethereal solution is decanted, and allowed to evaporate spontaneously. The residuum (if any) con-- tains the corrosive sublimate, which, after being dissolved in distilled water, is readily recognised by the above characteristics. When the substance under examination con- sists of food, or the contents of the digestive canal, or of animal tissue, it is in general necessary to destroy the organic matter in a nearly >imil.ir way to that described under Aesbnious acid. The process adopted by Devergie for this purpose consists in di-scilving the substance in concentrated hydrochloric acid, and passing a stream of chlorine throuarh the liquid.— Flandin tirst carbonises the mass with i or i its weight of concentrated sul- phuric acid, at 212° Fahr, and then saturates the acid in the cold, witli dry ' chloride of lime,' added in fragments, assisting the action by stirring, and further adding, by degrees, as the matter thickens and becomes white, a suf- ficient quantity of distilled water. — Lassaigne boils the suspected mixture for some time with a solution of sodium chloride; a method which, according to Orfila, is not sufficiently delicate to withdraw minute portions of mercury from flesh. — Millon agitates organic liquids (more especially blood, milk, &c.) in large flasks con- taining gaseous chlorine, which is frequently renewed. — Orfila either dissolves the matter in aqua regia, and passes a stream of chlorine through the liquid, or he carbonises it by means of concentrated sulphuric acid, in close vessels. — Personne proceeds by a similar me- thod, but avoids raising the temperature of the substances operated on. — Reveil employs either the last method or that of Millon. In all cases it is advisable to operate in close vessels, on account of the volatility of the bichloride; Orfila's apparatus consists of a matrass, provided with a bent tube, the one end of which is plunged into a jar of cold dis- tilled water. The corrosive sublimate is found both in the volatilised matter and in the ciir- bonised residuum, and is extracted from the latter by boiling it for 15 or 20 minutes in aqua regia. When the organic matter has been destroyed by any of the above processes, and a colourless and filtered solution in distilled water obtained, the usual tests may be at once applied. But in this way we can only detect the presence of mercury, but are unable to decide in what way it has entered the system, although we may infer it from other circumstances. It is, therefore, abAlutely necessary, in nil medico- legal investigations, to previously employ ether (see above), in order that we may be enabled to examine the deleterious matter in its original form, or that in which it was swal- lowed. Uses, &fc. Mercuric chloride is employed as an alterative, diaphoretic, and resolvent, in the chronic forms of secondary syphilis, rheu- matism, scrofula, cancer, old dropsies, nume- rous skin diseases, &c. ; and externally, as a caustic, in cancer, and made into an ointment, lotion, or injectiou, in a vast number of skin diseases, ulcers, gleet, &c., and as a preventive of contagion. It acts quicker than the other preparations of mercury, and it is less apt to induce salivation; but it has been said that its effects are less apparent. — Dose, xj; *<> i S^;' either made into a pill, or in solution. It is highly poisonous, and must be exhibited and handled with the greatest caution. Its use is contra-indicated in cases complicated with pul- monary affections or nervous derangement. Poi'i.— 1. Symptoms. Strong coppery or metallic taste; intense pain in the mouth, pharynx, oesophagus, stomach, and intestines; 1056 MERCUEY nausea, vomiting (often bloody), diarrhoea, and (sometiiuea) violent dysentery (tiicse evacua- tions are generally more frequent than in poisoning by other metallic compounds). After a certain time there is generally an abatement of the severity of the symptoms ; the circulation becomes slower, the pulse small and thready, the respiration gentle, and the skin cold ; syncope then supervenes, and great general insensibility, always commencing at tile pelvic extremities ; and sometimes con- vulsions occur ; the secretion of urine is gene- rally diminished, sometimes even entirely sup- pressed ; but the patients always urinate if the sublimate lias been employed in a very diluted state, and if drinks have been admin- istered. Death 'often appears to result from the shock to the nervous system, from intense exhaustion, or from mortification or intense inflammation of the primsB viae. Poisoning by corrosive sublimate is distinguished from that by arsenic, by the countenance being flushed, and even swollen; whereas, in poisoning by arsenic, it is wholly contracted and ghastly, and by the whitened condition of the epithe- lium of the mouth. 2. Antidotes. White of egg, hydrated ferric sulphide or ferrous sulphide, and gluten, are each of thein powerful antidotes. White of egg has proved efficacious in'numerous cases. It requires the white of one egg to decompose 4 gr. of corrosive sublimate. (Peschier.) The recently precipitated protosnlphuret of iron is, however, according to Mialhe, the antidote par excellence, not only to corrosive sublimate, but to the salts of lead and copper. The gluten of wheat has also been recommended (Taddei) ; or, what is equally efficacious, wheat flour mixed up with water. When any of the above are not at hand, copious draughts of milk may be substituted. Iron* filings have been occasionally used as an antidote. All these substances should be taken in consider- able quantities ; the dose should be frequently repeated, and the general treatment similar to that in cases of poisoning by arsenic. Vomit- ing should be, in all cases, immediately in- duced, to remove, if possible, the poisonous matter from the stomach. Mercuric- ammonium Chloride. HgNH2Cl. Si/n. Ammonio-chloeide op Meeoury, Am- MOIflATED OHLOEIEE OP MEECTJBY, WHITE PRECIPITATE, LeMERT'S W r., COSMETIO MER- CUEY ; HYDRAECfYEI AMMONIATUM (B.T.), IIydraegyei ammonio-ohxobidum (Ph. L.), HYDBARGYECM PRa;CIPITATUM: ALBUM (Pll. E.) J?rep. 1. (Ph. L.) Mercuric chloride, 6 oz. ; distilled water, 3 quarts; dissolve, with heat, and when the solution has cooled, add of liquor of ammonia 8 fl. oz., frequently shaking it; lastly, wash the precipitate with water, and dry it. The formula) of the Ph. E. & D. are nearly similar. 2. Mercuric chloride and ammonium chlo- ride, of each J lb. ; water, 3 quarts : dissolve. and precipitate with solution of potassium hydrate, q. s. JProp., ifc. A white, inodorous, light mass, or powder ; insoluble in alcohol, partially soluble in boiling water, and wholly dissolved by sulphuric, nitric, and hydiochloric acids, without effervescence. It is totally dissipated by heat. When heated with solution of potash, it exhales ammonia, and assumes a yellow colour. Used to make an ointment, which is employed in herpes, porrigo, itch, and other skin diseases, &c. ; and by the lower orders as a dusting powder to destroy pediculi, an appli- cation which, from its liberal employment, is not always a safe one. It is highly poisonous, and must not be swallowed. Mercuric and Ammouinm Chloride. NH4Cl,HgCl2. Syn. Chloride op meecuey AND AMMONIUM, SAL ALEMEROTH ; HY- drarotei bt ammonii chloeidum, L. Prep. (P. Cod.) From mercuric chloride and am- monium chloride, equal parts, triturated together. " The object in adding the am- monium chloride here is to render the corro- sive sublimate more soluble in water. The action of the latter is not otherwise altered." (Redwood.) It is chiefly used for lotions and injections. Mercuric and Quinine Chloride. Syn. Chlo- ride OF MEECUBY AND QUININE; HTDEAE- GYEI ET QUINiE CHLOEIDUM, L. Prep. (M'Dermott.) From mercuric chloride, 1 part ; quinine chloride, 3 parts ; separately formed into saturated solutions with water and then mixed ; the crystalline precipitate is collected and dried by a gentle heat. — Dose, ^ to i gr., made into a pill with crum of bread ; daily, as an alterative in debilitated habits; or combined with opium thrice daily, to produce salivation. Mercuric Cyanide. HgCy, or Hg(CN)2. Syn. Cyanide of meecuey ; Hydeaeoybi CYANIDUM, H. BICYANIDUM, H. CYAHUEETUII (Ph. U. S.), L. Prep. 1. (Ph. L. 1S36.) Ferric ferro- cyanide (pure Prussian blue), 8 oz. ; mercuric oxide, 10 oz. ; distilled water, 4 pints; boil for half an hour, filter, evaporate, and crystal- lise ; wash what remains frequently with boil- ing distilled water, and again evaporate, that crystals may form. 'I'his is Proust's process. The formula of the Ph. U. S. is similar. 2. (Ph. D. 1826.) Prussian blue (pure), 6 parts ; mercuric oxide, 5 parts ; distilled water, 40 parts ; as the last. 3. (Desfosses.) Potassium ferrocyanide, 1 part, is boiled for i hour with mercuric sul- phate, 2 parts, and distilled water, 8 parts; the deposit is separated by 61tration, and the liquid evaporated to crystallising point. 4. (Winckler.) Saturate dilute hydrocyanic acid with mercuric oxide ; evaporate and crys- tallise. Pure. Prop., Sfc. Heavy, colourless, inodorous, square prisms; tasting strongly metallic; soluble in 8 parts of cold water; slightly MERCURY 105 Bulublo in alcohol. Those made by the firnt two fornmliD iire uf a pale yellow colour. It is traQBpnrent and totuUy soluble in water. The solution, on the addition of hydrochloric acid, evolves hydrocyanic acid, known by its smell ; and a glass moistened with a solution of nitrate of silver, and held over it, gives a deposit soluble in boiling nitric acid. When heated it evolves cyanogen, and runs into globules of metallic mercury. It has been administered in some hepatic and skin diseases, and has been proposed as a substitute for corrosive sublimate. (Parent.) It has been said to act directly on the skin and bones, and to have proved useful in allaying the pain of nodes and in dispersing them. (Mendaga.) It is, however, principally used as a source of cyanogen and hydrocyanic acid. — Dose, ^-g to i gr. (be;,'inniag with the smaller quantity), made into pills with crum of bread, or in alcoholic solution ; as a gargle or lotion, 10 gr. to water, 1 pint; as an ointment, 10 or 12 gr., to lard, 1 oz. Mercnriclodide. Hglj. Syn. Peotiodide OP MEBOUBY, Red iodide op mebcuey. Io- dide OP MEBOtrilT, BiNIODIDE OFMEEOnET; UXDBABSYBI lODIDUM EUBBUM (B. P.), HtDEAEOYEI lODlDnM, H. BINIOBIDTIM (Ph. E), H. lODiDTTM eubeum (Ph. D.), L. Prep. 1. (B. P.) Mercuric chloride (corrosive sub- limate), <1; potassium iodide, O; boiling dis- tilled water, 80. Dissolve the mercuric chlo- ride In 60 of water, and the pot:assium iodide in the remainder, and mix the two solutions. Allow to stand, decant the supernatant liquor, and collect the precipitate on a filter, wash twice with cold water, and dry at 212° F. a. (Ph. L. 1836.) Mercury, 1 oz. ; iodine, 10 dr. J rectified spirit, q. s. (2 or 3 fl. dr.); triturate until the globules of mercury dis- appear, and the mixture assumes a scarlet colour, then dry it in the shade, and preserve it in a well-stoppered vessel. 3. (Ph. E.) Mercury, 2 oz. ; iodine, 2J oz.; spirit, q, s. ; triturate together as last, dissolve the product, by brisk ebullition, in concen- trated solution of sodium chloride, 1 gall., filter whilst boiling hot, wash the crystals that are deposited as the solution cools, and dry them. 4. (Ph. I).) Mercuric chloride, 1 oz. ; hot distilled water, 23 fl. oz. ; dissolve potassium iodide, 1^ oz. ; water, 5 fl. oz. ; dissolve ; when the solutions are cold, mix them, collect the precipit;ite on a paper filter, drain it, wash it with distilled water, 10 fl. oz., and dry it at a heiit not above that of boiling water. Prop., S(c. A bright scarlet powder, inso- luble in water, but soluble in alcohol and ether, and in the solutions of several of the iodides and chlorides. It is also soluble in cod-liver oil, and in several other fixed oils. Readily sublimed. — Dose, \ to \ gr., dis- solved in alcohol or made into a pill ; in the same cases as the subiodldes, from which it TOL. II, differs chiefly in its greater energy and poi- sonous qualities. Mercuric Oleate, See Ointment op Oleate OP MEUCtTET. Mercuric and Potassium Iodide. Hgl, . KI. Syn. Iodide op meboubt and potas- sium, lODO-HTDEAEGTEATB OP POTASSIUM; Hydeaeotbi kt potassii iodidum, L. Prep. 1. (M. Boullay.) Mercuric iodide, po- tassium iodide, and water, equal parts; dissolve by heat, and crystallise by evapora- tion or refrigeration, or gently evaporate to dryness. 2. (Puche.) From mercuric iodide and potassium iodide, equal parts, triturated to- gether.— Z)o*e, I'j to^ gr., dissolved in water; in the same cases as the binioilide, and in chronic bronchitis, hooping-cough, inflamma- tory sore throat, &c. Mercuric and Potassium lodo-cy'anide. Syn. HydBAEOYEI ET potassii lODO-OTANIDrM, L. Prep. To u concentrated solution of mercuric cyanide add a rather strong solution of potassium iodide, and dry the precipitate by a gentle heat. Prop., ifc. Small, white, pearly, crystalline plates or scales. It is chitfly used as a test of the purity of hydrocyanic acid. When put into this liquid it is instantly turned red if any mineral acid is present. Mercuric Nitrate. Hg(N03)j. Syn. Peo- TONITKATE OP MEECUEY, PeENITBATE OP MEBOUUY. Prep. 1, (Neittbal.) This is obtained by solution of mercuric oxide, in excess of nitric acid. The solution, evaporated in a bell-jar over sulphuric acid, yields crystals which are neutral. The same compound is obtained as a crystalline powder when the syrupy liquid is dropped into strong nitric acid. (Basic.) Ist. 2Hg(N0a)H0 . HjO. Prep, a. By saturating hot dilute nitric acid with mercuric oxide. The salt, which is bibasic, crystallises on cooling. h. By dissolving mercury in excess of nitric acid, with heat, until the solution, when di- luted with distilled water, ceases to give a precipitate with common salt. It is now a mixed , solution of the neutral and bibasic per- nitrates ; but by evaporation crystals of the latter salt only are deposited. The acid solu- tion (before evaporation) is used as a caustic in cancerous, syphilitic, and other ulcerations ; but it frequently produces intense pain, and occasionally the usual constitutional effects of mercury. It was formerly given in similar cases to those in which the bichloride is now employed. — Dose (of the dry salt), j\j to ^ gr. This is the preparation ordinarily referred to under the name ' pernitrate of mercury.' 2nd. 2Hg(N03)HO . HgO. c. By saturat- ing strong nitric acid with mercury, by heat, throwing the solution into cold water, and collecting and drying the precipitate. This salt, which is tribasic, is also formed when 67 1058 MERCURY the preceding crystallised salts are put into hot water. Obs, This last preparation is a heavy, yellow powder, but the shade varies according to its basicity, which increases with the temperature of the water employed to effect the precipita- tion, until, at the boiling temperature, the colour is a dull red. It is extensively em- ployed for the extemporaneous preparation of the ointment of nitrate of mercury, according to the formula on the following label which accompanies each bottle : — " Hydrarg. snb- nitras." " Two scruples, mixed with one ounce of simple cerate, make the ung. hydrarg. nit. of the London Pharmacopoeia." We need scarcely add that this statement, so unblush- ingly uttered, is a dangerous falsehood. An ointment so made possesses neither the quan- tity of mercury nor of nitric acid employed in the Pharmacopoeia preparation, besides wanting many of its most sensible and valuable properties. Mercuric Oxide. HgO. Syn. Peotozidb OF MEBCUET, ReD OXIDB OP MERCURY, Oxide of m., Binoxide of m., Deutoxide OF M., Peroxide of m. ; Hydkaboyei oxt- DUM, H. o. EUBEUM, B. & L. There are several methods by which this substance may be prepared. The following are those which have been ordered at different times in the Pharmacopoeias : — 1. By precipitation (Hydbae&yei binoxy- DUM — Ph. L. 1836.). Mercuric chloride (corro- sive sublimate), 4 07,. j distilled water, 6 pints ; dissolve and add of liquor of potass, 28 fl. oz. ; drain the precipitate, wash it in distilled water, and dry it by a gentle heat. Obs. A bright orange-red powder. It usually contains a little combined water ; hence its readier solubility in acids than the oxide prepared by heat. When heated sufficiently it yields oxygen, and the mercury either runs into globules or is totally dissipated. It is entirely soluble in hydrochloric acid. (Ph. L. 1836.) The preparation of the shops has fre- quently a bi'ick-red colour, and contains a little oxy chloride, arising from too little alkali being used. 2. By calcination of the nitrate (Red pre- cipitate ; Hydbaeoyri niteioi oxyditm Ph. L. Hydearoyri oxidum eubkum, B. P., Ph, L., Ph, D.) Prep. B. P. Mercury, by weight, 8; nitric acid, 4i; water, 2. Dissolve half the mercury in the water and acid, evapo- rate to dryness, and triturate with the rest of the mercury until well blended. Heat in a porcelain capsule, repeatedly stirring, until acid vapours cease to be evolved. Mercury, 3 lbs.; nitric acid, 18 fl. oz. (IJ lb.. Ph. L. 1836) ; water, 2 quarts ; dissolve by a gentle heat, evaporate to dryness, powder, and calcine this in a shallow vessel, with a gradually increased heat, until red vapours cease to arise. The process of the Ph. E. and D. are similar, except that the Dublin College directs the evaporation and calcination to be performed in the same vessel, without powdering or stirring the mass. Obs. Bright red crystalline scales, which usually contain a little undecomposed per- nitrate of mercury; in other respects it re- sembles the last two preparations. It is more generally used as an escharotic and in oint- ments than the precipitated oxide. It is vola- tilised by beat without the evolution of nitrous vapours. According to Mr Brande it contains about 2} per cent, of nitric acid. According to Mr Barker the process of the Ph. D. yields the finest coloured product j but Mr Brande states that " the nitrate requires to be constantly stirred during the process, which is usually performed in a cast-iron pot." On the large scale, the evaporation is generally conducted in a shallow earthen dish, and as soon as the mass becomes dry a second dish is inverted over it, and the calcination is continued, with- out disturbance, until the process is concluded. The heat of a sand bath is employed. 120 lbs. of mercury, and 48 lbs. of nitric acid (sp. gr. 1"48) yields 112 lbs. of red precipitate. (Brande.) Vses, l(c. Red oxide of mercury, whether obtained by calcination or precipitation, pos- sesses the same general properties. It is very slightly soluble in water, but sufficiently so to give that fluid an alkaline reaction, and a me- tallic taste. It was formerly employed in medicine to induce salivation; but is now chiefly used as an escharotic, either in the form of powder or made into an ointment. — Dose, I to 1 gr., combined with opium. It is very poisonous. Mercuric Sulphide. HgS04. 8yn. Peoto- SULPHATE of MEEOUEY; HyDEABQYEI SUL- PHAS (Ph. B.), H. PEHSULPHA3, H. BIPERSUL- PHAS, L. Prep. 1. (Neutral.) — a. By boiling together sulphuric acid and metallic mercury until the latter is wholy converted into a heavy, white, crystalline powder; the excess of acid is removed by evaporation. Equal weights of acid and metal may conveniently be em- ployed. b. (Ph. D. 1826.) Dissolve mercury, 6 parts, in a mixture of sulphuric acid, 6 parts, and nitric acid, 1 part, by boiling them in a glass vessel, and continue the heat until the mass becomes perfectly dry and white. Used to make calomel. c. (Ph. B.) Place 20 oz. of quicksilver in a porcelain capsule with 12 fl. oz. of sulphuric acid, and apply heat until nothing remains hut a white, dry, crystalline salt. Used to make perohloride and chloride of mercury. 2. (Basic.) HgSO^.jHgO. Syn. Tbibasio SULPHATE OF MERCUBY, TURPETH MINEEAL, TuEBiTH M., Queen's yellow, Subsdlphatb OF MEROURYf, TeIBASIC PERSULPHATE OF 31. J Hydbaeoyei subsulphas, H. s. flatus, Teepethum mineealb, L. — a. Dissolve mer- cury in an equal weight of sulphuric acid by boiling them to dryness, fling the mass into MERCURY 1059 hot water, and wash and dry the resulting yellow powder. b. (I'h. D. 1826.) Mercuric sulphate, 1 pnrt ; wnrm water, 20 parts ; tritarate together in an eiirthen mortar, wash well with distilled water, drain, and dry it. Prop., (fo. A heavy, lemon-yellow powder, soluble in 2000 parts of cold, and about 600 parts of boiling water. By long-continued wasliing with very hot water it loses all its remaining acid, and is at length converted into red oxide of mercury. — Dote. As an altera- tive, }^ to I gr. ; as an emetic, 3 to 5 gr. ; as an errliine, 1 gr. j mixed up with a pinch of liquorice powder or fine suofE. It is a powerful poisiin, and one of the least useful of the mercurial preparations. Oba, The temperature of the water em- ployed to decompose the neutral sulphate influences the shade of colour of the resulting salt in a similar manner to that pointed out under the nitrate. It is now superseded as a pigment by chrome yellow and orpiment, which are not only more beautiful, but cheaper preparations. Hercnric Sulphide. HorS. St/n. Photo- BULPHIDB OF MEBCnET, RED SULPHCEBT OF MKKCPET, FAOTtTIOtrs CINNABAR, VbEMILION, STTLPHUKBT of MEKUBT, StTLPniDE OF M., BlSUtPHCnET OP M.+ ; Htdeaeotbi bisul- PUUKETUM (Ph. B. & Ph. L.), ClNNABAniS (Ph. K), H. srLPnrEETijMEnBEtrM. L. Fre^'- (Ph. L.) Quicksilver, 24 oz. ; sulphur, 5 oz. ; melt together, and continue the heat till the mixture swells up, then cover the vessel, re- moife it from the heat, and when cold, powder and sublime it. (Ph. B.) Quicksilver, 2 lbs. ; sulphur, 6 oz. Prop., 1(0. Mercuric sulphide has n dark- red semi-crystalline appearance in the mass, but acquires a brilliant scarlet colour by pow- dering. It is tasteless, odourless, and in- soluble. It is chiefly used as a pigment; but it is occasionally employed in medicine as a diaphoretic and vermifuge, and in some cuta- neous diseases and gout. — Dose, 10 to 30 gr. ; Hs a fumigation, about \ dr. is thrown on a plate of iron heated to dull redness. For the last purpose it is inferior to mercurous oxide, owing to the more irritating nature of its vapour. Tetl>. Mercfhotjs SALTS. Sulphuretted hydrogen and ammonium sulphide give black precipitates, insoluble in dilute acids, ammo- nium sulphide, potassium cyanide, and hot nitric acid, but slightly soluble in sodium sulphide, and decomposed by nitrohydrochloric acid. Potassium hydrate and ammonia give black grey or black precipitates, which are insoluble in excess of the precipitant. Hydrochloric acid and the soluble metallic chlorides occasion a precipitate, which assumes the form of a very fine powder of dazzling whiteness, insoluble in excess, but soluble in aqua re).'ia and liquid chlorine. Pot.issinm hydrate and ammonia turn it dark grey or black. Potassium iodide gives a greenish-yellow precipitate, soluble in ether, and subliming in red crystals when heated. MercnroM Acetate. Hg(C2H3G3). Syn. Acetate of meecuet, Scbacetate. iVfp. (P. Cod.) Difsolve mercurous nitrate, 1 part, in water (slightly acidulated with nitric acid), 4 parts, and precipitate the liquid with a solution of sodium acetate, gradually added, until in slight excess ; carefully wash the precipitate with cold water, and dry it in the shade. Prop., Ifc. Small, white, micaceons, flexible scales ; insoluble in alcohol ; soluble in about 300 parts of water ; blackened by light ; and carbonised by a strong heat. It has been said to be one of themildestof the mercurials ; but this cannot be the case, as it occasionally acts with great violence on both the stomach and bowels, producing much pain and prostra- tion. — Dose, J to 1 gr., night and morning, gradually increased. Mercurous Bromide. HgBr. Si/a. SuB- BEOMIDE op MKBCUEY; HydEARQTKUM BBO- MIDUM, L. Prep. (Magendie.) By precipi- tating a solution of mercurous nitrate by another of potassium bromide. It closely resembles calomel in both its appearance and properties. — Vose, 1 to 5 gr. Mercurous Chloride. HgCI or Hg^CI;. Si/n. Calomel, SgscHLOEiDE of mebcubt, Mek- oitetchloeide; Htdeaeotbi suBCHLOEiDtiii (B. P.), HTDEABeTEI CHLOEIDCM (Ph. L.), H. 0. MiTB (Ph. U. S), Calomelas (Ph. E. &D.), L. This substance is one of the best known, and probably the most valuable, of all the mercurials. Prep. 1. (Ph. L.) Mercury, 2 lbs. ; sulphuric acid, 21) fl. oz. ; mix, boil to dryness (in a cast-iron vessel), and when the resulting mass has cooled, add of mercury, 2 lbs., and tritu- rate the ingredients in an eartheiiwiire mortar until they are well mixed; then add of sodium chloride, H lb., and again triturate until the globules are no longer visible ; next sublime the mixture, reduce the sublimate to the finest possible powder, diligently wash it with boil- ing distilled water, and ilry it. — Prod. 117 of 118§ of the weight of mercury employed. 2. (Ph. F.) Mercury, 4 oz., is dissolved in a Hiixture of sulphuric acid, 2 ft. oz. 3 fl. dr., and nitric acid, j fl. oz., by the aid of heat; when cold, mercury, 4 oz., is added, and the remainder of the process is conducted as before. 3. (CalOMELIS StTBLIMATUJI. — Ph. D.) Sulphate of mercury, 10 parts; mercury, 7 parts ; dry sodium chloride, 5 parts ; triturate, &c., as hefnre, and atterwiirds rcsublime it, into a large chamber or receiver. 4. (Ph. B.) Same as Dublin. 5. (Apothecaries' Hall.) Quicksilver, 60 lbs., and sulphuric acid, 70 lbs., are boiled to dry- ness in a cast-iron vessel ; of the dry salt, 1060 MERCUEY 62 lbs. are triturated with quicksilver, 40i lbs., until the globules are extinguished, when sodium chloride, 34 lbs., is ndded, and after thorough admixture the whole is sublimed, &c., as before.— Prod. 96 to 100 lbs. 6. (Jewel's Patent.) The receiver, which is capacious, is filled with steam, so that the calomel vapour is condensed in it in a state of extremely minute division. The engr. repre- sents the apparatus now usually employed when this plan is adopted. The product is extremely white, and of the finest quality, It is sometimes called ' hydrosublimed calomel ' and ' hydrosublimate of mercury.' The ' flow- ers of calomel,' of old pharmacy, were prepared in a nearly similar manner. a. Furnace. b. An earthenware retort, havinp a shoit and wide neck, coutaining the ingredients for making calomel. c. An earthen receiver, having three tuhulatures. (/. A vessel containing water. e. A Bteam-boiler. 7. (Soubeiran.) The crude calomel mixture is heated in an earthen tube in a furnace, and a current of air is directed uninterruptedly into the tube by means of a small ventilator. This sweeps away, as it were, the vapours of calomel, and in a straight tube will carry them a distance of 60 feet, to avoid whicli the end of the recipient is immersed in water, by which means the calomel is moistened and falls down. This plan, slightly modified, is now extensively adopted in this country. 8. (Peecipitated caiosiel; Calomelas PE^ffiOiPiTATUM, L.) Digest pure quicksilver, 9 parts, in nitric acid (sp. gr. 1 02 to 1'25), 8 parts, until no more metal will dissolve, apply- ing heat as the effervescence ceases ; then mix the hot liquid quickly with a boiling solution of sodium cliloride, 8 parts, dissolved in water (slightly acidulated with hydrochloric acid), 64 parts ; lastly, well wash the precipitate in boiling distilled water, and dry it. The pro- duct, when the process is skilfully managed, is perfectly white and pure. Prop. A heavy, white, tasteless powder; insoluble in water, alcohol, and cold dilute nitric acid ; volatilises at a temperature below redness, and yields a white or yellowish-white sublimate ; hot nitric acid oxidises and dissolves it ; alkalies, tlie alkaline carbonates, and lime water, decompose it, with the production of the black oxide ; ammonia converts it into a dark slate-grey coloured powder (black pke- CIPITAIB — Kane). Sp. gr. 7'14 (BouUay; 7-156— Pelouze and Premy ; 7'176— Ure). Pur. Calomel is frequently contaminated witVi small quantities of corrosive sublimate, which may he detected by digesting a little in alcohol, decanting the clear portion, and test- ing it with a drop or two of potassium hydrate, when a reddish precipitate will be formed if any mercuric chloride be present. It is pul- verulent, whitish, and sublimes entirely by heat. It becomes black on the addition of potassium hydrate, then, heat being applied, it runs into globules of mercury. Neither silver nitrate, lime water, nor sulphuretted hydro- gen, being added to the water in which it has been washed, or boiled throws down anything. Uses. Calomel is one of the milder mer- curials, and in this respect takes its position immediately after blue pill, mercury with chalk, and the grey oxide; but it probably ranks before all the other salts of mercury. Universal experience appears to show it to he a most valuable alterative when judiciously administered. With this intention it is given in doses of i to 1 gr., generally combined with antimonials, as in Plummer's pill, and re- peated every night, or every other night, for some time, tbllowed by a mild saline aperient in the morning. As a purgative, 2 to 5 gr., either combined with or followed by other purgatives, as jalap, rhubarb, senna, colocynth, Epsom salts, &c. As a vermifuge, 2 to 5 gr., over-night, followed by a suflacient dose of castor oil next morning. Combined with opium it is frequently used in various complaints to produce salivation, or bring the system under the influence of mercury. It is also employed as a sedative and errhine, and in a vast num- ber of other indications. It is, indeed, more frequently used, and in a greater variety of complaints, than probably any other medi- cine. Obs. Of the two methods of preparing calomel, that by precipitation is not only the best, hut the most economical. That by sub- limation is, however, the one generally adopted in England. Mr Brande states that " a small portion of sodium chloride is apt to remain combined with it, which might affect its me- dical uses." Such a contamination is not found in carefully prepared precipitated calo- mel, although we doubt whether the quantity of it which exists in any of the samples we have met with (being merely a trace) would at all interfere with its therapeutical action ; more especially when it is recollected that alkaline chlorides are present in, not merely the primas vige, hut also in every part of the animal body. The late Mr Fownes, a chemist who was unsurpassed in the accuracy of his researches, and the caution and delicacy with which he expressed his opinions, once assured us that calomel was more easily and cheaply prepared of the best quality by precipitation than by sublimation, and that if, from careless manipulation, it occasionally contained a minute quantity of common salt, this was of much less importance than the contamination MERCURY 1061 of corrosive Bublimnte, wliich was frequently proflent in samples of sublimed ctilomel. To produce a superior article of chIotucI in the dry way is a somewliHt difficult task, and tlie prcees-i frequently fails in the hands of inriperieneed operators. The solution of the mercury is best made in «n iron vessel, and the sublimation should be conducted (pre- ferably) in an cartlii'nware retort with a short but very wide necli, and fitted in a spacious receiver, having a large fiat bottom, also of earthenware, and containing a little cold water. On the small scale the heat may be applied by means of a sand bath. The form above given for CMlomel, by precipitation, prodiicesa large product, perfectly free from corrosive sublimate and raercurnua nitrate, and is conse- quently free from the objections frequently raised against that mode of preparing it. " The form in which calomel sublimes depends much upon the dimensions and tem- perature of the subliming vessels. In small vessels it generally condeiises in a crystalline cake, the interior surface of which is often covered with beautiful quadrangular pi-ismatio crystals, transparent, and of a texture fome- what elastic or horny. In this state it ac- quires, by the necessary rubbing into powder, a decided yellow or buff colour, more or less deep, according to the degree of trituration it has undergone. If, on the contrary, the calo- mel be sublimed into a very capacious and cold receiver, it falls in an impalpable and perfectly white powder, which requires only one eUitriation to fit it for use ; it then remains perfectly colourless." (ISrande.) The long-continued action of steam on calo- mel iu a state of minute division is attended by the (briiuition of a small quantity of corro- sive sublimate. (Righini.) Boiling water, hot air, and light, also produce a like effect. MercurouB Iodide. Hgl. Syn. Subiodide OF MKRoniY, Green iodide of meecuet, Mkecueotjs iodide ; Htdbaeqyei iodidum vihidb (b. p.), hrdkaegyei btjbiodum, h. IODIDUM (Ph. L.), H. I. TIEIDE (Ph. D.), L. Prep. 1. (U. p.) Mercury, 1 oz. ; iodine, 278 gr. J rectified spirit, a sufficiency. Rub the io.line and mercury in a porcelain mortar, moistening occasionally with a few drops of spirit, and continue the trituration until the mass assumes a uniform green colour, and no metidlic globules are visible. 2. Precipitate a solution of mercurous nitrate by another of mercurons potassium iodide ; wash the precipitate, first in a solution of si'dium chloride, and then in pure water ; lastly, dry it in the shade. 8. (Ph. L.) Mercury, 1 oz. ; iodine, 5 dr. ; tritnrate together, gradually adding of recti- fied spiiit, q. 8. (about 1 to 2 fl. dr.), until globules are no longer seen ; dry the powder, by a gentle heat, in the shade, as quickly as possible, and preserve it in a well-stoppered black glass vessel. The formula of the Ph. D. is similar. Frop., l(c, A heavy, greenish-yellow pow- der ; insoluble in water, alcohol, and a solution of common salt ; soluble in ether, and slightly so in an aqueous solution of iodide of potas- sium. " Freshly prepared, it is yellowish. Heat being cautiously applied, it sublimes in red crystals, which quickly turn yellow, and, on access of light, blacken. It is insoluble in a solution of chloride of sodium." The process of the Ph. L. and F. P. does not answer when larger quantities than 4 or 5 oz. are prepared at once, owing to the great heat generated by the reaction of the ingredients, and the con- sequent volatilisation of a portion of the iodine, by which the colour of the product sufiVrs. — Z)o«e, ^ to 1 gr., made into pills ; " iu syphilis and scrofula, especially where they occur in the same individual." It is also used exter- nally, in the form of ointment. It is very poisonous. UercuTons Nitrate. HgNO,. Syn. Subni- TEATE OF MERCO El' ; HydEAEGYEI SUBNITEAS, H. NITEAS, H. PE0T0NITEA8, L. Pref. 1. (Neutral.) By digesting mercury in excess of cold dilute nitric acid, observiuj; to remove the short prismatic crystals within a short time after they are formed ; these, when drained, and redissolved in water slightly acidulated with nitric acid, furnish crystals of pure neu- tral mercurous nitrate by cautious evaporation. 2. (Bas-ic.) Deposited after some time, when excess of mercury has been employed as above. A fine crystallised salt. Prop., S(c. Both the above are decomposed by water, but the former may be dissolved in a very small quantity without decomposition. When the neutral salt is triiurated with an excess of sodium chloride, and w.iter sub- sequently added, the whole of the u'ercury is thrown down as calomel, and the filtered supernatant liquid does not contain corrosive sublimate. If this salt is detected, the salt examined contained mercuric nitrate, and if any basic mercurous nitrate was present, the newly formed calomel has a grey or black colour, due to presence of oxide. — Dose. Of the ncutriil salts, -jV to J gr. It is seldom used internally, A solution is sometimes em- ployed as a mild caustic to ulcers ; and, more dilute, as a lotion in lepra, porrigo, psoriasis, &c. ; or made into an ointment, in the same diseases. Mercurous Oxide. HgjO. Syn. Suboxidb OF MKSCUET, GbET O. OF M., BLACK O. OF II., Meboueous o.. Dioxide of m., Peotoxide of M.t; Htdeaeotei suboxyddm, H. oxtdifm, H. o. oineeeum, H. o. nioeum, L. Prep. 1. (Ph. L. 1836.) Calomel, 1 oz. ; lime water, 1 gall. ; mix, agitate well together, decant the clear liquid after subsidence, and well wash the sediment with distilled water; lastly, drain and dry it, wrapped iu bibulous paper, in the air. 2. (Ph.D. 1826.) Sublimed calomel, 1 part; solution of potassium hydrate (warm), 4 parts ; triturate together, &c., as last. 1062 MERCURY 3. Brisldy triturate calomel in a mortar with pure potassium lij'drate, in excess; wash it with water, and dry it in the shade. Prop., tfc. A very dark grey or hlack powder, suffering decomposition hy exposure to liglit and air, becoming olive coloured, from a portion being resolved into metallic mercury and binoxide. Digested for a short time in dilute hydrochloric acid, it remains undis- solved, and the filtered liquid is not affected by potassium hydrate, or by ammonium oxa- late. It is totally solable in acetic acid, and entirely dissipated by heat. As a medicine pure mercurous oxide is one of the mildest of the mercurials, and is used both internally and externally ; but chiefly as a fumigant, or made into an ointment. — Dose, \ gr. to 3 gf. twice a day. MercnrcHS Phosphate, Syn. Htbeaegtei PHOSPHAS, L. Prep. Add a solution of mer- curous nitrate (slightly acidulated with nitric acid) to a solution of sodium phosphate, and wash and dry the precipitate which forms. In its physical characters it closely resembles calomel, than which it is said to be more ap- propriate in certain cases, especially in secon- dary syphilis. Alkalies turn it black. — Dose, I to 1 gr., made into a pill with sugar and aromatics. Mercurous Sulphate. Hg2S04. Syn. Stte- StTLPHATE OP MEECUET, SrLPHATE OF THE SUBOXIDE OF M., PEOTOSUIPHATE OP M.f ! HXDEAEGTEI SUBBUlPHAa, L. Prep. By adding sulphuric acid to a solution of mercu- rous nitrate. The salt falls as a white crys- talline powder. Mercurous Sulphide. Hg2S. Syn. Stjb- STTLPnATE OF MEEOUET ; HtDEAEOYEI SUB- SULPHtJEETUM CUM BTOPHTJEE, H. S. NI- aEUM, L. Prep. 1. (Pure.) This falls as a black precipitate when a solution of mercurous nitrate is treated with sulphuretted hydrogen or ammonium sulphide. 2. (Impure; Ethiops mineeal; Htdrae- GTEI SUIPHTJEETDM CDM BUIPHTJEE, H. S. wiaEUM— Ph. L. 1824 & Ph. D. 1826); jEthiops mineealis— Ph. L. 1836 & Ph. X>. 1826.) Quicksilver and sulphur, equal parts, triturated together in a stoneware mortar — Ph. U.) until globules are no longer visible. Prop., S^c. The last preparation of mer- curous sulphide is alone employed medicinally. It is a heavy, insoluble, black powder. It is frequently met with imperfectly prepared, and sometimes adulterated. It is said to be a mixture of" mercurous sulphide and sulphur, in variable proportions depending on the length of the trituration. On the large scale it is genenlly made by melting the ingredients together, and afterwards reducing the mass to a fine powder in a mill or mortar. It is said to be vermifuge and alterative, and has been used in some cutaneous and glandular dis- eases, but appears to be nearly inert. — Dose, 5 to 30 gr. Mercurous Tartrate. (P. Cod.) Syn. Peoto- TAETEATE OF MEEOITET. HtdEAEGTEI TAE- teas. Made by adding a solution of proto- nitrate of mercury in water, slightly acidu- lated with nitric acid, to a solution of tartrate of potash as long as a precipitate forms. Wash it with distilled water, dry it in the shade, and keep it in bottles covered with black paper. — Dose, 1 to 2 gr. MEKCUHT, Other Frepa,ratioiiB of. Mercury, Hahuemanu's. Syn. Hahne- mann's SOLTJBLE MBBCUEY, H.'s BI.ACB: OXIDE OP M., Black peeoipitate of m. ; Htdeae- OTEi PEa;cipiTAnrM niqeum, Mbecuehis SOLUBILIS Hahnemanni, L. — o. By dropping weak ammonia into a solution of mercurous nitrate as long as the precipitate formed is of a black colour ; the powder is washed, dried in the shade without artificial heat, and then preserved from the light and air. (Ph. Bor. 1847) Solution of mercurous nitrate (recent; sp. gr. I'l), 9i oz. ; distilled water, 2 lbs. ; mix, filter, and add to the solu- tion of ammonia (sp. gr. -960), i oz., diluted with water, 4 fl. oz. ; collect the powder im- mediately on a filter, wash it with water, 5fl. oz., and dry it, &c., as before. A very black powder. — Dose, i to 1 gr. Mercury, Precipitates of. 1. Black peeoi- pitate, Hahnemann's soluble mercury (basic mercurous and ammonium nitrate). 2. Geeen P. (MEECOBIUS PESCIPITATUS TIEIDIS, LA- CEETA TIBIDIS), from equal parts of mercury and copper, separately dissolved in nitric acid, the solutions mixed, evaporated to dryness, and then calcined until red fumes cease to arise. Caustic. 3. Red p., mercuric oxide. 4. White p., ammonio-chloride of mercury. Mercury, Ward's. Syn. Ammonio-niteate OP meecuey; Hydeaeoyei ammonij! kitsas, L. To nitric acid, 4 parts, contained in a spacious bolt-head or matrass, add, gradually, ammonium sesquicarbonate, 2 parts ; after- wards add of mercury, 1 part, and digest in a gentle heat, until the solution is complete. Mercury with Chalk. Syn. HYDEAEOTExna CUM Ceeta. Geey pow'dee (B. p.) Prep. Rub 1 oz. (by weight) of mercury, and pre- pared chalk, 2 oz., in a porcelain mortar, until metallic globules cease to be visible to the naked eye and the mixture acquires a uniform grey colour. — Dose. Prom 3 to 8 gr. A little water is said to aid in the extinc- tion of the mercury. Mr Bottle suggests a slight departure from the Grey modus operandi followed by the British Pharmacopoeia in the above preparation. He proposes to substitute for the tedious process of trituration in a porcelain mortar the agitation of the mercury with the chalk in a wide-mouthed glass bottle ; by which means the metal may be minutely subdivided, at a considerably less expendi- ture of time and labour. Mercury with Magnesia. (Ph. D.) Syn. Hydeaegyeum cum maonesia. Pure mer- cury, 1 oz., carbonate of magnesia, 2 oz. Bub together i n a porcelain mortar until the glo- MESLIN— METALS 1063 bulet cca.se to be visible and tbe mixture acquires a uniform grey colour. — Dote, 3 to 8 grainii. Mercury, YeUow Oxide of. (Ph. B.) Syn. HydBABQYRIOITDCM FLAVUM. Prep. Per- chloride of mercury, 4 oz. ; solution of soda (Ph. B.), i pints ; distilled water, q. s. Dissolve the perchloride in 4 pints of distilled water, adding the solution by the application of heat, and add this to the solution of soda. Stir them together, allow the yellow precipitate to sub- side, remove the supernatant liquor by d«- cantation, thoroughly wash the precipitated oxide on a calico filter with distilled water, and finally dry it by the heat of a water bath. MES'LIH. A mixture of various kinds of grain. (Brande.) BETAQAL'LIC ACID. Obtained by heating dry gallic acid, by a quick fire, to about 480° Fahr., or until it froths, melts, and becomes black and solid, then dissolving the residuum in an alkali, filtering, and precipitating by an acid. An insoluble, black powder. ME'TAl. Syn. Mbtallum, L. See Metals. METAL'LICA. [L.] Preparations of the mclaU. One of the divisions of the Ph. L. METAL'LIC TREES. See VEaETATiON (Metallic). METAL'LO-CHROMES. A name given by Nobili to extremely thin films of peroxide of load deposited by electrolytic action upon plates or polished steel, so as to produce an iridescent play of colours. The effect is olten very beautil'ul. MET'ALLOIDS. A name sometimes applied to the NON- METALLIC ELBMEMIS. METAL'LURGY. " The art of extracting metals from their ores, and adapting them to various processes of manufacture." (Percy.) "Notwithstanding the striking analogy which exists between common chemical and metallurgic operations, since both are era- ployed to isolate certain bodies from each other, there are essential differences which should bo carefully noted. In the first place, the quantity of materials being always very great in metallurgy, requires corresponding adaptations of apparatus, and often produces peculiar phenomena ; in the second place, the agents to be employed for treating great masses must be selected with a view to eco- nomy, as well as chemical action. In analyti- cal chemi^try, the main object being exactness of result and purity of product, little atten- tion is bestowed upon the value of the reagents, on account of the small quantity required for any particular process. But in smelting metals upon the large scale, profit being the sole object, cheap materials and easy operations are alone admissible."' The limits of this work do not permit of more than ■> general reference to the leading operations of metallurgy under this head. The»o are— digging, picking or sorting, stamp- « ' Ur«t Diet, of Arti, Manufacture«, and Mines," 441i edit. ing or crushing, and wa<>hing, included under the general term, • dressing ore ; ' — roasting or calcination, which is either performed with the fuel in contact with the ore, or in rever- beratory furnaces; and the liquation or reduc- tion to the reguline form. The application of these processes is noticed under the leading metals. Those who desire to study the sub- ject minutely are referred to the treatises of Dr Percy, Robert Hunt, Karsten, and Le Play. MET'ALS. Syn. MeTalla, L. Metals are elementary bodies, which are generally dis- tinguished by their lustre and power of con- ducting heat and electricity. When their solutions are electrolysed, the metals always appear at the electro-negative surface, and are hence termed electro-positive elements. Formerly, when science was much less ad- vanced than at present, the metals constituted a well-detined class. The propeities which were regarded as specially characteristic were physical, and were not founded on chemical relations ; thus, lustre and high specific gravity were considered to be essential cha- racters of all metals. But we are now ac- quainted with metals which have a lower specific gravity than water (litliiuin, sodium, &c.), and with so-called non-metallic elements which present a strong metallic lustre (carbon in the state of graphite,crystallised silicon). It will therefore be seen that the term 'metal' is rather conventional than strictly scientific. By far the greater number of elementary bodies at present known are metals. Their physical characters and leading chemical pro- perties are noticed under each of them in its alphabetical place. The following table ex- hibits some useful particulars : — Table of some of the properties of some of the metals. Names arranged in the order of their Dactility. MiilleuUility. Gold. Gold. Silver. Silver. Platinum. Copper. Iron. Tin. Nickel. Platinum. Caliper. Lead. Zinc. Zinc. Tin. Iron. Lead. Nickel. Nunies arranged in the order of their /puwer of coiidacting Beat. Silver. Copper. Gold. Tin. Iron. Lead. Bismuth. Power of conducting Electricity. Silver. Copper. Gold. Zinc. Iron. Tin. Lead. Antimony. Bismuth. 1064 METANTIMONIC ACID— MICBOSGOPE METANTIMON'IC ACID. HiSb^,. The name given by M. Fremy to that vai-iety of aattmonic acid obtained by decomposing pen- tacliloride of antimony with excess of water. It differs from common antimonio acid in being tetra, and forming two different classes of salts with the acids. The acid metanti- moniate of potassium is the only reagent which yields a precipitate with the sodium salts, and is therefore of great value in chemical analysis. It is prepared by fusijig antimonio acid with excess of potassa, in a silver crucible, dissolving the fused mass in a little culd water, and allowing it to crystallise in vacuo. The re- sulting crystals (metantimoniate of potassa), by solution in pure water, are resolved into free potassa and the acid salt. See Anti- mony. METAPEC'TIC ACID. See Pectin. METAPEC'TIN. See Pectin. METAPHOSPHOE'IC ACID. See Phos- THOEIO ACID. METHEG'LIN. Syn. Hydeomeli, H. TI- NOSUM, Mellis visum, L. JPrep. From honey, 1 cwt. \ warm water, 24 galls. ; stir well until dissolved ; the next day add of yeast, 1 pint, and hops, 1 lb., previously boiled in water, 1 gall.; along with water q. s. to make the whole measure 1 barrel; mix well, and ferment the whole with the usual precautions adopted for other liquors. It contains on the average from 7§ to 8f of alcohol. See Mead. ME'THYL. CHj. The hypothetical radical of PTEOXTLIO SPIKII (wOOD-BPIKIT, METHYLIC AICOHOL) and the methyl series. It forms a number of compounds analogous to those of ethyl. METHYLAMINE. Syn. Mbthyha. CHg, HjN. A colourless gas possessing a very powerful odour of ammonia, and a strongly alkaline reaction. It differs from ammonia, however, in being non-inflammable. In other respects it bears a considerable resemblance to It. Water at 55° Pahr. dissolves more than eleven hundred times its bulk of methylamine. It may be easily condensed to a liquid by means of a freezing mixture. To obtain it nascent hydrogen is made to react on prussic or formic acid. Methylia exists in herring brine, and is a frequent product of the destructive distillation of sub- stances containing nitrogen. Most of its salts are verv soluble in water. METHYLATED SPIRIT. A mixture of 1 part of methylic alcohol (wood spirit;) and 9 parts of ethylic alcohol (spirit of wine). See Spirit. METHYLENE CHLORIDE. CHjCla. Syn. Methylene bichloride. There are various methods of obtaining this compound : — 1. By heating chloroform with zinc filings and dilute sulphuric acid. 2. By acting on me- thylene iodide with chlorine. In this process prolonged treatment with chlorine, at ordinary temperatures, is required to remove the last traces of iodine. (Buttlerow.) Chloride of methylene is a colourless mobile fluid, having a smell like chloroform, and a burning taste. It is used as an aneesthetic in place of chloro- form. According to Dr Armstrong, the sub- stance known as methylene ethbe is a me- chanical mixture of bichloride of methylene and ethylic ether. Dr Richardson says of this latter it is not so quick in its action as the methylene chloride, bnt that it is safer. See Anjfsthettcs METHYLIC AIiCOHOI. See Wood Spibit. MEZE'EEON. Syn. Gaeou; Mezebeon BARK, MeZEEEI COETEX (B. P.); MeZEEEON —Ph. L., E., & D. The dried bark of the Daphne Mexereum, mezereon ; or Daphne Laureola, spurge, or wood-laurel. The " bark of the root of Daphne Mezereum," or spurge olive. (Ph. L.) A stimulant and diuretic. It is employed as a sudorific and alteiative, in syphilis, rheumatism, scrofula, and chronic cutaneous diseases, usually in conjunction with sarsaparilla. It has also been used as a mas- ticatory in toothache, paralysis of the tongue, &c. On the Continent it is used as a vesicant. For this purpose it is softened by soaking it in hot vinegar, and is then bound on the part, and renewed after intervals of some hours, until vesication is produced. MICE. See Rat3. MI'CEOSMIC SALT. NaNH4HP04, Syn. Teibasic phosphate op sodium and ammo- nium. Prep. 1. Phosphates of soda and ammonia, equal parts ; water, q. b. ; dissolve separately, mix the solutions, evaporate, and crystallise. A slight excess of phosphate of ammonia aids the crystallisation. 2. (Pownes.) Phosphate of sodium, 6 parts ; water, 2 parts ; liquefy by heat, and add of sal ammoniac (in powder), 1 part ; common salt separates, and after its removal the liquid is concentrated so that crystals may form. Used as a flux in blowpipe assays. MrCEOSCOPE. The value of the micro- scope in chemistry and the collateral sciences is now so generally acknowledged that it would be folly to do more than merely allude to the subject here. In the compound microscope, which has quite superseded the ' simple microscope' as an instrument of research, the object is magnified in the first instance by the object-glass, and then remagnified by the eye-piece. It follows, therefore, that the magnifying power of the instrument may be increased either by increas- ing the power of the object-glass or that of the eye-piece. It must be borne in mind, how- ever, that in increasing the power of the eye- piece we do not magnify the object itself in a greater degree, but simply increase the image of the object formed by the object-glass. Any imperfections which may exist in the latter are thus greatly increased. At first the great drawback to the use of the compound micro- scope was its deficiency in achromatism; but the researches of Mr licster and Dr Goring led to the aehromatising of the object-glass. MILDEW— MILIARY FEVER 1065 which n-as the first of the rapid stridea to- wxrda pertVction made by this instrument during the Inst twenty years. The two most useful ohject-glassea are the 'quarter-inch/ which ahould magnify from 200 to 220 dia- meters, and the ' inch,' which ahould magnify from 30 to 40 diameters. The definition of tlieae gliiascs ahould be good, and they should transmit plenty of light. Any linea in a structure examined by them should appear shiirp iinil distinct, and there should be no coloured t'ringea around the object. It is of great importance that the object-glasses are kipt pcrfeitly free from dust. A few shreds of wash-leal liir of the finest quality should be kept in n pill-box for cleaning them. Before rubbing them with the leather they may be breallied upon, but no whiting or liquid of any kind should be used, aa each object-glass, being achromatic, ia a very delicate piece of workmanship, consisting of two lenses of flint and crownglasa cemented together by Canada balsam. Compound microscopes are now aold by the best London makers at very low pricea. A really good instrument, adapted to most of the wants of the chemical, pharmaceutical, or me- dical student, may be obtained for five guineas. The following formuliD for the preparation of the chief substances, togetlier with the principal reagents required in the working of the microscope, are from Dr Lionel Beale's valuable book, ' How to Work with the Microscope :'' Seagents — 1. Alcohol, of various strengths. 2. Ether, to dissolve oil globules. 3. Nitric acid (1 part of atrong acid to 5 of water) 4. Sulphuric acid (1 to 5). 5. Hydrochloric acid. 6. Acetic acid, glacial and dilute (1 to 5). 7. Chromic acid, very dilute, to harden tissues. 8. Solution of potash, saturated and dilute (1 to 10). 9. Solution of soda (25 gr. of fused soda to 1 oz.). 10. Ammonia (1 part of the strongest solu- tion to 3 of water). 11. Nitrate of baryta, a cold saturated solu- tion of. 12. Nitrate of silver (120 gr. to 2 oz.). These two are for the mineral acids. 13. Oxalate of ammonia in solution. Test for lime. 14. Solution of iodine saturated, t". e. 1 to 7000 parts of water. Another solution is — 1 gr of iodine and 3 of iodide of potassium in 1 oz. of distilled water. 1. Cements. — I. Brumnoiek Black. Boil together k lb. foreign asphaltnm and i\ oz. of linseed oil (previously thickened with litharge), then mix to a proper consistence with oil of turpentine (about 1 pint). 2. Gold iSize. Boil 25 parts of linseed oil ' Hnrrisou, 69, Pall Mall. with 1 of minium and ^ri part of umber for 3 hours ; pour off the clear fluid, and mii with equal parts of powdered white lead, and yellow ochre, added in small succe-sive portions. Then boil well the whole again, and pour off the clear fluid. It dries slowly, but firmly. Both this and the last are dissolved by turpentine. 3. Ooadbtf's Marine Olue. Dissolve sepa- rately in coal naphtha equal parts of shell-lac and India rubber. Mix thoroughly with heat. 4. Sealing-wax Varnish. Dissolve the best sealing-wax in enough atrong spirit of wine to reduce it to the proper consistence. This is brittle. 5 Canada Balaam. This dries sponta- neously. Solutions of shell-lac, gum, and various other ccmentf and glues are employed by microscopic manipulators. Preservative Fluids. Canada balsam, spirit and water, glycerin, solution of gelntin, satu- rated solution of alum, chloride of zinc, and chloride of calcium, are all used to preserve microscopic objects. The following formulie will be found useful : — 1. Ooadbg's Solution. Bay salt, 4 oz. ; alum, 2 oz. ; corrosive sublimate, 4 gr. ; boil- ing water, 4 pints. Mix and filter. It may often be more diluted. 2. T/iwaite's Fluid, Mix spirit of wine, 1 oz., with creosote suflicient to saturate it; rub up with chalk to form a thin paste, and mix gradually with 16 oz. of water. To this may be added an equal quantity of water, saturated with camphor. 3. Simple Creosote Solution. Dissolve creo- sote, 1 dr., in pyrolifjneous acid, 1 dr., and mi."C gradually with cold water, 1 pint. 4. FassinVs Solution. For blood-globules, nerves, and white tissves generally . Perchloride of mercury, 1 part ; chloride of sodium, 2 parts; glycerin, 13 parts; distilled water, 113 oarts. MIL'DEW. Syn. KrsT, Blight." The mouldy appearance on the leaves of plants produced by innumerable microscopic fungi. The hop, wheat, and the choicest garden fruit trees, are those most commonly attacked. The causes are said to be excess of moisture, and absence of the free circulation of air and sun- shine. On the small scale, finely powereil sulphur is occasionally dusted over the parts affected, aa a remedy. MILIARY FEVEE. Syn. Miliabia, L. Among the other symptoms are — anxiety and frequent sighing, the perspiration has a strong and peculiar smell, and there is a sensation of pricking on the neck and breast, followed by an eruption of small red pimples, which in two or three davs become white vesicles, dry up, peel of, and are succeeded by others. The moist weather of spring and autumn are the periods in which it is most prevalent; and de- licate females, particularly in child -bed, are those most liable to its attacks. Snmetimes it assumes a m:dignant character. The treat- ment of this affection con.-.ists chiefly in com- 1066 MILK bating the depression of the system hy a sup- porting diet; but everything that lieats or stimulates the skin should be avoided. The apartment should be kept cool and well venti- lated, and cooling saline laxatives and bitter tonics, with cooling drinks, should also be had recourse to. MILK. Si/n. Lac, L. The value of milk as an article of food is clearly shown by the fact of it being sufficient to support, and to increase the growth of, the young of every species of the mammalia; at once supplying materials for the formation of the osseous, fleshy, and liquid portions of the body. " The substances present in milk are wonderfully adapted to its office of producing materials for the rapid growth and development of the animal frame. It contains an azotised mat- ter, casein, nearly identical in composition with muscular flesh, fatty principles, and a pecu- liar sugar, and, lastly, various salts, among which may be mentioned phosphate of lime, held in complete solution in a slightly alkaline liquid. " The white and almost opaque, appearance of milk is an optical illusion. Examined by a microscope of even moderate power, it is seen to consist of a perfectly transparent fluid, in which float about numbers of minute transpa- rent globules; these consist of fat surrounded by an albuminous envelope, which can be broken mechanically, as in the churning, or dissolved by the cliemical action of caustic potassa, after which, by agitating the milk with ether, the fat can be dissolved." (Fownes.) Comp. Cows' MILK, of average quality, contains from lOg to 12g of solid matter when evaporated to dryness by steam heat, and has the mean sp. gr. 1-030; while that of the skimmed milk is about 1'035; and of the cream, 1'0244. (Ure.) The average ceeam of cows' milk contains 4-5g of butter, 3-5§ of curd, and 92g of whey. (Berzelius.) The skim- med MILK consists of water, 92-9g ; curd, 2-8g 5 sugar of milk, 3-5g; lactic acid, lactate of potassa, and a trace of lactate of iron, -eg, chloride of potassium, phosphate of potassa, and earthy phosphates (lime), ■26. (Berzelius.) The following analysis of fresh milk is by M. Hnidlen :— Water 873-00 Butter 30-00 CasKin 48-20 Milk sugar 43-90 Phosphate of lime 2-31 „ magnesia •42 „ iron •07 Chloride of potassium 1-44 „ sodium •24 Soda in combination with' casein . . • •42 1000. Professor Wanklyn has devised and pub- lished in his excellent little manual 'Milk Analysis'' a process by which a very thorough chemical examination of milk may be accom- plished with great facility and expedition. In his preliminary remarks he condemns, as utterly unreliable and misleading, the infer- ences to be drawn from those hydrometric in- struments, the lactometer or lactodensimeter, and creamometer. " A very little considera- tion," he says " will suffice to make intelligible the obliquity of the indications of the lacto- meter and to show how untrustworthy it must be. The lactometer, as of course will be un- derstood, is simply the hydrometer applied to milk ; and readings of the instrument are nei- ther more nor less than speciflc gravities. The more milk-sugar, and casein, and mineral matter there is in a given specimen of milk, the greater (other things being equal) will be its density or specific gravity, and the higher the lactometer reading. " If, however, fat globules (as happens in the instance of milk) be diffused through the fluid, then, because fat is lighter than water, the eff'ect of the other milk solids on the gra- vity of the liquid, will be more or less neu- tralised. The density of milk -fat is about 0-9, water being 1-0. Now, if a solution of casein and milk-sugar, of specific gravity 1-030, be sufficiently charged with fat globules, its spe- cific gravity may be sent down even below the gravity of water. How much would be re- quired to bring about such a result is a mat- ter of simple calculation. " This being understood, it will be obvious that if the specimens of milk difl'er in specific gravity, there must be two distinct and equally valid ways of accounting for the difference. " The milk with the lower gravity may be milk let down with water, or let down with fat, i. e. milk let down by being enriched." In support of this last assertion Professor Wanklyn quotes corroborative instances af- forded by the examination of different speci- mens of milk known as ' strippings,' these being the last portions of milk yielded by the cow at the termination of the milking. All these 'strippings' had a, lower specific gra- vity than normal milk. Further, Professor Wanklyn points out that the specific gravity of organic fiuids is a falla- cious index of the amount of solids they may contain, as is illustrated by the fact, that whilst a 10 per cent, solution of chloride of Potassium has a specific gravity of 1-065 at 5° C, and a 10 per cent, solution of casein and milk sugar, has a specific gravity of only about 1-035. The creamometer meets with equal con- demnation in Professor Wanklyn's little book, since different specimens of milk vary consi- derably in their yield of cream, and a perfectly pure sample of milk may yield less cream than one which has been tampered with. A complete analysis of milk involves the determination of the water, the fat (the essen- ^ Trubuer and Co. MILK 10C7 tial constituent of tho cream), the casein, niilk-auL'iir, and ash. The following is an outline of Professor Wanltljn'a neat and ingenious method of analysis: — Ily means of an accurately {graduated pipette, lie tir>t places 6 cubic centimetres of tlie milk in a small weighed platinum dish (about 14 grammes in weight) just previously ensuring the sample from which the milk is taken being thoroughly mixed. The dish is then placed over a water-hath (the water in which must be kept vigorously boiling the whole time) for three hours, at the end of which time all the water having been driven off, there will remain in the dish a completely dried up residue. The increase in weight between the empty dish and the residue, will give the weight of the ' milk solids ' from 6 c.c. of milk. Of course, if tliis weight be multiplied by 20, the yield Irom 100 c.c. of milk will be obtained. To reduce this to a percentage statement it is necessary to remember that 100 c.c. of ave- rage milk weigh 102'9 grammes. The next proceeding consists in the determination of the fat. This is done by treating the dried milk solids resulting from the 5 c.c. of milk with ether. There are several important mi- nutiiB necessary to bo observed in connection with this part of the process, for the parti- culars of which the reader is referred to Pro- fessor Wanklyn's book. Suffice it to say, that if properly performed, the whole of the fat is dissolved by the ether, and being separated from the non-fatty portion of the residue is weighed and calculated as ' fat.' If, then, the amount found as fat be deducted from the whole of the milk solids previous to their treatment with ether, the ' milk solids, not fat,' will be arrived ut. Professor Wank- lyn estimates the casein ' as follows :— He treats the milk solids, not fat, with hot alcohol, by which moans he dissolves out from them, and removes the milk-sugar and the soluble chlorides. The remaining residue, consistinc; ol iMsein and phosphate of sodium (chemi- cally combined with the casein), is dried on a water-bath until it ceases to lose weight. It is tlieu weighed along with the vessel con- taining it, and ignited. The combined weight of tlie vessel and phosphate of sodium remaining after ignition being deducted from the weight previous to ignition, the difference is the casein. Another and quicker method, recommended by Professor Wanklyn, for the determination of the casein, is to measure it by the amount of albuminoid ammonia it is capable of yield- ing when subjected to the 'albuminoid am- monia process,' invented by Messrs Wanklyn, Chapman, and Smith. The alcoholic solution filtered off from the combined casein and posphate of soiiium, contains the milk sugar aud soluble chlorides. ' Under the head " Casein " Pr..f Wanklyn includes tlje entire nitru}£enuu3 nuitenaU uf niilk It is evaporated to dryness on a water-bath, and the residue with the vessel containing it, is weighed. It is then gently ignited, and the weight of the remaining residue being de- ducted from the total weight before ignition, gives the yield of milk sugar. Or the milk sugar may be determined by trituration with a standard copper solution. For the determination of the ash it is only necessary to ignite the milk solids from 5 c.c. of milk, in the small platinum dish, by which operation all the organic matter being driven otf, that which remains behind constitutes the ' ash ' aud is weighed .as such. It will be obvious that in order to deter- mine with anything like rigid accuracy the quality of any sample of milk by analysis, not only must a normal standard for tlie purpose of comparison bo adopted, but such normal standard must represent very closely and with but little variation the deKnite composition of all sound and genuine milk. Professor Wanklyn says that "the following, which is the result of several concordant ana- lyses of country-ted milk, may be taken as representing normal milk. In 100 grammes of milk — . 12'5 grammes. . 87-5 Solids (dry at 100° C) Water 100-0 " The 125 grammes consist of 9'3 grammes of ' solids which are not fat,' and 32 granimrs of fat." The above data, which are founded on the examination of a very large number of different samples of milk, are confirmed by the researches of Miillerand Eisenstuck, who were employed by the Rnyal Agricultural Society of Sweden in a similar investigation. The labours of these chemists extended over a twelvemonth, and the result of them was to show that the milk yielded day by day, for a whole vear, by a herd of cows was remark- ably constant in composition. Professor Wanklyn gives the following for- muliB for the calculation and statement of the results of milk analysis. He says. Treat- ing the question quite rigidly, which I believe is the proper way of dealing with it, we arrive at the following : — Prohlem 1. Given the percentage of ' so- lids, not fat' ( = o), in aspeiimen of sophisti- cated milk (i. e. milk, either watered, or skimmed, or both)— required the number of grammes of genuine milk which was employed U) form 100 grammes of it. Answer. Multiply the percentage of 'so- lids, not fat' by 100, and divide by 9-3. Or— 100 a. 9-3 Problem II. — Given the percentage of ' sohds. not fat ' (= a), also the percentage of fat (= h), in a specimen of sophisticated milk— required the number of grammes of 1068 MILK fat which have been removed by skimming from the genuine milk which was employed to form 100 grammes of it. Amuier. — 3'2 —^ a — b. 9-3 In translating fat into cream, the rule is that a removal of 0'2 gramme of fat equals a removal of 10 gramme of cream. This rule is directly founded on experiment. I do not, however, claim a high degreee of accuracy for the measurement of the cream. Finally, a slight refinement may he noticed. If a specimen of sophisticated milk has been produced by both skimming and watering, it will be obvious, on consideratiun, that the ex- traneous waters employed in manufacturing 100 grammes of it is equal to the difference between 100 and the quantity of genuine milk employed to make 100 grammes of sophisti- cated milk, together with a quantity of water equal to that of fat removed by skimming. 100 3-2 Extraneous water= 100 a + — a—b 9-3 9-3 100 + 3'2 = 100 a—b 9-3 Save for the purpose of finding out the presence of matters other than an excess of water in the milk (a contingency regarded as very improbable), the estimation of the casein and milk sugar is unnecessary. The deter- iiiination of the ash is for the object of learning If foreign mineral matters, such as chalk or any other inorganic impurity, are present. Professor Wanklyn says he believes that such like extraneous bodies are never em- ployed. The chief, if not the sole, form of dishonesty are watering and skimming. The amount of ash, however, is a good cri- terion as to the extent of dilution that has been practised, a deficient amount being, of course, confirmatory of a watered milk. The determination of the amount of ' solids, not fat,' is, in almost every instance, all that is necessary to enable an opinion to be arrived at as to whether the sample of milk has had water added to it or not. Out of filty-six samples of milk supplied to the different London unions in 1873, Professor Wanklvn reports that he found only fifteen unwatered, or nearly unwatered. Of these fifteen samples nine had been skimmed, leaving only six that were at once unwatered and unskimmed. These figures, therefore, show that only about 10 per cent, of the milk supplied iu the above year to the Metropolitan unions was genuine. He adds — " It is curious to compire the language of the contract under which (as it appears from Mr Rowsell's report) the dealer supplied the various unions with milk, with the quality of the article as exliibited by the analysis. ' New unskimmed milk una- dulterated,' ' genuine as from the cow,' * best new unskimmed milk, to produce 10 per cent, of cream,' occur in these contracts." Prop. These are well known. Perfectly fresh milk is slightly alkaline, but soon be- comes acid on exposure to the air, and after a time white coagula of casein (CI7SD8) sepa- rate from it. This change is immediately effected by the addition of rennet or an acid. That from the first, when dried and pressed, constitutes cheese. Fur., Tests, Sfc, The common frauds prac- tised by the milk-dealers are the addition of water and the subtraction of part of the cream. Sometimes potato starch is added to the milk, to give it a creamy or rich appearance, and this addition is still more frequently made to cream, to increase its consistence and quality. The presence of potato starch may be determined by boiling some of the milk with a little vinegar, and after separating the coagulum by a strainer, and allowing the liquid to become cold, testing it with solution or tincture of iodine. If it turns blue, starch, flour, or some other amylaceous substance, has been used to adulterate it. In most cases it will be sufficient to apply the test to the un- prepared suspected milk. It has frequently been stated that chalk, plaster of Paris, gum, gelatin, sugar, flour, mucilage of hemp-seed, the brains of animals, and other similar substances, are often added to London milk, but there is no reason to suppose there is auy truth in these assertions, as some of these articles are too costly to be used, and the presence of others would so alter the flavour or appearance of the milk, or would so soon exhibit themselves by sub- sidence, as to lead to their detection. Fres. Milk may be preserved in stout bottles, well corked, and wired down, by heat- ing them, in this state, to the boiling-point, in a water bath, by which means the oxygen of the small quantity of enclosed air becomes absorbed. It must be afterwards stored in a cool situation. By this method, which is also extensively adopted for the preservation of green gooseberries, green peas, &c., milk will retain its properties unaltered for years. A few grains of carbonate of magnesia, or, still better, of bicarbonate of potassa or soda, may be advantageously dissolved in each bottle before corking it. Under Bethel's patent the milk or cream is scalded, and, when cold, strongly charged with carbonic-acid gas, by means of a soda-water machine, and the corks are wired down in the usual manner. The bottles should he kept inverted, in a cool place. An excellent method of preventing milk from turning sour, or coagulating, is to add to every pint of it about 10 or 12 gr. of carbonate or bicarbonate of soda. Milk thus prepared may be kept for eight or ten days in tem- perate weather. This addition is harmless, and, indeed, is advantageous to dyspeptic patients. According to D'Arcot, ^trotb part MILE 1069 of the biciirbonnte is sufficient for tlie purpose. Au excess of nllcali uatd in this niauner may b.' detected by tlie milk turning turmeric paper brown, oven after it has been kept some hours, and by the ash obtained by erapo- ratinf^ a little to dryness, and then heating it to dull redness, ifftTveacing with an acid. (See baloto.) *«* Milk should not be kept in lead or zinc vessels, as it speedily dissolves a portion of tlienc metals, and becomes poisonous. Concluding Remarki. The piincipal differ- ence between cows' milk and human milk con- sists in the former containing more casein and less sugar of milk than the latter. The re- markable indisposition to coagulate is another character which distinguishes human milk from cows' milk. Prof. Falkland, who has practically investigated the subject has pre- pnrud II nutritive fluid for infants from cows' milk, closely resembling that of the iiealthy adult woman. His process is, however, unne- cessarily complicated, and, therefore, unsuited to those who would have to employ it in the nursery. To remove this objection we have adopted the following formula : — Sugar of luilk, 2 oz. ; hot water, \ pint ; dissolve, and, when the liquor has become quite cold, add it to fresh cows' milk, } pint, and stir them together. This quantity, prepared morning Hud evening, will constitute the proper food for an infant of from 5 to 8 months old. More may be allowed it if it 'craves' it; but there must be no 'cramming.' At first it will be advisable to remove a little of the cream from the milk before adding to it the saccharine solution ; but after a few days this will be found to be unnecessary, and, indeed, injnrious. One very important particular to be attended to is, the employment of pure cows' milk, obtained from a healthy grass-fed animal only. With this precaution, and the use of ft good FEEDlNGhBOTTLE, the infant will thrive nearly as well as on the breast of any humnu female, excepting its mother's. (See below.) ' AasES' MILE closely resembles human milk In eulour, smell, and consistence, but it con- tiins rather less cream. (See below.) Ewes' mile closely resembles cows' milk, than which, however, it is slightly richer in cream. Goats' milk, for the most part, resembles cows' milk, hut its consistence is much greater, and it contains much more solid matter. (See below.) Mabes' mile, in consistence; is between that of cows' and human milk. Its cream is not converted into butter by agitation. See BcTTEB, Cheese, Lactic Acid, &c. Mili as u cauae or carrier of disease. — Milk of a mother labouring under strong mental emotion is, as is well known, capable of seriously endangering the health of the suckling babe. Payne narrates the case of a wumim sutfering uuder a nervous aflection whose milk, two hours after an attack of the disease, became viscid, like the white of an egg. Similarly, a deterioration and consequent alteration in properties is iodnced in the milk of the cow if she be over driven, exhausted, or harassed. The food of the animal like- wise exercises au in6uence on the quality of its milk ; thus when cows are fed on turnips, wormwood, decayed leaves, and plants of the cabbage or onion famishes, the flavour of these substances is imparted to their milk. The milk of animals that have fed on poisonous or deleterious jilants is capable of setting np toxic symptoms in human beings partaking of it. In June, 1875, the inhabitants of a certain quarter of Rome were attacked with an epide- mic, distinguished by great gastro-intestinal irritation. The cause of the outbreak was traced to the use of goats' milk, yielded by goats that had eaten of the meadow saS'ron, the Colchimim autumnale. It also appears that in the Western States of America the milk of cows that have fed on the poison-oak, the Shus toxicodendron, has on several occa- sions given rise to attacks of illness in children, marked by extreme weakness, vomit- ing, fall in bodily temperature, swollen and dry tongue, and constipation. Boiling seems to remove the dangerous properties of the milk. Milk, as has been ^hown by Fuchs, is some- times infested by a fungus, the Oidium lactit or PenicilUum, which is capable of giving rise to gastric irritation, and sometimes to severe febrile gastritis.' Although the evidence as to the power of the milk of animals affected with epizootic diseases to convey the particular affection to human beings is contradictory, there is little reason to doubt that soured milk may become a carrier of infection from the ailing or con- valescent subject to the healthy one. Typhoid and scarlet fever have been known to have originated in this manuer. The outbreak of the former malady in Marylebone in 1874 was traced to the con- tamination of milk by the remains of the water which had been used in rinsing the milk pans. This water had been obtained from a well into which the excrete from a typhus patient had percolated from a privy. At Leeds a similar outbreak was caused by the absorption by the milk of the typhoid eflluvium. In the case of scarlet fever the malady has been conveyed by means of the throat-discharges and cuticle falling into the milk from the persons of servants and others employed in dairies. Milk, Al'mond. See EiinisiON and Mix- tube. Milk, Arrowroot. Prep. From arrowroot, 1 table-spoonful, first wetted and stirred with a little cold water, afterwards adding, gradu- ally, of boiling water, i pint ; and, lostly, of boiling milk, i pint ; with sugar, spice, wine, &o., to palate. Very nutritious, and excellent I ParkeB. 1070 MILK in chronic diarrhoea. Some persons employ all milk. Milk, Choc'olate. Prep. Dissolve chocolate (scraped), 1 oz., in boiling new milk, 1 pint. Nutritous; but apt to offend delicate sto- machs. Milk, Coffee. Prep. 1. C"ffee, 1 oz.; boiling water, i pint; infuse for 10 or 15 minutes in a warm situation, and add the strained liquid to bailing milk, | pint. 2. Coffee, 1 oz. ; tie it loosely in a piece of muslin, and simmer it for 15 minutes in milk, 1 pint. Both the above have been recom- mended for persons of spare habits, and for those disposed to affections of the lungs, more especially for the asthmatic. Milk, Faeti"tlons. Syn. AbtificiaIi miik. Of the numerous compounds which have been proposed as substitutes for natural milks, the following are examples : — 1. (Factitious asses' milk ; Lac asini- UUM PACTITIUM, LAC A. AETIFIOIALE, L.) — O Cows' milk, 1 quart ; ground rice, 1 oz. ; oringo root (bruised), 1 dr, ; boil, strain, and add sugar candy (or white sugar), 1 oz. b. Whites of 2 eggs ; lump sugar, 1 oz. ; cows' milk (new), % pint ; mix, then add syrup of tolu, f oz. c. Water, 1 pint ; hartshorn shavings, 1 oz. ; boil to a jelly ; then add lump sugar, 2 oz. ; cool, add new milk, 1 pint; syrup of tolu, i oz. Used as substitutes for asses' milk, taken freely as a beverage. A cupful, with or without a spoonful of rum, 3 or 4 times daily, is a popularremedy in consumption and debility. 2. (?. goats' MILK — A. T. Thomson.) Fresh mutton suet (minced), 1 oz. ; tie it in a muslin bag, and boil it in cows' milk, 1 quart; lastly, add of sugar candy, 2 gr. In scrofu- lous emaciation, and in the latter stages of phthisis. The proportion of suet in the above may be advantageously increased a little. The LAC CUM SERO of Guy's Hospital is a similar preparation. 3. (P. HUMAN MILK ; LaC HUMANUM PAC- TITIUM, L.) — a. See above. b. (Bosenstein.) Almonds (blanched), 2 in number ; white sugar, 1 dr. ; water, 4 fl. oz. ; make an emulsion, strain, and add of fresh cows' milk, 6 fl. oz. As a substitnte for the breast in nursing. Milk, Preserved'. Syn. Milk powdee; Laotis pulvib, Lao pulveeaium, L. Prep. 1. Fresh skimmed milk, 1 gall. ; carbonate of soda (in very fine powder), IJ dr. ; mix, eva- porate to l-3rd by the heat of steam or a water bath, with constant agitation, then add of powdered white sugar, 3i lbs., and complete the evaporation at a reduced temperature ; reduce the dry mass to powder, add the cream (well drained) which was taken from the milk, and after thorough admixture put the whole into well-stoppered bottles or tins, which must be at once hermetically sealed. 2. (Legrip.) Carbonate of soda, i dr.; water, 1 fl. oz. ; dissolve, add of fresh milk, 1 quart ; sugar, 1 lb. ; reduce it by heat to the consistence of a syrup, and finish the eva- poration on plates by exposure in an oven. Obs. About an ounce of the powder agitated with a pint of water, forms an agreeable and nutritious drink, and a good substitute for milk at sea. It may also be used for tea or coffee in a solid form. This process, whicii it very old, has been recently patented. See Milk {above). The condensed or preserved milk, now in such general use, and which is met with in tins as milk which has been more or less de- prived of water by evaporation in vacuo. It occurs in the market in two forms — in one simply as condensed milk, and in the other as condensed milk mixed with a large quantity of sugar. Milk preserved as above without sugar will keep only for two or three days ; whereas with sugar it may be preserved for an almost indefinite time. Either variety mixed wjth the proper quantity of water becomes normal milk again, the sweetened kind being, of course, milk with the addition of a considerable amount of cane sugar. Professor Wanklyn says be has examined the principals brands of preserved and condensed milk sent to the London market, and finds they contain their due proportion of fat. He gives the following analyses of the pro- duce of the English Condensed Milk Company : Pbesekved Milk. In 100 )arts by weight. Water . . . 20-5 Fat , . 10-4 Casein . , . 110 Ash , . 20 Cane and milk sugar . 561 100-0 Condensed Milk. Water . . 51-12 Fat . 1211 Casein . 13-64 Milk sugar . . 20-36 Ash . . 2-77 100-00 Eoses, Milk of. Syn. Lac boss, L. Prep. 1. (English.) — a. Almonds (blanched), 1 oz.; oil of almonds and white soft soap, of each 1 dr. ; rose water, 1 pint ; make an emulsion. b. Prom liquor ofpotassa and oil of almonds, of each 1 fl. oz. ; hot water, 2 fl. oz, ; agitate together until mixed, then add of rose water and distilled or filtered soft water, of each ^ pint, and again agitate well. c. As the last, but using half a tea-spoonful of salt of tartar for the liquor of potassa. d. (Redwood.) Blanched almonds, 8 oz. ; rose water, 3 pints; make an emulsion, add of white Windsor soap, white wax, and oil of almonds, of each J oz. ; previously melted together by ii gentle heat ; triturate until MILK FEVKR— MINERAL CHAMELEON 1071 united, and strain ; lastly, add a solution of oil of bergnmut, i oz.; oil of lavender, 1 dr.; and attar of roses, i dr. ; (dissolved in) recti- fied spirit, 12 oz. 2. (Kbbnch.) — a. From rose water, 1 quart j tinctures of benzoin and st;rax, of each 1 tt. oz. ; spirit of rosea, i fl. oz. ; rectified spirit, 1 fl. oz. ; mix. b. (Augustin.) Tincture of benzoin, i fl. oz. ; liquor of carbonate of potassa, 2i fl. dr. ; rose water, i pint; agitate well together. As a lotion in acne. C-. (Cfianinni.) Tincture of benzoin, 1 dr. ; tincture of balsam of Peru, 20 drops; rose water, 1 pint ; as the last. d. (Scliubartb.) Almond paste, 3 dr. ; rose water, ^ pint ; tincture ot benzoin, § fl. oz. As before. The addition to the last 3 of a little rectified spirit is an improvement. 3. (Ukuhan.) From dilute solution of di- acetate of lead (Goulard water), and spirit of lavender, of eacli 1 fl. oz. ; rose water, 6 fl. oz. ; soft water, 1 pint. Obt. All the above are used as cosmetic washes, and to remove scurf, pimples, and eruptions, in slight cases. Hilk, Sa'go. Si/n. Lac baoo, L. Prep. (Dr A. T. Thomson.) Sago, 1 oz. ; cold water, 1 pint ; macerate half an hour, pour oflP the water, add of milk, li pint, and boil slowly until the sago is dissolved. Very nutritious ; also in lieu of arrow-root milk. Milk of Snlphnr. See Svlfhitb (Precipi- tated). Uilk, Thick. Mix one tnble-spoonf ul of flour with a pint of milk, and boil for ten minutes, stirring it well the whole time. It may be flavoured either with a little salt, or sugar. Uilk, Vanilla. Sj/n. Lao takili.^, L Prep, 1. Essence of vanilla, 12 drops; lump sugar, 1 oz. ; triturate, and add gradually, new milk, 1 pint. 2. (Beral.) Vanilla sugar, i oz. ; milk, 16 oz. ; dissolve. MILK FEVER. S^n. Febdis laotea, L. A febrile condition of the system thut some- times occurs ut the time the milk begins to be secreted alter parturition. It often assumes a malignant character. See Puerpebal Fevek. UUi'LEX. S^n. Milium, L. Several va- rieties of grain arc known by this name. That commonly referred to under the name is the produce of Panicum miliaceum (' Indian millet'). The husked seeds (milium munda- TUm) are used to make gruel, and are ground for flour. ' Turkish millet,' or ' Guinea corn,' is produced by Sorgham vulgare ; and the * German ' and ' Italian millet ' by species of Setaria. In some parts of the world millet flour ii used for bread, but it is chiefly cultivated as food for domestic animals. Letheby says millets are a little more nutritious than rice. In the subjoined table, is given the compo- sition of three different samples of millet uical, free from bran. Pemcilla- Pamcum ria spicota BL knid ot Sorghum tulgare. miliaeeumj much used Dharra ot coin moil in India the AJ^lia, miilet. under the name of Bajia. Goar of India. 11-95 Water . . . 12-22 11-8 Nitrogenous 8-64 substances . 9-27 10-13 3-82 Dextrin . . 913 1-46 Sugar . . . 180 3-90 Pat . . . . 7-43 '4-62 70-23' Starch . . 59-04 71-75 Silicln . . . 0-11 MINCE MEAT. Prep. From stoned raisins, currants, sugar, and suet, of each 2 lbs. ; sul- tana raisins and boiled beef (lean and tender), of each 1 lb. ; apples 4 lbs. ; juice of 2 lemons ; the rind of 1 lemon, chopped very fine ; mixed spice, 1 lb. ; candied citron and lemon peel, of eiich 2. oz. ; brandy, a glassful or two ; the whole chopped very fine. It may be varied by adding other spice or flavouring, and by the addition of eggs, or the substitution of chopped fowl or veal for beef, according to the state of the cuisinier. MINCE PIES. Take 3 apples, 3 lemons, 1 lb. of raisins, J lb. of currants, 1 lb, of suet, i lb. of raw beef, 2 lbs. of moist sugar, i lb. of mixed candied peel, i of a rind of a fresh orange, 1 teaspoonful of powdered mixed spice, composed of equal parts of cloves, cin- namon, and nutmeg, i pint of brandy, and 1 glass of port wine. Peel the apples and cut out the cores very carefully, and then bake the pieces until tliey are quite soft. The raisins must be carefully stoned, and the cur- rants well washed, dried, and picked. Chop the suet very finely, as well as the raw meat and lemon-peel. Mix all the ingredients thoroughly together, add the brandy last of all, and press the whole down into a stone jar, and place u piece of paper soaked in brandy on the top. Remove the paper ond stir up the mixture thoroughly every three days, re- placing the paper. If this is done the mince- meat will keep a long time. To make the pies, roll out some thin pufl^-paste, butter a small round tin, and line it with a piece of paste, then put in a generous quantity of the mincemeat, cover it over with a similar piece of puff paste, and bake it in a moderate oven. Mince pies are none the worse for being warmed up, but pray take care they are sent to table hot. (Cassell.) MINDEEE"RUS' SPIRIT. See Ammonia (Acetate of), and Solution. MINERAL CHAME'LEOW. Prep. From a mixture of binoxide of manganese and potassa and nitre, equal parts, heated to redness. It « Witli husks. 1072 MINEEALISERS— MIXTURE must be preserved iu a well-corked bottle until required for use. Prop., S(c. When dissolved in water, its solution, at first green, passes spontaneously through all the coloured rays to the red, when, if potassa be added, the colour retrogrades until it reaches the original green. The addition of oil of vitriol, or of chlorine, renders the solution colourless. The addition of a weak acid, or even boiling or agitating the liquid, turns it from green to red. See Man- ganic Acid. MIN'ERALISEES. Substances which, by association with metallic bodies, deprive them of their usual properties, and impart to them the character of ores. Their removal belongs to metallurgy. The term ' mineealised' has been applied to caoutchouc, gutta percha, bitu- men, &c., which has been combined with sulphur, silica, or metallic matter. MIN'IM. Syre. Minimum, L. A measured drop, of which 60 are equal to a fluid drachm. The size of drops vary so greatly with different liquids and are also so much influeticed by the size and shape of the vessels from which they are poured, that they afford no reliable mea- sure of quantity for medicinal purposes. The poured drop has, in some cases, only ^rd the volume of the measured drop, or minim ; whilst, in others, it is nearly 3 times as large. Accord- ing to Mr Durande, " liquids which contain a small proportion of water, afford a small drop ; while, on the contrary, liquids con- taining a large quantity of water furnish a lai'ge drop." " Among liquids containing a large proportion of water, those which are not charged with remedial substances, give a larger and heavier drop than the same liquids when containing extraneous bodies in solu- tion." In all cases in which the word ' drop ' is mentioned in this work a minim is intended, and the quantity should be determined by means of a graduated minim measure, MUT'lUM. See Red Pioments. WINT. Si/n. Speaemint, Gkeen m. ; Men- tha TiEiDis (Ph. L.), L. " The recent and the dried flowering herb " of Mentha viridis. It is aromatic and carminative, but its flavour is less agreeable than that of peppermint. It is employed in flatulence, colic, nausea, diar- rhoea, &e. ; also to make sauce. MIR'EOES. See Amalgam (Silvering), Silvering, Speculum Metal, &c. MITES. See Acaei. MITH'KIDATE. Syn. Damooeaib's Con- PECTION; MiTHEIDATIUM, CoNFEOTIO DAMO- CEATis, L. " This composition originally con- sisted of but few injiredients; viz. 20 leaves of rue, 2 walnuts, 2 figs, and a little salt. Of this we are informed that Mithridates took a dose every morning to guard himself against the efl'ects of poison. It was afterwards altered, and the number of the ingredients increased to sixty-one. In this more complex form it contained opium, and was, in effect, an aromatic opiate, of which the confection of opium of the present day may be considered as a simplilication. The * mithridate ' is still prepared in ■ some shops, and is occasionally, though very rarely, prescribed." (Med. Lex.) " The formulse for CONIBCTION or eleoiuaet OF CATECHU may be considered as the repre- sentatives, in our modern Fbarmacopceias, of the once celebrated recipes for CONPECTIO Damockatis and Thkeiaca Anbeomachi." (Redwood.) Mithridate was formerly con- ceived to be good for nearly every disease, and an antidote for every known poison. MIX'TUEE. Syn. Mistuea, L. A com- pound liquid medicine, taken in divided doses. Mixtures are usually extemporaneous pre- parations, and in prescribing them care should be taken not to bring together substances that decompose each other, nor to order heavy powders, that speedily separate from the body of the liquid by subsidence. Emulsions, JULEPS, and MUCILAGES, are included in the ' MiBTUBiG ' of the London Pharmacopoeia. Mixtures are usually dispensed in flat octa- gonal 6- or 8-oz. bottles, with long necks ; or in regular * octagons ' with short necks, having the doses marked on the glass, to which the strength of the medicine is made to corre- spond. Our remarks respecting ' deaughts ' equally apply here. By putting tlie active ingredients of six draughts into a 6-oz. mixture bottle, and filling it up with distilled water, a mixture will be made of corresponding properties, of which the dose will be 2 table-spoonfuls. When the formula for the draughts includes a decoction or infusion as the vehicle, instead of water, four of them only must be taken, which will then fill the 6-oz. bottle, and the proper dose will be 3 table-spoonfuls, or a small wine- glassful. The following formulse embraces the whole of the ' MiSTUEiE ' of the British Pharma- copcela, as well as a few others in general use. These will serve as examples for the like pre- parations of medicinals which are not included in the list. (See also Deaught, Emulsion, Julep, Watee, &c.) Mixture, Absor'hent. See Mixtuee, Ant- acid. Mixture, Aca'cia. See Mixtueb, Gum. Mixture, Ace'tate of Ammo"nia. Syn. MiN- DEEEEUS'S MIXTUEB; MlSTUKA AMMONIii ACETATIS, L. Frep. From solution of acetate of ammonia, IJ fl. oz. ; nitre, 40 gr. ; camphor mixture, 6 fl. oz. ; rose syrup, i fl. oz. — Dose, 1 to 3 table-spoonfuls, every third or fourth hour, as a diaphoretic in inflammatory fevers, &c. Mixture of Acetic Acid. Syn. Mistuea ACIDI ACETici. Prep. Distilled vinegar, 2 fl. dr.; syrup, 4 fl. dr.; water, 2 fl. oz. A fourth part every three hours. For children with scarlatina. Mixture of Aconite. (Mr Fleming.) Syn. Mistuea aconiti. Prep. Tincture of aconite, MIXTURE 1073 1 fl. dr.; carbonate of soda, 1} dr.; sulphate of magnesia, 1} oz. ; water, 6 oz, A table- ipoonful when the pain is urgent. In gas- tralgia this should only be administered under medical supervision or advice. Mixture, Al'kaline. See Mixture, Antacid. Uizture, Al'mond. Si/n. Emclsion o; al- monds, Milk op a.; Mistcba amtgdalje (B. P., Ph. L., E., & D.), Lao AMTGDALa;, L. iVe;). 1. (Ph. L.) Confection of almonds, ii oz. ; distilled water, 1 pint ; gradually add the water to the confection while triturating, until they are mixed ; then strain the liquid through linen. 2. (Ph. E.) From almond confection, 2 oz., and water, 1 quart; as the last. Or, from sweet almonds (blanched), lOdr. ; white sugar. 5 dr. J mucilige, i fl. oz. (or powdered gum, 3 dr.); made into an emulsion with wuter, 1 quart. 3. (Ph. D.) Sweet almonds (blanched), 5 dr. ; refined sugar, 2 dr. ; powdered gum, 1 dr. ; distilled water, 8 fl. oz. ; as the last. 4. (B. P.) Compound powder of almonds (sweet), 1; water, 8; triturate and strain. Obs. The last formula produces the article usually employed in dispensing in the shops. The addition of a little more sugar renders it more pleasant ; and 2 or 3 bitter almonds, as in the formula of the Ph. D. 1826, or 1 or 2 fl. dr. of rose or orange-flower water, may occasionally be added, to diversify the flavour. — Done, 2 or 3 table-spoonfuls, ad libitum; as a demulcent and emollient in coughs and colds, or as a vehicle for more active medicines. Mixture of Ammonia, Muriate of. (Sir 6. Lefevre.) Si/n. Mistuba ammonije mubia- TI8. Prep. Muriate of ammonia, 60 gr. ; ex- tract of liquorice, 3 dr. ; tartarised antimony, 2 gr. ; distilled water, 8 oz. A tablespoouf ul every 2 hours in pleurisy, congestion of mucous membranes, &c. mixture, Ammoui'acum. 8gn. Emulsion of AUuoNiAcujf, Mile of a. ; Mibtuba amuo- NIAOI (B. P., Ph. L. k D.), Lac ammoniaci, L. Prep. 1. (Ph. L.) Prepared ammonia- cum, 5dr. ; distilled water, 1 pint; rub the ammoniacum with the wuter, gradually added, until they are perfectly mixed. 2. (Ph. D.) Ammoniacum, \ oz. ; water, 8 fl. oz. ; as the last, but straining through muslin. 3. (B. P.) Ammoniacum, i oz. ; rubbed down with water, 8 oz., and strain. — Dose, i to 1 gr. Obt. The last formula produces the best nnd most elfirtive mixture, owing to tTie use of the raw instead of the strained drug. — Dose, 1 to 2 table-spoonfuls, either alone or com- bined with gquills or ipecacuanha; as an expectorant and demulcent in chronic coughs, humoral asthma, &c. . Mixture, A'nodyne. Si/n. MiBTunA anodtna, JuLBPCM CALMANS, L. Prep. 1. Prepared chalk, 2 dr. ; syrup of poppies, 1 oz. ; fetid spirit of ammonia, li dr. ; oils of dill and ani- TOL. II. seed, of each 3 drops ; water, 4i fl. oz. — Dose. A teaspoonf ul 3 or 4 times a day ; in the diar- rhoea and colic of infancy. 2. (P. Cod.) Syrup of opium, 2 dr. ; syrup of orange flowers, 6 dr. ; lettuce water, 4 fl. oz. To allay pain, induce sleep, &c. Dose, 1 table-spoonful. 3. (Vicnt.) Ammoniated alcohol, i fl. oz. ; powdered opium, 1 dr. ; powdered camphor, i dr.; proof spii it, li A. oz. ; digest, with agita- tion, for 3 or 4 days, and filter. In toothache arising from caries, and as a lotion to the temples in headache. Mixture, Antac'id. JSi/n. Absorbent hix- TTTBE, Alkaline m.; Mistdba alkalina, 11. antacisa, L. Prep. 1. Liquor of potassa and spirit of nutmeg, of each 2 fl. dr. ; tinc- ture of rhubarb, 3 fl. dr. ; tincture of opium, 1 fl. dr. ; water, 5 fl. oz. In dvspepsia, heart- burn, &c.. accompanied with flatulence. 2. Spirit of sul volatile and orange-flower water, of e.ich 1 fl. oz. ; simple syrup, 1^ fl. oz j water, 2i fi. oz. In acidity, &c., accompanied with languor and low spirits. 3. Sesquicarbonateof ammonia, 2 dr.; syrup of orange peel and tincture of gentian, of each 1 fl. oz. ; water, 4 fl. oz. In dyspepsia, heart- burn, &c., arising from excessive indulgence in spirituous or fermented liquors. It also possesses considerable stimulating properties, and will partially remove the fit of drunken- ness. 4. (Collier.) Prepared chalk, 2 dr.; tine ture of ginger, 2 fl. dr.; compound tincture of cardamoms, li fl. oz. ; pimento water, 6 fl. oz. In diarrhoea accompanied with acidity. 5. (Collier.) Chalk mixture, 5 fl. oz. ; tinc- tures of catechu and cinnamon, of each i fl. oz. In chronic diarrhoea. 6. (Ryan.) Liquor of pota«sa, 2 fl. dr.; tinc- ture of opium, 1 fl. dr.; calcined magnesia, 1 dr. ; oil of peppermint, 5 drops ; lime water , 8 fl. oz. In dyspepsia accompanied with acidity, flatulence, and constipation. Mixture,. Anticroup'al. Si/n. Mistuba sbne- am, L. Prep. ( Jadelot.) Infusion of senega, 4 oz. ; syrup of ipecacuanha, 1 oz. ; oxymcl of squills, 3 dr.; tartarised antimony, li gr.; mix. By spoonfuls, in croup. Mixture, Anti-eme'tic. Syn. Mistuba anti- EMKTICA, L. Prep. 1. Creasote, 12 drops; acetate of morphia, H gr-; camphor, 10 gr. rectified spirit, i fl. oz.j syrup of orange peel, li fl. oz. ; distilled vinegar, 4 fl. oz. In sea- sickness, &c. — Dose, 1 table-spoonful on the approach of vomiting, and repeated at inter- vals of half an hour until the vomiting ceases. 2. (Dr. Barker.) Compound tincture of camphor, 1 fl. dr. ; burnt brandy, 1 fl. oz. ; sugar, i oz.; infusion of mint, 6 fl. <>z. — Dose, i to 1 table-spoonful, every i hour, until the vomiting ceases. Mixture, Anti- epilep'tic. Si/n. Mistuea anti-epilbptica, L. Prep. (M. Lemoine. ) Liquor of ammonia, 12 drops ; syrup of orange flowers, 1 oz. ; distilled water of linden flowei-s, 68 1074 MIXTURE 2 oz. ; do. of cherry laurel, i oz. ; mix. Accord- ing to M. Lemoine, this is a specific in epilepsy. — Dose, 1 table-spoonful, or more. Mixture, Antihyster'ic. Stftt,. Mistttba ak- TIHYSTEEICA, h. ; POTION ANTIHTSTBEIQTJB, Fr. Prep. (Dr Joaat.) Cyanide of potassium, If gr. ; distilled lettuce water, 4^ fl. oz. ; syrup of orange flowers, li fl. oz. — Dose, 1 or 2 tea- spoonfuls every ten minutes, whiin the fit is expected ; during the fit it may be given in double doses. Dr Josat declares its efBcacy to have been indisputably proved in upwards of 55 cases. 2. (Magendie.) Cyanide of potassium, 2 gr. ; lettuce water (distilled), 4 oz. j syrup of marsh- mallow, 2 oz. Resembles the last. 3. (Dr Paris.) Assafcetida, 1 dr. j pepper- mint water, 5 fl. oz. ; m-ike an emulsion, and add of ammoniated tincture of valerian, 2 fl. dr.; tincture of castor, 3 fl. dr.; sulphuric ether, 14 fl. dr. — Dose, 1 table-spoonful, 3 or 4 times a day, or oftener. 4. (P. Cod.) Syrup of wormwood, 1 oz. ; tincture of castor, i dr. ; valerian water and orange-flower water, of each 2 oz. ; ether, 1 dr. As the last. Mixture, Antimo"nlal. See Mixtube, Con- TBA-STIMULAHT. Mixture, AiitlpertuB'sic. S^n. Mistttba ANTIPEBTUBBIKKS, L. Pr«jC. 1. COOHIKEAL (powdered), 2 dr. ; carbonati of potassa, 1 dr. ; boiling water, 8 fl. oz. j infustfor 1 hour, strain, and add of lump sugar, IJ o«. 2. (Dr Bird.) Extract of hemlock, 12 gr. ; alum, 25 gr. ; syrup of red poppies, 2 fl. dr.; dill water, 3 fl. oz. 3. (Dr Reece.) Tincture of assafcetida, 1 fl. dr.; tincture of opium, 10 or 12 drops; powdered ipecacuanha, 10 gr. ; water, 2fl. oz. — Dose. A teaspoonful every 3 hours, in hoop- ing cough, for a child 2 or 3 years old, and other ages in proportion. Mixture, Antisorofulous. S^n. Mistuea ANiiacEOEnLOSA, L. Prep. Prom tincture of bichloride of gold, 30 drops ; tincture of iodine, 40 drops ; tincture of gentian, 1 fl. dr. ; simple syrup, 7 fl. dr. ; rose water, 5 fl. oz. — Dose. A dessert- spoonful, 3 or 4 times daily, in a wine- glassful of water ; observing to shake the bottle before pouring out the liquid. Mr Cooley states that he has seen repeated in- stances of the excellent efi'ects of this medicine in scrofula, sypl)ilis, and various glandular diseases, even under all the disadvantages of a salt-meat diet and confinement on ship- board. Mixture, Antlspasmod'ic. St/n. Mistttba ANTISPASMODIOA, L. Prep. 1. Tincture of castor, 6 fl. dr.; sulphuric ether and laudanum, of each 1 fl. dr. ; syrup of saffron, 1 fl. oz. ; cinnamon water, 4 fl. oz. 2. (Dr Collier.) Assafcetida and camphor mixtures, of each 24 fl. oz. ; tincture of va- lerian, 1 fl. oz. 3. (P. Cod.) Lime or linden-flower water and orange-flower water, of each 2 oz. ; syrup of orange flowers, 1 oz. ; ether, i dr. — Dose. (Of each of the above) 1 to 2 table-spoonfuls. Mixture, Ape"rieiit. Syn. Mistuba ape- BIEKS, L. Prep. 1. (Abernethy.) Sulphate of magnesia, 1 oz. ; mauna, ^ oz. ; infusion of senna, IJ fl. oz. ; tincture of seuna, J fl. oz. ; mint water, 2 fl. oz. ; distilled water, 4 fl. oz. ; mix. This is the true 'Abeenetht Black Dbaught.' 2. (Dr Christison.) Sulphate of magnesia, li oz. ; water, 4 fl. oz. ; dissolve, and add, of tincture of senna, 1 fl. oz. j infusion of roses, 4 fl. oz. — Dose. A wine-glassful hourly, until it begins to operate. 3. (Dr Collier.) Sulphate of iron, 20 gr.j Epsom salts, 1 oz. ; pennyroyal water, 1 pint j dissolve. — Dose. A wine-glassful twice a day, in atonic amenorrhoea. Mixture, Aromat'io. Si/n, Mistttba aeo- MATICA, L. Prep. 1. (P. Cod.) Syrup of clove gilliflowers, 1 oz. ; spirit of cinnamon, i oz. ; confectionof hyacinth, 2 dr.; peppermint water and orange-flower water, of each 2 oz. 2. (Guy's Hosp.) Aromatic confection (Ph. L., in powder), 3 dr.; peppermint water, 9 fl. oz. Sometimes a little tincture of calumba is added. 3. (St Barth. Hosp.) Aromatic confection, 2i dr. ; water, 5 fl. oz. ; pimento water, 3 fl. oz, ; mix. The last two are excellent aromatic absorbents in diarrhceaf heartburn, flatulence, acidity, &c. — Dose, 1 or 2 table-spuonf uls every 2 or 3 hours, or as required. Mixture, Aromatic Iron. Pale bark, in powder, 4; calnmba, in powder, 2; cloves, bruised, 1 ; iron wire, 2 ; compound tincture of cardamoms, 12 ; tincture of orange peel, 2; peppermint water, 50 ; macerate the first four ingredients in the last one for three days, agi- tating occasionally, filter, add the tinctures, and make up to 50. Used as a tonic. — Dose, 1 to 2 oz. Mixture, Arsen'ical. Si/n. Mistuea AESBifi- CAIJS, L. Prep. From liquor of arsenite of potassa — Ph. L., 2 fl. dr. ; compound tincture of cardamoms, 4 fl. dr. j cinnamon water, 2 fl. oz. ; pure water, 3 fl. oz. ; mix. — Dose. A small table-spoonful, twice a day, after a full meal; in agues, periodic headaches, lepra, psoriasis, chronic rheumatism, &c. It should be exhi- bited with caution, and its effects watched; and after 5 or 6 days the dose should be reduced to half the quantity. Mixture, Astrin'gent. St/n. Mistttba ASTBIKGEN3, L. Prep. 1. (Pradel,) Tannin, 12 gr. ; tincture of rhatany, 1 dr. ; simple syrup, 7 dr. ; mucilage, 1 oz. ; camphor mix- ture, 4 oz. 2. (A. T. Thomson.) Extract of catechu^ 2 dr. (or tincture 1 oz.); cinnamon water, 8 oz. ; dissolve. — Dose, 1 to 3 table-spoonfuls, after every liquid dejection, in diarrhoea and dysentery. Mixture, Atroph'ic. Syn. Mistttba atbo- PHioA, L. ; Potion ateophique, Fr. Prep. (Magendie.) Iodide of potassium, 4 dr. ; let- MIXTURE 10?5 tnce water, 8 oz. ; peppermiat water, 2 dr. j ■yrap of inarshmallow, 1 oz. — Dote, 1 table- spouiiful, twice a day ; in hypertrophy (en- largement) of the heart. Sometimes 1 to 2 dr. of tincture of foxglove is added to the miztare. Uixture, Balsainic. (P. Cod.) Syn. Mis- tuba BAL8AMICA. Prep. BaUam copaiho, 2 oz.; rectified spirit, 2 oz. ; syrup of toiu, 2 oz. ; peppermint water, 4 oz. ; nitric ether, 2 dr. Mix the alcohol and ether, add the balsam, then tlie syrup and water. Miztnre, Bar'ley. Syn. Misicba bobdei, L. See Decoction. Miztare of Bismuth. (St Th. Hosp.) S,tfn. MiSTURA BiSMUTiii. Prep. Subnitrate of bis- muth, 10 gr. ; compound powder of truga- canth, 5 gr. ; water, 1 oz. For 1 dose. Mixture of Bisulphide of Carbon. (Clarus.) Syn. MisTUHA bisuiphuukti oabbonis. Prep, liisulphide of carbon, 20 minims; sugar, 2 dr. ; milk, 6 oz. — Dole, i oz. 4 times u day. Miztnre of Boracic Acid. (Chaussier.) Si/n. MiSTCBA ACIDI BOKACICI. Prep. Camphor mixture, 4 oz. ; boraciu acid, 60 gr. ; s^ rup of orange peel, 1 oz. Miztnre of Burnt Hartshorn. See Decoc- tion, White. Miztnre, Brandy. Syn. Mixture of bpibit OP Fbench wine, Ego flipJ; Mistuba spi- EiTUs viNi Galhoi (B. P., Ph. L.), L. Prep. 1. (Ph. L.) Brandy and cinnamon water of each 4 &. oz. ; yolks of 2 eggs ; white sugar, ) oz. ; oil of cinnamon, 2 drops; mix. A va- luable stimulant and restorative in low fevers, and in extreme exhaustion from liaemorrliages, &c. ; but scarcely a fitting subject for the labours of the College of Physicians, since almost every cook and housewife could pro- duce a better compound than the product of the College Ibrmula. 2. (B. P.) Brandy, 4 gr. ; cinnamon water, 4 oz. ; the yolks of 2 eggs ; sugar, j oz. ; mix. — Do»e, i to li oz., in prostration and last stages of fever. Mixture of Caffein. (Vanden-Corpnt.) Syn. Mistuba caffkinje. Prep. Caffein, 7 gr. ; distilled water, 3 oz. ; hydrochloric acid, 2 drops ; syrup of orange-flower water, J oz. ; mix. — Dose, 1 tablespoonful. Mixture, Cam'phor. Syn. Camphoe julep, Cakphob water j Mistuba. CAMPHona; (Ph. L. & D.), E.MiLsio CAMPHOK* (Ph. E ) MieiURAOAMPnOBATA, L. Prep. 1. (I'll. L.) Camphor, i dr.; rectified spirit, 10 drops; triturate together, graduHlly adding of water, 1 pint; and strain through linen. 2. (Pli. D.) Tincture of camphor, 1 fl. oz. ; distillcil water, 3 pints; aifitate well together, and after 24 hours filter through paper. 3. (Ph. E.) See Emulsion. Uses, S;c. Camphor julep is chiefly used as a vehicle for other medicines. — Dose, J to 1 wine-gliissful. 4. (With MAONE.siA: Mistuba CAMPiiOBi: CUM MAGNESIA— Ph. E.&D.,AQI7A CAMPHORS — Ph. U. S.)— o. (Ph. E.) Camphor, 10 gr.. carbonate of magnesia, 25 gr. ; triturate toge- ther, then gradually add of water, 6 fl. oz., still continuing the trituration. b. (Ph.D.) Camphor, 12 gr.; carbonateof magnesia, i dr. ; water, 6 fl. oz. ; as last. c. (Ph. U. S.) Camphor, 2 dr.; rectified spirit, 40 drops ; triturate, add of carbonate of magnesia, 4 dr., and again triturate, adding, gradually, of water, 32 fl. oz. Antacid, anti- spasmodic, and anodyne. — Dose, 1 to 2 table- spoonfuls. Used without straining. It is stronger than the simple mixture. d. Cabbonated camphob mixture. Syn. Mistuba camphor cabbonica. Water strongly charged with carbonic acid gas, agi- tated with powdered camphor and strained. Mixture, Carmin'ative. Syn. Mistuba cab- MINATIVA, L. Prep. (Dr Paris.) Calcined magnesia, i dr. ; peppermint water, 2i fl. dr. ; compound tincture of lavender, i fl. dr. ; spirit of caraway, 4 fl. dr. ; syrup of ginger, 2 fl. dr.; mix. Antacid and carminative. For 1 or 2 doses. Miztnre of Cassia. (Fr. Hosp.) Syn. Mis- tuba CASSI.E, L. ; Eau de casse, F. Cassia pulp, 2 oz.; hot water, IJ pint. May be taken by the wineglus.q. Liixutive. Mixture of Cassia, Antimoniated. (Foy.) Syn. Mistuba OAssiiE antimoniata, Eau db casse. Emitis^e. Prep. Pulp of cassia, 1 oz. ; boiling water, 1 J pint. Macerate, strain, and add sulphate of magnesia, 1 oz. ; emetic tartar, 3 gr. By cupfuls. In painters' colic. Mixture, Cathar'tic. See Mixtubb, Ape- eient, M. Senna, &c. Mixture, Chalk. Syn. Cbetaceous mix- ture; Mistcea CEET.E (B. P.), Mistuba CHETA (Ph. h. E. & D.), M. ceetacea, L. Prep. 1. (Ph. L.) Prepiired chalk, \ oz. ; sugar, 3 dr. ; mixture of aciicia (mucilage), li fl. oz., trituriite together, then add of cin- namon water, IS fl. oz. 2. (Ph. E.) Prepared chalk, 10 dr. ; white sugar, 5 dr. ; mucilage, 3 fl. oz. ; spirit of cinnamon, 2 fl. oz. ; water, 1 quart; as the last. 3. (Ph. D.) Prepared chalk, 2 dr.; syrup and mucilaj^e, of each, i oz. ; cinnamon water, 7 fl. oz. 4. (B. P.) Prepared chalk, 1 ; gum Arabic, in powder, 1 ; syrup, 2 ; cinnamon water, 30 ; mix by trituration. — Dose, 1 to 2 gr., with astringent tinctures and opium. Obs. The above are antacid and absorbent. — Dose, 1 to 3 table-spoonfuls, either alone or combined with aromatic confection; in heart- burn, and in diarrhoea after every liquid mo- tion. In the latter affection, a little tincture of catechu or laudiinum is often added; and when there is vomiting or nausea, either pep- permint or spearmint water is genei'ally sub- stituted for the whole or a part of the simple water ordered in the above forniulse. Mixture of Chlorine. Syn. Mistuba chlo- 1076 MIXTURE BINII. Dr Watson prescribes 2 fl. dr. of the solution to 1 pint of water. The dose of the mixture is 4 fl. dr. every 3 hours, according to age, in scarlatina. Mixture of Chloroform. (Ph. U. S.) Syn. MiBTUEA CHLOEoroEMl. Frep. Chloroform, i 01. (by weight) ; camphor, 1 dr. ; yolk of 1 egg ; water, 6 oz. Rub the yolk first by itself, then with the camphor, previously dissolved iu the chloroform, and lastly, with the water gradually added. Mixture, Cincho'na. Syn. Babk mixture; MisTUEA ciifoHONiE, L. Prep. (Copland.) Confection ol rosea, J oz. ; boiling decoction of bark, 1 fl. oz. ; triturate, iu 10 minutes strain, and add diluted sulphuric acid, \\ fl. dr.; spirit of nutmeg, 4 fl. dr. Febrifuge, tonic, and stomachic. — Dose, 1 to 3 table-spoonfuls, 2 or 3 times a day. Mixture of Citrate of Caffein. Syn. Mis- TUEA caffeine; citeatis. Potion contee uiOBAiNiE. Syrup of citrate of caffein, 1 fl. oz. ; water (or any agreeable diluent), 5 oz. A table-spoouful frequently. Mixture, Col'chicum. Syn. Govt mixtuee ; MlSTUEA ANTAETHEITIOA, M. OOtCHICI, L. Prep. (Sir S. Scudamore.) Magnesia, IJ dr. ; vinegar of colchicum and syrup of orange peel, of each 4 fl. dr.; peppermint water, 3 fl. oz. A table-spoonful every 3 or 4 hours during the fit of gout. Mixture, Contra-stim'nlaut. Syn. Mistuea CONTEA-STIMULANS, JULEPtfH C, M. ANTI- MONII P0TASSI0-TAETEATI3, L. Prep. (Laen- nec.) Tartar emetic, 3 gr. ; infusion of orange leaves, 8 fl. oz. ; syrup of do., 1 fl. oz. — Dose. A wine-glassful, or more, every 2 hours ; in inflammation of the lungs, hooping-cough, &c. Mixture of Copaiba. (Guy's Hosp.) Syn. MiSTTTEA COPAIB.E. Prep. Balsam of copaiba, 3 dr. ; solution of carbonate of potash, 1^ dr. Rub together and gradually add decoction of barley, 8 oz. ; spirit of nitric ether, 3 dr. — Dose, 1 oz. 3 times a day. See Mixtuees, Balsamic. Mixture, Cough. Syn. Mistuea bechica, L. Prep. 1. Almond mixture, 4 fl. oz. ; oxymel of squills, 1 fl. oz.; ipecacuanha wine and syrup of tolu, of each i fl. oz. 2. Tincture of tolu, ^ fl. oz. ; paregoric elixir and tincture of squills, of each 1 fl. oz. ; syrup of poppies, 3 fl. oz. ; water, 3i fl. oz. 3. Mixture of ammoniacum, 4 fl. oz. ; syrup of squills, 2 fl. oz. In the coughs of old persons, 4. Antimonial wine, 3 fl. dr. j syrup of pop- pies, Ij fl. oz. ; water, 4 fl. oz. In dry, husky coughs.— Do«e (of each of the above), 1 table- spoonful, 2 or 3 times a day, or oftener. 5. (Dr Monro.) Paregoric, i fl. oz. ; sul- phuric ether and tincture of tolu, of each 4 oz — Dose. A teaspoonful in water, night and morning, or when the cough is troublesome. 6. (Dr Radcliff.) Syrup of poppies, syrup of squills, and paregoric, equal parts. — Dose, As the last. In all cases the bowels should be kept gently moved by some mild aperient. 7. (Dr Wood's Brown Mixture.) Extract of liquorice, 2 dr. ; powdered gum Arabic, 2 dr.; boiling water, 4 oz.; dissolve, and add antimonial wine, 2 dr.; laudanum, 20 minims. — Dose. A table-spoonlul occasionally. A popu- lar American remedy. Mixture, Cre'asote. Syn. Mistuea cbeasoti, M. CBEAZOII (B. P., Ph. E.), I,. Prep. 1. (Ph. E.) Creasote and acetic acid, of each 16 drops; mix, then add of compound spirit of juniper and syrup, of each 1 fl. oz. ; water, 14 fl. oz. J and agitate well together. — Dose, i to 1 wine-glassful, in nausea and vomiting, especially to prevent or relieve sea-sickness. 2. (B. P.) Creasote, 16 minims; glacial acetic acid, 16 minims; spirit of juniper,^ dr.; syrup, 1 oz. ; distilled water, 15 oz. ; mix. — 1 to 2 oz. Mixture of Cnbebs. Syn. Mistuea cu- BEB.S;. Powder of cubebs, 1 oz. ; sugar, 2 dr. ; mucilage, 2 oz. ; cinnamon water, 6 oz. — Dose, ^ oz. to 1 oz. Mixture, Demul'cent. Syn. Mistuea de- MULCEifs, L. See Almond Mixiuee, Gum M., &c. Mixture, Diaphoret'ic. Syn. Mistuea dia- phoeetica, L. Prep. 1. Solution of acetate of ammonia, 3 fl. oz. ; antimonial wine, 2 fl. dr.; tincture of henbane, IJ fl. dr. ; camphor mix- ture, 3 fl. oz. — Dose, 1 table-spoonful every 3 or 4 hours ; in fevers, &c. 2. To the last add of sweet spirit of nitre, J fl. oz. As above. Mixture for Diarrhoea. (Board of Health.) Syn. Mistuea peg diaeehcea. Aromatic powder, 3 dr. ; compound spirits of ammonia, 3 dr. ; tincture of catechu, 10 dr. ; compound tincture of cardamoms, 6 dr.; tincture of opium, 1 dr.; chalk mixture to make 20 oz. — Dose. For an adult, 1 oz. ; for a child of 12 years of age, i oz. ; for 7 years, \ oz. j after each liquid stool. Mixture, Siarrhoe'a. See Mixtuee, Chale, &c. Mixture, Diuret'ic. Syn. Mistuea diu- ebtica, L. Prep. 1. Nitrate of potassa, 2 dr. ; sweet spirit of nitre, 3 fl. dr.; syrup of squills, IJ fl. oz.; peppermint water, 4 fl. oz. 2. (A. T. Thomson.) Infusion of foxglove, 5i fl. oz. ; tincture of foxglove, J fl. dr. ; ace- tate of potassa, 2 dr.; spirit of juniper, i fl. oz.; tincture of opium, J fl. dr. In dropsy. — Dose, 1 to 2 table-spoonfuls, every 2 or 3 hours. The last must be used with caution. Mixture, Effervescing. (P. Cod.) Syn. Mistuea effeevescens ; Potion Gazeuss HE RiTiEEE. Frep. Dissolve i dr. of bicar- bonate of potash in 2 oz. of water, and add 4 dr. of syrup. Mix also J dr. of citric acid with i oz. of syrup of citric acid and 2 oz. of water. Mix an equal quantity of each, and give it while effervescing. Mixture of Elaterinm. (Dr Ferriar.) Syn. MIXTURE 1077 MiSTtTEA BLATEBII. Prej). Elaterium, 1 gr.; spirit of nitric other, 2 fl. oz. ; tincture of squills, i oz. ; oxjiuet of colcliicsm, i oz. ; •ymp of buckthorn, 1 fl. oz. — Vote, 1 dr. 3 times B day in water. Uiztare, Emet'ic. Syn. Mistubaemetica, L. Prep. 1. (Copland.) Sulphate of zinc, 40 gr. ; ipecacuanha wine and tincture of Rer- pentary, of each 4 fl. dr.; tincture of capsicum, 40 drops; oilof chamomile, 12 drops; pepper- mint water, 4^ fl. oz. As an excitant emetic; in cases of poisoning by narcotics, &c. 2. (Magendie.) Coloured emetine, 4 gr. (or white emetine, 1 gr.) ; acetic acid, 8 drops ; mix, and add of infusion of orange leaves or lime flowers, 3) fl. oz.; syrup of marshmallowB, 1 fl. oz. 3. (A, T. Thomson.) Ipecacuanha, \ dr. ; tartar emetic, 1 gr. ; tincture of squills, 1 fl. dr. ; water, 6 fl. oz. Dose, 1 to 2 table-spoon- fuls, followed by half the quantity every 10 or 15 minutes, until vomiting is produced ; at the same time assisting the action of the medicine by drinking copiously of warm water. mixture, Emmen'agogDe. See Mixtube, Steel, &c. Mlztnre, Expec'torant. Syn. Mistuba bx- PEOTOBANS, L. Prep. 1. (Collier.) Oxymel uf squills and mucilage, of each 1 oz. ; syrup of marshmallows, 2oz.; camphor julep, 8 fl. oz. — Do»e, 1 to 2 table-spoonfuls, 2 or 3 times a day; in coughs, hoarseness, astlima, &c. 2. (A. T. Thomson.) Almond mixture, 6 fl. (iz. ; ipecacuanha wine and tincture of squills, of eacli 1 H. d» ; syrup of tolu, 6 H. dr. — Doxe, 1 table-spoonful ; in humoral asthma, catirrli, &c., when the cough is urgent. Hixture, Feb'rifage. Syn. Mibtuba f£brI' ruoA, L. See Acetate of Ammonia Mix- TCBE, DiAPHOEETIO M., &C Uiztare of Gentian. (Ph. B.) Syn. Mis- tuba 0BNTIAII£. Prep. Macerate gentian root, sliced, i oz. ; bitter orange peel, cut suiall, and coriander fruit, bruised, of each 30 gr., in proof spirit, 2 fl. oz., for 2 hours. Add distilled water, 8 fl. oz. ; macerate aM)in suits, 7toz. (say i lb.). t>. (Redwood.) Infusion of senna, 18 oz. j tincture of senna, 3 oz. ; sulphate of magnesia; 6 oz. ; extract of liquorice and spirit of sal vola- tile, of each i oz. ; oil of cloves, 6 drops. 7. (B. P.) Infusion of senna, 14j sulphute of magnesia, 4 ; extract of liquorice, i ; tinc- ture of senna, 2i ; compound tincl are of car- damoms, li : dissolve and mix, — Dose, 1 to li oz. Obs. As the above mixture contains very littlu spirit, and from its great consumption being made in large quantities at a tiuie, it frequently spoils before the whole is sold especially in hot weather. To avoid this. It dr. of cloves, and 3 dr. of mustard seed, both bruised, may be added to every gall, of the strained liquor at the same time with the salts, spirit, and colouring, after which it must be shaken up repeatedly for a few days, and then allowed to repose for a few days more when it will become quite clear. It may be filtered through a ilunnel bag, but there is much loss and delay, owing to tlic consistence of the liquid. It is purgative in doses of 1 to li fl. oz. It is a singular cii-ouuietance, that although an enormous quantity of this preparation is consumed in these countries, there is no stand- ard formula for it in the British Pharmaco- poeias. !See MlXTtTBB, APEEIENT, &C. Miztare, Steel. Sun. Mistuba tebbi COMPOSITA (B. P.), MlSTtJEA CHALTBEATA, L. Two compounds of this class are officinal : — 1. (GaiFFiTn's MixTUBE, Compound ikon M. ; MiSTUEA FEBni, M. F. PEOTOXTDI, M. F. coMPoaiTA — Ph. L. E. & D.) Prep. — a. (Ph. L. i, E.) Carbonate of potassa, 1 dr. ; pow- dered uiyrrh, 2 dr. j spirit of nutmeg, 1 fl. oz. ; triturate together, and whilst rubbing, add gradually, of sugar, 2 dr. ; rose water, 18 fl. oz. ; mix well; then add of sulphute of iron (powdered), 50 gr. ; and place it at once in a bottle, which must be kept closely cnrked. i. (Ph. D.) Powdered my rrh and sugar, of each 1 dr. ; carbonate of potassa, i dr. ; essence of nutmeg, 1 fl. dr. ; rose water, 7 fl. oz. ; sul- phate of iron, J dr. ; (dissolved in) rose water, 1 fl. oz. ; — Dote, 1 to 2 oz., 3 or 4 times a day, as a mild aud genial chalybeate tonic and ati- mulant; in anienorrhcea, chlorosis debility, &c., when there is no determination of blood to the head. 2. (Hebeboen's mixtceb, H.'s ink ; Atba- MENTDM HeBEBDII ; MiSTUEA FEUKI ABOMA- TICA— Ph. D.) Pule cinchona bark, 1 oz. ; calumba root, 3 dr. (both in coarse powder ;) cloves (bruised), 2 dr. ; iron filings, { oz. ; pep- permint water, 16 fl oz. ; digest in a close vessel for 3 days, agitating frequently, then strain, and add of tincture of cardamoms (comp.), 3 fl oz. ; tincture of orange peel, 3 fl. dr. Biiter, stomachic, and aromatic. — Doae, 1 or 2 table-spoonfuls, or more, 3 or 4 times a day. It is very slightly chalybeated. See also JIlXTUKE. AeOMATIO IBON. 3. Sulphate of iron, 25 gr. ; carbonate of potash, 30 gr.; myrrh, 60 gr. ; sujfiir, 60 gr. ; spirit of nutmegs, i dr.; rose water, 91 oz. Keduce the myrrh to powder, add tlie carbonate of potash of sugar, and triturate them wiih a small quantity of rose water so as to form a thin paste, tlien gradually add more rose water, and the spirit of nutmegs, con- tinuing the trituration and further addition of rose water until about eight fluid ounces of milky liquid is formed, then add the sulphate of iron previously dissolved in the remainder of the rose water and cork the bottle imme- diately. — Dose, 1 to 2 oz. as a stimulating tonic. Mixture of Sulphuric Acid. (Ph. G.) Si/n. MiSTUEA ACIDI SULPHUBICI ; HaILEB'S ELIXIE. Prep. To 3 oz. (by weight) of rec- tified spirit add gradually 1 oz. (by weight) of pure sulphuric acid. — Dose, 5 to 20 drops diluted. Mixture, Ton'ic. Si/n. Stbenothening mix- tube ; MiSTUEA TONIOA, L. Prep. 1. In- fusion of cascaitilla, 5 fl. oz. ; tincture of orange peel, 7 fl. dr. ; aromatic sulphuric acid, 2 fl. dr. 2. (Collier.) Decoction of bark, 5i fl. oz. ; tineture of do., 3 fl. dr. ; aromatic coofnctiou, 20 gr. ; aromatic spirit of ammonia, 1 fl. dr. 3. (Thomson ) Infusion of calumba, 5i fl. oz. ; compound tincture of cinnamon and syrup of orange peel, of each 2 fl. dr. — Dose, 1 to 3 table-spoonluls, 2 or 3 times a day ; in debility of the digestive organs, loss of appe- tite, to check nausea and vomiting, &c. Mixture of Wine. (Guy's Hosp.) Si/n. MiSTUBA VIM. Wliite wine, 6 fl. oz. ; yolks of 2 eggs ; sugar, j oz. ; oil of cinnamon, 3 drops. — Dose, 1 oz. Mixture, Worm. Sv». Mistuea anthkl- MINTIOA, M. TEBMIFUGA, L. Prep. 1. (Col- lier.) Sulphate of iron, 20 gr. ; infusion of quassia, 8 fl. oz. — Dose. Two table-spoonfuls every morning fasting. 2. (Copland.) Valerian, 2 dr. ; worm-seed. 1080 MIXTURES 4 dr. ; boiling water, 8 fl. oz. ; macerate 1 hour, strain, and add of assafoetida, 1 dr., pre- viously triturated with the yolk of one egg. As the last. 3. (Richard.) Root of male fern, I oz. ; water, 9 fl. oz. ; boil to 6 fl. oz., s'rain, and add, of sulphuric ether, 1 dr. ; syrup of tansy, 1 fl. oz. In tapeworm ; a< above. Mixture, Zinc. Si/n. Mistcea zinci, M. z. SULPHATIS, [j. Prep. (Collier.) Sulphate of zinc, 5 gr. ; sulphate of quinine, 10 gr. ; compound infusion of roses, 2 fl. oz. Tonic. — Hose. A teaspoonful 2 or 3 times a day, in a glass of water. Said to be very efficacious in the cure of coughs of a spasmodic character. MIXTURES (Arithmeticof). The constantly recurring necessity in business and chemical manipulations of determining the value of mixtures, and of producing articles and prepa- rations of different strengths or prices to those already in slock, has rendered a ready means of making such calculations an indis- pensable qualification in almost every depart- ment of trade and industrial art. As we address ourselves to the intelligent operative and busy tradesman, as well as to those more blessed by education and leisure, we feel we are bestowing a boon on many of our readers iu giving a short, but sufficient, outline of this useful branch of commercial arithmetic, which is most intimately connected with the objects of the present work, 1. To determine the price of a mixture from the value and quantity of each ingredient of which it is composed. — Rule. Divide the * gross value ' by the * gross saleable ' or ' useful quantity)' the quotient is the value or cost per gallou, pound, &c., as the ease may be. — Example. Required, the value per gallon of a hogshead of wine containing — s. d. 30 gallons @ 10 6 20 „ „ 12 6 13 „ „ 14 6 63 Cost per gallon . £ s. d. . 15 15 . 12 10 .986 ) 37 13 6 . 11 llj 2. To determine the proportions of sub- stances or articles of different values or strengths which must be taken to prepare a mixture of any other value or strengtii.- RtflB. Arrange th6 ' prices ' or ' strengths of the ingredients ' in a column, and link them together in pairs ; each of those above the required price being always connected with another below it. Then set the difference between the required price and these num- bers, alternately against those they are linked to ; when they will indiiate the quantities to be taken, as in the following examijles: — a. Required the proportions of tea at 3*., 4s., 6s., and 7«., that must be taken to produce a mix- ture 5*. the pound. Here — . 1, or 1 lb. @ 3». . 2, „ 2 „ „ 4». . 2, „ 2 „ „ 6*. . 1, „ 1 „ „ 7.. h. (When the number of the ingredients or prices is odd.) Required the proportions of teas at 3s., 5s., and 6s., the pound, to sell at 4«. Here the odd number must be taken a second time : — [6 1 1 + 2, or 3 lbs. @ 3». • If „ 1 „ „ 6*. • 1. .. 1 ., » 6». c. When the number of the ingredients is not merely odd, but the prices are unequally distributed either above or below the required price.) A dealer having wines of the same name at 7s., 9s., lis., 12»., and 14s., per gallon, wishes to produce a mixture of them worth 10s. per gallon : — f 7 — I . . 1 -I- 4, or 5 galls. @ 7s. I 9—-, . . . 2, „ 2 „ „ 9s. 10-! 11— '. . ... 3, „ 3 „ „11«. 12 1 ... 1, „ 1 „ „12s. 14 ... 3, „ 3 „ „14s. It will be seen that by varying the manner of linking the numbers, different answers may often be obtained to the same question. It also often happens that the dealer or operator desires to use a given quantity of one particu- lar article, or to produce a certain quantity only of the mixture instead of those indicated by the above calculations. In these instances he has simply to apply the common rule of ' practice ' or the ' rule of three,' as the.partieu- lar case may demand. In the above manner the proportions of the constituents of a compound may be determined from their specific gravity, when no change of volume has arisen from their admixture ; hut when this is the case, as in alloys, alcoholic mixtures, &c., it is either quite inapplicable or the results obtained are mere approximations to the truth. It may, however, be conveni- ently employed for calculations connected with the 'mixing' and 'reduction' of spirits and other liquids, by substituting their per-centage value in 'proof gallons' or other corresponding denomination, for the prices in the above ex- amples ; water, when introduced be reckoned, =0. Thus: — A spirit merchant having two puncheons of rum of the strengths of 17 and 21 0. p., wishes to know what proportions of each and of water he must take to form a spirit 10 u. up. The proof value of 100 gallons of these spirits are respectively equal to 121, 117, 90, and (water). Therefore— 1 27 -I- 31, or 58 g. water. 117—1 . . 90, „ 90 „ rum @ 117 o. p. 121 1 . 90, „ 90 „ rum „ 121 „ Suppose the dealer required to use different proportions of the spirits referred to, instead of equal measures, he has only to take such aliquot parts of the quantities thus found referring to the smaller proportion ; or such 90 MOHAIR— MORDANT 1081 niiiltiples of those referring to tlie larger one, as he wishes them to bear to each in the new mixture. Numerous other applications of this rule will occur to tlie ingenious reader. Questions in ' alligation,' as the department of arithmetic above referred to is called, are very easily resolved by the ' method of inde- terminate analysis,' even by persons but slightly conversant with rudimentary algebra; of which, indeed, they form a simple class of problems, often admitting of an almost indtli- nit'' number of solutions. HO'BAIR. The hair of a goat indigenous in Asia Minor. It is dyed and manufactured by similar materials and in a similar manner to wool. UOIL. See Cideb. MOIBEE METALLiaUE. [Fr.] A beau- tiful crystalline appearance produced on the surface of tin plate by acids. The tin plate is submitted for a few seconds, whilst gently heated, to the action of dilute aqua regia, by which it acquires a variegated primrose ap- pearance. It is afterwards washed in hot water, dried, and lacquered. The degree of heat and dilution of tlie acid modifies the beauty and character of the surlacc. The effect is also varied by employing dilute sul- phuric acid, either alone or mixed with a portion of nitric or hydrochloric acid ; or by using a solution of citric acid or caustic po- tussa. According to Herberger, the best metal for the purpose is plate iron, which has been coatfd by dipping it into a tin bath composed of pure tin, 200 parts; copper, 3 parts; arsenic, 1 part. The varnish should consist of copal in highly rectified spirit. Moiree metal- lique ie in much less demand now than for- merly, UO'LASSES. See Tbeaole. MOLES. The small, suft excrescences and discolorations of the skin which are popularly known under this name may, when slight, be removed by touching them every day witli a little concentrated acetic acid, by means of a hair pencil, observing due care to prevent the application from spreading to the surrounding parts. This dues not discolour the skin. The application of lunar caustic is also very effec- tive, but it turns the spot temporarily black. In the puie mule there is always a consider- able production of hair. Whon other means fail, they may be easily and safely removed by surgical means. The operation is trifling; and when judiciously performed no trace of such a proceeding i'f left behind. MOLUCCA BALU. See Liqueur. MOLYBDATE OP AMMONIUM. (NH^)2 MoOj. Sl/n. MOLYBDENIO ACID, PEROXIDE OP MOLTBDENUM ; ACIDUM MOLTBDICtTlI, L. Prep. Native sulphide of molybdenum, after being well roasted, is reduced to fine powder, digested with ammonia, and the mi.\ture fil- tered, and the filtrate evaporated to dryness; the residue, uiolybdate of ammonium, is then dissolved in water, purified by crystallisation ; and, lastly, decomposed by heat. Prop., ^B. Small white scales, soluble in 670 parts of water ; the solution reddens lit- mus paper ; dissolves in the alkalies, forming alkaline molybdates, from which it is again precipitated by strong acids. It is used in the preparation of molybdenum blue, and in calico-printing, but its scarcity precludes its extensive employment in the aits. Molyb- date of ammonium is the salt principally used in dyeing. Silks and cottons pussed through a solotiou of this salt, then through a bath soured with hydrochloric acid, and, lastly (without washing), through another of proto- chloride of tin, are dyed of a rich and pernia- U'nt blue colour. A solution of mnlybdnte of ammonia in excess of nitric acid firms a valu- able agent as a test for phosphates, with which it gives a beautiful yell'jw precipitate (phospho-molybdate of ammonia). See Phos- phoric ACID.' MOLYBDENUM. Mo. A very rare metal, havmg a wJiite colour, discovered by Hielm in 1782. Prep. By exposing molylnlic acid, mixed with charcoal and placed in a covered crucible, to the strongest heat of a sinitli's forge. Prop., the clear solution is added ammonia, in slight excess ; the crystalline precipitate which forms as the liquid cools is collected on a paper filter, washed with cold distilled water, and, la>tlv, the filter is transferred to a porous brick, in order that the morphia which it contains may become dry. (From the liquids reserved from the expressions more morphia may be obtoined by dilution with water, precipitation with ammonia, resolution in boiling water, and treatment with a little animal charcoal, &o., as before.) 2. (Ph. L. 1836.) Hydrochlorate of mor- phia, 1 oz., is dissolved in distilled water, 1 pint; and ammonia, 5 fl. dr. (or q. s.), pre- viously diluted with water, 1 fl. oz., is added, with agitation ; the precipitate is well washed in distilled water, and dried by a gentle hent. By a similar process morphia may be obtained from its other salts. 3. (Merck.) A cold aqueous infusion of opium is precipitated with carbonate ot sodium, in excess; the precipitate washed, first with cold water, and then with cold alcohol of sp. gr. 85 ; the residuum is dissolved in weak acetic acid, the solution filtered through animal charcoal, and precipitated with ammonia ; the precipitnte is again washed with cold water, dissolved in alcohol, and crystallised. A good process where spirit is cheap. 4. (.Mohr.) Opium, 4 parts, is made into a strong infusion witli water, q. s. ; lime, 1 part, reduced to a state of milk with water, is then added; the mixture is next heated to boiling, at once filtered through ]inalso dissolves in the fixed and vola- tile oils, and in solutions of the alkalies; heated in close vessels, it forms a yellow liquid, like melted sulphur, which becomes white and crystalline on cooling j heated in the air, it melts, inflames like a resin, and leaves a small quantity of charcoal behind. Witli the acids it forms salts, which are mostly soluble and crystallisable. IHiese may all be made by the direct solution of the alkaloid in the dilute acid. The only ones of importance are the acetate, hydrochlorate, and sulphate. I'ur, Commercial morphia and its prepara- tions are often contaminated with codeine, iiarcotine, and colouring matter. The pro- portion of the first two may be estimated by the loss of weight which the sample suffers when digested in ether; or by dissolving out the morphine by digestion in weak liquor of potassa. Pure morphia " is scarcely soluble in cold water, sparingly so in boiling water, and readily so in alcohol. This solution is alkaline to test paper, and by evaporation leaves crys- tals, which are wholly dissipated by heat. It is soluble in pure potassa." (Ph. L. 1836.) Tests. 1. Potassium hydrate and ammonia precipitate morphia from solution of its salts, under the form of a white crystalline powder, which is very soluble in excess of hydrate of potassium, and, with somewhat more difficulty, in excess of ammonia. The solution formed by excess of the first is precipitated on the addition of bicarbonate of potassium. The precipitate in either case is soluble in n solu- tion of chloride of ammonium, and in dilute acetic acid, and is insoluble in ether. A care- ful inspection of the precipitate through a lens of small power shows it to consist of minute acicular crystals ; and seen through a glass which raagii ifies 100 times, these crystals pre- sent the form of right rhombic prisms. — 2. The carbonates of potassium and sodium pro- duce the Slime precipitate as hydrate of potas- sium, and which is insoluble in excess of the precipitant. — 3. The bicarbonates of potassium and siidium also give similar precipitates from neutral solutions, insoluble in excess. In each of the above eases stirring with a glass rod and friction on the sides of the vessel promote the separation of the precipitate. — 4. If to a mix- ture of morphia and oil of vitriol a minute fragment of bichromate of potassium be added, oxide of chromium is set free, and a fine green colour developed. — 5. A drop or two of solu- tion of terchloride of gold added to a weak solution of morphia gives a yellow precipitate. which is mostly redissolved on agitating the liquid, which then assumes various hues (green, blue, violet, purple) on the addition of a drop of liquor of potassa. — 6. A minute fragment of terchloride of gold and of hydrate of potassium very gently dropped into the liquid, occasion purple clouds or streaks in dilute solutions, fol- lowed by a precipitate, which is violet, purple, or blue-black, according to the strength of the liquid. Another test, given by Siebold,' is the fol- lowing: — "Heat the substance which is be- lieved to be, or to contain, morphia, gently with a few drops of sulphuric acid, add a very small quantity of pure perchlorate of potas- sium. The liquid immediately surrounding the perchlorate will at once assume a deep, brown colour, which will soon spread and ex- tend over the greater part of the acid. Warm- ing increases the delicacy of the test. O'OOOl gramme of morphia can be distinctly recog- nised in this way, and no other alkaloid is acted upon in a similar way by the substances named. It is indispensable, however, for the success of the experiment that the perchlorate of potassium be absolutely free from chlorate." See Alkaloids. The above are the most reliable precipitates for morphia ; the first two may, indeed, be regarded as characteristic, and the remainder as almost so. The following are often referred to by medical writers, but are less exclusive and trustworthy : — Morphia and its salts are — 7. Reddened by nitric acid, and form orange- red solutions, darkened by ammonia in excess, and ultimately turning yellow, with the pro- duction of oxalic acid.— 8. They are turned blue by ferric chloride, either at once or on the addition of an alkali, and this colour is destroyed by water and by alkalies, or acids in excess. — 9. Iodic acid added to their splu- tions turns them yellowish brown, by setting iodine free, and the liquid forms a blue com- pound with starch. Uses. Morphia and its salts are exhibited either in substance, made into pills, or in solu- tion, generally the latter; or externally, in fine powder, applied to the dermis denuded of the cuticle. They are principally employed as anodynes and hypnotics in cases in which opium is inadmissible, and are justly regarded as the most valuable medicines of their class. " In cases wherein both opium and the mor- phine salts are equally admissible, I prefer the former, its effects being better known and regulated ; moreover, opium is to be prefei-red as a stimulant and sudorific, and for sup- pressing excessive mucous discharges." (Pe- reira.) — Dose. Of pure morphia, J^ to J gr. ; of its salts, i to J gr. ; externally, i to li gr. Morphine is chiefly used for the preparation of the acetate, and some of Its other salts. Good opium yields from lOg to 13^ of mor- phia. See Opium. I 'Year Book of Pliarmai:y,' 1873. MORPHIA 1085 Morphia, Ac'etate of Si/n. MoBFHi^ ACETis (Ph. L., E., & D.), L. Prep. 1. (Ph. L. 1836.) Morphia, 6 dr. ; acetic acid (Ph. L ), 3 fl. dr. ; distilled water, 4 fl. o-i.; dissolve, gently evaporate, and crystallise. 2. (Ph. E.) Hydrochlorate of morphia, 1 part, is dissolved in warm water, 14> parts ; xnd the solution, when cold, is precipitated with ammonia, iu slight excess, the precipi- tate is washed in cold wnter, and dissolved by means uf acetic acid, in excess, in warm water, 12 p'./n. MobphIjB hydbiodas cnM iodinio; Botr- CHABDAT'S lODUEE D'foDHTDEATE, &c.; MOR- PHINE. Prep. Mix an acid solution of sul- phate of morphia with an ioduretted solution of iodide of potassium, keeping the liquid at the temperature of 140° for an hour. Pour off the liquid, wash the scales, and dry them. — Dose, J gr. at bedtime. Uorphia and Hydriodate of Zinc with Iodine. (Bouchardat.) :!>i/ii. MoEPHi^ kt zinci nrDBIOOAS CUM IODINIO. Prep. Boil 1 scruple of ioduretted hydriodate of morphia with 2 fl. oz. of water and 10 scruples of zinc. After some days' action filter the boilingliquid, which deposits the salt. Make IJ ^r. into 8 pills, with powdered marshmallow root and syrup. Morphia, HydrocUo'rate of. C„H,9N0j,HI. Stfn. MUEIATB OP MOKPHIA ; MoBPHI£ HTDKOCHLOEAS (Ph. L. & Ph. B.), M0BPHI.E MUEiAS (Ph. E., D., & U. S.), L. Prep. 1. (Ph. L. 1836.) Macerate sliced opium, 1 lb., in water, 4 pints, for 30 hours; then bruise it, digest it for 20 hours more, and press it; macerate wliat remains a second and a third time in water until exhau»tc>l, and as often bruise and press it; mix the liquors, and evaporate at 140° Fahr. to the consistence of a syrup ; add of water, 3 pints, and after de- fecation decant the clear portiim ; gradually add to this liquid crystallised chloiide ol lead, 2 oz. (or q. s.), dissolved in boiling water, 4 pints, until it ceases to produce a precipitate; decant the clear liquid, wash the residuum with water, and evaporate the mixed liquids, as before, that crystals may form ; press tlicse in a cloth, then dissolve them in distilled water, 1 pint, add freshly burnt animal chnr- coal, 1^ oz., digest at 120°, and filter ; finally, the charcoal lieing washed, cautiously evH}<0- rate the mixed liquors, that pure crystnls i)f hydroclilorate of morphia may form. To the decanted liquor from which the crystals were first separated, add of water, 1 pint, and drop in liquor of ammonia, frequently shaking, until all the morphine is precipitated; wash this precipitate with cold distilled water, saturate it with hydrochloric aciii, dij,'e.st with animal charcoal, 2 oz. ; filter, wash tlie filtrate as before, and evaporate the mixed liquors, cautiously, as above, that pure crystals may be obtained. 2. (Ph. E.) Opium, 20 oz., is exhausted with water, 1 gall., in the quantity of a quart at a time, and the mixed liquors are evaporated to a pint; chloride of calcium, 1 oz., dissolved ill water, 4 fl. oz., is added, and, alter aj^'itatiun, the liquid is placed aside to settle; the clear decanted liquid, and the washings of the sedi- ment, are next evaporated, so that they may solidify on cooling ; the cooled mass, after very strong pi essure in a cloth, is redlss^olved in warm water, a little powdered white marble added, and the whole filtered ; the filtrate is acidulated with hydrochloric acid, the solution again concentrated for crystallisation, and the crystals submitted to powerful pressure, as before ; the process of solution, clarification, with powdered marble and li\di'ichloric acid, and crystallisation, is repeated until a enow- white mass is obtained. This is the process of Gregory and Eubertson, and is one of the easiest and most productive on the huge scale. To procure the salt quite white, 2 to 4 crys- tallisations are required, according to the power of the press employed. The Edinburgh College recommends, on the small scale, the solution, after two crystallisation-, to be deee- 1086 MORPHIA loured by means of nulmal charcoal; but, on the large scale, to purify the salt by repeated crystallisations alone. 3. (Ph. B.) Macerate opium, sliced, 1 lb., for 24 hours with distilled water, 2 pints, and decant. Macerate the residue for 12 hours with distilled water, 2 pints, decant, and re- peat the process with the same quantity of water, subjecting the insoluble residue to strong pressure. Unite the liquors, evaporate on a water bath to the bulk of 1 pint, and strain through calico. Pour in now chloride of calcium, f oz., previously dissolved in 4 fl. oz. of distilled water, and evaporate until the solution is so far concentrated that upon cooling it becomes solid. Envelope the mass in a double fold of strong calico, and subject it to powerful pres- sure, preserving the dark fluid which exudes. Triturate the squeezed cake with about i pint of boiling dibtiUed water, and, the whole being thrown upon a paper 6lter, wash the residue well with boiling distilled water. The filtered fluids having been evaporated as before, cooled, and solidified, again subject the mass to pressure, and if it be still much coloured, repeat this process a third time, the expressed liquids being always preserved. Dissolve the pressed cake in 6 fl. oz. of boiling distilled water, add purified animal charcoal, J oz., and digest for 20 minutes ; filter ; wash the filter and charcoal with boiling distilled water, and to the solution thus obtained add solution of ammonia in slight excess. Let the pure crystalline morpliia which separates as the liquid cools be collected on a paper filter, and washed with cold distilled water until the washings cease to give a precipitate with solu- tion of nitrate of silver acidulated with nitric acid. From the dark liquids expressed in the above process an additional product may be obtained by diluting them with distilled water, precipitating with solution of potash added in considerable excess, filtering, and super- saturating the filtrate with hydrochloric acid. This acid liquid, digested with a little animal charcoal, and again filtered, gives upon the addition of ammonia a small quantity of pure morphia. Diffuse the pure morphia obtained as above through 2 oz. of boiling distilled water placed in a porcelain capsule, kept hot, and add, constantly stirring, dilute hydro- chloric acid, 2 fl. oz., or q. s., proceeding with caution, so that the morphia may be entirely dissolved and a neutral solution obtained. Set aside to cool and crystallise. Drain the crys- tals and dry them on filtering paper. By further evaporating the mother liquor, and again cooling, additional crystals are obtained. — Dose. From |th to \ gr. 4. (Mohr.) By dissolving the precipitate of morphia (see MoEPHii, Frep. 4) in dilute hydrochloric acid, and by crystallisation, as before. Fur., S[c. It "is completely soluble in rec- tified spirit, and in water. What ie precipitated from the aqueous solution by nitrate of silver is not entirely dissolved, either by ammonia, unless added in excess, or by hydrochloric or nitric acid." (Ph. L.) "Snowy white; en- tirely soluble; solution colourless; loss of weight at 212° Fahr.not above 13^; 100 mea- sures of a solution of 10 gr., in water, \ fl. oz., heated to 212°, and deconipcised with agitation by a faint excess of ammonia, yield a precipi- tate which, in 2t hours, occupies 12i mea- sures of the liquid." (Ph. E.) It takes 20 parts of cold and about its own weight of boiling water to dissolve it. The hydrochlo- rate of morphia of the shops is usually, like the acetate, under the form of a white crys- talline powder. Ois. Of all the salts of morphia, this one appears to he that most suitable for medical purposes, from its free solubility, and from its solution not being liable to spontaneous de- composition, at least under ordinary circum- stances. " The opium which yields the largest quantity of precipitate by carbonate of sodium yields muriate of morphia, not only in the greatest proportion, but also with the fewest crystallisations." (Ph. E.) Smyrna opium con- tains the most morphine. Morphia and Codei'a (Hydrochlorate of). Syn. Geeqoey's salt ; Moephi.e et ooDEia; HYDEOCHLOEAS, L. ; SeL BE GeEGOET, Fr. This is commercial HYDEOCHIOEATE OP MOKPHINE prepared according to Dr Gregory's process. Morphia Mec'onates of. (C,9H2oN03)2,C;H20;. Frep. 1. (Neuteal meoonate op moe- PHINE; MoEPHia; MECONAS, L.) By Saturat- ing an aqueous solution of meconic acid with morphia, and evaporating the solution by a gentle heat, so that crystals may be obtained'. (2.) BiMECONATE OP MOEPHINE ; MOEPHIffl BiMECONAS, L.) Oi-HigNOjHCyHjOy. Meconic acid, 11 parts; morphia, 14 parts; dissolve each separately in hot water, q. s.; mix the solutions, and either gently evaporate and crys- tallise, or at once evaporate to dryness. Obs. Morphia exists in opium under the form of bimeconate, and hence this preparation of that drug has been preferred by some prac- titioners. A solution of this salt for medical purposes may be directly prepared from opium, by treating its solution in cold water with a little animal charcoal, filtering, gently evaporating to dryness, redissolving the resi- duum, in cold water, filtering, and repeating the treatment with animal charcoal. The dose of the dry bimeconate is J gr., or more; and of the meconate rather less, " A powder is also sold, called ' bimeconate of morphia,' which is of the same stretigth as powdered opivim, and is given in similar doses. It is obviously incorrect to apply this name to a powder which consists principally of foreign matter. It is to be hoped that physicians will not prescribe this powder under the above name, as such a practice might lead to fatal MORPHIOM ETBT— MORTAR 1087 retnlti, if the prescription ahould be prepared with the substnnce which the name strictly indicates." (Rsdwood.) Morphia, Nitrate of. (A. T. Thomson.) Siin. MoBFUUi NiiBAB. Add morphia in slight excess to very dilute nitric acid, filter, concen- trate by gentle evaporation, and set aside that crystals may form. Horphia, Phosphate of. 8iin. Mobphix PHOSFiiAS. As the nitrate, substituting dilute phosplioric by nitric acid. Horphia, SaVphate of. Si/n. JUocfHiiB SULPHAS, L. Prep. Saturate very dilute sul- phuric acid with morphia, evaporate to one half, add a little animal charcoal, continue the evaporation for a short time longer at a gentle heat, filter whilst hot, and abandon it to spon- taneous evaporation. It is decomposed by driving oS the water of crystallisation. Sul- phate of morphia is included in the Fb. U. S. According to Mugendie, this salt sometimes agrees with patients who cannot bear the acetate. Horphia, Tartrate of. (A. T. Thomson.) Syn. liIoEPHi* TAETBAS. Prep. Saturate a solution of tartaric acid with morphia', con- centrate by evaporation, and set aside thut crystals niuy form. By using an excess of acid an acid tartrate may be formed. M0SFHI0a['£TIt7. A name given to the process of determining the richness of opium in morphia. See Opium. MOBISON'S PILLS. See PAiEyi medi- cines. UOBSU'LI. An old name applied to lozenges and mastlcatories. It is still retained in some foreign Pharmacopoeias. HOB'IAK is the well-known cement, made of lime, sand, and water, employed to bind bricks and stones together in the construction of walls, buildings, &c. In the composition of mortar stone lime is preferred to that obtained from chalk, and river eand to pit or roud sand. Sea sand is unfitted for mortar until it has been well soaked and wiished in fresh water. Sifted coal ashes are frequently Bubstituted for the whole or a part of the sand. Hydraulic moetabs or cements are those which, like Roman cement, are employed for works which are either constantly submerged or are frequently exposed to the action of water. The poorer sorts of limestone are chosen for this purpose, or those which contain from 85 to 25^ of alumina, magnesia, and silica. Such limestones, though caUined, do not slake when moist'ned ; but if pulverised, they absorb water without swelling up or heating, like I'at lime, and afford a paste which hardens in a few days under water, but in the air they never acquire much solidity. " The essential constituents of every good hydraulic mortar are caustic lime and silica ; and the hardening of this composition under water consists mainly in a chemical cumbina- tion of these two ingredients through the agency of the water, producing a hydiated silicate of lime. But such mortars niay contain other ingredients besides lime, as, for example, clay and magnesia, when Uuuule silicates of great solidity ace formed ; on whii-h account dolomite is a good ingredient in these mortars. But the silica must be in a peculiar state lor these purposes, namely, capal)le of affording a gelatinous paste with acids ; and if not so already, it must be brought into this condition , by calcining it along with an alkali or an alkaline earth, at a bright red heat, when it will dissolve and gelatinise in acids. Quartzose sand, however fine its powder may be, will form no water mortar with lime ; but if the powder be ignited with the lime, it then be- comes fit for hydraulic cement. Ground felspar or clay forms with slaked lime, no water cement ; but when they are previously cal- cined along with the lime, the mixture becomes capable of hardening under water. " All sorts of lime are made hydraulic, in the humid way, by mixing the slaked lime with solutions of common alum or sulphate of alumina; but the best method consists in employing a solution of the silicate of potash, called liquor of Hints or solultle glass, to mix in with, the slaked lime or lime and clay. An hydruulic cement may aNo be made which will serve for the manufacture of architectural oruanientx, by making a paste of pulverised chalk, witli a solution of thu silicate of potash. The said liquor of flints likewise gives chalk and plaster a stony hurdnes-, by merely soak- ing them in it after they are cut or moulded to a proper shape. On exposure to the air they get progressively induratid. Superticial hardness may be readily procured by washing over the surface of chalk, cic, with liquor of flints, by means of a brush. Tliis method affords an easy and elegant method of giving a stony crust to the plastered walls and ceilings of apartments ; as also to statues and busts cast in gypsum mixed with chalk." Under Prof. Kuhlmau's patent, dated April, 1811, " instead of calcining the limestone with clay and sand alone, as lias been hitherto com- monly practised, this inventor introduces a small quauti ty of soda, or, preferably, potash, in the state of sulphate, carbonate, or muriate ; salts susceptible of lorming silicates when the earthy mixture is calcined. The alkaline salt, equal in weight to about l-5th that of the lime, is introduced in solution among the earths." (Ure.) The hardening of the common mortars and cements is in a great measure due to the gradual absorption of carbonic acid; but even after a very great length of time this con- version into carbonate is not complete. Good mortar, under favorable circumstances, acquires exticmo hardness by age. Attempts have been made at various times 1088 MORTIFICATION— MOULDS to introduce the use of bituminous cements into this country, and thus to restore both to land and submarine architecture a valuable material which has now lain neglected for a period of fully thirty centuries; but, unfor- tunately, owing to the interest of our great building and engineering firms lying in another direction, these attempts have been hitherto unsuccessful. See Asphaltuh, Cemekt, Lime, &c. MORTIPICA'TION Sy». Gasgeenb; Giif- GEEN A, MOBTIFICATION, L. Local death ; the loss of vitality in one part of the animal body, whilst the rest continues living. " The terms gangrentj and mortification are often used sy- nonymously; but gangrene properly signifies the state which immediately precedes morti fication, while the complete mortification, or absolute deatli of a part, is called sphacelus. A part which has passed into the state of sphacelus is called a slough. MOSAIC GOLD. See Bbasb, GoI;I>, &c. MOS'SES. Syn. Musoi, L. Several vege- tables of the natural orders Alga, Fungi, Li- chenes, and Musci, commonly pass under this name with the vulgar. Of these the following are the principal: — Boa MOSS [Sphagnum palustre). Very re- tentive of moisture. Used to pack up plants for exportation. Ceylon moss {Oracilaria Candida). Very nutritive ; made into a decoction or jelly, which is highly esteemed as an article of diet for in- valids and children, more especially for those suffering: under affections of the mucous membranes or phthisis. Club moss {Lycopodiwm clavatum). See Ltcopodium. Coesican moss, C. woem m. {Oracilaria Selmintkocorton), — Dose, ^ to 2 dr., in pow- der, mixed up with sugar ; as a vermifuge. Cttp MOSS, C. LICHEN ( Cladonia pyxidata). Astringent and febrifuge. A cupful of the decoction, taken warm, generally proves gently emetic. Used in hooping-cough, &e. FlH OLtTB MOSS (Lycvpodium Selugo). Vio- lently emetic and purgative. It is also irri- tant and narcotic. Iceland moss (Cefrarialslandica). Highly nutritious and easy of digestion. The decoc- tion is a favourite alimentary substance in affections of the lungs and digestive organs. In Iceland, after the bitter has been removed by soaking it in hot water, it is made into jelly, or dried, ground to ilour, and made into bread. IeISH MOSS, Peael m., Caeeageen m. (Chondrus crispus). Very nutritious. The decoction or jelly is a useful and popular de- mulcent and emollient in pulmonary affections, dysentery, scrofula, rickets, &c. It is often employed by cooks and confectioners instead of isinglass, and by painters to make their size. Reindeek moss {Cladonia rangiferina). Esculent, very nutritious. MOTHER-OF- PEAEL. See Peaei. MOTH'EK WATEE. See Cetstallisation. MOULDS. Numerous materials and com- positions are employed for the purpose of taking moulds, among which are the follow- ing: 1. (CoMPo'.) — a From spermaceti, stearine or hard tallow, and white wax, equal parts, melted together. For fine work, as medals, small casts, &c. h. From black resin, f lb. ; hard tallow, J lb. ; beeswax, 6 oz. ; as the last. For coarse work, as architectural ornaments, <&c. The above are poured on the objects to be copied (pre- viously oiled) whilst in the melted state. Ar- ticles in plaster of Paris are first soaked in water, observing that none of it remains on the surface so as to interfere with the design. 2. (Elastic.) — a. Flexible or elastic moulds may be made of gutta percha softened in boil- ing water, and after being freed from moisture, pressed strongly against the object to be copied hy means of a screw press. A ring or support should be employed to prevent undue lateral spreading. b. By the use of gelatin or glue, elastic moulds are formed capable of reproducing, with accuracy, and in a single piece, the most elaborately sculptured objects, of exquisite finish and delicacy. Casts from these are now common in the streets. The credit of the application of this substance to this purpose is due to M. H. Vincent. The process of casting consists in simply dissolving a certain quantity of gelatin in hot water until it is reduced to tile state of liquid paste, when it is run over the object, previously oiled, intended to be reproduced. A< it cools, the gelatin assumes a consistency ofloring a considerable degree of resistance, and is highly elastic, which latter quality enables it to be easily detached from the work on which it has been fitted. In the hollow formed by the gelatin the finest plas- ter, mixed to a thick cream with water, is next run ; and when the plaster has acquired the requisite hardness, the gelatin mould is de- tached in the same manner as from the origi- nal. From this apparently fragile mould as many as six copies may be taken, all repro- ducing the original with unerring fidelity. 3. (Metallic.) — a. From fusible metal.' b. (Clich^e moulds.) From a fusible alloy formed of bismuth, 8 parts; lead, 5 parts; tin, 4 parts ; antimony, 1 part ; repeatedly melted together. The above are poured out in the molted state on a plate or slab, and after being stirred until in a pasty state, the object to be copied is strongly pressed on the alloy at the moment it begins to solidify. They are chiefly used for medals and other like objects. t. (Chameroy's Patent.) By melting together one part of some easily fusible metal in a cru- cible, and then mixing with it four parts of a metal far less readily fusible, steeped in am- monia and reduced to powder. Such a com- ' See FusiBLK Allots. MOUTH COSMETICS— MUMPS 1089 ponnd ia atatcd to be of gront solidity, hard- ness, facility of soldering, meltH at a low temperature, and has great tractability in iiiouMing; to any form; and in ciiHtijig tnkes the ahnr|)ost impressions, »hi!st in iu nature it is peculiarly unchangeable. Sue £L£Ciiio- TTPE. MOUTH COSMETICS. See Bbbath, Teeth, LozKNOE, Paste, Powdeb, &c. MOX'AS. Substances burnt apon the body, for the purpose of acting as counter-irritants, aud ulliiying deep-seated pains and inflamma- tion. They have been used in gout, rheuma- tism, &c. The small cone constituting the moxa is placed upon a part, lighted, and allowed to burn to its base. The Chin bse and Japanese moxas are made of the downy por- tion of the leaves of a species of wormwood {Artemisia sinensis) ; but various other sub- Ktnnces, lis the pitli of the sunflower, cotton, or paper, soaked in a weak solution of nitrate, chlorate, or chromate of potassium, answer as well. Larrey's moxas consist of lycopodiura, 4oz. ; nitre, 2 oz. ; formed into small cones, with alcohol, and dried for some diiys. Dr Osborne used quicklime enclosed in a hoop of card, and moistened with water. The actual cautery is said to be preferable to any of them. MU'CILAGE. Syn. Mtjoilaoo, L. An aqueous solution of gum, or other Jiki> sub- stance, that gives a considerable consistency to water. See Dkoootiok, Mixtuse, &c. Mucilage, Acacia. (Ph. B.) Si/n. Muci- LAOO ACACIA. Put gum acacia, in small pieces, 4 oz., and distilled water, 6 oz., into a covered earthen jar, and stir frequently until the gum is dissolved. If necessary, strain through muslin. Mucilage, Fenugreek. Si/n. Muoilaqo FENCOBEOI. Digest 1 oz. of fenugreek seed with i pint of water for 12 hours, boil, and str.iin with pressure. Mucilage, Linseed. (P. Cod.) %».. Mc- CILAOO LiNi. Linseed, 1 oz. ; "warm water, 6 o«. Digest for 6 hours, stirring now and then, and strain. Mucilage, Liquorice. Si/n. Mucilaoo OLTCTBBHIZJE. From liquorice root, as uabeh- HALLOW HlTCILAaE. Mncilage, Marshmallow. (P. Cod.) St/n. Mucilaoo althe*;. Marshmallow root, 1 oz. ; boiling water, 6 oz. ; digest for 6 houi-s, and strain. Mucilage, Qnickeilver. Si/n. Mvcilaqo mkbcubialis plenkii. Quicksilver, 1 dr.; gum Arabic, 3 dr. ; syrup of poppies, 4 oz. Mix. — Dose, i dr. Mucilage, Sassafras. (Ph. U.S.) Sj/n. Mv- cilaqo bassafbas. Infuse 2 dr. of pith of sassafras in 16 oz. (old measure) of boiling water for 3 hours, and strain. Mncilage, Slippery-Elm Bark. (Ph. U. S.) Syn. MpciLAOO ulmi. Slippery-elm bark, sliced and bruised, 1 oz. ; boiling water, 16 oz. Infuse for 2 hours. TOL. II. MncUage, SUrch. (Ph. B.) Same as Decoction op .Stabch (Ph. L), which see. Mncilage, Tra'gacanth. Sj/n. MrciLAGO TiiAOACANTH« (B. P., Ph. E., and Ph. D 1826), L. Prep. 1. (Ph. E.) Tragacaiith, 2 dr.; boiling water, 9 fl. oz. (8 fl. oz.— Ph. D.) ; macerate for 24 hours, triturate, and press through linen. 2. (B. P.) Tragocanth, in powder, 60 gr. ; distilled water, 10 <.z. To the water contained in a pint bottle add the tragacanth, agitate bri^kly lor a few minutes, and again at shoit interviils, until the tragacanth is perfectly diffused, and has finally formed a mucilage. — Dose, 1 oz. (Should be made as required. One part of tragacanth gives more viscosity to water than twenty-five parts of gum Arabic- Squire.) Used in medicine as a demulcent, and as an application to burns, &c., aud in pharmacy in moking up pills, aud to suspend heavy powders in liquids. MITDAB'IN. Syn. Madabine. A peculiar substance, possessing powerful emetic proper- ties, extracted from the root bark of Calotropit gigatitea, in which it exists to the extent of llg. (Duncan.) It is soluble in water and in alcohol, and its aqueous solution, unlike that of most other substances, gelatinises by heat, and becomes fluid again on cooling. MUF'FJNS. Prep. Take of fine flour, i peck; «arm milk-and-water,! quart; yeast, a wine-glassful; salt, 2 oz. ; mix for 15 mi- nutes, then further add of flour, i peck, make a dough, let it rise 1 hour, roll it up, pull it into pieces, make them into balls, put them in a warm place, and when the whole dough is made into balls, shape them into muffins, and bake them on tins ; turn them when half done, dip them into warm milk, and bake them to a pale brown. MUF'FLE. See Assaying. MUL'BEBRY. Sgn. Mobum, L. Mulber- ries (MOBA, MOBI BACCiE) are the fruit of Moras nigra, or blai^k mulberry tree. They are cooling and laxative ; but when eaten too freely are apt to disorder the stomach and bowels. Mulberry juice (jnori *«ecu») is offi- cinal in the Ph. L. A syrup (SYECPUS MOBi) is made of it. It is also, occasionally, made into wine. MUL'TUM. A mixture of extract of quassia and liquorice, used by fraudulent brewers instead of malt and hops. MUM. A beverage prepared from wheat malt, in a similar way to ordinary beer from barley malt. A little oat and bean meal is frequently added. It was formerly much drunk in England ; but its use at the present day is chiefly confined to Germany, and to Brunswick more particularly. MUMPS. Si/n. Parotitis, L. Inflamma- tion of the parotid gland, which is situated under the ear. There is little constitutional derangement, but the cheeks become swollen and painful, and there is some difficulty iu opening the mouth, and in swallowing. The 69 1090 MUREXID— MUSCULAR POWER treatment consists in simply keeping the part warm with flannel, and the use of warm fomentations, at the same time that tlie bowels are kept freely open with some mild laxative. The mumps are said to be contagious, as, when the affection appears in a school, it generally attacks every member of it. Low, damp situations are those most favorable to this affection. MUREX'ID. CgNsHgOj. Syn. Pitepweate OP AMMONIUM. Prep. (Gregory.) Alloxan, 7 parts ; alloxan- t.ii, 4 parts ; boiling water, 240 parts ; dissolve, and add the solution to a cold and strong solution of carbonate of ammonia, 80 parts; crystals of murexid will separate as the liquid cools. Obs. Murexid can be obtained directly from uric acid by the action of nitric acid and subsequent treatment with ammonia. This process is, however, very precarious, and often fails altogether. Prop., Sfe. It is only very slightly soluble in cold water J freely soluble in solutions of ammonia and the fixed alkalies ; the first, by exposure to the air, becomes purple, and de- posits brilliant crystals of murexid. These compounds are the purpurates of Dr Prout. It forms iridescent crystals, having a me- tallic lustre, of a magnificent green colour by reflected light, and an equally beautiful reddish purple by transmitted light. It is soluble in boiling water, only very slightly soluble in cold water, and insoluble in alcohol and ether. A few years ago murexid was extensively used in dyeing ; it is now almost superseded by rosaniline or magenta. An analogous substance, formed as above, by treating amalic acid with ammonia, is called ' caffein-murexid.' HU"EIATE. An old name for hydrochlo- rate and chloride. MURIATIC ACID. Syn. Hydeoohloeic ACID, which see. KUEIDE. The name originally given to bromine by M. Balard. MUU'EAIN. Syn. Blaok-le(J, Biack- QUAETEE. A disease affecting neafc cattle, more especially young animals, in the spring and autumn. The common symptoms are swelling and discoloration of one of the hind quarters of the animal, with consequent lameness and Inability to move; a peculiar emphysema and intumescence of various parts of the body, particularly over the region of the spine, accompanied with all the common indi- cations of putrid fever. In severe cases gan- grene soon follows, and death frequently ensues in from 12 to 24 hoars. The rapid progress of this disease admits of little being done in the way of care. Exten- sive scarifications of the affected part, charcoal 'or hot yeast poultices, or fomentations, and ■active purgatives, appear to constitute the most useful treatment. The following drenches have been recommended for this affection : — 1. (Blaine.) Sweet spirit of nitre, i fl. oz. ; powdered cascarilla, 2 oz. ; solution of acetate of ammonia, 4 fl. oz.; yeast, 8 fl. oz. ; given every 3 or 4 hours. 2 (Clater.) Laudanum and sweet spirit of nitre, of each i fl. oz. ; solution of chloride of lime, i fl. oz. ; prepared chalk, 1 oz. ; warm gruel, 1 pint. The apparent incurability of this disease renders it of the utmost importance to tlie farmer to adopt preventive measures. These should consist of the supply of wholesome food and pure water, the adoption of extreme cleanliness, and the free accessof pure air to all the stalls, sheds, and other buildings in which the cattle may be sheltered. As the dis- ease is regarded as contagious by many persons, it is prudent to separate, as speedily as possible, the healthy animals from those affected. The free use of sulphurous acid, chloride of lime, &c., as disinfectants, is also advisable. Otlier and more immediate preventives con- sist of the occasional exhibition of a saline aperient, and the introduction of a seton into the dewlap. MUSCULAR POWER. Pick and Wislicenus proved, in 1865, that muscular power is to a great extent produced by the oxidation of such non-nitrogenous substance as fat. Frankland has put the matter beyond dispute by a series of experiments determining the amount of potential eneigy locked up in muscle. Some of the conclusions at which he has arrived are extremely interesting. He considers that a muscle is a machine for the conversion of potential enerpy into mechanical force; that the mechiinical force of the muscles is derived chiefly, if not entirely, from the oxidation of matters either contained in the blood or deposited around the muscular fibres, and not from the oxidation of the muscles themselves ;_thnt in man the chief materials used for the production of muscular power are non-nitrogenous; but nitrogenous matters can also be employed for the same purpose, and hence the greatly increased evolution of nitro- gen , under the influence of a flesh diet, even with no increase of muscular exertion ; that like every other part of the body, the muscles are constantly being renewed, but this renewal is scarcely perceptibly more rapid during great muscular activity than during comparative quiescence ; that after the supply of sufiicient albuminoid matters in the food of man to pro- vide for the necessary renewal of the tissues, the best materials for the production both of internal and external work are non-nitrogenous matters, such as oil, fat, sugars, starch, and gum ; that the non-nitrogenous matters of food which find their way into the blood yield up all their potential energy as actual energy; the nitrogenous matters, on the other hand, leave the body with a portion (fit least one seventh) of their potential energy unexpended; MUSHROOMS 1091 and, lastly, that the tmDsformation of poten- tial ouei'i^y into muscular power is necessarily accompanied by the production of heat within the body, even when the muscular power is exerted externally. This ig doubtless the chief, rinj probably the only, source of natural heat. See KVKBOT, KXEECISE. UUSH'KOOMS. Edible fungi. The species commonly eaten in England are the Agaricua eampeitrU, or common field or garden mush- room, used to make ketchup, and eaten either raw, stewed, or broiled ; — the Morchella etcu- ienCa, or morel, used to flavour soups and gra- vies ; — and the Tuber cibarium, or common truflle, also used as a seasoning. Several fungi, which to the inexperienced closely resemble the common edible mushroom, possess poisonous narcotic properties, and their use has not unfrequently been productive of Ferious, and, in some cases, even fatal results. Unfortunately, no simple tests exist by which the edible and poisonous varieties can be dis- tinguished from each other. So strongly was the late Professor L. C. Richards, the eminent botanist, impressed with this feeling, that though no one was better acquainted with tlie distinctions of fungi than he was, yet he would never eat any except such as had been raised in (gardens, in mushroom beds. "This difficulty of distinguishing edible f roin poisonous and noxious fungi must not be ig- nored. If only one out of a hundred, or for the matter of that n thousand, species were poisunnus or noxious, it would not be sound advice to say thiit wo should eat all that come to hand, and stand the chance of baneful ri suits. Unfortunately It is the case that some of the most poisonous fungi are the most common, and there is scarcely a field, and perhaps not a single wood, which does not abound with varieties of Coprinus, the Agaricusfascicularis, and the beautifully coloured Thussula emetica, and several other very undesirable species. Some writers, and among them, if wc remem- ber i-ightly, the learned and enthusiastic my- cologist, Dr Badham, deny the existence of any poisonous fungi in our islands, and they account for the effects which are often pro- duced by eiitiug varieties different from our common mushroom by stating that some peo- ple, through idiosyncrasy of constitution, are injuriously affected by all fungi; and iu snppiTi of this statement they instance the well-known fact that some people experience the most unpleasant effects after eating the common edible mushroom, which chemically coutains noxious ingredients. We all know that idiosyncrasy of constitution may account for much and for very strange phenomenii; for inst;ince, oysters are almost poison to some persons, while roust beef will cause bystei ics in otlier eases ; and to not a few certain odours, barmU'Ss in themselves, are causes of serious attiK'ks of illness; but the fact remains that pci-sous who can e it with impunity and greatly eiijny the comiiion mushroom are unpleasuutly affected by other species of fungi. Not a year passes hut deaths are recorded of persons — sometimes of whole families — after eating noxious fungi, though they had no idiosyn- crasy of constitution ; and shortly prior to the writing of this article a learned botanist and enthusiastic mycologist, and a friend, in experimenting on some specimens of fungi sent to him, narrowly escaped death, while another person who partook of the dish pre- pared actually succumbed. A thousand and one tests have been given iu writing from time to time whereby our ordinary mushroom is to be distinguished from species which resemble it — and one species is to he dis- tinguished from another; but we fear that practically they are not to be depended upon. Fungi differ in appearance according to the localities in which they grow, and according to their age. The common belief that the edible species never change colour when cut or bruised is untenable, for three varieties at least are perfectly edible, and yet assume difEer- ent tints when injured in any way. Tlie test of taste, too, which is applied under the idea that those with a pleasant savour and an in- offensive smell are always wholesome, is falla- cious, for a raw mushroom is quite a different thing from the stewed or grilled one, and often what has an acrid taste when raw be- comes perfectly savoury when cooked; and, vice versa, .a tasteless fungus may be poisonous, but only develop its latent flavour when sub- mitted to the cook. Dr Christison declares that a sure test of poisonous fungus is an astringent, styptic taste, and a disagreeable pungent odour; but this, again, cannot always be depended on. Nor, again, is the popular idea that a mushroom » hicli will skin easily is wholesome altogether based on fact. What, then, is to be done to enlarge the held of our mushroom gatherers and to bring about the utilisation of food now suffered to run to waste, or, in other words, how is a knowledge of our fungi to be obtained ? The only an- swer is that knowledge on this matter is to be got, generally speaking, as knowledge on other matters — partly from books, but more espe- cially from oral instruction and demonstration. Such eminent authorities as Dr Badham, the Rev. JM. Berkeley, Mr Cooke, and Mr Worthing- ton Smith may be consulted with profit, and works such as that on ' Domestic Economy,' in which coloured plates bring accurately be- fore the eye the different species of our fungi. And here we may mention that the plates pre- pared by Mr \^'orthington Smith, which were once at the South Kensington Museum, but now, we believe, at Betlmal Green, have done much to help the Londoner when in search for mushrooms in the country to distinguish be- tween the good and bad species of fungi. It might be well that in our schools, where so many practically useless branches of knowledge are crammed into children both in town auci couutry, practical lessons on fungi should bo 1092 MUSHK00M8 given. Those, too, who wish to learn what is to be learned on this subject should avail them- selves of opportunities now often given at ex- hibitions and botanical meetings. At Paris, in 1876, there was an exhibition of edible and poisonous fungi, in a fresli and dry state, toge- ther with books and drawings; and a similar exhibition took place in Aberdeen two years before ; and, as most of our readers are pro- bably aware, there exists a Fungus Club, or, rather, a botanical society which makes fungi a special study. This is the Woolhope Club, which has its head quarters at Heref ord.and em- braces in its scientific investigations all the dis- trict between Shropshire and the Bristol Chan- nel. Onedayineachautumnisdevotedto afun- gushunt, and the numbers that are gathered by this enthusiastic baud are something enormous. The labours of the day are closed by a dinner, at which the main dishes are composed of the spoils of the chase, dressed in the most epicu- rean fashion, and of other good things fla- voured with the most appetising (fungus) sauces. In the annuiil volume published of the transactions of the club there is a descrip- tion of the fungi of the district, and the best modes of cooking them. It would be a great gain to the public if at least that part dealing with fungi were generally obtainable. " Gastronomically the ordinary mushroom, and a large number of our British fungi, are most estimable, and ketchup produced from them — not the ordinary ketchup ' of com- merce,' which is often innocent of any fungi whatever — is to the cultivated taste of the gourmet the best of sauces. Many an epicurean has been heard to aver that after that of an oyster that of a, mushroom is the finest in the whole world of gastronomy. Bacon, in his ' Naturall Historic,' says of mushrooms, 'they yield a delicious meat;' and to these com- mendations it may be added that they can be cooked in almost as many ways as the French can cook eggs. Their alimentary value is also great, for chemistry has revealed in them the presence of the leading principles which exist in the flesh of animals. Dr Letheby says that ' the edible varieties are highly nutritious ;' and that well-known dietist, the late Dr Ed- ward Smith, who was very chary of commend- ing anything, also has a good word for them. "Our word 'mushroom' is evidently an adap- tation of the French mousseron, which, of course, is from mousse 'moss' (Latin, mus- t'Ms) ; but the suggestion of the learned Sal- masius, that the French gave this name to the edible fungus 'because it grows only where the grass is the shortest and there is little else but moss,' strikes one as rather weak. The mushroom, like the moss, is a cryptogamous plant; but there is little connection in any way between the two. Perhaps, then, we must look to the Greek word muvos, though only used by the grammarians, for the origin of the French word and so of our own. This was one of the terms which signified a ' sponge,' and was probably applied to the 'fungi' be- cause of their sponge-like growth. It is evi- dent that some of our more exact botanists, or etymologists who compounded the word for them, consider the Greek word and not the Latin as the origin of the mu in the English word and the mou in the French, though, according to analogy, the « should have been changed into a t/, for the study of ' fungi ' is termed by them mycology. It is hardly necessary to add that the words ' fungology ' and ' fungologist ' are hybrid compounds of Greek and Latin, which are simply intolerable to ears correct, as are many other words similarly compounded, and recently introduced into our language. The Jj^tin fungus is plainly a weakened form of the Greek spongos, and goes to show that the idea of a ' sponge' was Irom the first associated with the fungi, and that the Greek mucos must be taken as the origin of the French mousseron and the Eng- lish ' mushroom.' It is curious that tlie Greek, Latin, and English ' fungous ' terms have all been used in a sense reflecting on some of our species. The Greek mucos repre- sented a silly, stupid fellow, and the Plautus couples the fungi — 'soft-pated' — with the ' fools,' ' stolid ' and ' fatuous.' In like manner in our own language. Bacon speaks of certain persons as ' mushrooms and upstart weeds ' because of their sudden growth from a lowly origin. South, in one of his sermons, reflects on "mushroom divines who startup of a sudden," and whose success is ' not so good as to recommend their practice.' Carrying out the same analogy, the late Albert Smith, if we recollect rightly, spoke of ' stuck-up people ' as springing like mushrooms sud- denly into notice, and, like them, from very questionable soil. " One word as to the connection between fungi and what are called ' fairy rings ' in our meadows. ITiese fairy rings unfortunately lose all their poetry when it is known that they are simply produced by the growth of various kinds of fungi. The fungi start from a centre, owing to some peculiarity of the soil and decaying vegetable matter in it, and when they have exhausted the spot on which they origi- nally sprang up, they enlarge their borders, as it were, and thus form circles, giving a darker tinge to the herbage affected by them. These rings increase in size annually, and thus they vary considerably in circumference. This is a prosaic but truthful explanation of the pheno- menon which so often attracts the attention of children and puzzles the heads of older persons."' In cases of poisoning by fungi, vomiting should be immediately induced by an emetic and tickling the fauces with the finger or a feather ; after which a purgative clyster or a strong cathartic should be administered, with J to 1 fl. dr. of ether in a glassful of water or weak brandy. As an antidote, a solution of 1 ' DaHy Telegraph.' MUSK— MUSTARD 1093 tanniD, \ dr., in wntcr, 1^ pint, or a decoction iif i oz. of powdert'd gaUe,or of 1 oz. of pow- dered cinchona baric, iu a lilco quantity of water, has been strongly recominended by M. Cliuiisitrel. Alexis Soyer recommendetl the excellent metliod of cooking uiushrooms by baking them under a gluts or basin on toant, along with scalded or clotted cream, or a little melted butter, with one clove, and salt, pepper, &c., to Incite. They take about i of nn hour in a gentle oven or belbre the fire. When they are taken up, do not remove the glass for a few minutes, by which time the vapour will have licH'ome condensed and gone into the bread ; but when it is, the aroma, which is the essence of the miisliroom,i8 so powerful as to pervade the whnk' apartment. MUSK. Si/n. MoscntTS (B. P., Ph. L., E., & U.), L. " A secretion deposited in a fol- liik' of the prepuce of Moxchut mosehiferus, Linn." (Ph. L.), an animal inhabiting the mountains of Eastern Asia. It is imported from Bengal, China, and Russia ; and, latterly, Irom the United States of America. That known as ToNQUiN MUSK is the most esteemed for its odour ; but that from Russia is the only kind which rcjiclios us in perfect bags, or which has not been tiiinpered with. Pod mdsk (Mosciiue IN VEsicis) is the bag In its natural htate, containing the musk. The average weight of one of the pods is about 6 dr.; that of the grain musk which it contains, about 2i dr. Pur, iic The musk of the shops is gene- rally adulterated. Dried bullock's blood or chocolate is commonly employed for this pur- pose, along with a little bone-black. The extent uf these additions varies from 25j to 75J of the gross weight of the mixture. The blo' ,' sore. The free ends or points of the nails should be pared about once a week ; nnd biting tliem should be particularly avoided, as being nt once destructive to their beauty and usefulness. "The (free) edge of the scarf- skin should never be pared, the surface of the nail never scraped, or the nails cleaned with any instrument whatever saving the nail- brush." (Eras. Wilson.) The consequences of wearing a shoe that is obviously too short for the foot are thus de- scribed by the above authority : — " In this case Natnre gives us warning, by means of her agent, pain, that such a proceeding is contrary to her laws. We stop our ears, and get accus- tomed to the piiin, which, perhaps, is not severe, and soon goes off; the shoes get a scolding for their malice, and nc forget all about it for a time. But does Nature check her course to suit the convenience of thonght- less men? No, no. In u short time we find that the nail, intercepted in its forward course, has become nnusually thick and hard, and has spread out so much upon the sides, that it is now growing into the flesh, and so makes a case for the doctor. Or, perhaps, the continuance of pressure may have intiamed the sensitive skin at the root, and caused n sore and painful place there. And instances are by no means infrequent in which the power of production of iho null at the ruot becomes entirely abrogated, and then it grows in thick- ness only." When the nails are stained or discoloured, u little lemon juice, or vinegar-and- water, is the best application. Occasionally, a little pumice- stone, in impalpable powder, or a little • putty powder,' may be used along with water and a piece of soft leather or flannel for the same pur- pose. The frequent employment of these sub- stances is, however, injurious to the healthy growth of the nail. NANKEEN'. The coloured cotton cloth which beurs this name was originally brought from Nankin, the ancient capital of China, and was prepared from a native cotton, of a brownish-yellow hue. It is now successfully imitated in England, and at the present time the English mannfacturera supply the Canton market. In this country the colour is gene- rally given to the cloth by successive baths of sulphate of iron and orudc carbonate ot soda or lime water. NANKEEN DYE. The liquid sold iin.ler this name in the shops is a solution of annott.i. It is employed to dye white ciilicocs of a nan- keen colour ; but chiefly to restore the colour of faded nankeen clothing. NAPH'THA. Sy». Mineral naphtha ; Naphtha, L. A name given to the limpid and purer varieties of peteolbum (which see), or ROCK OIL, which exudes from the surface of the earth in virions parts of the world. Frop. Naphtha possesses a penetrating odour and a yellow colour, but may be ren- dered colourless by distillation ; it usuiilly begins to boil at a temperature of about 180° I'ahr., but, being a mixture of several different hydrocarbons, it has no fixed boiling-point ; it is very inflammnble ; it does not mix with water, but imparts to that fluid its peculiar taste and smell; mixes with alcohol and oils, and dissolves sulphur, phosphorus, camplior, iodine, most of the resins, wax, fats, and sper- maceti ; and forms with caoutchouc a gela- tinous varnish, which dries with very great difficulty. Fur. Mineral naphtha is very frequently adulterated with oil of turpentine, a fraud which may be detected by — 1. The addition of some oil of vitriol, which will, in that cose, thicken and darken it. — 2. Hydrochloric acid gas passed through the liquid for an hour, will occasion the formation of hydrochlorate of camphine, either at once or after a few hours* repose, even if only 5 J of oil of turpentine is present. (Dr Bolley.) — 3. If a few grains of iodide of potassium and a little water are' rubbed with the suspected sample, the colour of the water should continue unchanged ; the presence of j^th part of oil turpentine will cause it to assume a red or orange colour. (Saladin.) Uae». Naphtha is chiefly employed for the purposes of illumination, as a solvent for india rubber, and in the preparation of a very supe- rior black pigment. It has been highly spoken 1096 NAPHTHALIN— NARCOTINA of as a remedy for cholera, by Dr Andreosky, a Russian physician. See Pbteoieum, and below. Naphtha, Coal-tar. St/n. Naphtha, Coal N. A mixture of volatile hydrocarbons, ob- tained by distilling coal-tar. It is one of the first products which comes over, and flows from the still as cr»de coal naphtha. To ob- tain rectified coal naphtha, this crude liquid is distilled, and the product agitated with 10§ of concentrated sulphuric acid j when cold, the mixture is treated with 5g of peroxide of manganese, and the upper portion is submitted to further distillation. The specific gravity of this purified product is '850. It is exten- sively used as a solvent of caoutchouc, and other allied substances, also of resins for the preparation of varnishes. By repeated puri- fication and fractional distillation, benzol, the chief and most important constituent of coal naphtha, is obtained. See Benzol. Naphtha, Wood. See Pyboxylic spirit. NAPH'THALIN. CioHj. Si/n. Naph- THALINB, Naphthalene. A white crysial- lisable, odorous, volatile substance, obtained from coal-tar. Prep. The last portion of the volatile oily product is collected separately, and allowed to repose, when crude naphthalin separates in the solid state. By pushing the distillation until the residuum in the still kegins to char, a further portion of dark-coloured napbtlialin may be obtained. It is purified byresublima- tion a seciiud, or even a third time. Prop., tSfc. Soluble in alcohol and ether j slightly soluble in boiling water; melts .at 176° iVhr.; boils at 412°; highly inflam- mable, burning with a red and smoky flame; with sulphuric acid, it unites to form sulpho- naphthalic acid. By the action of nitric acid upon naphthalin, numerous substances may be formed, the most interesting being nitro- naphthalin. Naphthalin has lately been ex- tensively employed as a stimulating expecto- rant. — Dose, 5 to 20 gr. ; or, preferably, J gr., frequently. Externally, made into an oint- ment, in dry tetters, psoriasis, &c. 30 gr. may be mixed with 1 oz. of lard. NA'PLES YEL'LOW. See Yellow pio- MENTS. NAR'CEIA. C23H20G5. Syn. Naboeina, Nakoeia. a peculiar substance discovered by Pelletier in opium. It is obtained from the aqueous solution of opium, after it has been freed from morphia, and narcotina, by am- monia, by adding to it hydrate of lime, or pre- ferably, baryta. On boiling the filtered solu- tion to expel the ammonia, and evaporating the liquid, crystals of narceine are gradually deposited. It may be purified by solution in hot alcohol and recrystallisation. Prop., S;o. White, silky, acicular prisms ; neutral; inodorous; bitter; pungent; soluble in 375 parts of water at 60°, and in 330 parts at 212 Fahr. ; insoluble in ether ; does not neutralise the acids, and is destitute of bapic properties. It is distinguished from morphia by its easier fusibility (190°), and by forming a blue liquid with the dilute mineral acids, which on gradual dilution changes to violet and rose red, and ultimately becomes colour- less. It does not strike a blue colour with ferric chloride, like morphia, but forms a blue compound with iodine, which is decom- posed by boiling water. It appears to be inert, and has not been applied to any useful purpose. NAR'COTICS. Syn. Stupepacientb ; Nab- OOTICA, Stupeeacientia, L. Medicines which produce drowsiness, sleep, and stupor. In small doses, narcotics mostly act as stimulants, but in larger ones they produce calmness of mind, drowsiness, and torpor ; and in poisonous doses, delirium, coma, and death. The general objects in the administration of these agents are the production of sleep and the alleviation of pain. Their action is modified to a greater degree by idiosyncrasy and habit than that of, perhaps, any other class of medicines. Hence the care necessary in their administration. Alcohol, camphor, chloroform, chloral hydrate, ether, foxglove, hemlock, henbane, morphia, opium, and tobacco, are narcotics. NAE'COTINA. C^^O^. Syn. Naeco- tinb, L. ; Sel d'opiom, Matiebe de De- BOSNB, Fr. A peculiar crystalline substance, found by Derosne in opium, and on which its stimulant property was at fu'»t supposed to depend. Prep. 1. From opium exhausted of soluble matter by cold water, by treating it with water acidulated with acetic or hydrochloric acid, filtering, neutralising, with ammonia, and dissolving the washed precipitate in boiling alcohol ; the narcotine is deposited as the liquid cools, and may be purified by solution in ether. 2. By acting on opium, previously exhausted by cold water, with ether. Prop., Sfc. White, inodorous, fluted, or striated prisms; neutral to test paper; in- soluble in cold water ; sparingly soluble in boiling water ; freely soluble in boiling alcohol and in ether. It is only feebly basic. Narcotine is distinguished from morphia by its insipidity, solubility in ether, insolubility in alkalies, giving an orange tint to nitric acid, and a greasy stain to paper when heated on it over a candle. Another test for narcotina, said by Orfila to he characteristic, is to add to a little of the suspected substance a drop or two of oil of vitriol, and then to add a very small fragment of nitrate of potassium ; the liquid speedily acquires a deep blood-red colour if narcotina is present. Morphia treated in the same viay strikes a brown or olive-green colour. Obs. The physiological action of narcotina is differently stated by different authorities. 1 gr. of it, dissolved in olive oil, killed a dog in 24i hours : but 24 gr. dissolved in acetic acid were given with impunity. (Magendie.) In the solid state it is inert; 120 gr. at a dose scarcely produce any obvious effects. (Bally.) Scruple doses have been given without injury. NATRIUII— NESSLERS TEST 1007 (Dr Roots.) It has been recently proposed as R auhstitute for quinine in the cure of iif^ucs. Fur this purpose the f>ul pliate or hvdro- chioniti' is preferable. 200 cases of inter- mittent and remittent fevers have lieen thus successlully treated in India. (Dr O'Sliaugli- nessy.) — Dote, 3 to 10 gr., as an antiperiodic •edtttive, lie. Turkey opium contains about 1§, and East Indian opium about Z%, of narcotine. NA'TRIUM. See Sodium. MA'TEOW. Native carlionate of soda. HAU'SEA. See SiCEMiiSS. NAU'SEAKTS. Syn. Nauseantia, L. Sub- stances wliich induce an inclination to vomit, without efEecting it. See E.MET1CS. NAVEL, Starting of. To remedy this, take a slice of cork about the circumference of a shilling, imd a little thicker; and having covered the projecting navel with a small cireular piece of clean, solt linen, place the cork on the linen, strapping it into position by means of cross strips of white sticking plaster (simple leiid plaster) over which the usual roller is to bo adjuBted. Be careful to have the plaster of sufficient length, and to see that it adheres tightly to the skin. NEC'TAE. The fabled drink of the my- thological deities. The name was formerly given to wine dulcified with honey ; it is now occiisionally applied to other sweet and plea- siiut beverages of a stimulating chiiracter. The following LIQVEUBB are so called ; — Prep. 1. Chopped raisins, 2 lbs. ; loiif snpar, 4 lbs. ; boiling water, 2 galls. ; mix, and stir frequently until cold, then add Z lemons, sliced; proof spirit (brandy or rum), 3 pints; miiceriite in a covered vessel for 6 or 7 days, occasiouall.v shakiug, next strain with pressure, and let the strained liquid stand in a cold place for a' week to clear ; lastly, decant the clear portion, and bottle it. 2. Red ratafia, 3 gall. ; oils cf cassia and caraw.iy, of each 25 drops (dissolved in); brandy, J pint ; orange wine, 1 gall. ; sliced oranges, 6 in no.; lump sugar, 2 lbs. ; macerate fur a week, decant and bottle. See AltBACE (Factitious.) N E'GUS. A well-known beverage, so named after iti originator and patron. Colonel Negus. It is made of either port or sherry wine, mixed with about twice its bulk of hot water, sweet- ened with lump sugar, and flavoured with a little lemon juice and grated nutmeg, and a small fragment only of the yellow peel of the lemon. The addition of about 1 drop of essence of ambergris, or 8 or 10 drops of essence of vanilla, distributed between about a dozen glas-:o8, improves it. KEPEN'THB. A drink calculated to banish the remembrance of grief. In the "Odvs-cy" Homer describes Helen as administering it to Telemachus. Nothing is known respecting the composition of the ancient nepenthe. The name is applied to a pnparatiou of opium by many old writers, and is now employed by a Bristol firm to designate a preparation re- xemhling in all essential points Battley's ' LIQCOB OPII BEDATIVU8.' NER'VOUSNESS. The indescribable de- rangement of health, and the complication of disagreeable sensations which are popularly described under thi< name, quite as much de- serve the serious attention of buth patient and physician as any otiier affection to which the liuman frame is liable. Although, in itself, not a definite disease, it is indicative of the vital system being out of order, that its energies are failing or overtasked, and that tlie functions of some of its orgnns are lan- g:uidly or imperfectly performed. This condi- tion, if not removed, may gradually lead to the development of actual disease, and imperil life if the conditions whereon it is dependent be not detected and subdued. The <«atic biiryta is added to the solution, the latter ev:iporttted to ilryness, and the pure nicotine extracted with ether. To estimate nicotine, weigh out 15 gr. of tobacco, digest for twenty-four hours with alcohol of 85 per cent, acidified with 15 drops of sulphuric acid, so as to make 150 cubic centimetres. Evaporate 50 cubic centimttres of the filtered liquid, and add iododydrargyrate of potassium to the residue. Thp number of cubic centimetres employed, multiplied by 0004O5 (0001 of the equivalent of nicotine), gives the quantity of alkaloid contained in 5 grams of tobacco. (Linoffsky.) Prop., Sec Nicotina is a colourless, volatile liquid; highly acrid and pungeut; smelling strongly of tobacco; boiling at 375° Kiihr. (482° — Pereira) ; soluble in water, ether, al- cohol, and oils; and combining with the acids, forming salts, many of whichare crystallisnlilo. It is a frightful poison; i of a drop will kill a rabbit; a single drop will kill a large dog. Nicotina is the substance which was employed by the Count Bocarme for the purpose of pois- oning his brother-in-law, Gustave B'ougnies, the particulars of which were developed in the celebrated trial, in Belgium, of that nobleman, in 1851. Good Virginia and Kentucky to- bacco, dried at 212° Pahi-., contain from 6g to 7J of nicotina; Havannah tobacco (cigars) less than 2%. (Schloesing.) NI&HT'MAEE. Syn. iNCUBrs, Ephialtes, L. The common causes of nightmare are indi- j,'estion and tlie use of narcotic and intoxicat- iiif; substances. Its prevention consists in the seleetiun of proper food, and in duly attend- ing to the state uf the stomach and bo"eN. Heavy and late suppers should be particularly avoided, as well as all articles of diet that are of difficult digestion, or apt to induce flatu- lency. When it arises from strong drink, to- bacco, or opium, these should be abandoned, oi employed in smaller quantities. A teaspoonful of aromatic spirits of ammonia, magnesia, or bicarbonate of soda, taken in a glass of eold water on going to bed, is a good and simple preventive. In cases acconip:mied by resth s-- ne>s, a few drops of laud. mum or tincture of henbane may he added. An occasional ape- rient is also excellent. See Chamomile. NIGHT'SHADE (Deadly). .Syn. Beliadonna (B. P , Ph. L. E. & D.). " Ttie leaf, fresh -.mi dried (leaves and root — Ph. D.), of Alropa belladonna, Linn." " The fresh leaves and branches to which they are attached ; also the leaves separate fi-om the branches, carefully dried, of Atropa belladonna, gathered, when the fruit has begun to form, from wild or cul- tivated plants in Britain" (U. P.). "Oval, 1104 NIGHTSHADE— NITRIC ACID acnte, very perfect, glabrous, when bruised, exhaling a disagreeable odour. Tlie lieib which grows spontaneously in hedges and unculti- vated places Is to be preferred to that which is cultivated in gardens." (Ph. L.) Belladonna is a powerful narcotic, and is used as an anodyne, antispasmodic, and discutient, in a variety of diseases, — neuralgia, arthritic pains, migratory rheumatic pains, spasmodic rigidity and strictures, angina pectoris, hoop- ing-cough, fevers, phthisis, &c. ; also as a pro- phylactic of scarlet fever, as a resolvent in enlarged and indurated glands, to produce di- latation of the pupil, &e., &c. — Dose. Of the powder, commencing with 1 gr., gradually and cautiously increased until dryness of the throat or dilation of the pupil occurs, or the head is afleqfed. See Atkopia. MIGHTSHADE (Woody). Syn. Bitter- sweet ; DuiiOAMAKA (B. p., Pli. L. E. & D.), L. The "new shoots (caules) of Solanum Dulcamara, Linn." " The dried young branches of the Solanum Dulcamara (Bitter- sweet) from indigenous plants which have shed their leaves" (B. P.). " It is to be collected in autumn, after the leaves have fallen." (Ph. L.) Diaphoretic, diuretic, and (in Inrge doses) narcotic. See Inpitsion ov DnLCAMAiiA. HIO'EIUM. See Tantalum. MIP'PLES (Sore). The most common form of this affection is that termed " chapped nip- ples*' by nurses. As a preventive measure, the part may be moistened morning and even- ing, tor some weeks before the period of lacta- tion, with a little rum or brandy, which is more eifective if slightly acidulated with a few drops of dilute sulphuric acid. Some per- sons employ tincture of tolu, or compound tincture of benzoin (Friar's balsam) for this purpose. When chaps, cracks, or like sores, arising from lactation, are once developed, one of the safest and most effective remedies is tincture of catechu, applied 3 or 4 times a day, by means of a camel-hair pencil. The celebrated nostrum of Liebert f or cracked nipples, '* Cosm^Hqueitifaillibleetpromptcontre ies gert^ures ou crevasses aux seins et autres/' is a lotion formed of 10 gr. of nitrate of lead dissolved in -4 fl. oz of rose water, and tinged with a little cochineal. The parts are moist- ened with the liquid, and are then covered with fine leaden nipple-shields, two of which are provided for the purpose. This is repeated soon after each time the child leaves the breast ; and the nipple is careluUy washed with a soft sponge and lukewarm water, and gently dabbed dry with a very soft towel, before the infant is again applied to it. This remedy is very sue ces»f ul, and has acquired great popularity and patronage in Brussels, Paris, Prankfoi't, aud other parts. It must be recollected, however, that all applications of an active or poisonous nature should be employed with the greatest possible caution, as, unless unusual care is taken, a portion of the remedy muy remain concealed within the delicate pores of the skin, and be sucked ofE by the infant, to the serious dis- turbance of its health. BITBAN'ILINE. This substance is obtained by acting on nitrobenzol with a mixture of fuming nitric acid and oil of vitriol ; Dinitro- benzol is formed, which is dissolved in alcohol, and the resulting solution subjected to the re- ducing action of ammonia and sulphuretted hy- drogen, as described under aniline. Nitrani- line forms yellow, acicular crystals, little so- luble in cold water, but freely soluble in alcohol and ether. Its salts are crystallisable. NI'TEATE. Si/n. Niteas, L. A salt of nitric acid (e. g. Ag.NOj, nitrate of silverj. The nitrates are very easily prepared by the direct solution of the metal, or its oxide, or carbonate, in nitric acid, which, in most cases, should be previously diluted with water. By evaporation, with the usual precautions, they may be obtained either in the pulverulent or crystalline form. The nitrates are characterised by deflagrat- ing when thrown on red-hot charcoal; also by their aqueous solutions, after being mixed with half their bulk of strong sulphuric acid and thoroughly cooled, yielding a brown cloud with a crystal or concentrated solution of ferrous sulphate. See NiiElo acid, and the respective metals. NI'TKE. Nitrate of Potassa. See Po- TASSIUJI. NI'TRIC ACID. HNO3. St/n. Azotic ACID; AOIDUM NITEIOCM (B. P., Ph. li., B., & D.); Aquaeoetis. Prep. 1. (Ph. E. and Ph. L. 1836.) Puri- fied nitre (dried) and sulphuric acid, equal parts ; mix in a glass retort, and distil with a moderate heat, from a sand bath (or naked gas flame — Ph. E.) into a cool receiver, as long as the fused materials continue to evolve vapours. " The pale yellow acid thus obtained may be rendered nearly colourless (if desired) by gently heating it in a retort." (Ph. E.) Sp. gr. 1'500. In the present Ph. L. this acid is included in the materia medica. (See below.) 2. (Ph. D.) The nitrate of potassa is dis- solved in water, the solution treated with a little nitrate of silver, filtered, evaporated to dryness, weighed, and then treated as above. 3. Nitrate of soda (cubic nitre, Chili saltpetre) is introduced, in quantities varying between 4 and 10 lbs., into a cylindrical iron retort, which it will only half fill, and after the lid is luted on and the connection made with the condensers, an equivalent of oil of vitriol is poured in through an aperture provided for the purpose, and the charge is worked ofl' with a gradually increased heat. The condensing apparatus consists of a series of 5 or 6 salt- glazed stoneware receivers, about ^th part filled with cold water. The product of this process is the strongest brown and filming ' HiTKOtrs ACID ' of commerce (aquatoetis, PDMINQ KITEIO ACID ; ACIDUM NITKOSnM NITRIC ACID 1105 iCiDCU KITBICUK TUMANs), and haa usually the sp. frr. 1'46. It is rendered colourleeg by ({cntly beating it in a glass retort, when it forms COMM£UCIAL NIIUIC ACID (sp. gr. 1'37 to 1-4.) •I. (PUBE MONOHTDEATED KITRIC ACID.) By mixing the strongest commercial acid with abnut an equal quantity of oil of vitriol ; re- dlHlilling; collecting apart the first portinn which comes over, and exposing it, in a vessel slightly warmed and sheltered from the light, to a current of dry air made to bubble through it until the nitrous acid is completely re- moved. Prop. Pure liquid nitric acid is colourless, highly corrosive, and possesses powerful acid and oxygenising properties. The sp. gr. of the strongest liquid acid (monohydrated nitric acid) has the sp. gr. 1"517 at 60° Fahr. " On boiling nitric acid of different degrees of concentratioD at the ordinary atmospheric pressure, a residue is left boiling at 249° Fahr., and 29 in. barometer, having a sp. gr. 1'414 at 60° Fahr." (Pownes.) Acidof less density than 1''114 parts with water, and gradually be- comes stronger by boiling; but acid of less sp. gr. than 1'414 is weakened by exposure to heat. When exposed to intense cold, liquid nitric acid freezes. It is rapidly decomposed, with loss of oxygen, by contact with most organic and many metallic and non-metallic bodies. In many cases these reactions occur with con- siderable violence, and the production of light and heat. Pit)'. The nitric acid of commerce is gene- rally contaminated by liydrochloric acid, ni- trous acid, sulphuric acid, or chlorine, or by their soda or potassa salts, and, occasionally, iodine, togither with an excess of water. The liist is readily detected by the sp. gr., and the others by llie appropriate tests. " Colourless. Contains 70f of HNO3. Sp. gr. 142. yO gr. by weight, mixed with \ oz. of distilled water, require for neutralisation 1000 grain measures of the volumetric solution of soda. Evaporated, it leaves no residue. Diluted with six volumes of distilled water, it gives no precipitate with chloride of barium or nitrate of silver — indi- cating absence of sulphuric and hydrochloric Bcids." (B. P.) 5 measures of acid, sp. gr. 1'5, mixed with 2 of water, condensed into 6^ measures, and makes the sp. gr. 142. " Free from colour. Sp. gr. 142. Exposed to the air, it emits very acrid vapours. Totally volati- lised by heat. Diluted with 3 times its volume of water, it givi'S no precipitate with either nitrate of silver or chloride of barium. 100 gr. of this acid (sp. gr. 1'42) are saturated by 161 gr. of crystallised carbonate of soda." ( Ph. L.) The Ph. E. states the density of commercial nitric acid is 1-38(1 to 1-390. " If diluted with distilled water it precipitates but slightly, or not at nil, with solution of nitrate of baryta or nitrate of silver." The best ' double aqua- fortis ' of the shops (aquafortis duplex) has usually the sp. gr. 1'3G; and the single aqua- TOL. II. fortis (aquafortis simplex), the sp. gr. 122 ; but both are commonly sold at much lower strengths. Te»t». — 1, It stains the skin yellow, — 2. When mixed with a little hydrochloric acid or chloride of ammonium, it acquires the power of dissolving gold leaf. — 3. Morphia, brucia, and strychnia, give it ii red colour, which is heightened by ammonia in excess —4. When placed in a tube, and a solution of protosul- phate of iron is cautiously added, a dark colour is developed at the line of junction, which is distinctly visible when only y^.i^gth p:irt of nitric acid is present. This test may be often conveniently modified by dropping iuto the liquid a crystal of protosulphate of iron; the fluid immediately surroundin.; this crystal then acquires a dark brown colour, which dis- appears upon simple agitation of the tluid.or by heating it. — 5. When mixed with a weak solu- tion of sulphate of indigo, and he:ited. the colour of the latter is destroyed. — 6. When saturated with carbonate of pi'tas>iuin or sodium, and evaporated to dryness, the resi- duum deflagrates when thrown on burninijf coals. — 7. When the mixture of a nitrate witii cyanide of potassium, in powder, is heated on a piece of platinum, a vivid dutlagralir>u fol- lows, attended with distinct i^'uition and detonation. (Frosenius.) It is stated that sulphate of aniliue is tin extremely delicnte test for nitric aeid. The foUnviing is the method of its application : — About a cubic centimetre of pure concentrated sulphuric acid (sp. gr. 1'84) is placed in a watch gli.-s; half a cubic centimetre of a solution of sul- phate of aniline (formed by adding ten drops of commercial aniline to 50 ce. of diluted sulphuric acid in the proportion of 1 to 6) is poured on, drop by drop; a ^l.iss tube is moistened with the liquid to be tested, and moved circularly in the watch-glass. By blowing on the mixture during the circular agitation, when a trace of nitric acid is present, circular striiB are developed of a very intense red colour, tinting the liquid rose. With more than a trace of nitric acid the colour becomes carmine, passing to a brownish red. This process serves to detect the presence of nitric acid in the sulphuric acid of commerce. It will also reveal the presence of nitrates in water.' — 8. Take a quantity of dipheuylamine, about the size of a mustard seed, put it iuto a test-tube, and pour a little sulphuric acid over it, then add a drop or two of water, >o as to increase the temperature snfiiciently to effect the solution of the diphenylamine, iind the test is ready for use. Now add very gently the solution to be tested, and if only a trace of nitric or nitrous acid be present, a beautiful and very permanent blue colouration is produced at the junction of the two liquids, but if there be any quantity of the nitrogen compound, the colour becomes almost black. This reaction is so delicate and certain that, in • Fluirmaceutical Year Book.* 70 1106 NITRIC ACID the case of a solution of nitric acid containing about 1 pai-t B. P. acid in 10,000 of water, tile reactioa is most distinct; one part of nitrite of potassium in 80,000 of water gives also almost unmistakable evidence of the presence of the nitrogen acid. The following process for the quantitative estimation of nitric acid is by Fischer:' — Indigotin prepared by reduction of indigo by means of grape sugar, alcohol, and caustic soda, oxidation in the air, and solution in sulphuric acid, may be kept unchanged for years. Five c.c. of such a solution, diluted with water and mixed with 30 c.c. of pure sulphuric acid, is titrated by adding a standard nitric acid Folution until the blue colour gives place to a light green; the indigo solution is then diluted, so thiit 1 c.c. shall be equal to 0'0025 milligrammeequivalents of nitric acid,or 02525 millij.'r«mme of potassium nitrate. If a water is being examined it is run into 4 c.c. of the titraled indigo solution, mixed with 20 c.c. of sulphuric acid, until the blue colour changes to light green. Ten, divided by the number of c.c. of water u.*ed, expresses the milligramme equivalents of nitric acid per litre; thus, if 4 c.c. of water are used, there are 2-5 millisramme equivalents of nitric acid, equal to 2525 milligrammes of potassium nitrate per litre. If a preliminary test with bruoine has shown that the water contains very little nitric acid, 2 c.c. only of the indigo solution must be used, or sometimes as little as 1 c.c. If more than 8 c.c. of water is required to destroy the blue colour, 100 c.c. must be evaporated down to the volume of 8 c.c. and then titrated. The volume of sul- phuric acid must be at least double the sum of the volumes of indigo and water; the temperature must not sink under 110°. The nitrates may all be tested as above by first adding a small quantity of pure sulphuric acid, which will liberate the nitric acid of the salt. Estim. — The strength of nitric acid may be roughly estimated by its sp. gr. ; but more accurately by ascertaining the amount of car- bonate of sodium, or other salt of known com- position, which is required to neutralise it. To rentier this assay trustworthy, it must be, in all cases, also tested to detect the presence of impurities. See Acidimetet. Ani., Sec. See AOIDS. Uses. Nitric acid is employed in assaying, in dyeing, iu etching on copper, in the preparation of gun-cotton, oxalic and sulphuric acids, &c. In medicine it is used as a caustic to corns and warts ; and in doses of 1 to 10 drops, in a tumbler of water, in liver complaints, fevers, dyspepsia, syphilis, to remove the effects of mercury, or as a substitute for that drug, &c. Externally, it is employed in the form of baths, lotions, and ointment. • Dr Collier states that a strong lotion of nitric acid is almost a specific 1 Hinal., 'Polyt. Journ.,' cc\iii, 423 — 437; ' Journ Chem. Sue.,' ^ud series, xiii, 4bl. in lepra, and several other kindred skin diseases. Concluding Itemarks. — The common source of nitric acid is nitrate of potassium, but it may also be obtained from other nitrates by a similar process. Nitrate of sodium is fre- quently used instead of nitrate of potassium, and is more convenient in some respects, as the residuum is more easily dissolved out of the retort or cylinder. The residuum of the common process with nitre ('sal enixum') is chiefly employed as a fiux by the glass-houses, and as a source of potash in the manufacture of alum. By proper management nitre yields more than I of its weight of pure nitric acid, sp. gr. 1'500 ; and nitrate of soda, its own weight of acid, sp. gr. 1"4. By the patent process of M. Mallet, dried nitrate of soda is decomposed by dried or monohydrated boracic acid, by heating the two together. ' The products are liquid nitric acid, which distils over, and biborate of soda (borax), which remains in the retort. The crude coloured nitric acid of commerce (aquafortis) was originally prepared by dis- tilling a mixture of nitre and copperas, and is still sometimes obtained in this way. The nitric acid of commerce may be freed from the impurities alluded to above by one or other of the following methods : — 1. By the addition of a little nitrate of silver, as long as it produces any cloudiness, and, after repose, decanting the clear acid, and rectifying it at a heat under 212°. To ensure a perfectly colourless product, a small portion of pure black oxide of manganese should be put into the retort. (Murray.) 2. By agitating the acid with a little red oxide of lead, and then rectif ving it, as before. 3. By adding \% of bichromate of potassa to the acid before rectifying it. This answers well for acid not stronger than sp. gr. 1-48. 4. By rectification at a gentle heat, rejecting the first portion that comes over, receiving the middle portion as genuine acid, and leaving a residuum in the retort. (Ure.) According to Apjohn and others, the strongest liquid nitric acid, sp. gr. 1-520, is a mono- hydrate; that of the sp. gr. 1-500, a sesqui- hydrate; that of 1'486, a binhydrate; and that of 1-244, a quadrihydrate; or containing I'espectively 1, ij, 2, and 4 atoms of water. (See heloio.) Nitric Acid, Anhy'drons. N2O5, Syn. NiTBic ANHTDEIDE. This interesting substance was first obtained in a separate lorm by M. Deville, in 1849. Prep. (M. Deville.) Nitrate of silver is dried by exposure to a current of dry carbonic acid at a temperature of 356° Fahr., and the tube containing it is then immersed in a water bath heated to 203° Fahr. ; pure dry chlorine gas is next passed through the apparatus, and, as soon as the reaction commences, the tem- NITRIC ANHYDRIDE-NITROGEN 1107 pcretnre is rcilviced to 154° or even 136°, but not lowiT; the production of cnBtals^ in the nceiver, which must be co As the specific gravity of nitro-glycerin is 1-6, one part by bulk will yield by coujbus- tion : — Aqueous vapour , 554 volumes Carbonic acid . . 469 Oxygen . . 39 Nitrogen . . 236 „ 12981 „ Other experimenters affirm that, instead of free oxygen, nitrous oxide is one of the pro- ducts of the combustion of nitro-glycerin. According to Nobel the heat liberated when nitro-glycerin is exploded, causes the expansion of the gases to be eight times their original bulk ; therefore, one volume of the substance will yield 10,384 volumes of gas, whilst one part by bulk of gunpowder only yields 800 volumes of gas. If these data be correct the explosive force of nitro-glycerin is thirteen times greater than that of powder, bulk for bulk, and eight times greater weight for weight. Bottger has devised a process for the pre- paration of nitro-glycerin, which being, as he affirms, entirely free from danger, adapts it for lecture experiments : — A few grains of pure ' Wagner. glycerin, free from water, is poured into a test-tube, which is surrounded by a freezing mixture, and containing a mixture of one volume of the most concentrated nitric acid (1'52 sp. gr.), and two volumes of the strongest sulphuric acid (1'83 sp. gr.). Then, as quickly as possible, the whole is poured into a larger quantity of cold water. The nitro-glycerin, which has formed like oil drops, sinks rapidly to the bottom, being specifically the heavier liquid. It is then washed several times by decantation with fresh water, and, lastly, with a weak solution of soda. Remove the water with a few pieces of fused chloride of calcium. Then the nitro- glycerin is in such purity that it may, with- out danger, be kept any length of time fur lecture experiments. iriTRO-HYDEOCHXiO'EIC ACID. Syn. Nt- TEO-MUEIATIO ACID; AQTJA EEGIA, AOIDTJM NITEO-HYDEOOHLOEICtIM (B. P.), A HITKO- MUEIATICUM, L. ; Eau eeq-ale, Fr. Prep. 1. (B. P.) Nitric acid, 3 ; hydrochloric acid, 4; water, 25. Mix the acids twenty-four hours before adding the water. (This precaution is necessary to allow of the development of the chlorine, and the chloronitrous and chloronitric gases which result from the mutual decompo- sition of the two acids, and upon which the therapeutic activity of the agent depends). Colourless. Keep the mixture in a cool and dark place. 2. (Ph. D. 1826). Nitric acid, 1 part ; hy- drochloric acid, 2 parts (both by measure); mix in a refrigerated bottle, and keep the mix- ture in a cold and dark place. Used to dissolve gold and platinum ; and in medicine, in liver complaints, syphilis, the exanthemata, &c., either externally, in doses of 5 to 15 drops in water, or • externally, as a foot- or knee- bath. It is also occasionally employed as a caustic. 3. (Aqua eegia with sai ammoniac.) Nitric acid (sp. gr. 1'2), 16 fl. oz. ; sal ammo- niac, 4 oz. ; dissolve. Occasionally used by djers; does not keep well. 4. (Dykes' AQnAFOETis.) Colourless nitric acid (sp. gr. 1'17), 10 lbs.; hydrochloric acid (sp. gr. 119), 1 lb.; mix. Used by dyers. HITEO-PEUS'SIDES. A series of salts dis- covered by Dr Playfair, and obtained by the action of nitric acid ^on the ferrocyanides and ferridcyanides. The most important of these salts is the nitroprusside of sodium (NAj (NO) FeCyj . 2Aq.). Prep. Dissolve 2 parts of pow- dered ferrocyanide of sodium in 5 parts of common nitric acid, previously diluted with its own volume of water. When the evolution of gas has ceased, digest the solution on a water bath until it no longer yields a blue but slate- coloured precipitate with ferrous sulphate. Cool the liquid, filter, neutralise the filtrate with carbonate of sodium, and again filter. This filtrate, on evaporation, yields crystals consisting of a mixture of uitro-prusside of NITUOUS ACID— NOMENCLATURE 1111 sodium and nitrate of potaBBinm ; the former, which may bo recognisod by their rhombic abape and their fine ruling colour, ahould be picked out and preserved.— Vie. As a test for soluble sulphides, with which nitro-prusside of sodium strikes a beautiful violet tint. Accord- ing to Playfair this is the moat delicate teat for alkaline sulphides. NI'TROUS ACID. HNO^ See NiTEOUS Anhydbide, under Nitbogkn, Oxides op. NITEOUS OXIDE. Sec NiTHoaBlT, Oxides OP. NODE, Syn. NoDUS, L. A hard tumour pro- ceeding from a bone, and caused by the swell- ing of its external membrane. The bones of the leg, forehead, and forearm, are those most commonly attacked. Nodes are generally ac- companied with considerable pain, and often with caries and loss of vitality. NOLI ME TANGERE. See Lupus. NOMENCLAIUBE (Chemical). The f>d- lowing information will doubtless prove useful to many of our readers, as serving to explain terms which are necessarily of frequent occur- rence in this work : AoiDS.^o. When a substance produces only one acid compound, the name of tliis acid is formed by adding the termination -10 to tliat of the radical, or to the leading or character- istic portion of it; as sulphuric acid, an acid of sulplmr. This is Latinised by changing -10 into -louM ; as, acidum, sulphuncvM. — b. When u b.jdy forms two aiid compounds containing oxygen, the name of the one con- taining the sinnller proportion of that substance ends in -ous j as nitrova aciil, which con tains 1 atom of nitrogen and 2 of oxygen ; nt'^rio acid, containing 1 atom of nitrogen and 3 of oxygen. In this case the Latin name ends in -OSUM ; as, acidum ' miirosUM. — o. When a substance forms more than two acids with oxygen, the Greek preposition HTPO- (below or under) is prefixed to the name of the acid in -ous or -ic next above it ; as, HY- FOcA^orous acid. — d. When a new acid com- pound of a substance is discovered, containing more oxygen than another acid of the same substances already known, the name of which ends in -ic, the prefix peb- or htpeb- is added ; as, pfiBio^ie acid. This may be illus- trated by the oxygen acids of chlorine : — Ilypoclilorous acid tacidum hiipocktoronim) 11CI0 Clilorous „ ( „ cluoroaiim) . . HClOg Cliloric „ ( „ ehtoricvm) . . HClOj FCduinc} .- ( .. P-*'--"»). HCIO. Oxides. The names ofthese have, in general, reference to the number of atoms of oxygen which they contain. When a metal forms only one ba^ic compound with oxygen, this compound is simply called the oxide of such base ; but as most substances form more than one compound with oxjgen, certain prefixes are introduced to express the proportions. In such cases it is generally found th.it one out of the nambcr bos a strongly marked basic cha- racter, and contains 1 atom of each of its constituents. This is called the oxido, prot- oxide,or monoxide, and forma the .si:indardto which those both above and below it are preferred. Thus, supposing M to be the metal, we may have: — Suboiide or dioxide ^luhorydum diunidnm) . MjO Oxide, protoxide, or iiioiiuxide (oxy^um pro- t(txydutn) .... , , MO iiciqiuoxide H'squiozydum) .... >IJJ, Binojide, dioxide, or deutoiide (hmox)dtm deutoxydum) MO2 Teroude or (rioxide {liroii/diim, trilozudiim . MU, ^ That couttuii- ?mxiie (perozuium) . . 3 i"!! tl'' '"r*"' '^ ' ' 1 prormrtion ot (.oxygen. Salts. — a. Acids having name-* ending in •10 give rise to salts whose mimes end in ate; thus nilrlO acid yields niVrATES, 0. g. nitrate of silver. -ATE is Latinised by -as, e. g. nitrate of silver becomes argen ti nitrAS. b. Acids po-^^essin;^ names ending in -ous form salts having names ending in -itk ; thus ««ZpA«r0US acid produces sulphiTSS, e. g. sul- phite of sod ittm. -iTEis Ijatinised by -isj e.g. sulphite of sodium becomes sulphis. c. The preceding names are jiresnmerl to refer to neutral compounds. In acirf ^iilts the prefixes noticed above are added to express the preponderance of the aeid radical over the metal. KHSO4 is called acid sulphate of potassium, ■aisulphate of potassium, or Bi- sulphate of potash, the neutral sulphate bein^ KjSO^. d. in basic salts, or those in whieh the metal is in excess of the acid radical, the prefixes •SUD and -DI are employed j e.g, the formula of neutral acetiite of lead is PbAg. This salt, when boiled with oxide of lead (a Ims-e), fui"- nishes [PbAjPbO] and [PbA22Pb0]. Tli.y are both, therefore, ftcwic acetates; and to dia- tiiiguish one from the other the former is called macetate und the latter lUlacetate of lead ; -di referring to the presence of two atoms if lead and -tri to three. Formerly the salts of the metals of the alka- lies and alkaline earths received names which indicated the existence in them of the oxides of such metals. Thus, the terms carbonate of soda, nitrate of potash, carbonate of lime, sulphate of magnesia, names by which these fluids are still designated by some chemists are now substituted by the more systematic and less speculative n;i >es of carbonate of sodium, nitrate of potassium, carbonate of calcium, and sulphate of magnesium. An- other, and in the opinion of the editor, a still better-system of nomenclature is that in whieh the metallic or basic radiciil is mentioned first ; e,g. calcium sulphate instead of sulphate of calcium, ammonium chloride for chloride of ammonium. When the same radicals form more than one series of salts, each series is disi;inguished by appending the terminations -IC and -ous to that part of the name which refer to the basic radical; e. g. mercuro\ss chloride (HgCl), mercuric chloride (HgClj) ; 1112 NORFOLK FLUID— NOTICES ferrovs sulphate (FeSOi),ferrl0 sulphate (Fe^ (S0,)3). IsoN-METALLio BODIES, &c. The names of the compounds formed by the union of the non-metallic elements.nud certain other bodies, with the metals and with each other, either terminate in -IDE, Latinised by -idum, or in -URET, Latinised by -ubetum ; as, ar*e»iDE or orseMJUKET ((waeniDUM, arsenivusxTJu), bromlD'E, caj'ilDE or carSUKET, chlorlD'E, eyan- IDE, fluoriTi^, /ii/drmE, iodlDS, sulphlDE or sulphXJRET, &c. The first of these termina- tions now prevails among English scientific cliemists. Tlie prefixes already noticed are also employed here. Metals, The names of the metals (those of tljeni, at least, tliat have been given during the present century) end in -IUM or (less fre- quentlj') in -UM ; as potassioiif sodiVM, pla- tinvu. The Latin names of several of the non-metallic elementary bodies also end iu -IUM; as, iodinivsij nitrogenlVTA^ &c. Alkaloids. The names of the organic bases which resemble the alkalies in their properties end either in -lA, -NA, or -INE ; as, morphjAf quiNA, strychnl'SE. These termina- tions are now limited, as much as possible, to sub-tances exhibiting basic properties, but were formerly very loosely applied. Many chemists reject the first two termina- tions, and apply -INK to every substance of this class; as, morphlJSB, quiniSE, anilllSE, &c. Othee oeoanic substances. The names of organic radicles generally terminate in -YL ; as, ethYI; methYL, hemOYJi, &c. ; they mostly contain carbon, hydrogen, and oxygen. Compounds corresponding to the electro-nega- tive elements have the termination -ogen, as cganoaETH, amidoess. Neutral compounds ot carbon and hydrogen, mostly liquid, have the termination -OL, or -OLE ; as, benzOTj, pffrojjE. Other neutral substances, generally solid, have the termination -llil ; iis,parafflN,naphthallll. Compounds resemblingammonia, and generally considered as 'substitution compounds* of that body, terminate in -amine ; as, ethylAMlSE, propyltxiTSE. The Latin genitive or pos-essive of the above compounds iu — -as is -atis -is „ -itis -icum M -ICl -osum ^^ -osi -idum J, -idi -etnm » -eti -inm tt -ii -um « -i -ia "I -a t -naj ^x. Acetas (acetate), acetatis of acetate ; arsenis, arsenitis ; citricum, citrici ; arse- niosum, arseniosi ; iodidum, iodidi ; sulphu- retnni, sulphnretij sodium, sodii; platinum, platini; morphia, morphiae; quina, quinsej narcotina, iiarcotinae. The genitives of com- mon names vary with the termination. Most of those ending in -a make se, and most of those in -us and -um make -i ; but there are many exceptions, among which cornu (a horn) and spiritus (spirit) which are unaltered in the genitive singular, may be mentioned as examples. HOilFOLK FLUID. Frep. Take of linseed oil, 3 pints; black resin, \ lb.; yellow wax, 12 oz. ; melt, and add, of neat's-foot oil, 1 quart ; oil of turpentine, 1 pint. Used to pre- serve and soften leather. NOS'IUM. An unexamined metal, the oxide of which, according to Svanberg, exists in certain varieties of zircon. NOS'TRUMS. See Patent Medicines, &c. NOTICES. The following sections of the Public Health Act refer to serving and de- livery of notices under that Statute : (S. 266.) Notices, orders, and other such documents under the Public Health Act may be in writing or print, or partly in writing and partly in print ; and if the same require au- thentication by the local authority, the signa- ture thereof by the clerk to tlie local authority or their surveyor or inspector of nuisances shall be sufiicieut authentication. (S. 267.) Notices, orders, or any other docu- ments required or authorised to be served under the said Act may be served by deliver- ing the same to or at the residence of the person to whom they are respectively ad- dressed, or where addressed to the owner or occupier of premises, by delivering the same or a true copy thereof to some person on the premises, or if there is no person on the pre- mises who can be so served, by fixing the same on some conspicuous part of the premises ; they may also be served by post by a prepaid letter, and if served by post shall be deemed to have been served at the time when tlie letter containing the same would have been delivered in the ordinary course of post, and in proving such service it shall be sufficient to prove that the notice, order, or other docu- ment was properly addressed and put into the post. Any notice required to be given to the owner or occupier of any premises may be addressed by the description of the ' owner' or 'occupier' of the premises (naming them) in respect of which the notice is given, without further name or description. Enforcing the Drainage of Souses, (S. 23.) Notice is to be given to the owner or occupier, but in case of the failure of either to comply, and the authority having to do the work, the expenses fall on the owner. Insufficient Privy Accommodation. (SS. 36 and 37.) The same procedure as under the above section. The Cleansing and Whitewashing of Mouses. (S. 46.) Notice to the owner or occupier. — NOVARGENT— NUISANCE 1113 The person on whom the rotice is eerved is liable to a penttlty if it is not complied with. TAa Removal of Manure or Filth, ^o., in an Urban District. (S. 49.) Notice to he served on the person to whom the manure belongs, or to the occu- pier of the preinisea whereon it exists. If the urban authority have to remove it themselves, the expense of removal falls upon the owner of the nmnure, &c., or the occupier of the pre- mises, or where tliere ia no occupier, the owner of the pi'cmisee. In the case of Nuisances, (S. 94) Notice is to be served upon the pernon causing or permitting the nuisance to remain, or, if he cannot be founil, on the owner or occupier of the premises on which the nuisance arises ; but if the nuisance arises from tlie want or defective construction of any structural convenience, or where there is no occupier, notice ia to be served on the owner. In the ease of Souses, Sfe., requiring Dis- infection. (8. 120.) Notice is to be given to the owner or occupier, and in case of non-compliancp, the person on whom the notice is served is liable to penalties, and the expenses of the authority doing the necessary works falls upon tliat l>ersou (with certain exceptions, in case of poverty). NOVAE'GENT. Fref. Prom recently pre- cipitated chloride of silver by dissolving it in a solution of either hyposulphite of sodium or of cyanide of potassium. Used chiefly to restore old plated goods. The liquid is rubhiil over the metal to be coated with a little prepared chalk, and the part is afterwards polished off with a piece of soft leather. A powder re- cently sold unod for man. The husked grain constitutes OBOATS, and its meal oat- meal. The latter does not form a dough with water, as wheaten meal or flour does. Oats consist of from 24g to 28a of husk, and 743 to 7s5 of grain. According to M. Payen, they contain of starch,60'59g ; azotised matter, 14'39g ; saccharine and gummy matter, 9-25 g ; fatty matter, 5-50g; cellulose, 7'60g; silica and saline matter, 3-25g. The husks contain be- tween 6 and 7g of saline matter. (Prof. Norton.) The ash amounts to 2'18g, and consists of potassa and soda, 26'18g; lime, 5"95J; magnesia, 9'95g; oxide of iron, -401; phosphoHcaiid,43'843; sulphuric acid, 10'455j chlorine, •2G|j; silica, 2-67s; alumiua, 'Oeg. (Johnston.) The yield of oats is from 20 bushels per acre in poor soils, up to 60, 70, and even 80 bushels per acre in rich soils. The weight per bushel varies from 35 to 45 lbs., and the pro- duct in meal is about one half the weight of the oats- White oat— Long, sect., Slid and Srd coats not scparaljU. ». Compouuil grains x 100; h. One do. x 600. A larpe proportion of the onts given to horses passes off undigested. It has hence been proposed to prevent this loss, by either coarsely bruising them in a mill, or by pour- ing boiling water over them, and allowing them to macerate till cold, when tlicy arc to be given to the horses without straining off the water. It is stated on good authority that oats thus tre:ited nill not only fatten quicker, but go twice as far as without pre- 1118 OATMEAL— OBSTRUCTION OF LOCAL AUTHORITY paration. Oat bruisers are now manufactured by most agricultural implement maljers. Under the microscope the oat is seen to con- sist of two or three envelopes j the outer being composed of longitudinal cells ; the second ob- liquely transverse and not very clearly seen ; in this, the cells are wanting in part or pass into the cells of the third coat; the third en- velope consists of a layer, usually single, of cells, like whe^it. Before the envelopes are searched for the husks must be removed. The starch-cells are small, many sided, and cohere into round composite bodies, which are very characteristic, and which, by pressure, may be divided into separate grains. A high power is necessary for the examination of these latter. The starch of the oat does not polarise light. OAT'MEAL. S^n. Aven J3 faeina, F. ex SEMINIBUS ATEN« (Ph. D.), L. Oatmeal is the grain of the oat deprived of the skin, kiln-dried, and afterwards ground. It is rega;rded as one of the most nutritious of our cereals, being rich in nitrogenous matter, fit, starch, and sugar. According to Letheby it contains in 100 parts : — Nitrogenous matter . 12-6 Carbo-hydrates . 63-8 Fatty matter . 5-6 Saline matter . 30 Water .... . 15-0 100-0 Kreusler has shown that the nitrogenous principle of oatmeal contains gluten-casein, a substance very similar to the legumin of peas and bi'ans. Letheby points out that, although it contains more nutrient material than wheat, its liigher price renders it less economical as an article of diet. Oatmeal forms the staple of the food of the farm labourer both in Scotland and in England, being consumed more largely by the Scotch than the English peasant. Scotch oatmeal is superior to English in nutri- tive value. Oatmeal, when mixed with water, does not possess sufficient tenacity to enable it to be made into bread. It can, however, be baked into excellent cakes, which, when made in Yorkshire, are leavened, and when in Scot- land, unleavened. The qualities of indigestibility and a ten- dency to produce irritability of the bowels and skin, have been ascribed to oatmeal; before it was so prepared as to effectually remove from it the husk and hairs by efiBcient screening, it was in Scotland a frequent source of intestinal concretion. These concretions, the nature ol' which Wiis unravelled by Dr WoUaston, con- sisted principally of phosphate of lime mixed with the hairs and husks of the oat. Of thirty samples of oatmeal examined by the * Lancet Sanitary Commissioner,' no fewer than sixteen samples, or more than one half, were adulterated. The substance generally used for this purpose is barley meal, which is only half the price of oatmeal. Husks of barley, wheat, and of the oat itself, are also fre- quently used. Rice and maize are also some- times added. That supplied to the army, navy, and the workhouses, was very commonly adul- terated with whiting, plaster of Paris, or ground bones. The mineral sophisticant may be detected by the excess of ash, which should not exceed 2'36 per cent. These frauds are readily detected by the microscope. Orits or Oroats are the decorticated grain of the oat, which when bruised or crushed constitute Embden groats. Flummery (known in Scotland as sowans) is made by steeping the husks of the grain in water, until they be- come slightly sour, the strained liquid being boiled down to the consistence of gruel. Oat- meal soon becomes sour and rancid. It should be purchased at such shops as have a quick sale for it. See Aoaki, Stibabout. OBE"SITY. Si/n. Obesitas, Poltsaeca, L. Unhealthy or troublesome fatness or cor- pulency. Sometimes the secretion of fat, and its accumulation in the adipose membrane, is almost as rapid as that of water in anasarca; on which account some of the old writers have called obesity a dropsy of fat. Persons in easy circumstances, of indolent habits, who live freely, and who are of a cheerful and con- tented deposition, are those most liable to obesity. The treatment consists in the very gradual reduction of the diet, until it falls rather below the average quantity required by a healthy adult ; the very gradual disuse of fermented liquors, more especially beer; the gradual abridgment of the time devoteJ to repose, until it does not exceed 5 or 6 hours ; the employment of several hours daily in exercise in the open air, at first moderate, but increased day by day in energy, until it becomes laborious; and, lastly, arousing the mind from a state of lethargy to one of active or even harassing employment. In some cases the accumulation of fat has been enormous. Bright, of Maldon, weighed 728 lbs.; Daniel Lambert, of Leicester,739 lbs. ; a girl,4 years old, noticed in the ' Phil. Trans.,' 1813, weighed 256 lbs. Persons affected with obesity are generally short-lived. OBSTEUCTION OF LOCAL ATTTHORITY. Various penalties are mentioned in different sections of the Public Health Act for the of- fence of obstructing oflBcers, &c., representing the local authority, in carrying out the Act. The following section, which we select, deals with the subject generally : — Sec. 306. "Any person who wilfully ob- structs any member of the local authority, or any person duly employed in the execution of this Act, or who destroys, pulls down, injures, or defaces any board on which any bye-law, notice, or other matter is in- scribed, shall, if the same was put up by au- thority of the Local Government Board or of OCHRES— OILS 1119 tlio local nuthority, be liable for every such ullt'iioe to a penalty not ezceediiiu; £5. '• Where the occupier of any preminea pre- veiiU tlie owner thereof from obeying or carrjing into effect any of the provisions of thin Act, any justice, to whom application is made in this behalf, shall by order in writing require such occupier to permit the execution of any works required to be executed, provided that the same appear to such justice to be ne- cessary for the purpose of obeying or carrying into effect the provisions of this Act; and if within 24 hours after the making of the order sucli occupier Calls to comply therewith, he shall he liable to a penalty not exceeding £5 for every day during the continuance of such non- compliance. " If the occupier of any premises, when re- quested by or on behalf of the local authority to state the name of the owner of the pre- mises occupied by him, refuses or wilfully omits to disclose, or wilfully niistates the same, he sbiill (unless ho shows cause to the satisfac- tion of the court for his refusal) be liable to a penalty not exceeding £5." O'CHRES. These are native earthy com- pounds of clay, coloured with oxide of iron, with frequently a little chalk, or magnesia The differences in the colour arise partly from the quantity of iron present, and partly from the state of oxidation in which the iron is lound. Several varieties are known in com- merce — Bkown oohbe, French o., Oxfoed o., Red o., Roman o., Yellow o. All these, with the exception of the Krst and fourth, have a yellow colour. Aemenian bole, Indian bed, Venetian e., and Spanish BHOWN, are also ochres. All the ochres are darkened by calcination. The yellow ochres acquire a red or reddish- brown colour by this treatment. The pigment called Might red' is thus prepared from yellow ochre. ODONTAL'GIA. See Toothache. O'DORAMENTS. Si/n. Odoeamenta, L. Substances employed in medicine on account of their odour. They differ from disinfectants, in only disguising, but not destroying, noxious vapours, &c. Ammonia, steono tinegae, and PASTILLES, furnish the most familiar examples of this class of substances. See Disinfectants, Perfumes, &c. O'DOUE. The emanation of an odoriferous or scent-giving body. See Pbefcmes. (ENAN'THIC ETHER. See Etpee ((Enan- thic). OFFICIHAL. Sytt. Officinalis, L. A term applied to substances or medicines ordered in the Pharmacopoeia. OIL. Sj/ii. Oleum, L.; Huile, Fr. This name is given to numerous liquid or semi-liquid substances, expressed or drawn from animal or vegetable bodies; to various products of the distillation of bituminous minerals ; and to several unctuous mixtures in perfumery and pharmacy. To facilitate reference, we have grouped the principal substances generally called ' oils ' into classes, under the following heads:— Oils (Drying); OiL8(EnipyreumJtic) ; Oils (Fixed) ; Oils (Medicated) ; Oils (Mine- ral); Oils (Mixed); Oils (Perfumed); Oils (Volatile). See these articles also below .— Oil, Cansol'idated. 5yi>. Campticon, Fac- titious caoutchouc. a substance havini; most of the properties of India rubber, pre- pared by oxidising boiled linseed oil, or any other oil that hardens on exposure to the at- mosphere. To obtain the solid oil, plates of glass are dipped into Unseed oil, the films are then allowed to dry, and the process is repeated again and again until the plates are coated with many layers of perfectly oxidised oil. Instead of plates of glass, extensive sur- faces of prepared cloth arc employed when the manufacture is carried out on a large senle. The solid oil, having been scraped or petli d off the surfaces, is worked with a small pro- portion of shell-lac, by means of a mixing machine with hot rollers, until a material singularly like caoutchouc is produced. The consolidated oil can be rolled on to fabrics, so as to form a waterproof cloth, having the finish and flexibility of ruhhir-clotli. liy the action of heat the consolidated oil may be converted into a hard substance resembling vulcanite and ebonite. Its useful applications appear to be very numerous, but its manufac- ture has not as yet made much progress. 0IL-6AS. A mixture of several pa'seous hydrocarbons, obtained by passing common whale fat, resin, the heavy petroleum or sh de oil, or the tarry re-idues left after the distil- lation of these two latter substanees, or other cheap animal oil, through red-hot tulio<, or by allowing it to fall in drops on red-hot .stones or bricks arranged in an iron retort, or other suitable apparatus. The i^as has great illu- minating power, requires no purification, and is quite free from the ammoniacal and sulphur compounds which vitiate coal-gas. The sp. gr. of oil-gas varies with the heat employed in its production. It averages from 0-76 to 90, but it may rise as high as 11. The composition of coal gas, as given by Payen, is as follows: — Oil Gas. Gas from Petroleum residuea. Olefiant gas and homo- logues Marsh gas . Hydn.gen . Ciirbouie oxide Nitrogen 22-5 50 3 / / 15'5 4-0 17-4 58-3 24-3 OILS (Drying). All the fixed oils have an attraction more or less powerful for oxyiren, and, by exposure to the air, they citlier become 1120 OILS bard and reeinous, or they only thicken slightly, and become sour and rancid. Those which exhibit the first property in a marked degree, as the oils of linseed, poppy, rape, and walnut, are called ' drying oils,' and are used as vehicles for colours in painting. The others are frequently termed ' glutinous' or ' non- drying oils.' The resinifying or drying property of oils is greatly increased by boiling them, either alone or along with some litharge, sugar of lead, or white vitriol, when the product forms the ' boiled oil ' or 'drying oil ' (oleum desic- cativum) of commerce. The efficacy of the process, according to Liebig, depends on the elimination of substances which impede the oxidation of the oil. The following'formulse are adopted for this purpose : — 1. Linseed oil, 1 gall.; powdered litharge, I lb.; simmer, with frequent stirring, until a pellicle begins to form ; remove the scum, and when it has become cold and has settled decant the clear portion. Dark coloured; used by house-painters. 2. Linseed oil and water, of each 1 quart ; white vitriol, in powder, 2 oz. ; boil to dry- ness. Paler than the last. 3. Pale linseed or nut oil, 1 pint ; litharge or dry sulphate of lead, in fine powder, 2 oz. ; mix, agitate frequently for 10 days, then set the bottle in the sun or a warm place to settle, and decant the clear portion. Very pale. 4. Linseed oil, 100 galls. ; calcined white vitriol (' sulphate of ziuc'), in fine powder, 7 lbs. ; mix in a clean copper boiler, heat the whole to 285" Fahr., and keep it at that tem- perature, with constant stirring, for at least oue hour ; then allow it to cool, in 24 hours decant the clear portion, and in 3 or 4 weeks more rack it for use. Used for varnishes. 5. (Liebig.) Sugar of lead, 1 lb., is dissolved in rain water, ^ gall.; litharge, in fine powder, 1 lb., is then added, and the mixture is gently simmered until only a whitish sediment re- mains; levigated litharge, 1 lb., is next diffused through linseed oil, 2J galls., and the mixture is gradually added to the lead solution, pre- viously diluted with an equal bulk of water ; the whole is now stirred together for some hours, with heat, and is, lastly, left to clenr itself by exposure in a warm place. The lead solution which subsides fiom the oil may be used again for the same purpose, by dissolving in it another lb. of litharge, as before. 6. (Wilks.) lutolinseedoil, 236 galls., pour oil of vitriol, 6 or 7 lbs., and stir the two to- gether for 3 hours ; then add a mixture of fuller's earth, 6 lbs., and hot lime, 14 lbs., and again stir for 3 hours ; next put the whole into a copper, with an equnl quantity of water, and boil for about 3 hours , lastly, withdraw the fire, and when the whole is cold, draw off the water, run the oil into any suitable vessel, and let it stand for a few weeks before using it. Patent. 7. ('Allg. Polytech. Zeitung.') Binoxide of manganese (in coarse powder, but not dusty), 1 part; nut or linseed oil, 10 parts; mix, and keep the whole gently heated and frequently stirred for 24 to 36 hours, or until the oil begins to turn reddish. Recommended for zinc paint, hut is equally adapted (or other purposes for which boiled oil is employed. Obs. There is often a difficulty in obtaining the oils ' bright' after boiling or heating them with the lead solutions ; the best way, on the small scale, is either to filter them through coarse woollen filtering paper, or to expose the bottle for some time to the sun or in a warm place. On the large scale, the finer oils of this kind are often filtered through Canton-flannel bags. The litharge and sulphate of lead used in the above processes may be again rendered available for the same purpose, by washing them in hot water, to remove adiiering mu- cilage. OILS (Empyrenmat'ic.) Sj/n. Olea empt- EEFMATICA, L. The * empyreumatic oils' of the old pharmaceutical writers we're oily fluids obtained by the dry distillation of various substances, animal, vegetable, and mineral. But few of them are in use at the present day, though formulae are given for them in some of the foreign pharmacopceias. Two or three have useful applications in the arts, and it is therefore necessary that we should briefly describe their preparation. When the ingre- dients are of a liquid or pasty nature, or become so when heated, they are usually mixed with about twice their weight of sand, pow- dered glass, or other like substance, to divide them, and thus expose them more effectually to the action of^ the fire. Care must also be taken to provide a well-cooled receiver, which must be furnished with a tube to carry off the non-condensable gases liberated at the same time as the oil. The products of the first distillation are generally purified by recti- fication, either alone or along with water. In general, they require to be preserved from the light and air. The following are the principal substances belonging to this class : — Oil of Al'oes. Si/n. Aloetic oil ; Olettsi ALOETicuM, L. 1. From Socotrine or hepatic aloes distilled along with sand. 2. (Batavian — Cadet de Gassicourt.) Olive oil, 1 lb. ; hepatic aloes and myrrh, of each in powder, 2 t'Z. ; olibanum, ^ oz. ; distil in a sand bath, from a stoneware retort. Used as an external vermifuge for children ; a portion is rubbed 2 or 3 times a day over the umbi- lical regions. Oil of Am'ber. Sj/n. Oleum sticcini, L. From coarse pieces of amber, distilled in an iron retort, either alone or reduced to powder and mixed with sand. The oil is separated from the fetid liquor and succinic acid which passes over, and rectified along with about 6 times its volume of water, by a gentle heat. It then forms 'eectified oil of ambeii' (OLEUM SUCOINI — Ph. L. 1836, O. S. BECTI- OILS (FIXED) 1121 FICiTUM— Ph. D. 182(3. O. 8. PUEISSIMiril — Ph. E. 1841). Prod. 20?. Prof., S[c. It has a pale yellow colour, n stroni;, ungmtcful odour, and a hot, acrid !»it«; hcitt nnd nir blacken and thicken it; it boiU at IBS' Fahr. Sp. gr. -758 at 75° Fnbr. It is antispasmodic, rubefacient, and stimulant. — Dose, 5 to 12 drops, made into an emuUioii with mucilnge; in hysteria, epilepsy, and convulsive aflections. Externally, as a friction, either alone or combined with lauda- num or sweet oil, in rheumatism, tic doulou- reux, hooping-cough, &c. Oil of Amber, Ozydated {Artificial Musk). Put into a cup 1 dr. of oil of amber, and add to it, drop by drop, SJ fl. dr. of strong nitric acid ; let it stand for 36 hours, then separate and wash the rusi nous matter. Antispasmodic and nerviuo. — Dose, 5 to 10 gr. For children, i gr. to 1 gr. Oil, An'imal. 1. (Empyreumatic or Fetiil j Oil OB nAiiTsHOBN, Dippel's o. ; Olkum ANIMALB EMPyEEOKATIOUM, 0. COENC OEBVl, (J. DlPPELii, L.) Chietiy obtained as a ht'condttry product in the manufacture of bone- black. Fetid and dark coloured. Used chiefly tn make lampblack. 2. (Kllicroill; RECTIFIED OIL OP HAHTS- iioiiN ; Oleum animale juTnEiiiUM, O. counu CEBTI BEOTIFICAIUM, LoCO OLEI ANIMALIS DiPPELii, L.) — a. A finer kind of animal, oil, made by %\on \y distilling oil of hartshorn, and collecting only the first portion that comes over. Pale and limpid. Exposure to light discolours it. b. (Ph. Bor.) Fetid animal oil distilled in a sand bath, and the product rectified with four times its volume of water. White, limpid, fragrant. Light discolours it. Prof. The refined product is said to be antispasmodic, anodyne, and diaphoretic. — Dose, 5 to 30 drops, in water j in large doses it acts as an irritant poison. Oil of Birch. Syn. Oleum betul^, L. From the inner bark of the birch, by heating it in an earthen pot with a hole in the bottom, to allow the oil to flow through into another jar sunk in the ground nnd luted to it. Thick, balsamic, fragrant. Used chiefly to dress russia leather. Oil of Box-wood. Sijn. Oleum buxi, 0. B. KMPYBEUMATicuM (I'll. L. 1746), L. From box-wood sawdust. Reputed resolvent; ano- dyne, antispasmodic, and diaphoretic. — Dose, 5 to 20 drops ; in convulsions, epilepsy, gonor- rhoea, &c. Externally, in toothache, &e. Oil of Bricks. Syn. Oleum lateritium (Ph. L. 1746), L. Prom olive oil, mixed with brickdust, and distilled ; or, from hot bricks stfcpi'd in olive oil, then broken to pieces, and distilled. Oil of Bricks (Factitious). Syn. Oleum LATSBITIUM PACTITIUM, L. From linseed oil, 1 lb. ; oil of turpentine, \ lb. ; oil of bones or of hartshorn and Burbadoes tar, of each 1 oz. ; VOL. II. simply stirred well together. This is generally sub'itituted for the preceding in the shops. Oil of Cade. Syn. Oleum cadisum, L. ; HuiLE DB CADE, Fr. From the Junipenu oxyeedrua or Languedoc juniper. Used as oil of tar, which is commonly sold for it. Oil of Coal. Syn. Coal oil. From the gas-works. See Naphtha. Oil of Ona'iacum. Syn. Oleum ouaiaci, O. G. KMPYBEUMATICUM, L. From guaiacum shavings or raspings. Reputed balsamic, pec- toral, and resolvent. Oil of Hartsliorn. Bone oil and rectified bone oil are commonly sold for it, but are inferior to it. See Oil, Animal (above). Oil, Paper. Syn. Rao oil, Pyeothonidj! ; Oleum chabtje, L. On the small scale, by burning paper on u cold tin plate, and col- lecting the oil ; ou the large scale, by the destructive distillation of paper or lini'u rags. In baldness, toothache, ear-ache, &c. Oil, Far'affin. See Oils, Minkbal. Oil, Petro"leum. See Oils, Mineeai, Pe- TBOLEUM. Oil, Sag. See Oil, Papeb, above. Oil, Sock. See Naphtha, Oils, Minebal, Peteoleum. Oil, Shale. See Oils, Minebal. Oil of Soot. Syn. Oleum fdlioinis (Ph. L. 1746), L. From wood-soot. Fetid ; re- puted antispasmodic and nervine. Oil of Tar. Syn. Spieit of t. ; Oleum PINI, 0. p. eubeum, O. tmos, 0. PICIS li- QUID.S, L. By simple distillation from wood- tar. Reddish and strong scented. By one or more rectifications it becomes colourltss and limpid. It soon gets thick. Used in ringworm and several other skin diseases, made into an ointment with lard. It is poi- sonous if swallowed in larfjc doses. Oil of Tobac'co (Empyreumatic). Syn. Oleum tabaoi empteeumaticum (Ph. U. S.), L. From tobacco, in coarse powder, gradually heated in a green-glass retort to dull redness, and kept at that temperature as long as auy oil passes over ; the oily portion is then sepa- rated from the water in the receiver, and kept for use. Highly narcotic and poisonous. Oil of Wax. Syn. Oleum ceiue, L. From beeswax and sand distilled together; the product is rectified once or olteiier. Reputed diuretic. — Dose, 3 to 6 drops. OILS (Fixed). Syn. Fat oils. Unctuous o. ; Olea rixA, 0. expeessa, L. ; HuiLES geasses, Fr. The fixed oils are compounds of carbon, hydrogen, aud oxygen (oxyhydro-car- bons), obtained from the organic kingdom, and characterised by their insipidity, unctu- o.^ity, insolubility in water, and being lighter than that fluid. Olive oil, which is obtained from the vegetable kingdom, and spermaceti oil, which is obtained from the animal king- dom, may be taken as types of the rest. The fixed oils are chiefiy found in the fruit and seeds of plants, and in thin membranous cells, forming what is called the adipose tissue, 71 1122 OILS (FIXED) in the bodies of animals. According to their consistence, they may be classed into ' OILS,' ' BUTTEES,' and • TALLOWS.' Prop., Sfo. Among the best-known proper- ties of the fixed oils are — the permanent stain they give to paper, which they render trans- lucid; their non-TOlatility at the ordinary temperature of the atmosphere, or at that of boiling water, or, indeed, at any temperature insufficient for their decomposition j their con- stantly floating on the surface of water when added to it ; and, lastly, their inability to mix with that fluid. Some of them, as palm oil and cocoa-nut oil, are solid at ordinary tem- peratures; but the majority are fluid, unless they have been considerably cooled, when they separate into two portions — the one solid, consisting chiefly of stearin, or some analogous substance, and the other liquid, consisting chiefly of oleiu or elain. Nearly all of them, when exposed to the air,absorb oxygen rapidly, and either gradually harden or become rancid and nauseous. Prom the first are selected the ' drying oil ' used by painters ; the last are used as food, in cookery, and for machinery, lamps, &c. The whole of these oils, when heated to their boiling points (500° to 600° Fahr.), sufier decomposition, yielding various hydrocarbons; and when suddenly exposed to a red heat, tliey furnish a gaseous product (oil-gas), which was formerly employed for illumination. It is owing to this property of oil and liquid fats that candles and lamps give their light. The wick is a gas-producing apparatus in miniature. With the caustic alkalies and water the fixed oils unite to form soap. When some of these oils are absorbed by porous bodies, and thus expose a vastly in- creased surface to the air, they absorb oxygen with such rapidity as to generate a consider- able degree of heat. Paper, tow, cotton, wool, straw, shavings, &c., slightly embued with oil, and left in a heap, freely exposed to the air or sun, often spontaneously inflame. In this way many extensive fires have arisen. The above is more particularly the case with linseed, rape, nut, and olive oil. The first, made into a paste with manganese, rapidly becomes hot, and ultimately inflames spon- taneously. The specific gravities of the fixed oils range between -865 and -970, water being 1-000. Prep. The fixed oils, except where other- wise directed, are obtained from the bruised or ground fruit or seed, by means of powerful pressure, in screw or hydraulic presses, and are then either allowed to clarify themselves by subsidence or are flltered. Both methods are frequently applied to the same oil. In some cases the impurities, are removed by ebullition with water, and subsequent sepa- ration of the pure oil. Heat is frequently employed to increase the liquidity of the oil, and thus lessen the difficulty of its expulsion from the mass. With this object the bruised mass, placed in bags, is commonly exposed to the heat of steam, and then pressed between heated plates of metal. This is always neces- sary with the ' butyraceous oils.' Another method is by bailing the bruised seed in water, and skimming ofE the oil as it rises to the surface. This is the plan adopted for castor oil in the West Indies. In a few cases, for medicinal purposes, the bruised mass is mixed with i its weight, or an equal weight, of alcohol or ether, and after 24 hours' digestion the whole is submitted to • pressure, and the alcohol or ether removed by distillation at a gentle heat. The first men- struum is commonly employed for croton oil on the Continent; the second, for that of ergot of rye. Pwrif. Several methods are adopted for refining or purifying the fixed oils, among which are the following : — 1. The oil is violently agitated along with li to 2§of concentrated sulphuric acid, when it assumes a greenish colour, and, after about a fortnight's repose, deposits much colouring matter, becomes paler, and burns with greater brilliancy, particularly if well washed with steam or hot water,and clarified by subsequent repose or by filtration. This answers well for most of the recently expressed vegetable oils. It also greatly improves most of the fish oils. 2. A modification of the last method is to well MUX the acid with the oil, then to blow steniii through the mixture for some time, and afterwards to otherwise proceed as before. 3. Fish oil (whale, seal, &c.) is purified by— a. Violently agitating it with boiling water or steam, by placing it in a deep vessel with perforated bottom, through which high pres- sure steam is forced for some time ; it is after- wards clarified by repose, and filtered through coarse charcoal. i. The oil is violently agitated with a boil- ing hot and strong solution of oak bark, to remove albumen and gelatin, and next with high-pressure steam and hot water; it is, lastly, dried and filtered. I c. The oil, gently heated, is stirred for some time with about 1 § of good chloride of lime, previously made into a milk by tritura- tion with water ; about 1 J ^ of oil of vitriol, diluted with 20 times its weight of water, is then added, and the agitation renewed and maintained for at least 2 hours ; it is, lastly, well washed with steam or hot water. d. Mr Davidson treats the oil first with a strong solution of tan, next with water 'and chloride of lime, then with dilute sulphuric acid, and lastly, with hot water. c. Mr Dunn's method, which is very effec- tive, and admirable ouaccount of its simplicity, is to heat the oil by steam to from 180° to 200° Fahr., and then to force a current of air of corresponding temperature through it, under a flue or chimney, until it is sufliciently OILS (FIXED) birached and deodorised ; it is, lastly, either at once llltcrod i>r is previoasly washed with •team or hot wuter. /. Another method, formerly very generally adopted iind still in use, is to violently agitate the oil for some time with very strong brine, or with a mixed solution of blue vitriol and common salt, and then either to allow it to clarify by repose or to filter it through freshly burnt charcoal. 4. AlUOND, CA8T0B. LINSEED, NUT, OLtVE, RIPE, and some other vegetable oils, are readily bleached by either of the following processes : — a. KipoBure in glass bottles to the sun's rays, on the leads or roofs of houses, or in any other suitable position, open to the south- east and south. This is the method employed by druggists and oilmen to whiten tlieir castor iirid linseed oils. 14 to 21 days' exposure to tlie sun in clear weather during summer is usually sufficient for castor oil when contained in )i to 4-qiiart pale green glass bottles (pre- (erably the former), and covered with white gallipots inverted over tliem. The oil is fil- tered before exposing it to the light, as, if only in a slight degree opaque, it does not bleach well. Almond and olive oil are, when thus treated, apt to acquire a slight sulphur- ous smell ; but this may be removed by fil- tration through a little animal charcoal, or, still better, by washing the oil with hot water. A. Another method employed to decolour these oils is to heat them in a wooden, tinned, or WL'll-glazed earthen vessel along with some dry 'filtering powder ' (1 to 2 lbs. per gall.), with agitation for some tims, and lastly, to filter them in the usual manner throu,'h an oil-bag. In this way the West-end perfumers prepare their ' white almond oil ' (oleum AMYODALa; AiBUM), and their ' white olive oil' (oLECM OLIV.E ALBUM). Formerly, freshly burnt animal charcoal was used for this purpose, and is still so employed by some houses. 5. Mr Bancroft refines OILS FOE MACni- NBBT AND LITBSIOATINO PURPOSES i,'euerally, by asritatint; them with a lye of caustic soda of the sp. gr. 1'2. A sufficient quantity is known to have been added when, after re- pose, a portion begins to settle down clear at the bottom. About 4 g to 8 J is commonly required for lard oil and olive oil. After 21 hours' repose the clear supernatant oil is decanted frum the soapy sediment, and fil- tered. 6. Not only the oils above referred to, but all other oils and fats, may be rendered per- fectly coluurless by the use of a little chromic acid ; or, what is the same, by a mixture of a solution of bichromate of potassa and sufli- cieiit sulphuric, hydrochloric, or nitric acid, to seiie on pII the alkali, ami thus liberate the chromic aeid. 7. Palm oil and Cocoa-hut oiw are gcue- 1123 rally refined and bleached by either chromic acid or chlorine, or by heat : — a. The 'butyraceousoil ' is liquefied by beat in a wooden vessel, and 7g to 9^ of good chlo- ride of lime, previously made into a smooth cream with water, is added, and the whole assiduously stirred until the ingredients appear united ; the mixture is then allowed to cool, and is next cut up into small lumps, which are exposed to a free current of air for 2, 3, or even 4 weeks ; these are melted in a wooden vessel heated by high-pressure steam circulat- ing through leaden pipes, or in a cast-iron boiler lined with lead, and an equal weight of oil of vitriol (diluted with about 20 times its weight of water) is poured in, and the whole gently boiled until the oil is discoloured and runs clear ; the fire is then moderated, and the whole allowed to settle ; lastly, the fire is removed, and the oil is left to cool very slowly. b. The process with chromic acid has been already noticed, but is more fully explained below. c. The oil, heated to the temperature of about 250° Fahr., is exposed to the action of hish-pres-iure steam, which is continuously ' blown ' through it for 10 or 12 hoiixs, or even longer, 'fhe process is greatly facili- tated by the introduction of some chromic acid. S. Mr Watt's inethods of purifying fats and oils are very effective, more especially for those intended f >r lllumiiiatiou. Tiicy are as follows: — a. (For FISH oils.) Each ton is boiled for i an hour with caustic soda, i lb., previously made into a weak lye with water ; or steam is blown through the mixture for a like period; oil of vitriol, i lb., diluted with 6 times its weight of water, is next added, the whole again boiled for 15 minutes, and allowed to settle for an hour ur longer, when the clear oil is run off from the water and sediment into the bleaching tubs; here solution of bi- chromate of potash, 4 lbs., in oil of vitriol, 2 lbs., previously diluted with water, q. s., together with a little nitric acid and some oxalic acid, are added, and after thorough admixture of the whole, by blowing steam through it, strong nitric acid, 1 lb., diluted with water, 1 quart, is poured in, and the boiling continued for i an hour longer ; a small quantity of naphtha or rectified spirit of turpentine is then mixed in, and the oil is, finally, well washed with hot water, and left to settle. b. (For PALM OIL.) The oil is melted by the heat of ste im, and, after it has settled and cooled down to about 130° Fahr., is carefully decanted from the water and sediment into the steaming tubs ; here a mixture of a satu- rated solution of bichromate of potash, 25 lbs., and oil of vitriol, 8 or 9 lbs., is added, and after thorough admixture, hydrochloric acid, 50 lbs., is poured in ; the whole is then constantly stirred until it acquires a uniform greenish 1124 OILS (FIXED) colour, or is sufficiently decoloured, a little more of the bleaching materials being added if the latter is not the case, after which it is allowed to repose for half an hour to settle ; it is next run into a wooden vat, where it is washed, &c., as before. c. (For TEOEXABLE OILS.) These are treated with a solution of chromic acid, or with a solution of bichromate of potassa, or some mineral acid, as noticed at No. 6. For colza, MNSBED, MUSTAKD, NUT, and BAPE Olt, a little hydrochloric acid is added; but for ALMOND, CASTOB, OLITE OIL, and POPPY OIL, no such addition (at least in excess) is re- quired. 9. Bancid oils and pats are recovered by boiling them for about 15 minutes with a little water aud calcined magnesia ; or, by filtering tliem through freshly burnt charcoal. In reference to the above processes, it may be useful to remark, that chlorine, the com- mon bleacher and deodoriser of other sub- stances, cannot be well employed directly in tlje purification of oils, as certain chemical re- actions occur when these substances are brought together, which increiise the colour instead of removing it, and are often otherwise injurious. The same remaiks apply to the use of the * chlorides,' which frequently fails in unskilful hands, and is, indeed, of questionable utility, except, perhaps, in the case of palm oil. Even charcoal exerts little of its usual energy on the oils, and whilst it removes or lessens their offensive odour, sometimes increases their co- lour. The addition of 1§ or 2g of very pure and recently rectified naphtha or oil of tur- pentine (camphine) to lamp oil is a real im- provement, since it increases its combustibility and its illuminative power. Oils pok medical pdkposes, as castoh oil, COD-LIVBB OIL, &c., must not be subjected to any process beyond mere clarification by sub- sidence, filtration through Canton flannel or porous paper, or, at the utmost, washing with warm water, as otherwise their active and valuable properties, if not wholly removed, will be considerably lessened. See FlLlBA- TION. Furity. The fixed oils vary greatly in their value, aud hence the constant inducement which leads the unprincipled dealer to adulte- rate the more expensive ones with those of a similar character, but of an inferior kind of grade. Various methods are adopted to de- tect these frauds, among which the following are the most valuable of those capable of general application. Others referring to indi- vidual oils will be found under the respective heads. 1. (From the odour.) The method of ap- plying this test is to heat a few drops of the oil under examination in a small porcelain, platinum, or silver spoon or capsule (a watch- glass answers well), and to carefully compare the odour evolved with that arising from a known pure sample of the same kind and quality of the oil similarly treated. The odour of the two, when each is pure, is precisely alike, and immediately suggests the plant or animal from which it has been obtained. The presence of linseed, kut, bape, seal, TEAIN, or WHALE OIL, is thus readily detected, and the imperfections of the sample, even if pure, rendered much more perceptible. 2. (From the density.) — a. According to M. Penot, every oil supposed to come from the same plant, or the same animal, has its own particular density, which, at the same tempe- rature, never deviates more than a few thou- sandths. To apply this test, the relative den- sity or specific gravity of the sample must be determined. This may be done by means of a thousand-grain bottle or an ordinary 'aeeo- METEB ;' or, more conveniently, by an ' elaio- meteb' or ' OLEOMETEE,' constructed and gra- duated for the purpose. ' Tiseher's elaiome- teb' or 'OIL-BALANCE' is much employed on the Continent for this purpose, and is a very useful instrument. On the large scale, the weight of an accurately measured imperial gallon of the oil may be taken. i. M. Lauret, an eminent Pari-iau chemist, a short time since observed that the variations of the density of an oil from adulteration are rendered much more apparent when it is ex- amined in a heated state. To render this dis- covery practically available, he plunges an ' elaiometer,' graduated for the given tempera- ture, into a small tin cylinder nearly filled with the oil, and then places this in a vessel contain- ing boiling water j as soon as the whole has acquired a uniform temperature, he observes the point on the scale of the instrument at which it fioats. This point for — Colza oil is . . . . 0° Fish oil 83° Poppy oil ... . 124° Hemp-seed oil , ... 136° Linseed oil . . . . 210° u. By employing a specific gravity bottle or small glass globe, fitted with a stopper in which is hermetically fixed a capillary tube of atiout 8 or 9 inches in length, we may apply the above principle of M. Lauret with the greatest accuracy. This little apparatus is filled with the oil, and then immersed in boiling water for a sufliclent length of time for it to acquire that temperature; it is then removed and weighed. The smallest adulteration is, it is said, in this way immediately detected. When the density of the given sample has been taken, and the name of the oil used to adulterate it is known, the quantity of the latterpresentmaybe approximately determined from the specific gravities by the common method of alligation.* 3. (Sulphuric-acid test.) — a. Heidenreich was the first person who gave a useful and general application to the reactions which occur when oil of vitriol is mixed with the fatty oils. As soon as these substances are placed toge- ' See MiXTUBGs, Antliiuetic of. ther, very interne chemical action cominenoes, tlie temperature of the mixture rises, and the inaM becomes coloured. These changes are sufficiently varied in the case of the different oils to lurnish us with the means of identifying many of them, and of determining their pu- rity. Tlie method of M. Ueldenrelch is to lay a plate of white glass over a sheet of white paper ; on the glass he places 10 or 15 drups of oil, and then adds to it a small drop of con- centrated sulphuric acid (' oil of vitriol'). The appearances which follow dilfer with the cha- racter of the fatty oil examined, and whether the acid is allowed to act on the oil unilis- turhed (without stirring) or the two are stirred together with a glass rod. In many cases, as with tallow oil, a peculiar odour as well as a change of colour is developed, Rnd a farther means of detection supplied. M. Heideureich bus minutely described these reactions, which, for the most part, closely resemble those given in the table, p. 1129. It is necessary, however, in order to ensure great accuracy, to compare the effect of the reagent on the sample with those which it produces on pure oil of the same kind and character under precisely similar circumstances. OILS (FIXED) 1125 b. M. Penot, who has followed up the re- searches of M. Hoidenreich with considerable success, recommends the employment of 20 drops of oil, instead of only 10 or 15 ; and the use of a small capsule of white porcelain, in- stead of a plate of glass, fie also employs a saturated solution of bichromate of potash in sulphuric acid, which be uses in the same pro- portion as before ; but in this case the oil and the reagent are always stirred together. The observations of M. Penot have been repeated in many cases by Mr Cooley, and the results, with additions, and rearranged, are given in the table, p. 1129. " By perusing this tnble," writes M. Penot, " it will be observed that the same oil does not, under all circumstances, yield precisely similar results with the same reagent. This depends on the place of growth, the age, and the man- ner of pressing. If, however, any oil be ex- amined comparatively with a perfectly pure one, the proof of adulteration may be ren- dered, if not certain, at least probable, by noting the difference. Thus I obtained, by adding 1 part of either whale- train, or linseed oil, or oleic acid, or 10 parts of rapeseed oil, the following results: — Naur of Oil, Rkaoknts. Sulphuric Acid. Solution of Qichruiiiuteor Potaali. Not stirred. Stirred. Stirr^ 5 .5 5 B .9 ='.S .5'.9 .S "^ .S ^ * -S "^ ■e>|'|'"& ^■E''E'|'|''&-| |"i -i &" ti 6i sil 60 si' a e B e B cs a a a c .SJ e .2 .2 s ■?>■ ooooo- Iz; |2i ;zi ^ IZi >">>.£ ■?>■>. a Sio^ .5 ^ . . S.5 60 bDji OB a B^ ». 5 § § § § 5 S S S -C S -S •= 5 ST C C-n !? C 5 p r 5 "C .§=■5 5, tJ ^ c* s W0SN00t"'mi-IinOCCia>Q0>Oe0C0M0500'*t>"«"M rHrHiHr-t-*^rHiHrHi-t iHrHr-HrHrHtH rH *^*' 00 CO « o 00 tr- "^ CO o eg 9 = Iziiz; ^ So s M S to p< >> >> B J< CJ © o © © © s C S P fl 9 S a 6 W) o ^ d;zi ^5> 03 >■ 'o u,= r-( iH lMiHi-lr-li-liHi-li-(i-l(MrHOCO(M«^"^»niHCD„«^ CDCO-^-*(MtMCClfl-^COiO-*Tj(»ncOCO>#m-<# OO-? rH t^ CO "^ CD ^ ^Q0CD0i(MC0OCDOI>e5i0iHQ e^ P 12 rt .S O J3 V 0) o • rt • » « S • cSCQOoatCOFQPLiiJlllCLioSoaWOtB s CD a '►5^1 OILS (FIXED) 1129 Tablb giving the reactions of various OTLS with siTtPHtrsio acid and with a saturated solution of BIOHitOMATB OP POTASH in sulphuric ocid. Re-arranged from M. Penot's table, with additions, by Mr Cooley. *fi* The result indicated is obtained in each case hy the action of one drop of the BBAOEKT on twenty drops of OIL. Nauk or Oil. Almond oil . Castor oil . . . Cod-liver oil {fine tample of pale oil) Hemp-seed oil Linseed oil {from the Upper Rkine) n {from Paris) „ ( EngUsk) . Liver-train oil . MudiB-BUtiva oil Black-mustftrd oil . XeatVfuotoil Nut oil {recent) I, {oHs year old ) . „ (still older) Olein, ok'ic ucid, Inrd, or tallow oil . Olive oil . . . . „ {another sample) » {from fermented olives) Poppy oil {recent cold drawn) „ {recent, ex- pressed witli sliglit Ileal) . „ {one year old, expressed with Asat) Rape or colza oil (trade) . M {recent) . „ (one year old) „ (oHi year old, rough hoi-pressed) Wbale-train oil Ekagkrts. Sulphuric Acid. Not stirred. Gffenflnch yellov, with oruDge spots Ycltow, K'ith slight spots Deep purple in the centre, rapidly turning bruwn, whilst viuli^t or purple clouds or streaks sprcHd out tovs-ards the circum- ference, the colour of which remains unaltered for some minutes after the central portion has turned nearly black Small bruwn lumps or clots ou a yellow ground Dark reddish brown Eeddisli brown, less dark coloured Chestn.it brown Dark red Sliglitly reddish brown un- derneath a thin greyish film Bliiisli green Yellow alight spots Yellowish brown Yellow Orange yellow Reddish spots, witli red- dish circlua Yellow Ortmge yellow Orange yellow Yellow spots Greenish-yellow spots Greenish spots Yellowish -brown streaks surrounded by a bluish- green ring Green Green Qreen Small reddish Inmps on a brownish grouud Stirred, Dirty green Little reaction Deep purple, passing into purple brown, reddish brown, and gradually deepeuing to au in- tense brown, approach- ing btack Greenish brown Brown small lamps on a grey ground Brown clots on a greea ground BroH-n clots on a greenish- grey ground Dark rtd. Olive grtien Olive ercen Dirty orown Clotted, dark brown Dirty bruwn, less dark Coloured Dirty brown Reddish brown Dirty brown. Bruwuiflh grey Brownish grey Olive brown Olive brown, turning more on the ((reen Olive green « Brownish, turning on the olive green Bluish green Bluish green Olive green Resembles wine leeg .SHturated Solution of Bichromate of Polaasa in Sulphuric Acid. Stirred. Tellowish, small lumps. Slightly green Reddish - brown clntg, ctmntiint; to a clear bright greeu. Smnll yellow lumps or clots on a green grouud. Brown smHll lumps on an almost colourless ground. Brown small lumps on a green ground. Brown lumps ou a green- ish-grey ground. Dark red. Light l)rown small lumps on au olive-cnloured ground. Olive brown. Blown spots ou a brown- ish ground. Small brown lumps or clots. Small brown lumps. Small brownish lumps. Bright chestnut colour. Olive brown. Brown. Small yellnw lumps on a white grouud. Small yellow lumps on a greeiiisli-grey ground. Sm^ll yellow lumps on a green ground. Yellow small lumps on a green ground. Yellow small lumps on a green ground. Yellow lumps on a brighter grcon ground. Sin;i 1 yt-lt.iw lumps, more numeious, on an ohve- green ground. Small, briiht, chestnut- coloured lumps on a brown ground. 1130 OILS (FIXED) nuts, gently heated over the fire, and then de- corticated, and pressed between hot iron plates. Sp. gr. -892. Oil, Cas'tor. St/n. EiciNi oleum (B. P.), Oleitm castoeei, 0. kicini (Ph. L., E., & D.), L. " The oil prepared by heat, or by pres- sure, from the seed" of " Micinis communis, Linn." (Ph. L.), the Palma Christi, or Mexican oil-bush. The best oiistor oil (ooLD-DBAWN oastoe OIL ; olbum: bicini sine i&ne) is prepared by pressing the shelled and crushed fruit (seed) in hemp bags, in an hydraulic press, and heating the oil thus obtained along with water in well tinned vessels, until the water boils and the albumen and gum separate as a scum ; this is carefully removed, and the oil as soon as it has become cold is filtered through Canton flannel, and put into canisters. The commoner kinds are prepared by gently heating the crushed seeds, and pressing them whilst hot. Another method, sometimes adopted, is to put the crushed seed into loose bags, to boil these in water, and to skim off the floating oil. Prop. It is the most viscid of all the fixed oils; when pure it mixes in all proportions with alcohol and ether, and also dissolves, to a certain extent, in rectified spirit, but a portion of the oil separates on standing. Camphor and benzoic acid increase its solubility in spirit. By long exposure to the air it be- comes rancid, thick, and is ultimately trans- formed into a transparent yellow mass ; light liastens tliese changes. Exposed to cold, a solid, white crystalline fat separates from the liquid portion, and when cooled to 0° it con- geals into a yellow transparent mass, which does not again liquefy until the temperature rises to about 18° Fahr. Sp. gr. -9611 to •9612, at 60°; -9690, at 55° (Saussure) ; •9575, at 77° (Saussure). Frod. 38g to 40§ (62a-Ure). Pur. Castor oil is sometimes adulterated with rape oil or with lard oil, a fraud which may be detected by its diminished density ; and, when the added oil exceeds 33§, by its insolubility in its own weight of alcohol of •820. In many cases crotou oil is added to increase the purgative quality of the mixture. A compound of this kind is vended in gela- tine capsules under the name of * concen- trated CASTOa OIL,' the use of which is fraught with danger. " I have heard of several cases in which very violent a^d dangerous effects were produced by these capsules." (Pereira.) The best is imported from the East Indies in tin canisters. The oil obtained from the seeds of Uiciims viridis (WiUd.), or lamp-oil seeds, is often mixed with or sold for castor oil. Uses, Sfc. Castor oil is an exceedingly useful mild purgative, particularly when abdominal irritation should be avoided, as in inflamma- tions of the stomach and bowels, pregnancy, surgical operations, &e. — Dose, 2 fl. dr. to 1 fl. oz. Oil, Cocoa-nut. Si/n. Coooa-nft BtriTEoj Oleum cooois nuoifbe«, L. By expression from the kernels of the cocoa nut, or fruit of the Cocos Muoifera, Oil, Cod-liver. Si/n. MoBEHUa: oleum (B. P.), Cod-pish oil; Oleum jecoeis aselli, 0. aADi, 0. a. MOBBHua;, Oleum mobbhu^e (Ph. L.), L. "The oil extracted from the fresh liver of the Gadus morrhua by a steam heat or water bath not exceeding 180° Fahr. Yellow," " The oil prepared from the liver of &adus morrhua, Linn." (Ph. L.^ The common cod-liver oil of commerce drains from the livers of the cod-fish when freely ex- posed to the sun, and just beginning to putrefy. It is dark coloured, strong, and nauseous, and is now chiefly employed in this country by the curriers, for dressing leather. It is the 'OLEUM JECOEIS ASELLI PUSOOM ' of Conti- nental writers. Formerly, the less fetid varieties of this crude oil, after the impurities were removed, either by subsidence or filtra- tion, constituted the only cod-liver oil used in medicine. As its employment as a remedy increased, its revolting flavour, and its great tendency to permanently disorder the stomach and bowels, was found, however, to be a serious obstacle to its general use. It was observed that the oil as it exists in the liver of the cod is bland and nearly colourless, and has only a slight fishy, but not a disagreeable flavour. The attention of persons interested was there- fore immediately directed to the subject, and improved methods of obtaining the oil were suggested, and ere long adopted on the large scale. The methods of preparing cod-liver oil are noticed in another part of this work, but we think it advisable to add to these a description of the plan adopted by Messrs Charles Pox and Co., of Newfoundland, Scarborough, and London, the well-known manufacturers and importers of cod-liver oil : — " The Newfoundland fisheries are entirely carried on in small boats, principally by the hand-line system, and quite close to the shore. The boats go out early in the morning, and return about four o'clock in the afternoon. The fish, on landing, are handed over to a ' fish-room keeper,' whose duty it is to split and open the fish, and to deposit the livers in small tubs holding 17 or 18 gallons each. The tubs are soon afterwards collected from the different * fish-rooms,' and conveyed to the manufactory. The livers are here thrown into tubs filled with clean cold water, and, after being well washed and jerked over, are placed on galvanised iron-wire sieves to drain. They are next put into covered steam-jacket-pans, and submitted to a gentle heat for about three quarters of an hour, after which the steam is turned off, cold air again admitted, and the whole allowed to repose for a short time, during which the livers subside, and the oil separates and floats on the top. The oil is then skimmed off into tin vessels, and passed OILS (FIXED) 1131 through flannel strninera into tubs, where it is l«ft to subside for abnnt 21 hours. From these the purer upper portion of oil is run into a very deep, firnlvanized-iron cistern, and again left to clarify itself by defecation for a few days. It is now further refined by carefully passing it through clean and very stout mole-skin filters, under pressure. The transparent fil- tered oil is received in a clean, galvanised- iron cistern containing a pump, from which the casks are filled for exportation. The latter, before being filled, are carefully seasiined and cleaned, to prevent their im- parting cither flavour or colour to the pure oil." The suppriority of the oil prepared as above consists essentially in every part of the process of extraction being performed whilst the livers are fresh, and in no chemical means being adopted to give the oil a factitious appearance. Its natural pale colour is thus preserved from contamination, and its medicinal virtues main- tained intact. Much of the light brown oil of commerce is obtained from Oadui callarius (tlie dorse), O. carbonariut (the coal-fish), and &. pollaohiua the pollack). Fur., ^0. "The finest oil," remarks Dr Pereira, " is that which is most devoid of colour, odour, and flavour. The oil, as con- t;iined in the cells of the fresh liver, is nearly colourless, and the brownish colour possessed by ordinary cod-liver oil is due to colouring mutters derived from the decomposition (putre- fying) of hepatic tissues and fluids, or from the action of the air on the oil (age). Chemical analysis lends no support to the opinion, at one time entertained, that the brown oil was supe- rior, as a therapeutic agent, to the pale oil. Chemistry has not discovered any substance in the brown oil that would confer on it superior activity as a medicine. On the other hand, the disgusting odour and flavour and nau- seating qualities of the brown oil preclude its repeated use. Moreover, there is reason to suspect that, if patients could conquer their aversion to it, its free use, like that of other rancid and empyreumatio fats, would disturb the digestive functions, and be attended with injurious effects." ' Among the tests of purity, that generally relied on is known as the ' sulphuric acid test.' See Oils (Fixed) : Furity. Douse on and other fish oix, sold as 'lIOnT-DROWN COD-LITEB OIL,' exhibit with this test much lighter reactions, which closely resemble those of livek-tbain and whale- TBIIN OIL. To detect the presence of combined iodine, upon which, by some, the therapeutic value of cod-liver oil is thought to depend, the sample is saponified by trituration with a little caustic potassa 11 nd hot water, the result! n? soap cau- tiously incinerated, the ashes digested with water, Hnd the whole thrown on a filter. The ■ 'Klem. Mat. Med.,' &c., Srd edit., iii, S339. usual tests for iodine may be then applied to the filtered liquid. The presence of iodine artificially added is best detected by agitating the oil with a little rectified spirit, and then testing this last for iodine. Or, s little solution of starch and » few drops of sulphuric or nitric acid may be at once added to the oil, when a blue colour will be developed if iodine, or an iodide, has been mixed with the sample. The sp. pr. of the pale oil is -9230 to -9238; of the light-brown oil, •9240 to -9245 ; of the dark-brown oil, 9290 to -9315. The density is, however,apt to vary a little with the quantity of moisture present. Uset, ^c. Cod-liver oil is a most valuable medicine in a great variety of diseases, more especially in glandular indurations and en- largements, scrofula, phthisis, rheumatism, gout, certain cutaneous diseases, amenorrha^a, chlorosis, caries, rickets, &c. To be of service, however, its use must be continued lor several weeks, and the oil must be recent. — Dose, 1 to 2 table-spoonfuls, 3 or 4 times daily, or oftener. Oil, Col'za. From the seeds of Brastica cam- peatru, var. oleifera, or colza de printempt, n variety of Sratsica campestria (Linn.). It may be regiirilcd as a superior sort of rajie oil. Burns well in lamps, especially after being refined. Sp. gr. -9136. Frod. 393. The term ' colza oil ' is commonly applied to ordi- nary refined rape. Oil, Cotton. seed. Syn. OLEtru gossipii SEMINUM, L. From the seeds of Oossypium Barbadense. Drying. Oil, Croton. Sifn. Cbotonis oleum (B.P.), Oleum ceotonis (Ph. E.), 0. tiglii (Ph. L.), L. Prom the shelled seeds of Croton tiglium or Molucca grains. Imported chiefly from the East Indies. It is one of the most powerful cathartics known, and acts when either swal- lowed or merely placed in the mouth. Exter- nally, it is a rubefacient and counter-irritant, often causing a crop of painful pustules, like tartar emetic. — Voae, 1 to 2 drops, on sugar ; in apoplexy, &c. It is poisonous in larger doses. Sp. gr. -947 to -gSS- Frod. Un- ahelled seeds, 22% to 25? ; shelled do., 32g to 35&. Pure croton oil is soluble in an equal volume of alcoliol of •796, but in 2 or 3 days about 96§ of the oil separates. In France the marc is exhausted with alcohol, and the oil thus obtained is added to that previously obtained from the same seeds by expression. The East Indian oil (oleum cbotonis exoticum) is usually of a pale yellow; that pressed in England (o. ceotonis Anqlioanum) is much darker. Oil of Cu'cnmber Syn. Oleum cucuebit^, L. From the seeds of Cucurbita pepo or squash, and the C melopepo or pumpkin. Pale; used in lamps; and, sometimes, as a soothing application to piles. Sp. gr. '9231. Frod. 24g. 1132 OILS (FIXED) Oil of Eggs. Si/n. OiEiTM ovi, 0. o. vitelli, 0. OVOEUM, L. From the yolks of eggs, gently heated until they coagulate and the moisture has evaporated, and then pressed or broken up, digested in boiling rectiKed spirit, the tincture filtered whilst hot, and the spirit distilled off. Bland j emollient. The common plan is to fry the yolks hard ; but the oil is then darker coloured and stronger. The P. Cod. orders them to be exhausted with ether, by displacement. Formerly commonly used to 'kill ' quicksilver, and still held in great esteem in some parts of England for sore nip- ples and excoriations. Prod. 10 to 12 eggs yield 1 oz. See Mixed oils. Oil of Garden Cress. Si/n. Oleum lepidii SATivi, L. From the seed. Drying. Sp. gr. •9240. JProd. 54§. Oil of Gar'den Spurge. Syn. Oleum la- THYRIS, O. ECPH0EBI2E L., L. From the seeds of Euphorbia lathyris or garden spurge. Cathartic. — Dose, 3 to 8 drops. Sp. gr. -9281. Prod. 30g to 410. Croton oil mixed with 6 times its weight of nut or rape oil is usually sold for it. Oil of Gingel'ly. Syn. Oil oe Sesamum, Benhb oil, Tebl o., Tel o. ; Oleum sesami, L. From the seeds of Sesamum orientate (Willd.), or gingelly. Pale ; bland. Used in salads, paints, &c. ; also to adulterate oil of almonds. Prod. 46g. Oil, Gourd. See Oil op Cucumbee. Oil of Ground Nuts. From the nuts of Araehis hypogeea. Glutinous. Oil of Gurgun. See Balsam, Guegun. Oil of Hemp. Si/n. Oleum cannabis, L. Prom the seed of Cannabis sativa (Linn.), or common hemp. Mawkish. Sometimes used tor frying, but chiefly for paints, soaps, &o. Freely soluble in boiling alcohol ; does not thicken until cooled to 5° Fahr. Sp. gr. •9276. Prod. 182 to 24i. Oil of Jatro'pha. Syn. Oil op wilb castoe SEEDS; Oleum JATEOPHiE, L. From the seeds of Jairopha purgans. Somewhat re- sembles CEOTON OIL. Used for lamps in the East Indies. Oil, Kundah. Syn. Tallicoonah o. ; Oleum TOULOUCOUNjs, L. From the fruit of Carapa Touloucouna. Rancid, nauseous, vermifuge, rubefacient, emetic, and purgative. Chiefly used in lamps. Oil, lard. Syn. Tallow o., Ceude olein, C. OLEIC acid ; OlEUM ADiPis, L. By sepa- rating the olein of lard from the stearin by means of boiling alcohol. Only applicable where spirit is cheap. The product is, how- ever, excellent. The crude oleic acid, or lard oil of commerce, is chiefly obtained as a secon- dary product in the manufacture of stearin. It is purified by agitation with sulphuric acid, and subsequently by steaming it, or washing it with hot water. Burns well in lamps, if the wick-tube is kept cool. Sp. gr. ^9003. Oil, Linseed. Syn. Oleum lini (B. P., Ph. L., E. & D.), L. 1. (COLD-DEAWN LINSEED OIL; Oleum lini sine isne.) From the seed of Linum usitalisaimum (Linn.), or common flax, bruised or crushed, and then ground and ex- pressed without heat. Pale, insipid, viscous ; does not keep so well as the next. Prod. 17ij to 20g. 2. As the last, but employing a steam heat of about 200° Fahr. Amber coloured ; less viscous than the last; congeals at 2°; soluble in 5 parts of boiling and 40 parts of cold alcohol. Both are drying and cathartic. — Dose, 1 to 2 oz. J in piles, &c. Chiefly used in paints, varnishes, &c. Sp. gr. '9347. Prod. 22g to 27g. 3. (Boiled linseed oil.) See Oils (Dry- ing)- Oil of Mace (Expressed). See Oil op Nut- meg (Expressed). Oil of Male Fern. See Exieact of Male PEEN. Oil of Mustard. Syn. Oleum sinapis, L. 1. (Oil of white mustaed.) Prom Sinapis alba, or white mustard, but chiefly from Sinapis arvensis, S. chinensis, S. dichotoma, S. glauca, S. ramosa, and S. tori. Sweet. Used for the table. Sp. gr. -9142 (-2160— Ure). Prod. 36s. 2. (Oil of Black mustard; Oleum sina- pis nigei, L.) From the ' hulls' of black- mustard seed. Viscid, stimulant. Used in rheumatism, Sp. gr. '9168 to 9170. See Oils (Volatile). 3. (Oil op White mustaed ; Oleum ea- PHANi, L.) From the seed of Saphanns ra- phanistrum (Linn.), or jointed charlock or wild mustard. Prod. 30g. Oil, Neat's-foot. Syn. Nkeye oil, Thot- TEE o. ; Oleum bubulum, 0. neevinum, Axungia pedum tauei, L. From neat's-feet and tripe, by boiling them in water, and skim- ming ofE the oil. Does not thicken by age. Used to soften leather, to clean fire-arms, and for other purposes. Oil, But. Syn. Hazel-nut o. ; Oleum NUCis, 0. coeyli, L. From the kernels of Corylus Avellana (Linn.), or hazel-nut tree. Pale, mild tasted, drying ; superior to linseed oil for paints and varnishes. It is commonly sold for oil of almonds and oil of ben, and is extensively employed to adulterate both. Walnut oil is also frequently sold ibr nut oil. Sp. gr. •9260. Prod. 63g (Ure). Oil of Nut'meg (Expressed). Syn. Ex- PEESSBD OIL OF MACE, BuTTEE OP M. ; Oleum myeistic^ (conceetum) (Ph. L.), MYEISTICiE ADEPS (Ph. E.), M. BUIYEUM, 0. MYEIBTICiE EXPEESSUM (B. P.), 0. MOSCHATiE. O. NDOIST*;, L. " The concrete oil expressed from the seed of Myristioa officinalis," Linn. (Ph. L.), or common nutmeg. The nutmegs are beaten to a paste, enclosed in a bag^ ex- posed to the vapour of hot water, and then pressed between heated iron plates. Orange colimred, fragrant, spicy ; butyraceous, or solid. It is a mixture of the fixed and volatile oils of the nutmeg. When discoloured and OILS (FIXED) 1133 burdened by age, it i» called 'Bahda soap* (Oc. MACis IN UA88J8). When puri>, it is soluble in 4 parts of boiling alcohol and in 2 parU of ether. It has been used in rhea- matism and paUy, but is now chiefly employed for its odour and aromatic qualities. From tlie East Indies. Prod. 17-g to 20J. Oil, Ol'ive. Syn. Salad oil, Sweet o. ; Ouy« OLEUM (H. P.), Oleum olivaeum, 0. OLiviE (Ph. L., E., & I).), L. The " oil ex- pressed from the fruit " of " Olea europcea, Linn." (Ph. L.), or common olive. Five dif- ferent methods are employed to obtain the oil, from the fruit : 1. (VlEOIN OIL ; O. O. TIBOINEITM L.) ; Hnim viEEGB, Fr.) From olives, carefully garbled, cither spontaneously or only by slight pressure, in the cold. That yielded by the pericarp of the Iruit is the flnest. 2. (Ordinary 'JINE OIL.') This is obtained by either ijresfing the olives, previously crushed and mixed with boiling water, or liy pressing, at a gentle heat, the olives from which the virgin oil has been obtained. The above processes furnish the liner salad oils of commerce. The cake which is lelt is called ' GEIGNON.' 3. (Second quality.) By allowing the bruised fruit to ferment before pressing it. Yellow ; dnrlter than the preceding ; but mild and sweet tasted. Much used for the table. 4. (' GOEOON.') IJy fermentin)? and boiling the pressed cake or marc in water, and slum- ming off the oil. Inferior. 5. (Oil ot the infeenal bbgionb ; OiErw omphacinum) is a very inferior quality of oil, which is skimmed off the surface of the waier in the reeervoii'S into which the waste water which has been used in the above operations is received, and allowed to settle. The In-t two are chiefly used for lamps, and in so.ip- making, &c. Of tiie principal varieties of olive oil known in commerce, and distinguished by the place of their production, ■ PnovENOE oil' is the most esteemed j ' Floeence oil' and ' Lucca oil' are also of very fine quality; 'Genoa oil' comes next, and then ' Gallipoli oil,' which Ibrnis the mass of what is used in Enp:- landi 'Sicily oil,' which has a slightly re- sinous flavour, is very inferior; and ' Spanish oil' is the worst imported. Prop., Sfc. Olive oil is a nearlv inodorous, pale greenish-yellow, unctuous fluid, with a purely oleaginous taste, peculiarly grateful to the palate of those who relish oil. It does not suffer active decomposition at a heat not ex- ceeding I'OU' Fahr.j and when cooled to 36° it congeah into a granular solid mass. It is very siigbtly soluble in alcohol, but its solubility is increased by admixture with castor oil. It is soluble in IJ part of ether. When pure it has little tendency to become rancid. Sp. gr. ■9170 to -giTS; 0192, at 53^° (Saussure) ; ■9176, at 59' (Heidenreich) j and ^9109, at 77° F.ihr. (Saussure). Prod. 32?, of which 21g is furnished by the pericarp, and the remainder, which is inferior, by the seed and woody matter of the fruit. Pur. Olive oil, with the exception of that of almonds, being the most costly of the ordi- nary flxed oils of commerce, is, consequently, the one most subject to adulteration. Nut, poppy, rape, and lard oil, are those most commonly used for this purpose. Refined tallow olein, including that obtained from the 'knackers' yards' of Paris, is said to have been used in the same way. The addition of any other oil to olive oil renders it far less agreeable to the palate, and, by increasing its tendency to rancidity, much more likely to offend and derange the stomach and bowels of those who consume it. Parties who indulge themselves in the use of this luxury would, therefore, do well to ascertain that what they purchase is pure. When pure, and also fresh, olive oil is most wholesome as an article of food or as a condiment. The detection of the sophistication of salad oil is a matter of no great difficulty, The palate of the connoisseur will readily perceive the slightest variation in the quality of his favourite condiment. Other methods, however, of a more accurate and certain description, and of more general application, are adopted. Amongst these, in addition to those mentioned above, are the following : — a. When pure olive oil is shaken in a phial, only half filled, the ' bead ' or bubbles rapidly disappear ; but if the sample has been mi.xed with poppy or other oil, the bubbles continue longer before they burst. b. Olive oil congeals at 36° Fahr., and is completely solidified when a small bottle con- taining it is surrounded by ice, or a freezing mixture ; but when mixed with poppy oil, it remains partly liquid, even when the latter forms only l-4th of the mass; if more than l-3rd of poppy oil is present, it does not so- lidify at all, unless cooled much belov. the freezing point of wateix c. (Ph. E.) When olive oU is "carefully mixed with -f'^tb part of its volume ol a solu- tion of 4 oz. of mercury in 8 fl. oz. 6 dr. of nitric acid (sp. gr. I'SOO), it becomes in 3 Or 4 hours like a firm fat, without any separation of liquid oil." d. M. Pontet recommends the mercurial solution to be made by dissolving 6 parts of mercury in 7i parts of nitric acid (sp. gr. 1^35), without heat ; of this solution he adds 1 part to every 48 parts of the oil, and well shakes the mixture every 30 minutes, until it begins to solidify. This it does after about 7 hours in summer and 4 or 5 hours in winter, and when the oil is pure it will have fbimed, in 2:1 hours, a mass so hard that some little force must be employed to thrust a glass rod into it. The other edible oils do not furnish a hard mass with nitrate of mercury. The solidity of the mass is exactly in proportion to the quantity of foreign oil preseut. When 1134 OILS (FIXED) the sophistication is equal to l-8th of the whole, a distinct liquid layer separates ; when the mixture contains half its volume of an inferior oil, one half only of the mixture becomes solid, and the other half continues liquid. A temperature of about 90° Fahr. is the best to cause the oil and coagulum to separate perfectly from each other. When the oil has been adulterated with animal oil, the mixture solidifies in about five hours ; but in this case 'the coagulum consists of the animal oil, whilst the oliv^ oil floats on the surface, and may be decanted for further examination. This coagulum, on being heated, exhales the well-known odour of rancid fat or melted tallow. B. Dr Ramon Cordina Langlies states that the best reagent for the examination of olive oil is that of Hauchecorne. This reagent is composed of three parts of pnre nitric acid at 40° with one part of distilled water. The following is Dr Langlies' process for proving that olive oil does not contain seed oil, and more especially cotton oil : — He mixes three grammes of the oil to be tested with one gramme of the reagent in a test lube, or a small stoppered flask, and heats the liquid in a water bath. If the oil is pure the jnixture becomes clearer, and takes a yellow colour, like purified oil ; if it is adulterated with seed oil, it acquires the same transparency as the pure oil, but becomes red. With 5 per cent, of seed oil the reddish colouring is characteristic j with 10 per cent, it is decided. The reaction does not require more than from 15 to 20 minutes. The colouring of the oils lasts for three days. Uses, Sfc. The dietetical uses of olive oil are well known. In Spain and Italy it is com- monly employed as a substitute for butter. It is highly nutritious, but is digested with difiiculty by some persons, and hence should be avoided by the dyspeptic. Like almond oil, it is occasionally employed as a laxative and vermifuge, and is, perhaps, one of the mildest known, \npharmacy it is extensively employed in the preparation of cerates, lini- ments, ointments, and plasters.— jDose. For an adulf, i to 1 wine-glassful as a mild aperient; for an infant, J to 1 teaspoonful, mixed up with an equal quantity of honey, syrup of roses, or syrup of violets. The white fibrous sediment which forms in the recently expressed oil is the ' amueoa' of Pliny, and was formerly highly esteemed in medi- cine. Oil, Olive, Droppings. Syn. Swbet-oii d. The ' foots' or ' deposits,' and the ' drippings' of the casks, cisterns, and utensils. Used for machinery, making soap, &c. Oil, Olive (Oxygenated). Syn. Oleum oiiva) OTTOENATUM (Ph. Batav.), L. Olive oil, 16 oz., is placed in a receiver surrounded with ice or very cold water, and chlorine is slowly transmitted through it for several days, or until it becomes thick and viscid, after which it is well washed with warm warm. Oil, Palm. St/n. Palm butter; Oleum VAiMM, L. From the fruit ofElais Guineensis, and JS. melanocooca, the Guinea oil palms. Orange or red coloured ; butyraceous or solid ; smells of violets; unchanged by alkalies; bleached by sunlight, age, exposure, chlorine, chromic acid, and oil of vitriol ; melts at 117i° Fahr. Sp. gr. '968. Demulcent. Used to colour and scent ointments, pomades, &c. ; but chiefly to make soap and candles. From Africa. Oil, Pi"ney. Syn. Pinet tallow, P. dam- MAB, P. EESIN. Prom Valeria Indica (L\nn.), or paenoe tree. Resinous flavoured, fragrant ; made into candles. Sp. gr. -926. Oil, Pop'py. Syn. Oleum papatbeis, L. ; Oliete, Huile blanche, Fr. From the seeds of Papaver somniferum (Linn.), or white poppy. Sweet ; pale ; dries and keeps well. Used for salads, paints, and soaps ; also (extensively) to adulterate almond oil, for the inferior qualities of which it is frequently sold. It does not freeze until cooled to 0° Fahr. Sp. gr. -9243 to -9245. Prod. 48g to 54^. Oil of Pumpkin. Syn. Oleum cucuebit*;. Expressed from the seeds of the pumpkin ; a soothing application to piles. Oil, Rape. Syn. Colza oil, Beown o. ; Oleum eap^, L. From the seed of Braanica napus (Linn.; cole or rape), and from Brassiea campestris (Linn. ; wild navew or rape). Glu- tinous ; buttery at 25° Fahr. Dries slowly ; makes soft soaps and good ointments, but bad plasters ; smokes much in burning, un- less well refined. Sp. gr. -9135 to -9136 Prod. 32iJ. Oil, Repined or pale eapb (Oleum eap^ EEFINUM, Ol. e. album) is prepared from crude rape oil, by agitating it with about 2§ of oil of vitriol, previously diluted with about twice its weight of water, and, after 10 or 12 days' repose, decanting the clear oil, and fil- tering it through Canton flannel or felt. The quality is improved by washing it with hot water or steam before filtration. Used for lamps, blacking, and machinery; also exten- sively employed to adulterate both almond and olive oil. It forms the common * sweet oil' of the oilmen and druggists. Sp. gr, -9136 to •9140. Oil, Seal. Syn. Oleum PHOoa;, L. From the hood seal, and harp seal, and other species of PhocidcB. Pale seal oil is that which drains fi-om the blubber before putrefaction commences, and forms about 60g of the whole quantity of oil obtained. It is very clear, free from smell, and, when recently prepared, not unpleasant in its taste. Repined seal oil is the last, washed and filtered. Ranks close after sperm oil. Beown or dark seal oil is that which subsequently drains from the putrid mass. It is very strong-scented and nauseous, and smokes in burning. Both are used for lamps and dressing leather. A full- OILS (MEDICATED 1185 );rown seal yields 8 to 12 galls, of oil ; a small oDo, 4 to 6 ^kIIs. Oil of Ses'amnm. Sgn. Oil of Ginoellt {abort). OU, Shark-Uver. Tlie lightest of the fixed oils. Sp. gr. -865 to '867. Oil, Skate. 8gn. Olevu bal£, L. From the livers of Raia batit (Linn.), or common skate, as cod-liver oil ; also from Raia rhino- batu; »r whitn skate, and Raia clavala, or thornbnck. Often sold and mixed with cod- liver oil. Oil, Spermace'ti. Syn. Sfebu oil; Oleum CETAOBI, L. From the 'head matter' of JPhyeter macroeephalu», or spermaceti wliale ; u species once common in all the principal Kom, but now chiefly confined to the Southern Ocean. It is very limpid, smells little, and burns well; and has lon^ heen reputed the best oil for lamps and machinery, as it does not thicken by agi! or friction. It is frequently adulterated with refined seal oil. Sp. gr. ■875. Oil, Sun'flower. Syn. Olepm nELiAirrnr, L. From the seeds of Helianthua annuua and H. perennls. Clear, pale yellow, tasteless ; thickens at 60° Fahr. Used lor salads and lamps. Sp. gr. -9261. Prod. 15J. Oil, Teel. See Oil, Ginoellt. Oil, Tobao'co-seed. S/in. Oleum tabaci(bx- PBE38UH), L. From the seeds of NiooUana tabaoum (Liiin.), or true tobacco plant. Pale; dries well ; equal to nut oil. Its production liaa recently been carried on with consiilerable succi'ss iu some parts of Kussia. Sp. gr. •9232. Oil of Touloucou'na. See Oil, Kundah. Oil, Train. See Oil, Whale. Oil, Wal'nut. Syn. Oleum juglandis, 0. KUCI9 J., L. Prom the kernels of the nuts of Juglant regia (Linn. ), or cunimon walnut tree. Soon gets rank ; dries well. Used in paints, and ocoasioually in plasters. When 'cold drawn' and washed it is sometimes eaten with ealaJ. Sp. gr. -9260 to 9202. Prod. 48g to 529. Oil of Wax. Syn. Uutteb op wax; Oleum ceb£, L. From beeswax, by quick distillation in a close vessel. Butyraceous. Hv rectification along with quicklime it yields a liquid oil. Oil, Whale. Syn. Tkain oil, Whale-tbain 0.; Olkim DAL.kmji, O. Oeti, L. From the blubber of the £altena mysiicetus (Linn.), or the common or Qreeuland whale, by heat. Coarse; stinking. Southeun whale oil is the best. Used for lainp^, machinery, &c. Sp. gr. '9231. Prod, per fish, about 1^ ton for each foot of bone. Oil of Wheat. Syn. Oleum tbitioi, L. From bruised Colne wheat, with heat. In chilblains, ringworm, and several other skin diseases. Oil of Wine-stones. Syn. Geape-stone oil ; Oleum vitis vinifekj; lapidum, L. From the secdi of grapes, separated Irom the marc. Pale yellow, bland, emollient. Used for salads and lamps. Sp. gr. -9202. Prod. 14& to 18g. •«• The numbers given above, under • pro- ducts,' unless when otherwise stated, refer to the respective fruits, kernels, nuts, seeds, &c., deprived of their husks, pods, shells, and every other portion destitute of oil. OILS (Medicated). Syn. Olea cocta, O. INPUSA, O. MEDIOATA, L. These are prepared by infusion or decoction. The bruised ingre- dients are either simply digested in 2 to 4 times their weight of olive oil for some days, or they are gently boiled in it until they be- come dry and crisp, great care being taken that the heat towards the end of the process is not greater than that of boiling water. As soon as the process is complete, the oil is al- lowed to drain from the ingredients, which are then (if necessary) submitted to the action of the press. The product is commonly run through flannel or a hair sieve whilst still warm, after which it is allowed to repose for a week or ten days, when the clear portion is decanted from the dregs. The green or recent plants are usually employed for this purpose, but, in many cases, the dried plants, riduoed to powder, and digested for 6 or 8 hours in the oil, at the heat of hot water, witli frequent agitation, yield a much more valuable product. They are nearly all employed as external appli- cations only. *»* The following are the most important preparations of this class : — Oil of Adder's Tongue. Syn. Oleum ophio OLOSSI, L. From the herb, as oil of bella- donna. A popular vulnerary. Oil of Ants. Syn. Oleum fobmioabum. Digest 4 oz. of ants in 16 o/,. (by weight) of olive oil with a gentle heat, and strain. Oil of Bal'sam Apple. Syn. Oleum balsa- MIN^. Prep. Balsam apple (deprived of seeds), 1 oz. ; oil of almonds, 4 oz. ; digest and strain. Oil of Belladon'na. Syn. Oleum bella- dokNjE (P. Cod.), L. Prep. From the fresh leaves, bruised, 1 part; olive oil, 4 parts; di- i;ested together at a gentle heat until the mois- tuie is evaporated; the oil is then strained off with pressure, and filtered. Oil of Cantha'rides. Syn. Oleum cantha- Bims, 0. CAKTHABIDIBUS, L. Prep. (P. Cod. 1839). From Spanish Hies (powdered), I part ; olive oil, 8 parts; as Oil of Belladonna. Sti- mulant and rubefacient. Used as a dressing to indolent sores, blisters, &c. ; and in dropsy, rheumatism, gout, &c.. Oil of the oil-beetle (Meloe prosearabaus — Linn.) is prepared in a similar manner. Oil of Cap'sicnm. Syn. Oleum capsici, L. Prep. (Dr Turnbull.) From powdered capsi- cum or Cayenne pepper, 4 oz., olive oil, 1 pint ; digested together for 6 hours, with heat, and strained. Stimulant; rubefacient in colic, cholera, &c. Oil of Cham'omile. Syn. Oleum asthe- 1136 OILS (MEDICATED) MiBis, Oi. CHAMa;MEi.i, L. From the dried flowers (rubbed to pieces), 1 part, olive oil, 8 parts; digested together, with heat, for 6 hours. Stimulant, emollient, and vermi- fuge. Oil of Col'ocyntli. Syn. Olehm: coioctn- THiEis, L. From the pulp, as Oil op Ohamo- MIIE. Diuretic. In dropsy, neuralgia, rheu- matism, worms, &o. Oil of Earth'worms. Syn. Oleum: iitiibei- COKUM. (E. Ph. 1744.) Washed earthworms, i lb. ; olive oil, li pint ; white wine, J pint. Boil gently till the wine is consumed, and press and strain. Oil of Elder-flowers. Syn. White oil oe BLDEB; Oleum sambuci album, O. bambu- CINUM (P. Cod.), L. Prep. From the flowers, as Oil op Chamomile. Emollient and discus- sive. Oil of Elder-leaves. Syn. Green oil, Gbeen OIL OF elder. Oil oe Swallows; Oleum VIEIDE, 0. SAMEUOI VIBIDE, L. Frep. 1. Green elder leaves, 1 lb. ; olive oil, 1 quart ; boil gently until the leaves are crisp, press out the oil, and again heat it till it turns green. 2. As before, but by maceration, at a heat under 212° Pahr. More odorous than the last. 3. Elder leaves, 1 cwt. ; linseed oil, 3 cwt. ; as No. 1. Obs. The last form is the one usually em- ployed on the large scale. It is generally coloured with verdigis, J lb. to the cwt., just before putting It into the casks, and whilst still warm ; as, without great skill and a very large quantity of leaves, the deep. green colour so much admired by the ignorant cannot be given to it. The oil is got from the leaves by allowing them to drain in the pan or boiler (with a cock at the bottom), kept well heated. Emollient; in great repute among the vulgar as a liniment, in a variety of affec- tions. Oil of Pen'ugreek. Syn. Oleum tcbnu- GB.ffiCI, L. Prep. (P. Cod.) From the seeds, as Oil op Canthaeides or of chamomile. Emollient and resolvent. Oil of rox'glove. Syn. Oleum dioitalis, L. Prep. (P. Cod.) From the fresh leaves, as Oil op Belladonna. Used as an applica- tion to chronic ulcers and indurations, painful swellings, &o. As usually met with, it is nearly inert. Oil of Garden Ifight'shade. Syn. Oleum SOLANI, L. Prep. (P. Cod.) From the leaves, as Oil op Belladonna. Anodyne and discus- sive. Oil of Garlic. Syn. Oleum allii inpusum, L. Prom garlic, as Oil op Belladonna. Used as a liniment in deafness, diarrhoea, infantile convulsions, palsy, rheumatism, &c. Oil, Green. Syn. Oleum tieidi, L. From bay leaves, origanum, rue, sea wormwood, and elder leaves, of each 2i oz. ; olive oil, 1 quart; as Oil op Elder. Detergent, stimulant, and resolvent. Green oil of elder is now usually sold for it. Oil of Hem'lock. Syn. Oleum cokit, L. Prep. (P. Cod.) As Oil op Belladonna. Anodyne and emollient; in painful ulcers, glandular tumours, &c. Oil of Hen'bane. Syn. Oleum hyosctami, L. Prep. (P. Cod.) As Oil op Belladonna. Used as the last, in various painful local affec- tions. Oil lodizeo, Marshall's. Syn. Oleum ioda- TUM. Frep. Oil of almonds, 15 parts ; iodine, 1 part. Triturate and digest till dissolved. Oil of Ju"niper (by Infusion). Syn. Oleum JUNIPEBI INPUSUM, L, From the crushed berries, as Oil op Belladonna. Diuretic and vulnerary ; in frictions, &c. Oil of lil'iea. Syn. Oleum lilioeum, L. From white lilies, 1 lb.; olive oil, 3 lbs. ; as Oil op Belladonna. Emollient; used to soften and ripen tumours, indurations, &c. Oil of Mel'ilot. Syn. Oleum meliloti, L. As the last, avoiding much heat. Emollient and resolvent. Oil of Mu'cilages. Syn. Oleum muoila- ginum, O. cum muoilaoihieus, L. Frep. 1. (Ph. L. 1746.) Marshmallow root, J lb. ; linseed and fenugreek seed, of each, bruised, 3 oz.; water, 1 quart; boil 1 hour, -add of olive oil, 2 quarts, and boil until the water is consumed. 2. Fenugreek seeds, 8 oz. ; linseed oil, 1 quart; infuse a week, and strain. Once a highly popular emollient application in various local affections. Oil of Mn'dar. Syn. Oleum mudaeis, L. From mudar bark (in coarse powder), 1 dr. ; warm olive oil, \ pint ; digest 24 hours and strain. Used as an application to cutaneous ulcers, the bites of venomous animals, &c., and as a friction in worms. Oil of 0"pinm. Syn, Anodyne oil. Opiated o. ; Oleum opiatum, L. Prep. Prom opium (in powder), 1 dr.; olive oil, 2i fl. oz. ; digest at a gentle heat, with frequent agitation, for 5 or 6 hours. The powder should be rubbed in a mortar with a few drops of the oil before adding the remainder. As a local anodyne. The above is the only reliable formula for this preparation. Others are extant, but whilst the products of several are much stronger, those from others have only l-5thor l-6th the strength. Oils, Ozonised. (Dr Thompson.) Syn. Oleo OZONAIA. Prep. Pass oxygen gas into the oil (cocoa nut, sunflower, cod-liver oil, &c.) until it will dissolve no more. Then expose for a considerable time in the direct rays of the sun. Used in phthisis. Oil of Pel'litory. Syn. Oli:um pteethbi, L. Prom bruised pellitory root, as oil op BELLADONNA. Used as the last. Oil of Black Pep'per (by Infusion). Syn. Oleum pipeeis inpusum, L. From black pepper, in coarse powder, as Oil op Capsicum. Stimulant and rubefacient ; in frictions. OILS (MINERAL) 1137 Oil of FoUon Oak. Si/n. Olsttu buois TOXIOODE.VDBI, L. Kroiii the leaves, as oil or BELLLDOKNA. Externally ; in paralysis. Oil of Bha'barb. Sya. Olkum bhei, L. From rhubarb (in powder), 1 part ; oil of al- monds, 8 parts ; digested together in a gentle heat for 4 hours, and strained, with expression. As an application to indolent ulcers, and as a friction over the abdomen in diarrhoea, Gjii^IIsIi cholera, &c., or as n laxative when the stomach will not hear medicine. Oil of Ro"8eB. Syn. Oleum bos.e, 0. bosa- CEUM, 0. a. INFOaUM, 0. nOSATUM, L. Frep. Kiom the fresh petals, pulled to pieces, crushed, and digested for 2 or 3 days in the sun, or a warm »itaatian, in 4 times their weight of olive oil, and then pressed ; the process being repeated with fresh roses. Ph. E. 1744 and Jr". Cod. are nearly similar. Almond, ben, or olive oil, coluured with ALKANET, and scented with attar of roses, is now almost universally sold tor it. Used for the hair. Oil of Ene. Syn. Olecm eut^ (iNrtJsnM), L. Prep. (P. Ciid.) From fresh rue, bruised, as Oil of chamomile. Reputed antispasmo- dic, emnienagogue, stimulant, and vermifuge. In frietiiin'*. Oil of St John's Wort. Syn. Oleom hy- PEUICI (Pil. L. 1746), 0. H. SIMPLEX, Bal- SAMUM u., L. From the flowers, 1 part j olive oil, 6 parts ; digested together until the oil is well coloured. Antispasmodic, stimulant, and resolvent. A mixture of equal parts of RAPB oil and qbeen eldeb oil is usually sold for it. Oil of Scam'mony. Syn. Olettm scam- MONii, 0. rouoANS, L. Frep. (Van Mons.) From scinnmony (in powder), 1 dr. ; hot oil of almonds, 3 fl. oz. ; triturate together until cold, and the next day decant the clear portion. — Vosa, i to 1 table-spoonful. Oil of Stramo"nium. Syn. Olevm sira- MONir, L. Prep. (P. Cod.) From the leaves of thorn apple or sli-amonium, as oil op bel- ladonna. Anodyne and dircussivc ; as an application to painful tumours, joints, &c. Oil of lobac'co (by Infusion). Syn. Oleum TABAor, O. T. INPDSUM, L. From fresh to- bacco leaves (bruised), like oil op chamo- mile. As an application in ringworm, irri- table ulcers, pediculi, &c. ; and as a friition in itch, neuralgia, painlul indurations, &c. It must be used with extreme caution, as it is poisonous. Oil of Tooth'wort. Syn. Olkum sqcamaei.*;, L. From the herb of Lathrtsa squamaria (Linn.), as Oil op St John's wobt. Astrin- t.'ent and vulnerary. This must not be con- tounded with another preparation sometimes called ' Oil op toothwokt ' (Oleum plum- BAOINIS £cB0F^^:),and which has been occa- siounlly used in itch, as the latter is acrid and apt to cause much irritation. Oil of Worm'wood. Syn. Olbum absinth ii, VOL. II. L. Prom the fresh herb, ns oil, OF liiies. The P. Cod. and Ph. Wuriom. order only part of the herb to 8 parts of oil. Applied to the abdomen in dyspepsia, diarrhcea, heart- burn, worms, kc. It is seldom u^ed in tins country. OILS (mineral). ,^». Hydbocabbon oils. An important class of liquids, con8i.'s is entirely difl'ereiit, because with the vapours, say of tar, permanent gases are always gene- rated. On coming into contact with the con- densing surfaces a portion of the vapours is liquefied, leaving a layer of gas as a coatinsom, myrtle-blossom, narcissus, tuberose, violet, and, in general, of all the more delicate flowers, are prepared in the above manner. h. The native perfumers of India prepare their scented oils of bela, chumbul, jasmin, &c., in the following manner : — A layer of the scented flowers, about 4 inches thick and 2 feet square, is formed on the ground ; over this is jilnced a layer of moistened tel or sesa- raum seeds, 2 inches thick, and on this ano- ther 4-inch layer of flowers. Over the whole a sheet is thrown, which is kept pressed down by weights attached round the edges. The flowers are replaced with fresh ones after the lapse of 24 hours, and the process is repeated a third and even a fourth time, when a very highly scented oil is desired. The swollen sesamum seeds, rendered fragrant by contact with the flowers, are then submitted to the action of the press, by which their bland oil is obtained strongly impregnated with the aroma of the flowers. The expressed oil is then set aside in dubbers (bottles made of un- tanned hides) to settle. We have employed poppy seed in this country, in a similar manner, with great success. c. The flowers are crushed in a mortar or mill, with one half their weight of blanched sweet almonds, and the next day the mass is gently heated and submitted to the action of a powerful press; the liquid thus obtained is allowed to repose for a week, when the upper portion of oil is decanted and filtered. This plan is occasionally adopted in this country for the oils of roses and of a few other flowers. (See below.) The solution of a few grains of benzoic acid, or of gum benzoin (preferably the first), in any of the above oils, will materially retard the accession of rancidity, if it does not prevent it altogether. The oils of the last two classes (2 and 3) are chiefly used to impart their respective odours to the simple oils, pomades, &o.; and in the manufacture of scented spirits or esprits. The following formulsa are given as examples of both classes of preparations : — Oil of Am'bergris. From ambergris, 2 dr. ; oil, 1 pint ; by infusion. Oil of Ben'zoin. From gum benzoin, 7 dr. ; oil, 1 pint ; by infusion. Oils for the Hair. Si/n. Httiles antiques, Fr. These are numerous. All those scented with the simple perfumes are prepared in the way explained under' class 1 {above). The selection depends entirely upon the judgment of the operator or the fancy of the purchaser. In general, a mixture of two or three per- fumes is preferred in these countries to the pure fragrance of any single flower, and a grossness of taste is exhibited in these matters which surprises our Continental neighbours, and the inhabitants of Italy more particularly. Some of these oils are coloured. A red tinge is given to them by allowing the oil to stand for a few hours over a little alkanet root (2 dr. to the pint) before scenting it. The applica- tion of a gentle heat facilitates the process. Yellow and orange are given by a little an- notta or palm oil ; and green, by steeping a little green parsley or lavender in them for a few days ; or by dissolving 2 or 3 dr. of gum guaiacum in each pint by the aid of heat, and, when cold, decanting the clear portion. Huile antique au jasmin, Huile antique a la fleurs d'oranges, Huile antique a la rose, Huile antique a la tuberose, Huile antique a la violette, &o., are simple oils flavoured with the respective perfumes or their preparations. — Huile antique rouge a la rose is the ordinary oil of roses coloured with alkanet root. — Huile antique verte is simple oil coloured green, as above, and scented. — Huile antique aux mille- fleurs is so scented with several perfumes that none predominate. A mixture of bergamotte, lemons, lavender, neroli, pimento, and amber- gris or musk, is commonly employed for the purpose. Oil, Macas'sar. S^n. Huiie de macassae. Prep. 1. (Rowland's.) Oil of ben or almonds (reddened by alkanet root), 1 pint ; oils of rosemary and origanum (white), of each 1 dr. ; oil of nutmeg and attar of roses, of each 15 drops; neroli, 6 drops; essence of musk, 3 or 4 drops. 2. (De Naquet.) Oil of ben, 1 quart ; nut oil, 1 pint ; rectified spirit, ^ pint ; essence of bergamotte, 3^ dr. ; tincture of musk and esprit de Portugal, of each 2 dr. ; attar of roses, ^ dr. ; alkanet root, q. s. to colour. Oil, Mar'row (Perfumed). 1. Simple marrow oil, scented at will. 2. (FiuiDE DE Java.) Marrow oil, coloured with a little palm oil and scented. 3. (Huile comooene.) Marrow oil, 4 oz. ; spirit of rosemary, IJ oz. ; oil of nutmeg, 12 drops. 4. (Huile philocomb d'Aubbh.) Cold- OILS (VOLATILE) 1147 drawn not oil and marrow oil, eqnal parts ; •rent at will, q. b. 5. (H01LE DB FH^Nrx.) ClariRcd beef mar- row, iurd, pale nut oil, and expressed oil of in:)c<',of each 4 oz. ; melt together liy the heat ofhot water, strain through linen into a warm stone mortar, add, of oils of cloves, lavender, mint, rosemiiry, sage, and thyme, of each i dr. ; rectified spirit, 1 oz., in whiuh has been dissolved by a gentle heat balsam of tolu, 4 dr. ; camphor, 1 dr. ; triturate until the whole ia cold, and then put tt into bottles. All the obove are used to make the hair grow, and to prevent it falling off. Oil of Musk. Prom grain musk, 1 dr. ; am- bergris, i ilr. J oil of lavender, 20 drops ; oil, 1 pint, by infusion. A second quality is made by working the same ingredients, after the oil is poured from them, with | pint of fresh oil. This also applies to Oil of Ambebobib and HCILE BOYALB. Oil of Musk and Am'bergrlB. S^n. Hcile liOTALE. From ambergris, 2 dr. ; grain musk, i dr. ; oils of cassia, lavender, ncroti, and niit- inog, of each lU drops ; oil, 1 pint ; by infusion. (See above.) Oil of Sty'rax. From liquid styraT (pure), 6 dr. ; oil of nutmeg, 10 drops; ambergris, 6 gr. ; oil, 1 pint; by infusion. Oil of Vaniria. Si/n. Huile A L\ vanillh. Kiom purest olive or almond oil, li pint j va- nilla (finest, in powder), 2 ot.; oilofberga- motte, 1 dr. ; attar of ruses (finest), 16 drops j by infusion. OILS (Volatile).' Sj/a. Or,EA destillata, Olea dibtillata, Olea essentialia, Olea VOLATILIA, L. ; HUILES VOLATILES, Fr. The volatile oils are an extensive and important class of bodies, derived from the vegetable kingdom, and ibund in almost every part of tlie majority of the plants which produce tlioin, except tlic cotyledons of the seeds, in which, in general, the fixed oils are exclu- sively stored up. Their presence confers upon flowers, leaves, fruit, seeds, roots, bark, and woods their peculiar and characteristic odours; but among these they are not equally distri- buted in the same individual, and are often altogether absent from some of them. To them we are indebted for our most delightful perfumes, and our choicest spices and aro- niatics. Some of them are found to possess valuable medicinal properties, and others are invested with the highest possible interest on account of their peculiar chemical constitution, and the reactions which occur when they are brought into oontait with other bodies. The volatile oils are often called ' essences,' and the same loose and unmeaning terra is also commonly applied to their alcoholic solutions. ^ Although eisential oili are*volati!e oils, volatile oils nre not slirays fft-t-nttal ones as tlie term is understood. This is the case with the petroleum Hnd parutnii oils - taiaed l>y tlie distillation of native petroleum anil hitu- miuous bottles. To describe the two as syuoitjuious is therefore incorrect. — £0. Prop. The volatile or essential oils are usu- ally more limpid and less unctuous than the fixed oils ; but some of them are butyraceous or crystalline. Nearly all of them consist of two or more oils, diflering in their sp. gr. and boiling points, one of which is generally liquid, the other, in some cases, crystalline. All of them, when perfectly pure, are colour- less, though before rectification nearly the whole of them have a pale yellow tint," and some. of them are brown, blue, or green. Their odour is that of the plants which yield them, and is usually powerJFul ; their taste is pungent and burning. They mix in all pr 1- portions with the fixed oils, dissolve frceli in both alcohol and ether, and are sparingly »"- Inble in water, forming 'perfumed 'or 'me- dicated waters.' Their boiling point usually rangi-s between 310° and 325° Fahr., and is always considerably higher than that of water. They resist saponification, and (px- eepting oil of cloves) do not combine with the salifiable bases. Their density fiuctuatcs a little on either side of water. The lightest oil is that of citrons (sp. gr. "847), and the heaviest that of sassafras (sp. gr. 1'096). When coided sufficiently, they all solidify. The common temperature of the atmosphere is sufiicient for this with some of them, as the oils of roses and aniseed; whilst others re- quire to be cooled below the freezing point of water before they assume the solid form. In this state they appear to consist of a crystal- line or semi-crystalline substance (stearopten, stearessence), and .1 fiuid portion (eleopfcen, oleiessence). The two may be separated by pressing the concrete oil between the folds of bibulous paper, in the cold. By exposure to the air the volatile oils rapidly absorb oxygen, and become partially converted into resin. This is the cause of the deposit that usually forms in them (especially in the expressed oil of orange) when kept in an ill-corked vessel. The solid crystalline matter which sopirates from them when kept in closed vessels is stearoptene. Class. Chemically considered, the essential oils may be divided into three grtat cliisses: — 1. Oils composed of carbon and hydrogen only (binary volatile oils, carbo-bydrogens, hydro-carbons, terebenea, eamphenea), of which oil of turpentine may be regarded as the type. I'liese are characterised by bein?, as a class, less soluble in rectified spirit and in water than the other essential oils. The oils of bergamot, capivi, cubebs, elemi, hops, juniper, lemons, oratige peel, pepper, the grass oil of India, the laurel oil of Guiana, and some others, belong to this class. 2. Oils containing carbon, hydrogen, and oxygen (oxygenated oils), including most of those used in medicine and perfumery. These, as a class, are more soluble in rectified spirit and ill water than those containing carbon and hydrogen only. To this class belong the oils of almonds, aniseed, cassia, cedar-wood. 1148 OILS (VOLATILE) cinnamon, cumin, jasmin, lavender, meadow - sweet {Spiraea ulmaria), orange flowers, penny- royal, peppermint, spearmint, rosemary, rose- petals, valerian, winter green (Oauliheria\ procumbens), and others too numerous to men- tion, A few of these oxygenated oilx contain nitrogen. 3. Oils containing sulphur (sulphuretted oils). These are characterised by their ex- treme pungency, suffocating odour, vesicating power, property of blacking silver, and, being decomposed by contact with most other me- tallic bodies. The oils of assafoetida, blacli mustard seed, garlic, horseradish, and onions, are of this kind. Some sulphuretted oils eon- tain nitrogen. Prep. Tile volatile oils are generally pro- cured by distilling the odoriferous substances along with water; but in a few instances they are obtained by expression, and still more rarely by the action of alcohol. According to the common method of pro- ceeding, substances wliich part freely with their oil are put into the still along with about an equal weight of water, and are at once submitted to distillation. Those sub- stances which give out their oil with difficulty are first soaked for 24 hours, or longer, in about twice their weight of water, to each gallon of which 1 lb. of common salt has been added, in order to raise its boiling point. The distillation is conducted as quickly as possible, and, when one half the water has come over, it is returned into the still, and this cohoba- tion is repeated, when necessarv, until the ilis- tilled water ceuses to be mixed with oil. The heat of steam or a salt-water bath should be preferably employed. When a naked fire is used, the still should be deep and narrow, by which means the bottom will be better pro- tected by the gradually decreasing quantity of water towards tlie end of the process, and empyreuma prevented. When the distilled water is to be repeatedly cohobated on the in- gredients, a convenient and economical plan is to so arrange the apparatus that, after the water has separated from the oil in the re- ceiver, it shall flow back again into the still. An ordinary worm-tub, or other like condens- ing apparatus, may be employed; bnt in the case of those oils which readilv solidifv, the temperature of the water in the condenser must not tall below about 55° Fahr. The mixed vapours which pass over condense and fall as a n.iiky-looking liquid into the re- ceiver. This separates after a time into two portions, one of which is a solution of a part of the newly eliminated oil in water, and the other is the oil itself. The latter either occu- pies the upper or the low er portion of the re- ceiver, according as its specific gravity is less or greater than that of distilled water. The separation of the oil and water is i fftcted by allowing the mixed liquids to diop into a 'Florentine receiver' (see engr^ when the oil is the lighter of the two, by which means the latter accumulates at a, and the water flows over by the spout i. Lt^mJi Ct. The same receiver may be employed for oils heavier than water, by reversing, the ar- rangement ; but a glass ' separator' (see engr.') is, in general, found more convenient. In this case the oil accumulates at the bottom of the vessel, and njay be dijawn off by the stop-cock provided for the purpose. The essential oils of lemons and orangi s of commerce, and of some other fruits, are chiefly obtained by submitting the yellow rind to powerful pressure; but in tliis way they are not so white, nor do they keep so well, as when distilled, although in the case of the fruits referred to the oils are more fragrant than when prepared by any other method. The London College excluded the usual directions for the preparation of the essential oils from their Pharmacopoeia of 1851, on the ground that these substances are seldom pre- pared by the druggist or apothecary, or at all on the small scale. " The fruit of anise, caraway, and juniper, the flowers of chamomile, lavender, and elder, the berries of allspice, the tops of rosemary, and the entire recent plants of the other herbs, are to be employed." " Put any one of these into an alembic, then pour in as much water as will cover.it, and distil the oil into a large vessel, kept cool." (Ph. L. 1836.) The Edinburgh College directs — " As much water only is to be employed as will prevent empyreuma during the distillation. The dis- tillation may be immediately commenced after a proper maceration, and the oil afterwards separated from the water," in the manner already noticed. OILS (VOLATILE) 1149 " It in hIot necessary to observe, in preparinp; these oils, its well iia the distilled waters, that the qu;ility of the substances, their texture, the seitson nf the year, and similar circum- stances, must occasion so many differences, that it is scarcely possible to give any certain and general rules which shall strictly apply to every example. Many things, therifore, must be regulated by the judgment of the operator." The Dublin College directs the vegetable substances to bo macerated in the still with about 5 times their weight of water, for 24 hours, when one half of the water is to be drawn over. The oil having been separated from this in the usual manner, it is to bo re- turned to the still, and the same quantity drawn over, as be I ore, from which the oil must again he separated. Chevallier gives the fallowing rules for the distiUatiou of essential oils : — 1. Operate upon as large quantities as pos- sible, ill order to obtain a greater product, and one of finer quality. 2. Cinnluct the distillation rapidly. 3. Divide the substances minutely, in order to facilitate the extrit^ation of the oil. 4. Employ only sufficient water to prevent tlie matter operated on from burning, and the proiliu't from being coutaminated with euipjii'uma. 5. For substances whose oil is heavier than water, saturate or nearly saturate the water in the still with common salt, to raise the boiling |>olnt, and thus to enable the vapour to carry over more oil. 6. Employ, when possible, water which has been already distilled from off the same sub- stances, and lias thus become saturated with oil. 7. For oils naturally fluid, keep the water in the refrigerator cool ; but lor those oils which easily become solid, pi-eserve it at 80° to aO" Fahr. (?) To the above may he added — 8. Collect the oil as soon as possible after it separates from the water with which it passes over, and in its subsequent treatment keep it, as much as passible, from free contact with the air. Dr Ure remarks, " The narrower and taller the alembic is, within certain limits, the greater will be the proportion of oil, relative to that of the aromatic water, from like pro- portions of aqueous and vegetable matter em- ployed." " Some place the plants in baskets, and suspend these immediately over the bot- tom of the still, under the water, or above its surface in tho steam ; but the best mode, in my opinion, is to stuff an upright cvlindcr full of the plants and drive down through them steam of any desired force, its tension and its temperature being further regulated by the size of the outlet-orifice leading to the condenser. The cylinder should be made of strong copper, tinned inside, and encased in the worst conducting species of wood, such as soft deal or sycamore." The newly distilled oils may be separated from adhering water, which frequently ren- ders them partially opaque or ' cloudy,' by repose in a temperature between 60° and 70° Fahr., and subsequent decantation ; bat to ren- der them quite dry (anhydrous), it is necessary to let them stand over some fragments of fused chloride of calcium. This is not, however, required with tho commercial oils. The rectification of the volatile oils is com- monly performed without water, by the careful application of a heat just sufficient to make them flow over pretty rapidly, so that they may he kept heated for as »liort a time as possible. One half, or at most two thirds only, is drawn off, that left in the retort being usually mixed with raw oil intended to be sold in that state. This method often leads to much loss and disappointment, and we have known more than one rather dangerous explo- sion result from its use. A better plan is to rectify the oil from strong brine, and then to separate any adherine water, either by repose or chloride of calcium. Pres. Volatile oils should be preserved in well closed and nearly full bottles, in the shade, and should be opened as seldom as possible. By age tliey darken, lose much of their odour, increase in density, and become thick and clammy. It is then neces-ary to distil them, by which the undecom)iosed por- tion is separated from the resin. Agitation along with animal charcoal will restore tlieir clearness and original colour, but nothing more. Pur., Tests. The essential or volatile oils of commerce are very frequently adulterated with the tatty oils, resins, spermaceti, or alcohol, or with other essential oils of a cheaper kind or lower grade. The presence of the first three of these may be readily detected by placing a drop of the suspected oil on a piece of white paper, and exposing it for a short time to heat. If the oil is pure, it will en- tirely evaporate ; but if adulterated with one of these substances, a greasy or translucent stain will be left on the paper. Tliese sub- stances also remain undissolved when the oil is agitated with thrice its volume of rectified spirit. The presence of alcohol may be detected by agitating the oil with a few small pieces of dried chloride of calcium. These remain un- altered in a pure essential oil, but dissolve in one containing alcohol, and the resultmg solution separates, forming a distinct stratum at the bottom of the vessel, \^'hen only a very little alcohol is present, the pieces merely change their form, and cxhiliit the action of the solvent on their ansrles or edges, which become more or less obtuse or rounded. Another test for alcohol in the essential oils is the milkiness occasioned by agitating them IISO OILS (VOLATILE) with n little water, as well as the loss of volume of the oil when it separates after repose for a short time. A more delicate test of alcohol in the essen- tial oils than either of the preceding is potas- sium, as employed by M. Beral : — 12 drops of the oil are placed on a perfectly dry watch- gla-fs, and a piece of potassium, about tlie size of an ordinary pin's head, set in the middle of it. If the small fragment of metal retains its integrity for 12 or 15 minutes, no alcohol is present ; hut if it disappears after the lapse of 5 minutes, the oil contains at least 4§ of alcohol ; and if it disappears in less than 1 minute, it contains not less than 25§ of alcohol. Boettger states that anhydrous glycerin possesses the property of dissolving in al- cohol, without mixing with the volatile oils. The mode of applying the glycerin is as follows : — The oil to be examined is well shaken in a graduated tube, with its own volume of glycerin (sp. gr. 1"25). Upon being allowed to settle, the mixture separates into two layers. The denser glycerin sepa- rates rapidly, and if the essence has been mixed with alcohol, this is dissolved in the glycerin, the augmentation in the volume of glycerin showing the proportion of alcohol Jlre^ent. This species of adulteration is very common, as it is a general practice of the druggists to add a little of the strongest rectified spirit to their oils, to render them transparent, espe- cially in cold weather. Oil of cassia is nearly always treated in this way. The admixture of an inferior essential oil with one more costly may be best detected by pouring a drop or two on a piece of porous paper or cloth, and shaking it in the air, when, if occasionally smelled, the difference of the odour at the beginning and the end of the evaporation will show the adulteration, espe- cially if the added substance is turpentine. The presence of tlie latter may also be de- tected by agitating the oil with rectified spirit, when it will remain undissolved. The following method, which may also be used as a test lor the presence of turpentine, is based upon its power of dissolving fats : — Take about 50 gr. of oil of poppy in a graduated glass tube, and add an equal quan- tity of the sample of essential oil. Shake the mixture up thoroughly and then allow it to stand ; if the essential oil be pure, the mixture becomes milky, and does not clear until after several days have passed, whereas it will remain transparent if even so little as 5 per cent, of essence of turpentine be present. The purity of essential oils may likewise, in many cases, be determined by taking their sp. gr. ; or, with still greater accuracy and convenience, by measuring their index of re- fraction, as suggested by Dr Wollaston. A single drop of oil is sufficient for the applica- tion of the last method. The adulteration of a heavy oil with a light one, or the reverse, may be detected by agi- tating the suspected oil with water, when, in most cases, the two will separate and form distinct strata. Miss Crane believes that the cohesion figures aSbrded by the volatile oils, like those of the fixed ones, will be found useful indica- tions of their purity. The application of her method is precisely similar to that followed in her examination of the fixed oils as already described. She finds that — Oil of Turpentine, by itself, spreads in- stantly to the whole size of the plate (a com- mon soup plate), and almost immediately the edge begins to break into irregular shapes, when a rapid motion takes place over the surface of the film, and there seems to be a contest between the cohesion of the oil par- ticles and the adhesioVi between them and the water. The oil makes repeated efforts to gather itself closer together, when the water inst.^ntly reacts, giving a wavy appearance to the whole figure. The play of colours at this point is beauti- ful, and serves to bring out the lines more perfectly. In a few seconds innumerable little holes appear over the surface, which soon are separated only by threaded lines, and the figure is like the most exquisitely fine lace. Oil of Cinnamon forms a figure not more than half the size of tlie last-named. In a few seconds small portions are detached, and shortly separate into distinct drop:«, four or five larger, and a number of smaller ones, scattered about. With mixtures in different proportions of oil of turpentine, the figures formed differently, taking more of the char- acterislics of the adulterant as it predomi- nated. Oil of l^utmeg forms a large figure instantlv, the edgeshowing a beaded line. Itgathers itself together and spreads again, very like oil of tur- pentine, but the surface presents more the appearance of watei-ed silk. Within sixty seconds some holes appear, and in eighty more the surface is covered with them ; these scarcely spread to more than a sixteenth of an inch in diameter, but from the fir»t each is bordered with a dotted edge. The figure lasts some time without changing materially, except the openings lengthen out into an olilong shape, remaining entirely distinct. The play of colours is very fine. With the addition of one third of the oil of turpentine, the first spreading is little different, but openings appear in liall' the time, and the dotted border does not come as soon ; in about four minutes the figure is most characteristically marked, and soon breaks up entirely, this being the distinctive difference between the pure oil and the mixture. Oil of Peppermint spreads instantly to a large figure, and in ten or fifteen seconds openings appear, which increase rapidly in OILS (VOLATILE) llSl eize. At flnt they look Bomewliat like the iRitnamcd, bat are not nearly so numerous, nnJ tlie border soon ig more like tiny drops. In one and a hall' or two minutes they begin to run together, and the figure breaks up. With the addition of turpeittiTte oil the 6gure forms more slowly, and the breaking up is less rapid, but in five minutes the out- line* only remain. Oil of Bergamot spreads instantly ; in thirty seconds tiny openings appear, not very abun- diint, and increase in size slowly ; in five minutes they arc not larger tlian oil of nut- meg wl one and a half minute. At first they have a dotted border, but as they increase in size this changes to a scalloped film, which spreads, until, in eight or ten minutes, they are joined together over the whole surface. This, with the turpentine oil, gives a watered surface in spreading, much more marked, and with a fine play of colours. {7»e«, S(o. The volatile oils are chiefly used by perfumers and rectifiers, and in medicine. Some of the cheaper kinds are largely era- ployed IIS vehicles for colours, iind in the manufacture of varnishes. The dose of the aromatic and carminative oils is from 1 to 10 drops, on sugar, or dissolved in a little weak spirit. This iloes not apply to oil of bitter iilinonds, the dose of which is i to ^ a drop. •»• The following list includes short notices of nearly all the volatile oils which have been examined, as well ns of some other substances ol a similar chniiicter, which commonly pass under the name. Oil of Allia'ria. From the roots of Alliaria ojjficinalie, or snuce-iiloue. Identical with the oil of black mustard. Oil of All'spice. See Oil of Pimento. Oil of Al'monds. See Oil of Bitieb al- monds. Oil of American Arbor Tita. Sgn. Huile CEDEE BLAKO, Fr. From the fresh tops of Thuja occidentalism or Aiiktu'iiii arbor-vitffl tii'e. Yellow ; fratrraut j stimulant. Used in frictions for rheumatism. I'l-od. IJ to 2J (nearly). Oil of Angel'ica. From the dried root of Angelica Archangelica. Prod. 25§ (fully). Oil of An'iseed. Sgn. Oleoii anisi (Ph. L., E., & I).), O. ES3ENTIALE ANISI, L. From the fruit (si'i'iis) of Pimpinella anistim, or anise. Nearly colourless. It is very frequently adul- terated with one or other of the cheaper oils, in which case spermaceti or camphor is addtd to it, to make it * eaiuiy.' Prop., Sjc. When pure it congeals into a solid crystalline mass on being cooled to 50° Fahr., and does not melt again until heated to about 63°. Treated with iodine, it quickly congeals into a solid hard mass, with a per- ceptible iniTease of temperature, and the development of ornnge-coloured and grey fumes. Sulphuric acid, with heat, turns it of a rich purple-red colour, and the compound soon afterwards becomes inspissated aud hard (resiniOed). In alcohol of -806 it is soluble in all proportions, but rectified spirit (-838) dissolves only 42* of this oil. Sp. gr. (recent) ■9768 ; (one year old) -9853 to -9855 ; (old) •9856 to -9900. The foreign oil ia generally the heaviest. Oil of aniseed is carminative and pectoral ; and both itself and preparations have long been in favour with the masses in coughs, colds, &c. In preparing it care must be taken that the temperature of the water in the re- ceiver and refrigerator does not fall lower than about 68° Fahr. Prod. (From the dried fruit of commerce) avoir. 2g (nearly). See Oil op Staeanise. Oil, Ap'ple. See Amyl (Valerianate of), and Essence op Apple. Oil of Ar'nica. Syn. Oleum aenice, 0. A. EADICITM, L. From the roots of Arnica mon- tana. Yellowish brown. Spgr. -910. Prod. 16 lbs. yielded 1 oz. of oil. The oil from ihe flowers of arnica is blue. Oil of Asarabac'cB. Sgn. Oleum asabi, 0. ASABi LIQUIDUM, L. From the roots of Ana- rum Europaum. Yellow; glutinous. Two butyraceous oils pass over at the same time. Oil of AssafiBt.'ida. Syn. Olkum A8«- P(ETiDA, L. From the gum resin. Contains sulphur. Very fetid and volatile. Oil of Balm. Syn. Oleum melissjj, L. From the herb {Melissa officinalis). Pnle yel- low ; f riigrant. Sp. gr. -970 to '975. Prod. 100 lbs. of the fresh floweriii;^ herb yielding i oz. of oil (M. Riiybaud). A mixture nf oil of lemons iind rubcmary is commuuly sold for it. Oil of Balsam of Pern. See Cinnameine. Oil of Ber'gamol. Syn. Beuoamot, Es- sence OP B. ; Oleum beboamii, O. beeoa- M01\s:, L. By expression from the yellow portion of the rind of the fruit of Citrus Bergamia, or bergumot oruiige. Pale greenish yellow; highly fragrant. It is obtained purer by distilhitiun, but its perfume is theu slightly less delicate. Sp. gr. •875 to 885. Prod. The rind of 100 bergumot omiigcs yielded by distillation nearly 3 oz. of oil. (AI. Ray- baud.) Oil of bergamot is frequently adulterated with rectified spirit, or with tlie oils oflcmons, oranges, or turpentine. The presence ot these substances may be detected in the manner explained under Oils (Volatile), I'urily and Tests (anH, and has the density '897 ; the remaining pnrtion is green, and has the density '920 to '925. Its (irecn colour is derived from chlo- ri'le of copper, the presence of which may be recognised by the red precipitate occasioned by agitating the oil with a solution of terro- ryanide of potassium. (Guibourt.) From the Kiist IndieH. Pure oil of cajeput is slightly soluble in water; intirely and freely soluble in alcohol; dissolves iodine ; and when dropped on water, rapidly diffuses itself over the surface, and soon completely evaporates. A spurious kind (factitious OIL OP cajeput), made of oil of rosenmry, flavoured with camphor and the oils of peppermint and cardamoms, and coloured with verdigris, is occasionally met with iu the shops. Oil of cajeput is a powerful antispasmodic and diffusible stimulant. — Dose, 3 to 6 drops, on sugar ; in cholera, colic, epilepsy, hysteria, rheumatism, spasms, toothache, &c. Oil of Camphor. Si/n. Liqitid oamphoe ; Oleum camphob^, 0. c. volatile, L. Ob- tained from incisions in the wood of the cam- phor tree of Borneo and Sumatra {Diyobala- nopi aromatica), in which it exists in cavities in the trunk ; also by distillation from the branches of the Com;;Aoroo/^cinarum, or laurel camphor tree. Colciurless when rectified. Sp. gr. -910. Prod. CO lbs. of the crude brown \(iL. n. oil yields 40 lbs. of pure white oil and 20 lbs. of camphor. It rapidly oxidises in the air. Used tfl scent soap. See Camphoe (Liquid). Oil of Car'away. ;^n. Oleum cahui (B.P. Ph. L. E. & D.), 0. c. ESSE.NTiALE, L. From the fruit of Carum Carui (caraway seeds). Nearly colourless ; aromatic ; carminative. Sp.gr. -940; (old) '946 to '950. Prod. Av. 55 (nearly). It is frequently adulterated with oil of cumin. Added to purgative medicines to prevent griping. Oil of Car'damoms. Sj^n. Oleum cabsa- MOMi, 0. c. E83E1ITIALE, L. From the seed of Eleltaria cardamomum, or true cardamom. Colourless ; fragrant ; carminative. Sp. gr. ■943. Prod. 55 (nearly). The capsules ('lesser cardamoms') yield only about Ig of oil. (M. Raybaud.) Oil of Caecarilla. Syn. Oleum cascaeil- LS. L. From the bark of Crolon elevteria (Swartz.), or cascarilla tree. Very fragrant. Prod. '4'„' to 'T^",. Oil of Cas'sia. Syn. Oil op China cinna- mon ; Oleum cassia (Ph. E.), L. From cas- sia buds, or from cassia bark. Golden yellow ; aromatic ; fragrant. It is generally adul- terated with rectified spirit. Nitric acid con- verts the pure oil into a crystalline mass. Sp. gr. 1-071 to 1'073; (old) 1078 to 1'090 Prod. Prom the buds of I5 (barely); from the bark of commerce, •To". It is frequently sold for oil of cinnamon. Oil ot Cehadil'la. Syn. Oil op sabadilla ; Oleum oebadilljx:, L. A green butyraceous matter, obtained from Asagraa ojfficinalia. Oil of Ce'dar-wood. From the wood of a species of Cedrua. It consists of two hydro- carbons. One, a volatile liquid (cedrene), and the other a solid, crystalline compound con- taining oxygen. Prod. '2% to 25^. Oil of Ce'drat. %». Essence of cedea; Oleum cedei, 0. citei pinum, L. From th« exterior yellow rind of the fruit of Cilruii luedica (Kisso), or citrons, either by expression or distillation, as oil of bergamot. The first portion of oil that comes over is colourless; the latter portion greenish. Very fragrant. Sp. gr. '847. Prod. 100 citrons yield nearly 1 fl. oz. of pale, and \ fl. oz. of green oil. See Oil op Citeon (below). Oil of Cel'ery Seed. Syn. Oleum apii. L. From the fruit (seed) of Apium graveolens. Diuretic; stimulant. Prod. |g to 1§ (nearly). Oil of Cham'omile. Syn. Oil op Roman chamomile; Oleum anthemieis (Ph. L. E. & D.), O. CBAMiEMELI, O. C. PLOBUM, 0. ksskntiale ex plobibus c, L. From the flowers of Anthemis nobilis. In the Ph. L., English oil of chamomile (anthemidis oleum Anglicum) is ordered. Blue; turns yellow and brown by exposure and age ; odour cha- racteristic. Sp. gr., English (from the flowers), -9083 ; foreign, '9289. Prod. Fresh flowers, •!% (barely) ; recently dried (finest commercial), 5f ; av. of 6 dried samples, ■25g (nearly). If much water is employed, even 1154 OILS (VOLATILE) the above small quantities of oil will not be obtained. Oil of chamomile is reputed antispasmodic, tonic, and stomachic. 1 to 3 drops on a lump of sugar, taken just before retiring to rest, is an excellent preventive of nightmare, and will frequently induce quiet sleep where more active substances have failed. Unfortunately, the oil of the shops is generally either adul- terated or old, and commonly both, in which I ase the oil acts as an irritant. A common plan is to mix it « ith old oil of lemons, a fraud wliieh may be detected by the lessened density of the oil, and by its diminished solubility in rectified spirit. Oil of Cher'ry-laurel. Syn. Oletjm laueo- CEEASi, L. From the leaves of Cerasus Lauro- cerasus, or common laurel. Closely resembles oil of almonds, but is said to be weaker. Like that substance, it is powerfully poisonous. Frod. 100 lbs. fresh leaves (undeveloped, June), 1013 oz. ; do. (half grown, June), 7'2 oz. ; do. (full-grown, 8 weeks on tree, July), 4"96 oz. J do. (do., 3 months on tree, Sept.), 7'04 oz. ; do. (15 months on tree), 2-24. (Christison.) Oil of Caier'vil. Syn. OrEUM ohseophtlli. L. From the bruised fresh herb, macerated for 2 or 3 days in salt and water, and then distilled. Oil of Cincho'na. Syn. Oleum ciNcnoN.s;, L. From cinchona bark. Butyraceous; smells of the bark. 20 lbs. yield only 2 gr. (Tronimsdorff.) The odour of hark is imitated by a solution of turmeric in potash, and by chloride of iron. OilofCin'namon. Syn. Htdeibe ofcinna- MTl ; Oleum oinnamomi (B. P., Ph. L. E. & D.), 0. c. VEEI, L. From the bark of Cinna- momum zeylanicum, macerated for several days in salt and water, and then distilled. Yellowish or red ; very aromatic ; both odour and taste resemble that of the bark. Sp.gr. 1-035. Prod. II lbs. yielded 1 oz. ; 100 lbs. yielded 1-56 oz. (M. Raybaud.) Fur. Oil of cinnamon, owing to its hijrh piice, and the consequent premium for its adulteration, can scarcely be obtained pure from the sliops of this country. Oil of cassia and highly rectified spirit are the substances usually employed for this purpose. The in- creased sp. gr. resulting from the first, and the diminished sp. gr. from the second, afford ready means of detecting these frauds. The presence of oil of cassia may also be detected by an experienced person by the odour, which differs a little from that of pure oil of cin- namon. Oil of cassia is less limpid than oil of cinnamon, and it stands a greater degree of cold withontbecoming turbid or congealing. " Wine-yellow, when recent; cherry-red, when old ; odour purely cinnamonic ; nitric acid converts it nearly into a uniform crystalline mass." (Ph. E.) During this reaction the odour of bitter almonds is perceptible. Both oil of cassia and oil of cinnamon are thus con- verted into a brown balsam ; with oil of cassia, however, a brisk decomposition occurs sooner, and at a slighter beat. It also forms a crys- talline compound with ammonia. These re- actions, unfortunately, are not characteristic. " The most distinguishing characteristic of the cinnamon oils is, perhaps, their relation to the alcoholic solution of caustic potash. Both dissolve in it readily and clear, with a reddish, yellowish-brown colour; after some time, how- ever, the solution becomes very turbid, and a rather lieavy undissolved oil precipitates, when the solution gradually becomes clear again, (Ure.) The palest oil is considered the best. Obs. Oil of cinnamon is chiefly imported from Ceylon, where it is distilled from bark that is unfit for exportation. The dark coloured oil is usually rectified, when two pale oils are obtained, one lighter, and the other heavier, than water ; but 10^ of oil is lost by the process. The oil distilled from the root of the tree (o. cinnamomi eadicis) is much weaker than that from the bark. The oil from the leaves (o. c, folioeum), also imported from Ceylon, smells of cloves, but has a less density than oil of cloves. Oil of cinnamon consists essentially of hy- dride of cinuamyl, but, unless when very recently prepared, it also contains a variable proportion of cinnamic acid formed by the oxidation of the hydride. Oil of Cit'ron. Syn. Essence or citbon; Oleum citei, L. From the lees of citron juice; or, fjom the peels, as oil of lemons or bergamot. The last generally goes by the nameof oil ofcedrat. Both are fragrant. (See above.) Oil of Citron-flowers. Syn. Oleum citei PLOEUM, L. Amber-coloured ; highly frag- rant. Frod. 60 lbs. yield 1 oz. Oil of Cloves. Syn. Essence oj cloves ; Oleum caeyophtiloeum, 0. caetophtlli (B. P., Ph. L. E. & D.), 0. Euqeni^ c. (Ph. D. 1826), L. From the unexpanded flowers (cloves) of the Caryophylus aromaficus, or Molucca clove-tree, soaked for some time in salt and water, and then submitted to distilla- tion ; the distilled water, after having depo- sited its oil, being returned 3 or 4 times into the still, and again 'worked off' from the same materials. Nearly colourless, when recent, gradually becoming pale yellow, and ultimately light brown, by age; highly aromatic, with the characteristic odour and flavour of cloves. It is the least volatile of all the essential oils. Sp. gr. 1-055 to 1-061 (1-034 to 1-061, B. P.). Frod. 16J to 223. Fur. Oil of cloves is frequently adulterated with inferior essential oils, especially with those of pimento, pinks, and clove-gillyflowers, and, occasionally, with castor oil.— 1. Pure oil of cloves forms a butyraceous coagulum when shaken with pure liquor of ammonia, which crystallises after fusicin by a gentle heat. — 2. Treated with an alcoholic solution of potassa, OILS (VOLATILE) 1156 it entirely congeals into a crystHlliiie mass, with totul loss uf its characteristic odour. — 3. Shaken with an equal volume of strong caustic suda lye, it forms, on repose a mass ol delicate lamellar crystals. — 4. Solution of chromate of potassa converts it into brown flakes, whilst the salt loses its yellow colour. — 5. Chlorine turns it first green, and then brown and resinous. — 6. Nitric ucid turns it red, and a reddish-brown solid mass is formed ; with heat, it converts it into oxalic acid. — 7- It dissolves freely in sulphuric acid (oil of vitriol), yielding a trunsparent, deep redilish- browii solution, without any visible decompo- sition. — 8. Mixed, gradually, with about jid of its weight of oil of vitriol, an acid liquor is formed, together with a resin of a rich purple colour, which, after being washed, is hard and brittle, and forms a red tincture with rectiHed spirit, which is precipitated of a blood-red colour by water. — 9. It dis- solves iodine freely, without any marked reaction. — 10. It dissolves santaline freely. — 11. Mix one drop of the oil with a small trace of solution uf aiiiliae by means of a glass rod, and then shuke with 5 or 6 c.c. of distilled water. By the addition of a few dropi of sodium hypochlorite to the mixture the charac- teristic blue coloration due to phenol will be developed in a few minutes, if the adulterant bo present; whereas with the pure uil nothing but the purplish-violet colour of aniline will be perceived. Stirring or shaking must be avoided after the addition of the hypoohloriie. The presence of 1 per cent, of phenol can thus be demonstrated in one drop of the oil. Oh». Clove oil contains a heavy oil, sp. gr. 1"079 (cnryophyllic acid), and a light oil, sp. gr. '918 (clove hydrocarbon) ; by rectification, much of the light oil is lost, and the product becomes denser. (1'361 — Bonastre.) Oil, Cog'nac. See Oil, Gbape (beloto). Oil of Copai'ba. Sj/n. Oil of capiti; Olbum C0PAIB« (B. P., Ph., L. & E.), L. 1. (Ph. E.) Balsam of capivl, 1 or,.; water, IJ pint ; distil, returning the water into the still, until oil ceases to pass over. 2. (Wholesiilf.) From the crnde oil wliich separates during the iiiaiiufaetiire of * specific solution of copaiba' and 'soluble Ciipivi,' by distillation along with a little salt and water. Pur., ij-c. Colourless when pure ; that of commerce has frequently a greenish tinge, derived from the copper utensils ; odour, not di-ugreeiiblo when recent. Sp. gr. '876 to ■878. Prod. 5liU to 55 ;|. When adulterated with oil of turpentine, its solubility in rectified spirit is t;rcatly diminished, and the solution is turbid. — Duse, 10 to 15 drops, in sugar; in the usual cases in which copaib.i is ordered. 20 til (10 minims, three times a day (B. P.). Oil of Corian'der. Sj/n. Oleum cohiandri, L. From the fruit (seeds) of Coriandrum salivum. Yelhnvisli ; aromatic; c:iriniuative. Prod. (Dried truit) 5i to eg. Oil, Com. The name given by Mulder to a peculiar fatty compound found in the fusel oil of the distilleries of Holland. It has a very powerful odour, resembling that of some of the umbelliferous plants, and is unaffected by caustic potassa. 8.;e Oil, Fusel (page 772). Oil of Cn'bebs. Si/n. Olbum cubebabau, 0. cuBEBs: (B. P., Ph. E. & D.), L. From the fruit of Cubeba officinalis, or cubebs, coarsely ground. Aromatic, hot, and bitter tasted ; odour, that of the fruit ; faintly green, colourless when pure. Sp. gr. 129. Prod. 9g to llg. Pur., iSfo. When pure, iodine has little action on this oil, and immediately gives it a violet colour, without any very marked relic- tion ; nitric acid turns it opaque, and the mixture changes to a pale red when heated ; sulphuric acid turns it of a crimson red. When adulterated with oil of turpentine, both its vis- cidity, solubility in rectified spirit, and its density, are lessened; when mixed with castor oil it leaves a greasy stain on paper.— i)o«, 10 to 15 drops, in the usual cases in which cubehs iu sub'taiue is given. 5 to 20 minims (B. P.), suspeuded in water by mucilage and sugiir. Oil of Cumin. Si/a. Oleum cUMiifi, O. 0Y5IINI, L. From the fresh fruit (seed) of Cuminum Ci/minum, or cumin. Pale yellow; stnelh and tastes strongly of the seeds. Sp. gr. ■975. Prod. 2i3 to 3g. Ohs, Oil of cumin is a mixture of two oils differing iu volatility, and which m^iy be sepa- rated by careful distillation. The more vola- tile one has been named cymol ; the other, cuminol. Oil of Sill. Syti. Oleum anethi (Ph. L. & E), L. From the bruised fruit (seed) of Ani/teum graveolens. Pale yellow ; odour, that of the fruit; taste, hot and pungent; carminative. Sp. gr. -188 to -8^2. Prod, li (nearly). Oil of El'der. Sj/n. Attar op elder flow- ers; Oleu.m sAmbuoi, L. From elder Hnw- ers {Sambucus nigra). Butyraceous; odour not very marked. OilofEl'emi. Syn. Oleum elemi, L. From the resin. Isomeric with oil of turpentine. Oil of Er'ROt. Si/n. Ethereal o. of e. ; Oleum erootjj, O. e. iETHEREiM, 0. sEOALia COKNUTI, L. Prepared by evaporating the ethereal tincture at a very gentle heat, and, prel'eralily, allowing the last portion of the ether to escape by spontaneous evaporation. Brownish-yellow; lighter than water ; soluble in ether and solution of potass i; only partly soluble iu alcohol. It appears to be a mixture of volatile and fi.wd oil, with some resinous matter.— Dow, 10 to 20 drops, in hiemor- rhages; 10 or 12 drops every 3 or 4 hours, in diarrhoea ; 20 to 50 drops, as a parturifacient, &c. Externally, in rheumatism, toothache, U. Obs. The above is the oil of erjiot now employed in medicine. It must not be con- 1156 OILS (VOLATILE) founded with other preparations occasionally called by the same name, but which differ from it in character. Among the latter are the following : a. A fixed oil obtained by distilling ofE the spirit from the alcoholic tincture. It has the odour of rancid fish oil, and the distilled spirit has also a putrid odour. b. A fixed oil, obtained from coarsely pow- dered ergot by strong pressure between iron plates, at a heat of about 212° Fahr. It is fluid, coloured, smells strongly of the drug, but is nearly destitute of its leading qualities. Both the preceding contain some volatile oil and resinous matter. c. An cmpyreumatio oil obtained by dis- tilling ergot per se. It is light brown, viscid, acrid, and nauseous. d. A volatile oil obtained by digesting pow- dered ergot ill solution of potassa at 125° Fahr., diluting the saponaceous mass thus formed with one half to an equal weight of water, neutralising the alkali with dilute sulphuric acid, and then submitting the whole to dis- tillation in a chloride of sodium or oil bath. It is white, adhesive, butyraceous, and taste- less. It appears a product, rather tlian a simple educt. B. This is the ethereal oil, first described, in its purest form. It is colourless, translucent, oily, and acrid-tasted, with the odour of ergot ; it lias a high boiling-point, at which it suffers partial decomposition, but may be volatilised at a lower temperature, like the other oils. By long exposure to heat, it thickens and partly solidifies; licjht and air darken it; it is lighter than water, very slightly soluble in water, but sufficienily so to impart to it its peculiar odour; it is soluble in pure alcohol, in ether, the volatile and fixed oils, alkaline lyes, liquor of ammonia, creasote, and naphtha. The dilute mineral acids clear it but do not produce any marked reaction. Oil, Ethe"real. See Oil op Wine (below). Oil of Eucalyptus. Syn. Oleum eucalypti QLOBULi. See Eucalyptus. Oil of Fen'nel. Sj/n. Oleum tceniculi (Ph. L.), 0. F. OEPIOINALIS (Ph. E. & D.), O. p. DULCis, L. From the fruit or seed of Fceniculum dtilce, or sweet fennel (Ph. L.), Colourless ; odour that of the plant ; tastes hot and sweetish ; congeals at 50° Fahr. ; carminative and stomachic. It consists of two oils; the one solid and identical with that of oil of aniseed. When treated with nitric acid, it affords benzoin, Sp. gr. '997. Prod. Dried fruit (of commerce), 3§to3'5g. The flowering herb yields 'SSg of a similar oil. Obs. The oil of fennel of the shops is the product of the fruit of Fceniculum vulgare, or common, wild, or bitter fennel. It closely resemble that of sweet fennel, but is scarcely so agreeable either in taste or smell. It is chiefly used to scent soaps. Oil of Firwood. Syn. Oleum piki syltes- TEIS. An essential oil, distilled from the leaves of Pinus sylvestris. Oil of Fleabane. (Ph. U. S.) Syn. Oleum EEi&EEONTis CANADENSIS. An essential oil, distilled from Canada erigeron. — Dose, 5 minims in haemorrhage. Oil, Fu'sel. Noticed at page 772. Oil of GaVbanum. Syn. Oleum oalbani (Ph. Bor.), L. From galbanum, 2 lb. ; water, 16 fl. oz.; distilled together. Yellow; re- sembles oil of asafoetida, but milder. Oil of Gar'Iic. Syn. Sulphide of allyl. From the bruised bulbs or ' cloves ' of Allium sativum, or garlic. It possesses the peculiar odour, taste, and other properties of the bulbs, in a highly exalted degree. Obs. When a mixture of oil of black mustard and sulphide of potassium is exposed in a sealed glass tube to a temperature above that of 212° Fahr., sulphocyanide of potassium and garlic oil are formed. On the other hand, when the compound of garlic oil and chloride of mercury (formed by adding to an alcoholic solution of the oil a like solution of the chol- ride) is gently heated with sulpho-cyanide of potassium, mustard oil, with all its characteris- tic properties, is called into existence. Oil of Gaulthe"ria. See Oil op Paeteidge beeey (below). Oil of Gen'tian. Syn. Oleum gentians, L. From the root. Butyraceous ; smells strongly of gentian. 3 cwt. yield 1 dr. (barely). Oil of Gera"nium. Syn. Oil op gingee geass, O. op spikenaed. The oil of com- merce which passes under this name and which was formerly imported from the East Indies, was not obtained from any species of Gera- nium or Frlargonium, but probably from a species of Andropogon. Of recent years, how- ever, genuine geranium oil, obtained from the rose geranium (Felargonium roseum) has been and continues to be met with in our markets. This essential oil is manufactured in immense quantities, at La Trappe de Staonelli not far from the Bay of Sidi Ferruch, in Algiers, where about forty acres of the plant are in cultivation. "Three harvests are gathered every year, and each yields from 170 to 200 kilograms of oil, or equal to 500 to 600 kilograms per annum. The value of this product never falls below forty francs the kilogram, the average gross value being there- fore from 20,000 to 25,000 francs or at least £20 per acre. Seven distillatory apparatus are employed in this manufactory."* A flner oil is yielded by the rose geranium, when grown in France, but it is much dearer. It is often employed to adulterate otto of roses. See Oil, Geass (below). Oil of Gin'ger. Syn. Oleum zingibeeis, L. From the dried root (rhizome) of Zingiber officinale, or ginger of commerce. Bluish- green ; possesses a less agreeable odour than ' " Tlie Pinis Exliibition," Si-d series. No. 433. 'Pharmaceutical Journal,' OILS (VOLATILE) 1157 th^it of good u'lnger, without any pungency. Prod, fiol 1^ (M. Unybaud). OU of Qoosefoot. (Ph. U. S.) iSy». OLErsi CHKNorouii. Di-tilled from the seeds of Chenopodiwn anlhelminticum. — Do»e. From 4 to 8 drops, with treacle or imlk, for 3 nights in succession, for cliildren. For adult, i dr. Vi-rraifuge. OU of Qrain-spirit. Si/n. Gb*in on. Two distinct substances are found in spirit distilled fiom fermented grain ; one of which is buty- raeeous and highly ofEonsive (corn oil of Mul- der — ?), the other liquid (crude fusel oil). 'I'he relative proportions of these substances to each other, and to the spirits which they con- taminate, vary with the mat erials and the man- agement of the )iroce8s. The ' Grain oil ' of the London rectifiers consl-ts chiefly of fusel or potato oil, mixed with alcohol and water, and with small and variable proportions of solid etliyl and amyl-conipounds of certain (kitty acids (oenantbic and niargaric). The latter arc said to be similar to the butyraceous matter In fore referred to, as well us the solid fat of the whisky distilleries conducted on the old plan. According to Mr. llowney, the fusel oil of the Scotch di^tilleries contains capric acid. Sic Oil op Cohn (above), and Fusel oil. Oil, Orape. S,(/n. Bbandt oil, Cognao o. This is cst^entialiy the sulphate of amvl. It is prepared by dissolving the fusel oil of marc- brandy in strong rectified spirit, and then adding concentrated sulphuric acid ; alcohol and c\ccs8 of acid is removed by washing' the newly formed compound with water. Dis- solved in rcc ified 8|iii'it, it forms ' BUANiiY ESSENCE,' which is used to impart the Cognac flavour to plain spirit. See Sulphate op Amtl and Amtl-etheb, also Uil of Mabo- BliANDY (below). OU, Grass. Several of the grasses (Grami- naceow, 1 to 3 drops, on sngar. Oil of Petro'leum. See Naphtha, Oils (Mineral), PsTBOLErM, &c. Oil of Flm'eiito. Si/n. Oil op allspice ; Oleum pimkntj! (B. P., Ph. L., E , & D.), L. From the bruised fruit of Eugenia pimento, atUpiee, or Jamaica pepper. Pale yellow, growing reddish brown by age; odour, a cotn- bination of cloves and cassia ; taste pungent. Sp. gr. 1-021. Prod. ^ to 8g. Obf. Oil of pimento contains two oils similar to those found in clove oil. When pure, nitric acid turns it red, with active efFervescence and the assumption of a rusty brown colour. It combines with the salifiable bases in a nearly similar manner to oil of cloves. It is much us, when there is much pain or irritation. Obs. Carbonate of potassa is thought to be preferable to carbonate of soda, when the above affections occur in scorbutic habits. A little camphor is also occasionally added. Ointment of Aloes. See Ointment ice WOBMS. Ointment of Aloes, Compound. See Oint- ment TOR WOEMS. Ointment of Al'um. S,i/n. Unguentum aif- MlNis, L. Frep. 1. Alum, in very fine pow- der, 1 dr. ; lard, IJ oz. In piles. 2. To the last add of powdered opium, 7 gr. In piles, when there is much pain. See OllfT- MENT, BaNTEE'S. Ointment, Ammoni'acal. Si/n. UNOUENTtTM AMMONIACALE, U. AMMONIA:, L. ; LiPAEOLE d'ammoniaque, Pommade de Gondeet, Fr. Prep. 1. (P. Cod.) Suet and lard, of each 1 oz. ; melt in a strong wide-mouthed bottle, add of liquor of ammonia (sp. gr. '923), 2 oz., at once close the bottle, and agitate it until its contents concrete. As little beat as possible should be employed, to prevent unnecessary loss of ammonia. 2. (Gondret.) Lard, 3 parts; suet, 2 parts; almond oil, 1 part; strong solution of ammonia, 6 parts; mix, as before. Rubefacient, vesicant, and counter-irritant. Smeared over the skin and covered so as to prevent evaporation, it raises a blister in 5 or 6 minutes. Its general effects and uses are similar to those of com- pound liniment of ammonia. Ointment of Car'bonate of Ammo"nia. Si/n. UNaUENTUM AMMONIA CABBONATIS, U. A. SESCjniCABBONATls, L. Prep, From carbo- nate of ammonia, 1 dr. ; lard, 9 dr. An ex- cellent application to painful joints, indolent tumours, scrofulous sores, &c. Ointment of Ammo'niated Mercury. St/n. Unouentum htdeae&tei ammoniati (B. P.). Ammoniated mercury, 62 gr.; simple ointment, 1 oz. ; mix. See next preparation. Ointment of Ammo"nio-chloride of Hercnty. St/n. White peecipitate ointment; Un- guentum htdeaegyei ammonio-chloeidi (Ph. L.), U. H. pbeoipitati albi, U. pee- oip. A. (Ph. E.), U. H. submueiatis ammo- niati (Ph. D. 1826), L. Prep. 1. (Ph. L.) Ammonio-chloride of mercury, 2 dr. ; lard, 3 oz. ; triturate together. 2. (Ph. E.) As the last, but employing heat. Uses, ^-c. Alterative ; detergent ; stimu- lant. In itch, scald-head, and various other skin diseases; in inflammation of the eyes; as an application to scrofulous and cancerous tumours ; to destroy vermin on the body, &c. It " may be safely used" (in small quantities) " on infants." (A. T. Thomson.) Ointment, An"glo-Saxon. Prep. Heat olive oil, 1 pint, and beeswax, \ lb., until the mix- ture acquires a reddisii-brown colour; then add red lead (levigated), \ lb., and continue the heat, with constant stirring ; when the union appears complete, add of amber and burnt alum, of each, in fine powder, \ oz. ; lastly, when considerably cooled, add of pow- dered camphor, 8 dr. As a dressing to foul ulcers. Ointment, Au'odyne. See Ointment oe Opium, Hemlock, &c. Ointment of An'thracoka'li. Syn. Pomade DE anthbaookali, Pr. Prep. (Dr Polya.) Anthracokali, in very fine powder, 1 part; lard, 30 parts. See Antheaookali. Ointment, Antiherpet'io. Syn. Unguentum ANTiHEBPETicuM, L. Prep. \. (Alibert.) Eed OINTMENT 1167 SDlphide of raercnry, 3 dr. ; powdered cam- phor, 1 dr. ; lurd, 3 oz. 2. (Chevullier.) ' Sabsnlphnte of mercury' (Turpiitb mineral), 2 dr.; chloride of lime, 3 dr. ; Rlmoiid oil, 6 dr. ; lard, 2 oz. In herpes or tetters. Ointment, Antimo'nial. See Ointment op POTASSIO TABTUATB OF ANTIMONY. Ointment, Antiperiod'ic. Si/n. Aoxte oint- ment ; Unohentum antipbbiodicdm, U. PEBBIFUOUM. L. Prep. 1. Disulphate of quinine, It dr. j sacchnrine carbonate of iron, 1 dr.; oil of cajeput, 30 drops ; fresh butter, 1 oz. 2. (Antonini.) Sulphate of quinine, 1 oz. ; rectified spirit and sulphuric acid, of each q. s. ; lard, I oz. Uaes, Sfc. About \ oz. of either of the above to be rubbed on the vertebral regions once every li or 3 hours for 3 or 4 days, in intermittent fevers, more especially in those accompanied by vomiting; or, into the epi- gastrium, in cholera, diairhoea, or dysentery. Ointment of Araroba. See Asaboba. Ointment, Aromat'ic. Syn. Balsamitm btomachalb Wackebi, Ungubntum aeo- maticcm, L. Prep. (Ph. Austr. 1836.) Simple ointment, 2i lbs. ; yellow wax and oil of laurel, of each 3 oz. ; melt together, and, when considerably cooled, add of oils of juniper, mint, lavender, and rosemary, of each 2 dr. Anodyne, balsamic, and stimulant. Ointment, Arsen'ical. Syn. Ointment op WHITE ARSENIC ; UnGUENTUM AUSENICALE, U. AllSENIcr, U. ACIDI AnSENIOSI, L. Prep. 1. Arsenious acid (levigated), 3 gr. ; lard or simple ointment, 1 oz. In lepni, psoriasis, malignant whitlows, &c. 2. (Hosp. P.) Levigated white arsenic, 15 to 20 gr. ; lard, 1 oz. As a dressing for can- cerous SOI'CS. 2. (Soubeiran.) White arsenic, 1 dr. ; lard, and spermaceti ointment, of each 6 dr. In malignant, cancer. The above must be care- fully prepared, and used with great caution. See Cebate. Ointment of ArBe"niate of I'ron. Sy». Un- gcentum pebei aeseniatis, L. Prep. 1 (Carmiehuel.) Arseniate of iron, \ dr. ; phos- phate of iron, 2 dr. ; spermaceti ointment, 6 dr. 2. (Dr Percira.) Arseniate of iron, \ dr. ; lard, li oz. In oincer. Ointment of Arseniate of Soda. Syn. Un- ouentum 80D.E aeseniatis. Prep. Ar.-(.niate of soda, 1 dr. ; lard, 2 oz. Mix. Ointment, Astrin'gent. Syn. Ungitentum asthinoens, L. Prep. Triturate powdered catechu. It dr., with boiling water, 2 fl. dr., add, gradually,of>perm«cetiointment (melted), li oz.. and cnntiiiue the trituration until the mass coniTites. An excellent dressing for ill- disposed sores and ulcers, especially during hot weather. See the several LEAt> oint- ments. Ointment op Galls, cfec. Ointment of Atro"pia. Sya. Ungdenxcjm ATBOPI.E (B. P.), L. Prep. 1. Atropia, li gr; simple ointment, 1 dr.; mix by careful tritu- ration. 2. (Dr Brookes.) Atropia, 5 gr. ; lard, 8 dr. ; otto of roses, 1 drop. In neuralgia, rheumatic pains, &c , when the affection is not deeply seated. 8. (B. P.) Atropia, 8 gr.; rectified spirit, i dr. ; lard, 1 oz. ; dissolve the atropia in the spirit and mix with the lard. Ointment, Bailey's See Ointment, Itch. Ointment of Bal'sam of Pern. Syn. Uno0- ENTtlM BAL8AMI PeEUTIANI, L. Prep. 1. Lard or spermaceti ointment, 1 oz. ; balsam of Peru, 1 dr. ; melt together by the heat of boil- ing water, stir for & or 6 minutes, allow it to settle, and pour ofi' the clear portion. In chaps and abrasions. 2. (Compound; UNO B. P. COMPOSITUM — Copland.) Lard, 1 oz. ; white wax, i oz. ; balsam of Peru, 1 dr. ; melt as before, and when nearly cold, add of oil of lavender, 10 or 12 drops. As the last, and. to restore the hair. Ointment, Banyer's. Syn Compound alum OINTMENT; UnGUENTUM ALCMIHIS COMPO- 8ITUM, U. CAL0MELAN08, U. HaNYKRI, L. Prep. From burnt alum and calomel, of each It oz. ; carbonate of lead, or litharge (levi- pated), 2 oz. ; Venice turpentine, t lb. ; lard, 2 lbs. ; carefully triturated together. In milk- scald, porrigo, &c. Ointment of Bark. See Ointment of Cin- chona. Ointment, Basil'icon. Syn. Basilicon, Yellow B.; Ungubntum basilicum; U. b. platdm, L. Prep. (Ph. L. 174G.) Olive oil, 16 fl. oz.; yellow wax, yellow resin, and Bur- gundy pitcli, of each 1 lb. ; melt, remove the vessel from the fire, and stir in of common tur- pentine, 3 oz. This form is still oceusionally employed in some shops, but is {^emrally super- seded by the resin cerate and resin oint- ment of the Pharmacopoeias. A nearly similar preparation under the name of ' basilion oiut- ment,' is contained in the Ph. Bor. 1817. (See Je?OM>.) Ointment, Basilicon (Black). See Ointment op Pitch. Ointment, Basilicon (Ween). Syn. Ungcbn- TUir BASILICUM TIKIDE, L. Prep. (Ph. L. 1746). Prepared verdigris, 1 oz. ; yellow basi- licon, 8 oz. ; olive oil, 3 fl. oz. Detergent. Used to keep down funijou-^ iriuwtlis, to dross syphilitic ulcers, &c. 8tu Cerate and Oint- ment OP Veedigeis. Ointment, Bateman's. See Ointment, Itch. Ointment of Bay-leaves, t-ee Ointment, Laubel. Ointment of Belladon'na. Syn. Ungubntum BELLADONN.E (B. P., Ph. L.). Prep. 1. (Ph. L.) Extract of belladonna (deadly nightshade), 1 dr. ; lard, 1 oz. ; mix by tvitiuation. 2. (Soubeiran.) Frosli belladonna leaves (bruised), 1 part ; lard, 2 parts ; simmer toge- ther until the leaves become cri-p, and, alter- 1163 OINTMENT digestion, for a short time longer, drain with pressure. 3. (B. P.) Extract of belladonna, 1; rubbed with a few drops of water and mix with lard, 5^. Uses, Sfo. As a local anodyne, in painful and indolent tumours, nervous irritations, &o. Also as an application to tlie neck of the uterus in cases of rigidity, (Chaussier.) 4. (Compound; Unghjentum belladonna COMPOSITUM, L. — a. (W. Cooley.) Compound iodine ointment, 7 dr. ; extract of belladonna, 1 dr. Powerfully discutient. A most excel- lent application to all glandular tumours and indurations, buboes, &c., which it is desirable to disperse instead of mature, more espe- cially where there is much priin. It is parti- cularly suitable to cases occurringon shipboard, and when its application (at least twice a day) is accompanied with the internal use of the mixture of iodine and gold (See Antisceopu- I.O0S mixtuee), this treatment has seldom failed, even when the parties were dieted chiefly on salt food. h. (Debreyne.) Extract of belladonna and lard, of each 3 dr. ; powdered opium, i dr. As an external anodyne and benuuiber, more especially in neuralgia, painful cancerous tu- mours, &c. A small piece is to be applied to the part, and the friction continued for 6 or 8 minutes. The above preparations are use- less unless the extract employed is receut, and of good quality. Ointment of Benzoin. (Ph. U. S.) Syn. Ointment of benzoin. Frep. Tincture of benzoin, 2 oz. j lard, 16 oz. ; melt the lard over a water bath and add the tincture, stir- ring constantly, and when the spirit has evaporated, remove from the water bath, and stir whilst cooling. Ointment of Bismuth. Syn. Unottentum BiSMUTHi, L. Frep. 1. Nitrate of bismuth (' white bismuth '), 1 dr. ; simple ointment, 1 oz. 2. (Fuller.) Nitrate of bismuth, 1 dr. ; sper- maceti ointment, 19 dr. In itch, and some chronic cutaneous diseases. Ointment, Blist'ering. See Ointment op Canthaeides, and Vesicants. Ointment, Blue, lliis is the vulgar name in England of mercurial ointment. On tlie Con- tinent, an ointment made of smalts and Gou- lard water is commonly so called. Ointment of Bo"rax. Syn. Unottentum BOEAOIS, L. Prep. From borax (in very fine powder), 1 dr. ; pimple ointment or lard, 7 dr. In excoriations, chaps, &c. Ointment of Bromide of Potas'sium. Sfyn. Unguentom potassii BEOMim, U. potassjj; HYDKOBEOMATis, L. jPrep. (Magendie ) Bro- mide of potassium, J dr. ; lard, 1 oz. llesol- vent; in bronchocele, scrofula, &c. Ointment of Bro'mine. Syn. Unguentum BEOMINII, 0. B. COMPOSITUM, L. Frep (Ma- g'cndie.) Bromide of potassium, 20 gr. ; bro- mine, 6 to 12 drops; lard, 1 oz. As the last, but more active. Ointment, Brown. Syn. Fkench pooe-mah's PEiEND; Unguentum puscum, U. Htdbab- GTBi, F., L. iVep. (P. Cod.) Nitric oxide of mercury (levigated). \ dr.; resin ointment, 1 oz. In ophthalmia (cautiously), after the inflammatory stage is over ; as an application to sore legs, &c. Ointment of Cad'minm. Syn. Unguentum CADMii, U. c. sulphatis, L Frep. (Radius.) Sulphate of cadmium, 1 to 2 gr. ; pure lard, 1 dr. ; carefully triturated together. In species on the cornea. Ointment of Cadmium, Iodide of. (B. Ph.) Syn. Unguentum cadmii iodibi. Frep. Mix thoroughly iodide of cadmium in fine powder, 62 gr., with simple ointment, 1 oz. Ointment of Caffeine. Syn. Unguentum CAFEEiNiE. Frep. Citrate of caffeine, 8 gr. ; lard, 10 oz. Mix. Ointment of Cala'mine. Syn. Unguentum calamine:, U. lapis caiaminaeis, U. zihci CAEB0NATI3 IMPUBI, L. Prep. (Ph. D. 1826.) Prepared calamine, 1 lb. ; ointment of yellow wax, 5 lbs. Desiccative and healing. This is the old Dublin form for Turner's cerate. Ointment of Cal'omel, Syn. Unguentum HYDEAKGYEI SUBCHLOEIDI (B. P.), UNGUEN- TUM CALOMELANOS, U.HTDBAEGYBI CHLOEIDI, L. Prep. 1. From calomel, 1 dr. ; lard, or simple ointment, 1 oz. Ohs. " Were I required to name a local agent pre-eminently useful in skin diseases generally, I should fix on this. It is well de- serving a place in the Pharmacopceia." (Pe- reira.) Dr Underwood uses elder-flower oint- ment as the vehicle. 2. (Compound ; UNGUENTUM CALOMELANOS COMPOSITUM — Dr A. T. Thomson.) Calomel, 1 dr. ; tar ointment, 4 dr. ; spermaceti oint- ment, 1 oz. 3. (B. P.) Calomel, 1 ; prepared lard, 5^ ; mix. In lepra. Ointment of Cam'phor. Syn. Unguentum CAMPHOB^, L, Frep. 1. Camphor, 1 to 2 dr.; lard, 1 oz. ; dissolve by a gentle heat and stir until the mass is nearly cold. Stimu- lant and anodyne ; in prurigo, psoriasis, &c. 2. (Compound.) From powdered opium, \ dr. ; powdered camphor, Ij dr. ; lard, li oz. ; mix by trituration. As an anodyne friction in rheumatic pains, swelled ioints, colic, &c. Ointment of Canthar'ides. Syn. Unguen- tum CANTHiEIDIS (B. P., Ph. L., D., & U. S.), U. LTTTiE, L. Frep. 1. (Ph. L.) Caritharides (in very fine powder), 3 oz. ; distilled water, 12 fl. oz. ; mix, boil to one half, to the strained liquid add of resin cerate, 1 lb., and evaporate to a proper consistence. 2. (Ph. D.) Liniment of Spanish flies, 8 fl. oz. ; white wax, 3 oz. ; spermaceti, 1 oz. ; melt together with a gentle heat, and stir until it concretes. 3. (Ph. E.) — a. Unguentum inpusui can- IHABIDIS — Ph. E.) Powdered cautharidcs OINTMENT 1169 1 ox.; boiling water, ^ pint; infuse one niglit (12 honra), straia with (.'xpression, add of lard 2 oz., and boil until the water h expelled ; then add beeswax and re»in, of each 1 07.., and wlien these are liquefied, remove the veaael from the lire, and further add of Venice turpentine, 2 oz. i. (UNOPK.NTUM rCLVBBIS OAHTHAEIDIS— Ph. E.) Resin ointment, 7 oz. ; mult, add of rantbarides (in fine powder), 1 oz., and stir until the whole is nearly cold. 4. (B. P.) Cantharides, in fine powder, 1 ; olive oil, 6 ; yellow wax, 1 ; digest the cantha- rides in the oil for 12 hours, and for i hour at 212° ; strain, add the melted wax, and stir till cold. Obt. The above preparations are frequently csUed ' blister ointment' or ' epispastic oint- ment.' They are used to keep blisters open after they have been produced by stronger compounds. The first three compounds are regarded as milder than the last (3, b), whicli contains the flies in substance. The P. Cod. contains an ointment (uNO. epibfasticum TLATDu) which is weaker than the above, prepared by digesting the bruised flies in lard, for 8 hours, over a warm bath ; about ^th part of wax is next added to the strained I'at, which is then coloured with turmeric, and scented with oil of lemon. See Cebatb, Pouuase, Vesicants, and below. Ointment of Cautharides, Extract of. (M. Cap.) St/H. Unqdentcm OtJM extkaoto oan- THABIDI8. Prep. Alcoholic extract of can- tharides, 8 gr. ; oil of roses, 1 dr. ; beef mar- row, 2 oz. ; oil of lemon, 40 minims. To promote the p;rowth of the hair. Ointment of Cantharides with Mercnry. Syn. Omocbntum oanthaeidis cum hydbah- OYBO. Prep. Lard, 65 parts ; Spanish flies, 29 parts ; strong mercurial ointment, 6 parts. Mix. Used in Normandy to indolent tumours. Ointment of Canthar'idine. Syn. Unguen- TUM CANTHAHiDiNa:, L. Prep. (Soubtiran.) Cantharidine, 1 gr. ; white wax, 1 dr, ; lard, 7 dr. ; mix thoroughly. (See above.) Ointment of Cap'sioum. Sy». Unguektum 0AP8ICI, L. Prep. (Dr TurnbuU.) Tincture of capsicum (pure), q. s. ; gently evaporate it until it begins to gelutinise, then mix the ex- tr.ict with twice its weight of lard. As n powerful stimulant and rubefacient. When very freely used, it vesicates. Ointment of Car'bonate of Am"monia. See Ointment, Ammoniacal. Ointment of Carbolic Acid. (Ph.U. S.) Syn, Unouk.vtcm acidi CABBOLici. Prep. Car- bolic acid, fiO gr. ; simple ointment, 480 gr. Ointment of Carlianate of Lead. Si/n. White LBAD OmTUEXT; UnGUEHTUM PLUMBI OAE- noNATiB (P. B., Ph. E. & D.), U. cektjss^, L. Prep. 1. (Ph. E.) Carbonate of lead, 1 oz.; simple ointment, 5 oz. ; mix thoroughly. 2. (Ph. D.) Carbonate of lead, 3 oz. ; oint- ment of white wax, 1 lb.; mix with heat. Vol. II. 3. (B. P.) Carbonate of lead, in fine powder, 1 ; simple ointment, 7. Mix. 4. UnoUENTUM PLUMBI CAMPnOEATUM — (E., 1744). Add to the lust 2 scruples of cam- phor ground with a little oil. Use», cj-c. Cooling ; desiccative. Useful to promote the healing of excoriated parts and "light ulcerations. The camphorated white ointment of old pharmacy (Ung. album cam- PHOBATUM— Ph. L. 1744) was made by add- ing 40 gr. of camphor to the first of the above. Ointment of Cat'echn. Syn. Unouehttjm CATECHU, L. Prep. From alum, 1 oz. ; ca- techu, 3 oz. ; (both in very fine powder ;) added to olive oil, i pint, and yellow resin, 4 oz., pre- viously melted together. Used to dress ulcers in hot climates, where the ordin«ry I'at oint- ments are objectionable J also in this country during hot weather. See Ointment, Asteik- GENT. Ointment of Chalk. Syn. Unouehtuu CEETfi. Prep. Prepared chalk, 1 oz. ; lard, 4 oz. Mix. Ointment of Chamomile. (M. Bazin.) Syn. Ukguentum anthemidis. Prep. Freshly powdered chamomile flowers, olive oil, and lard, in equal quantities. For the cure of itch. Ointment of Char'coal, Syn. Unguentum 0AEBONI8, L. Prep. 1. Resin ointment, 10 dr. ; recently burnt charcoal (levigated), 3 dr. As a dressing to foul ulcers, especially those of the legs. 2. (Caspar.) Lime tree charcoal and dried carbonate of soda, of each 2 dr, ; rose oint- ment, 1 oz., or q. s. In scald-head. 3. (Radius.) Animal charcoal (recent), 1 part ; mallow ointment, 2 parts. As a friction in glandular enlargements and indurations, as a dressing to fetid ulcers, &c. Ointment of Cher'ry-Laurel. Syn. Ukguen- tum LAUEO-CEEASi, L. Prep. (Soubeiran.)' Essential oil of cherry-laurel, 1 dr. ; lard, 1 oz. To alleviate the pain in cancer, neuralgia, and other local affections. Ointment, Chil'blain. Syn. Unquentum ad PEENIONES, L. Prep. 1. From made mus- tard (very thick), 2 parts ; almond oil and gly- cerine, of each 1 part; triturated together. To be applied night and morning. 2. (Cuttereau.) Acetate of lead, camphor, and cherry-laurel water, of each 1 dr. j tar, 11 dr. ; lard, 1 oz. 3. (Devergie.) Creasote and Goulard's ex- tract, of each 12 drops; extract of opium, li S'' '< Isrd, 1 oz. Twice or thrice daily. 4. (Giacomini.) Sugar of lead, 2 dr.; cherry-laurel water (distilled), 2 fl. dr. ; lard, 1 oz. 5. (Linna!us.) Balsam of Peru, 1 dr. ; hydrochloric acid, 2 dr. ; spermaceti ointment, 2^ nz. Obs. For Swediaur's, Vance's, and Wahler's ointments, see article Chilblain. Ointment of Chloral Hydrate. (Dowault.) 74 1170 OINTMENT Sl/n. UKaUENTUM CHLOEALIS HTDBAS. Prep. Chloral hydrate, 2 parts; lard, 20 parts. Stimulant ; stronger if required as a rube- facient. Ointment of CUo "ride of Carcium. Si/n. Un- GtTENTUM OALOII CHLOEIDI, U. CAIOIS MUEI- ATist, L. Frep. (Sundelin.) Chloride of calcium (dry), 1 dr. ; strong vinegar, 40 gr. ; foxglove (recent, in fine powder), 2 dr. ; lard, 1 oz. In bronchocele, scrofulous tumours, &c. Ointment of Chloride of Lead. St/m. Un- GUENTUMPLUMBICHLOEIBI, L. JPrep. (TuSOn). Chloride of lead, 1 part; simple cerate, 8 parts ; carefully triturated together. In pain- ful cancerous ulcerations and neuralgic tu- mours. See Lead (Chloride). Ointment of Chloride of Lime. See Oikt- MKNT OF HyPOOHLOBITE OP LiME. Ointment of Chloride of Mercury. See Oint- ments OF Calomel and Coeeosite subli- mate. Ointment of Chlo"rine. 8gn. Unguentum Chloeikii, L. Prep. (Augnstin.) Chlorine water, 1 part ; lard, 8 parts; well triturated together. In itch, lepra, ringworm, fetid ulcers, &e. Ointment of Chlor-i'odide of Mercury. /Syra. Unguentum hydbaegyei chloeiodidi, L. Prep. (M. Eecamier.) Chloriodide (iodo- chloride) of mercury, 3 gr. ; lard, 5 dr. Re- commended as a powerful discutient or resol- vent. See Ointment op Iodo-chloeide op Meecuet. Ointment of Chlo"roform Syn. Unguentum chloeofoemi, L. Prep. (M. Louis.) Chloro- form, 1 dr. ; simple ointment, 1 oz. In neu- ralgia and rheumatic pains, &c. It must be kept in a stoppered, wide-mouthed phial. Ointment of Cin'ohona. Si/n. Ointment of BAEK ; Unguentum cinchoNjE, L. Prep. (Biett.) Red cinchona bark (in very fine powder) and almond oil, of each 1 part; beef 'marrow (prepared), 3 parts. In the variety of scald-head termed porrigo decalvans. A little oil of mace or tar is a useful addition. Ointment, Cit'rine. See Ointment of Ni- TEATE of Meecuet. Ointment of Cobalt, Oxide of. (Amst. Ph.) %n. Unguentum oxidi cobalti. Frep. Simple cerate, 16 oz. ; liquid subacetate of lead, 4 oz. ; powdered smalt, 4 oz. Ointment of Coc'culus In'dicus. S^ti. Un- guentum OOCOULI (Ph. E.), L. Prep, (Ph. E.) Kernels of Cocculus indicus, 1 part ; beat them to a smooth paste in a mortar, first alone, and next with a little lard ; then fur- ther add of lard, q. s., so that it may be equal to 5 times the weight of the kernels. Used to destroy pediculi, and in scald-head, &c. Ointmentof Cod-liver Oil. Syn. Uisouentum OLEI IIOEEHU^, U. O. JECOEIS ASELLI, L. Prep. Cod-liver oil (pale and recent), 7 parts ; white wax and spermaceti, of each 1 part ; melted together. In ophthalmia and opacity of the cornea, either alone or combined with a little citrine ointment; as a friction or dress- ing for scrofulous indurations and sores; in rheumatism, stiif joints, and in several skin diseases. It often succeeds in porrigo or scald- head when all other remedies have failed. Scented with oil of nutmeg and balsam of Peru, it forms an excellent pomade for strengthening and restoring the hair. Ointment of Col'ocynth. Syn. Unguentum COIOCYNTHIDIS, L. Prep. (Chrestien.) Co- locynth pulp (in very fine powder), 1 part ; lard, 8 parts. Used in frictions on the abdo- men as a hydragogue purgative, in mania, dropsy, &c. Ointment of Corrosive SuVlimate. Syn. Ointment of ohloeide of meecuet; Un- guentum HTDEAEGTEI OHLOBIDI, L. Prep. 1. From corrosive sublimate, 2 to 5 gr. ; rub it to powder in a glass ot wedgwood-ware mor- tar ; add of rectified spirit, 6 or 7 drops, or q. s. ; again triturate; lastly add, gradually, of spermaceti ointment (reduced to a cream- like state by heat), 1 oz., and continue the trituration until tlie whole concretes. Used as a stimulant, detergent, and discutient ap- plication in various local affections ; in lepra, porrigo, acne, &c., and as a dressing to syphi- litic and some other ulcers. 2. (Ph. Chirur.) Corrosive sublimate, 10 gr. ; yolk of 1 egg ; lard, 1 oz. As a dressing. 3. (PoMMADE DE ClEiLlo — P. Cod.) Cor- rosive sublimate, 1 dr. ; lard, 1 oz. Caustic ; must not be contounded with the preceding. Ointment, Cosmet'ic. Syn. Unguentum oos- METICUM, L. ; POMMADE DE LA JEUNESSE, Fr. Frep. (Quincey.) Spermaceti, 3 dr. (better, 44 dr.) ; oil of almonds, 2 oz. ; melt together, and, when cooled a little, stir in of nitrate of bismuth (' white bismuth'), 1 dr. ; and, lastly, of oil of rhodium, 6 drops. In itch and some other cutaneous eruptions ; but chiefly as a pomade for the hair. Its frequent use is said to turn the latter black. Ointment of Cre'aaote. Syn. Unguentum CEEASOTi (B. P., Ph. L. E. D. & U. S.), L. Prep. 1. (Ph. L.) Creasote, i fl. dr. ; lard, 1 oz. ; trituriite together. 2. (Ph. E.) Lard, 3 oz.; melt it by a gentle heat ; add of creasote, 1 dr., and stir the mix- ture until it is nearly cold. 3. (Ph. D.). Creasote, 1 fl. dr. ; ointment of white wax, 7 dr. ; as the last. 4. (B. P.) Creasote, 1 ; simple ointment, 8. Mix. Uses, Sfc. In several skin diseases, especially ringworm ; as a friction in tie-douloureux ; a dressing for scalds and burns ; an application to chilblains, &c. Ointment of Cro'ton Oil. Syn. Unguentum CEOTONis, L. Frep. 1. Croton oil, 15 to 30 drops ; lard (softened by heat), 1 oz. ; mix well. This is the usual and most useful strength to prepare the ointment. Rubefacient and counter-irritant; in rheumatism and various other diseases. When rubbed repeatedly on the skin, it produces redness and a pustular OINTMENT 1171 eraption. It also often affects the bowels by abiwrplion. The only aUvautuge it possesses over other preparations of tlie class is the rapidity of its action. 2. (BoBEPACiKNT POMADE — Caventou.) White wax. 1 part; lard, 6 parts; melt toge- ther, and, wliun quite cold, mince it small, add of croton oil, 2 pnrts, and mix by tiituration. Stronger than the last. " Ointment of Cy'amde of Mer'cury. St/n. UKOnKNTUM nTDllABOYEI CTANIDI, L. Prep. 1. (Cazenave.) Cyanide of mercury, 8 gr. ; lard, 1 oz. ; carefully triturated together. 2. (Percira.) Cyanide of mercury, 10 to 12 gr. ; lard, 1 oz. As a dressing for scrofu- lous and syphilitic ulcers, &c. ; as an applica- tion in psoriasis, moist tetters, and some other skiu diseases, &c. liiett orders the addition of a few drops of essence of lemon. Ointment of Cyanide of Fotas'slom. Si/n. UnqUBNTDM P0TAB8II CTANIDI, L. Prep. (Cazenave.) Cyanide of potassium, 12 gr. ; oil of almonds, 2 dr. ; triturate, add of cold cream (dry), 2 oz., and mix by careful tritura- tion. As an anodyne in neuralgia, rheuma- tism, swelled joints, &c. ; also as a friction over the' spine in hysteria, and over the epi- gastrium in gastrodynia, &c. Ointment of Delphin'ine. St/n. ITnoventitm DELi'niNIiB, L. Prep. (Dr Turnbull.) Uel- phinine or delphinia, 10 to 80 gr. ; olive oil, 1 dr. ; lard, 1 oz. ; mix as the last. Used as a friction in rheumatism, and the other cases in which veratrino is employed. Ointment, Depil'atory. Si/n. Unouentcm DEPiLAToniUM, L. See UEriiATOisr (Caze- nave's). Ointment, Deslc'cative. Si/n. Detino oint- ML.VT; Unouentusi desiccativdm, U. ex- siccANS, L. See the Ointmbnis of Cala- mine, Lead, Zino, &c. Ointment, Deter'gent. Si/n. Unguentfji DKTEBOENS, L. The OINTMENTS OF NITRATE OP MEKCDBT, NITEIC OXIDE OF MEECUEY.TAK, TEBui&Eis, &c., when not too strong, come under this head. Ointment, Diges'tive. Si/n. Unouentum di- oSsTivuM, L. Prep. 1. (P. Cod.) \enice turpentine, 2 oz. ; yolks of 2 ejins ; mix, aud add of oil of St John's wort, J oz. -. (Digestif anim^ — P. Cod.) As the lash, with an equal weight of liquid styrax. 3. (Digestif meecubiel — P. Cod.) As No. 1, with an equal weight of mercurial oint- ment. 4. (Uno. d. vibidb— Dr Kirkland.) Bees- wax, gum cicmi, and yellow resin, of each 1 oz. ; green oil, 6oz. j melt them toi;eiher, and, when considerably cooled, add of oil of turpentine 2 dr. Ointment, Edinburgh. Two compounds are knmvn under this name : — 1. (BiiOWN.) From hhick basilicoii, 6 parts ; milk of sulphur, 2 parts ; Pal ammoniac, 1 part. i. (WuiTE.) From white hellebore, 3 oz.; sal ammoniac, 2 oz. ; lard, 1 lb. Both are used in itch. Ointment of Eggs. Syn. Unouentum OVOEUM, L. Prep. 1. Yolk of 1 egg ; honey and fresh linseed oil, of each 1 oz. ; balsam of Peru, i dr. ; mix well. 2. (Soubeiran.) Beeswax, 4 dr. ; oil of almonds, IJ oz. ; yolk of 1 egg. As an emol- lient and soothing dressing to excoriations, irritable ulcers, &c. Ointment, Egyp'tian. Prep. (Giordano.) Burnt alum, 1 part; verdigris, 10 parts; strong vinegar, 14 parts ; purified honey (thick), 32 parts ; mix by heat and agitation. As a deter- gent application to foul ulcers. It is a modifi- cation of the ' UNOUENTUM iEOYPTIACUM ' of old pharniaey. Ointment of Elder-flowers. Si/n. White ELDEEOINTMENT j UnoUBNTUM SAMBUCI FLO- BUM, U. SAMBUOi (Ph. L.), L. Prep. 1. (Ph. L.) Elder flowers and lard, of each 1 lb. ; boil them together until the flowers become crisp, then strain, with pressure, through a linen cloth. The same precautions must be observed as are necessary in the preparation of the medi- cated oils, by infusion. Emollient; less white and odorous than the following : — 2. (Wholesale.) Take of lard (hard, white, and sweet), 25 lbs. ; prepared mutton suet, 6 lbs.; melt them in a well-tinned copper or earthen vessel,addofelderflower water 3 galls., agitate briskly for about i nn hour, and set it aside; the next day gently pour off the water, remelt the ointment, and add of benzoic acid, 5 dr. ; otto of roses, 20 drops ; oil of bergamot and oil of rosemary, of each 1 dr.; again agi- tate well, let it settle for 10 minutes, and then pour off the clear portion into pots for sale. Very ap^recahle, and keeps well. Obs. The last formula is the one now generally adopted by the large wholesale houses. Ointment of Elder-leaf. 61bs. ; boil till crisp, strain off the oil, put it over a slow tire, add hard prepared mutton suet, 14 lbs., and gently stir it until it acquires a bright green colour. Obs. The above ointment is reputed to be emollient and cooling, and has always been a great favourite with the common people. Both elder-flower and elder-leaf ointment arc, however, unnecessary preparations. *' They are ve^ti^es of the redundant practice of foi'mer times." (A.T.Thomson.) The above formuljE are those now almost exclusively em- ployed in trade. The ointment should be allowed to cool very slowly, and after its tem- perature has fallen a little, and ic begins to thicken, it should not be stirred, in order that it may ' grain' Hell, as a granular appearance 1172 OLNTMENT is much admired. It is a common practice to add powdered verdigris to deepen the colour, but then the ointment does not keep well. This dangerous fraud may be detected in the manner noticed under Ceeate, Savinb. Ointment of Elecampane. St/n. UisaxjETSTVM Inttii^. Prep. Fresh elecampane root (boiled till soft and pulped), 1^ oz. ; lard, 1 oz. Mix. Ointment of El'emi. Si/n. Balsam ov ab- O^USt, UNaUENTUM BtEMI (B. P., Ph. L. & U.), L. Prep. 1. (Ph. L.) Elemi, 3 oz. ; suet, 6 oz. ; melt them together, remove the vessel from the fire, and stir in of common turpentine, 2i oz. ; olive oil, J fl. oz. ; lastly, strain the whole through a linen cloth. 2. (Ph.D.) Resin of elemi, 4 oz. ; ointment of white wax, 1 lb ; melt them together, strain through flannel, and stir the mixture constantly until it concretes. 3. (B. P.) Elemi, 1 ; simple ointment, 4 ; melt and strain. Uses, Sfc. Stimulant and digestive. It is frequently employed to keep open issues and setons, and as a dressing for old and ill-con- ditioned sores. The ' uhg. elemi cum rnnv- iiihe' of St George's Hospital is made by ailding 1 dr. of finely powdered verdigris to every 6 oz. of the ointment. Ointment of Emetina. (Dr Tarnbull.) Syn. Unottentttm emetikje. Prep. Emetine, 15 gr. ; rectified spirit, q. s.; lard, J oz. (Jsedas a rubefacient. Ointment Escharot'ic. Syti. Vsavssivis. ESCHAEOTICUM, L. Prep. 1. (Sir B. Brodie.) Corrosive sublimate, 1 dr. ; nitric oxide of mercury, sulphate of copper, and verdigris, of each 2 dr. (all in very fine powder) ; lard, q. s. See Ointment, and Cebate, Ae- SENICAL. Ointment of Euphorbinm. (Dr Neligan.) Syn. Unouentum euphoeeii. Prep. Pow- dered euphorbinm, 25 to 30 gr. ; lard, 1 oz. ; mix. To keep up a discharge from issues. Ointment of Glycerin.' 8yn. Unouentum <CEEINI. Prep. Glycerin, 4 fl. oz. ; oil of almonds, 8 fl. oz. ; wax and spermaceti, of each \ oz. Ointment, Eye. Syn. ErE salve ; Unguen- tum ophthalmioum, L, Prep. 1, (Dr Col- lier.) Buint alum, i dr.; powdered opium, 20 gr, ; olive oil, 1 fl. dr.; spermaceti ointment, 2 dr. In inflammation of the eyelids, purulent ophthalmia, &c. 2, (W. Cooley.) Chloride of barium, 6 gr. ; calomel, 10 gr. ; simple ointment, 1 oz, ; otto of roses, 1 or 2 drops. In scrofulous oph- thalmia, 3, (Dessanlt.) Nitric oxide of mercury, carbonate of zinc, acetate of lead, and dried alum, of each 1 dr, ; corrosive sublimate, 10 gr, ; rose ointment, 1 oz. In chronic oph- thalmia, profuse discharges, &c. ; in general, diluted. 4, (Dupuytren,) Red oxide of mercury, 10 gr, ; sulphate of zinc, 20 gr, ; lard, 2 oz. For chronic inflammation of the eyelids, chronic ulcers, &c. 5. (Fricke). Nitrate of silver, 10 gr. ; zinc ointment, 2 dr, ; balsam of Peru, i dr. In ulceration of the cornea, and in acute, purulent, and chronic ophthalmia, &c,, employing great caution in its use. 6. (Guthrie.) Spermaceti ointment, 1 dr. ; solution of diacetate of lead, 15 drops; nitrate of silver, 2 to 10 gr. As the last, and in cases wherein a direct caustic action is desired. The stronger ointment often occasions intense pain. 7. (Hufeland.) Black oxide of mercury, 2 gr. ; spermaceti cerate and walnut oil, of each 1 dr. In chronic affections of the eyes or eyelids, particularly in those of a syphilitic character, 8. (Janin.) Ammonio-chloride of mercury, 1 dr. ; tutty and bole, of each 2 dr, ; lard, 1 oz. In debility of the conjunctiva, in chronic inflammation with excessive secretion, &c. 9. (Marsiiall.) See Ceeate (Marshall's). 10. (Parker.) Iodine, 1 gr. ; iodide of po- tassium, 5 gr. ; simple ointment, 3 dr. In scrofulous ophthalmia, thickening of the con- junctiva, opacity of the cornea, &c, 11. (Pellier.) Nitric oxide of mercury and carbonate of zinc, of each IJ dr, ; tutty, | dr. ; red sulphuret of mercury, 20 gr. ; lard, 2 oz. ; balsam of Peru, 15 drops. In specks in the eye arising from small ulcers which have healed up; in excessive defluxions, &e, 12. (Ratier.) Liquor of diacetate of lead, J dr. ; wine of opium, 1 dr. ; lard, 5 dr. In exco- riations, and the variety of chronic ophthalmia popularly termed ' blear eye.' 13. (Regent). Acetate of lead and red pre- cipitate, of each 1 dr. ; camphor, 6 gr. ; washed fresh butter, 2i oz. As the last, and in chronic ulcerations. 14. (Singleton's GOLDEN OINTMENT.) Ac- cording to Dr Paris, this compound consists of lard medicated with orpiment (native yellow sulphuret of arsenic). There appears, however, to be some mistake in this, as that sold us under the name had nearly the same composi- tion as the ointment or niteio oxide ov MEECUET of the Pharmacopoeia. It did not contain even a trace of either arsenic or sul- phur. The action of this nostrum, and the reputation which it has acquired, fully justify this conclnsion. 15. (Smellome.) From verdigris (levigated), Jdr. ; olive oil, 1 fl. dr. ; triturate together; add of yellow basilicon, 1 oz, and again tri- turate until it begins to concrete. A popular nostrum, sometimes useful In chronic inflam- mation and ulcerations of the eyelids, &c., especially in those of a scrofulous character. 16. (Spielmann.) Acetate of lead, 20 gr. ; spermaceti cerate, 5 dr. ; compound tincture of benzoin, 40 gr. Cooling ; desiccative. In inflamed eyelids, excoriations, &c. 17. (St Yve.) Fresh butter (washed), 1 oz. ; white wax, 1 dr, ; camphor, 15 gr, ; melt by a OINTMENT 1173 gentle Vient, and, when cooled a little, add of red precipkiito (levigated), i dr. ; oxide of zinc, 20 gr. In clironic inflammation of the coats of the eyo, or of the eyelids, specks on tlie cornea, &c. IH. (Thomson.) Levigated oxide of zinc, 1 dr. ; lird, 9 dr. ; wine of opium, 20 drops. In chronic ophthalmia depending on want of tone in the vessels and integuments of the eye. 19. (Velpean.) Precipitated sesquioxide of iron (recent, but dry), i dr. ; lard, 5 dr.; oil of almonds, 1 fl. dr. ; balsam of Peru, 1-5 drops. As the 1:1st, especially in 'blear eye.' 20. (Ware.) Wine of opium, I fl. dr. ; simple ointment, 3 dr. In oplithaluiia, after the in- flammatory symptoms have subsided, and the vessels remain red and turgid. Obi. The ingredients entering into the composition of all the above ointments must be rc'tuced to the state of impalpable powder before mixing them ; and the incorporation should he made by long trituration in a wedg- wood-vviire mortar, or, preferably, for those that coiit:iIn substances that are very gritty, by levi},'ation on a porphyry slab, with a muller. The most serious consequences, even blindness, huvi' resulLi'd from tlie neglect of these pre- cautions. They slioiild all be employed in ex- ceedingly small quantities at a time, and they should be very carefully applied by means of a camel-hair pencil or a feather; and, in ^cne ral, not until acute inflammation luis subsided. The stronger ont's, in most eases, re(|uire dilu- tion with 1(11 equal weight to twice their weight of lard or simple ointment, and should only he used of their full strength under proper medi- cal ailvice. Various other formultc for oph- thalmic OINTMENTS will be found under the nauii'H of their leading ingredients. Ointment of Fig'wort. See Ointment of SCHOPK0LAKIA. Ointment of Fox'glove. Syn. Unquentum DIGITALIS, L. Prep. 1. From fresh foxglove as ointment of hemlock — Ph. L. As an ap- plication to chronic ulcers, glandular swellings, Itc. 2. (Rademacher.) Extract of foxglove, 2 dr. ; lard, 1 oz. In croup; spread on lint, and applied as a plaster to tlie throat. Ointment of Fu'ligokali. See Fttliqokali. Ointment of Galls. iS^n. Unquentum OALL.K (B. P., Ph. D.), L. Prep. 1. (Ph, D.). li. ill-nuts (in very fine powder), 1 dr.; oint- ment of white wax, 7 dr. ; rub them together until a uniform mixture is obtained. 2. (B. P.) Galls, in very fine powder, 80 gr. ; benzouted lard,l oz. Mix. An excellent appli- cation to piles, either alone or mixed with an equal quantity of zinc ointment ; also highly useful in ringworm of the scalp. Ointment of Glalls and Opium. Unquentum OALLji ecu opio (B. P.); Unquentum OALLA OPIATUM, U. GAhLM 00MPO9ITUM — Ph. L., U. OALLiB ET opii,— (Ph. 'E.)—Prep. 1. (Ph. L.) Gall-nuts (very finely powdered). 6 dr.; powdered opium, IJ dr.; lard, 6 oz. ; rub them toirether. 2. (Ph. E.) Galls, 2 dr.; opium, 1 dr.; lard, 1 oz. ; as the last. 8. (B. P.) Ointment of galls, 1 oz. ; opinm (in powder), 32 gr. Mix. Use», ifc. A most valuable astringent and anodyne in blind piles, slight cases of pro- lapsus ani, &c. Some practitioners add 1 dr. of camphor. The ointment of the Ph. E. is much the strongest. Ointment of Galls with Mobphia. Un- GULNTUM OALL2E ET MOttPHI «— (Dr Paris.) MorphiH, 2 gr. ; olive oil (hot), 2 fl. dr. ; triturate, add of zinc ointment (Ph. L.), 1 oz. ; powdered galls, 1 dr.; and mix thoroughly. In piles. The quantity of galls should be doubled. Ointment of Galls with Camphor. Syn. Unquentum gall^ cum oamproba. Prep. Galls, 2 dr. ; camphor, \ dr. ; lard, 1 oz. Mix them. Ointment of Garlic. Syn. Unquentum ALLII, L. Prep. 1. Fresh garlic (bruised), 2 parts; lard, 3 parts; simmer together for \ an hour, and then strain with expression. Rubbed on the abdomen in chronic diarrhoea anil colic, and over the chest and spine in hooping-cough. 2. (Beasley.) Fresh garlic and lard, equal parts; beaten together. Applied to the teet. in hooping-cousrh. Ointment, Giacomlni's. See Ointment, Chilblain. Ointment of Gold. Syn. Unquentum auki, L.; Pommaoed'ob, Fr. Prep. 1. (Legrand.) Gold (in powder^, 12 gr. ; lard, 1 oz. As a dressing for syphilitic ulcers; and as a friction in glandular indurations, &c. ; also endcrm;- cally. 2. (Magendie.) Amalgam of gold, 1 dr. ; lard, 1 oz. For endermic use, chiefly. When the surface becomes dry, the ointment of ter- chloride of gold is to be substituted as a dress- ing. In rheumatic pains, neuralgia, &c. Ointment, Gold'en. See Ointment, Eye, Citkine 0., &c. Ointment, Gondret's. See Ointment, Ammoniacal. Ointment, Goulard's. Syn. Unquentum GOULAEDI, U. litkabqyei acetatib, L. Prep. (Ph. Chirur.) Goulard's extract, 1 dr.; simple ointment, 2 oz. See Cerate (Lead). Ointment, Green. See Ointment, Elder. Ointment of Guarana. Syn. Unquentum OUABAK.E. Prep. One part of extract of guarana to eight parts of lard. Ointment of Hellebore. Syn. Ointment of white hellebore; Unquentum veeatri, L. Prep. 1. (Ph. L. 1836.) White heUebore (in very fine powder), 2 oz. ; lard, 8 oz. ; oil of lemons, 20 drops. In itch, lepra, ringworm, &c. ; and to destroy insects in the hair of children. It should be used with caution, and, preferably, diluted with an equal weight of lard. 1174 OINTMENT 2. (Compound ; Ungubntum vebatri com- POSITUM.)— a. (liuyer.) White hell shore, 1 oz. ; sal ammoniac, i oz. ; lard, 8 oz. Used as the last. b. See SxTLPHUE ointment (Compound) — Ph. L. Ointment of Hemlock. Syn. Unqfentum 00NH.(Ph. L.), L. Prep. 1. (Ph. L.) Fresh hemlock leaves and lard, of each 1 lb.; boil them together (very gently) until the leaves become crisp, then strain through linen, with pressure. See Oils (Medicated). 2. Extract of hemlock, 1 dr.; lard, 9 dr.; triturate together. Uses, Sfc. As a local anodyne in neuralgic and rheumatic pains, glandular enlargements, painful piles, &c. ; and as a dressing to painful and irritable ulcers, cancerous sores, &c. Ointment of Hen'bane. Syn. UNOtrENTUM HTOSOXAMI, L. Prep. 1. Fresh henbane leaves, 1 lb.; lard, 2 lbs.; boil until nearly crisp. 2. (Taddei.) Extract of henbane, 1 dr. ; lard, 1 oz. Anodyne; in painful piles, sores, &c., as the last. Ointment, Holloway's. See Patent medi- cines. Ointment of Hops. Syn. T7NauENTUM ltt- PtlLI, L. Prep. (Swediaur.) Hops (com- mercial), 2 oz. ; lard, 10 oz. ; as extract of hemlock, Pli. L. In painful piles and can- cerous sores. Ointment of Hydri'odate of Ammo"nia. Sya. UNOtTENTUM AMMONiaS SYDEIODATia, L. Prep. From hydriodate of ammonia (iodide of ammonium), ^ dr. ; simple ointment, 1 oz. Used chiefly as an application to scrofulous tumour and ulcers, in irritable subjects. Ointment of Hydrochlo"ric Acid. Syn. Un- GUEKT0M AOIDI HTDEOOHLORICI, L. Prep. (Dr Corrigan.) Hydrochloric acid, 1 dr.; simple ointment, 1 oz. As a dressing for scald- head, after the scabs have been removed by emollient liniments or poultices. Ointment of Hypoclilo"rite of Lime. Syn. Ointment of chlobide of limb ; UNauEN- TCM CALOIS HTPOOHLOEITIS, U. C. CHLOBI- NATiE, L. Prep. 1. From chlorinated lime (chloride of lime), X dr.; lard, 1 oz. ; carefully triturated together. In scrofulous swellings, goitre, chilblains, indolent glandular tumours, &c. 2. Chlorinated lime, 1 dr. ; powdered fox- glove, 2 dr. ; simple ointment, 2 oz. As an application to fetid and malignant ulcers, &c. Ointment of Hypoclilo"rite of Snl'phur. Syn. Unucentum sulphueis htpoohlobitis, L. Prep. (Dr Copland.) Hypochlorite of sulphur, 1 dr. ; simple ointment, 1 oz. It is generally scented with oil of almonds. Used in psoriasis iuveterata, and some other skin Ointment of I'odide of Ar'senic. Syn. Un- GCENTUM AESENICI lODIDI, L. Prep. (Biett.) Iodide of arsenic, 2 to 3 gr. ; lard, 1 oz. ; carefully triturated together. In lepra, psoriasis. &e, ; and in corroding tubercular diseases. It should be used with caution, and not more than i dr, applied at once. Ointment of Iodide of Ba"rinm. Syn. Un- GUENTUM BABII IODIDE, L. Prep. (Magen- die.) Iodide of barium, 3 to 4 gr. ; lard, 1 oz. As a friction to scrofulous swellings and indura- tions. The usual proportions are now 5 gr. to the pz. Ointment of Iodide of Iron, (Pierquin.) Syn. Unguentum feeei iodidi. Prep. Iodide of iron, 1 dr.; lard, 1 oz. Mix them. Ointment of Iodide of lead. Syn. Un- GUENTtTM PLUMBI IODIDI (B. P., Ph. L., & D.), L. Prep. 1. (Ph. L.) Iodide of lead, 1 oz. ; lard, 8 oz. ; rub them together. 2. (Ph. D.) Iodide of lead (in fine powder), 1 dr. ; ointment of white wax, 7 dr. 3. (B. P.) Iodide of lead, in fine powder, 62 gr. ; simple ointment, 1 oz. Mix. An excellent application to scrofulous tumours and swelled glands, especially when accompanied with pain. Ointment of Green Iodide of Mer'cnry, Prep. 1. (Ointment of subiodide of mbeouet, 0. OF pbotiodidb of m.* ; Unguentcm HTDEAEGrEI lODIDI — Ph. L.) o. (Ph. L.) White wax, 2 oz ; lard, 6 oz. ; melt them together, add of iodide (green iodide) of mer- cury, 1 oz., and rub them well together. 2. (Magendie.) Green iodide of mercury, 23 gr. ; lard, li oz. Vses, S(c. In tuberculnr skin diseases, as a friction in scrofulous swellings and indolent granular tumours, jind as a dressing for ill- conditioned ulcers, ' especially those of a scrofulous charactsi'. Ointment of Red Iodide of Mercury. Un- GITENTUM HTDEAEGTEI iodidi ET7BBI, B. P., O. OF BINIODIDE OF M.* ; UnGUENTUM HT- deabgybi biniodidi,* U, h. iodidi eubei— (Ph. D.)— 1. (Ph.D.) Red iodide of mercury, 1 dr.; ointment of white wax, 7 dr.; mix by careful trituration. 2. (Soubeiran.) Red iodide of mercury, 20 gr. ; lard, 1^ oz. 3. (B. P.) Rediodideofmercury (in very fine powder), 16 gr. ; simple ointment, 1 oz. Mix. Uses, <^o. Similar to those of the preceding, but it is much more stimulant, and is regarded as better adapted for obstinate syphilitic sores. Largely diluted with lard or almond oil, it is applied to the eyes in like cases. Ointment of Iodide of Potas'sium. Syn. Un- guentum potassii iodidi (B. p.. Ph. L. & D.). L. Prep. 1. (Ph. L.) Iodide of potassium, 2 dr., dissolved in boiling distilled water, 2 fl. dr.; lard (softened by heat), 2 oz. ; triturate together until united. 2. (Ph.D.) Iodide of potassium, 1 dr.; dis- tilled water, 5 fl. dr.; ointment of white wax, 7 dr. ; as before. 3. (Magendie.) Iodide of potassium, 1 dr. ; lard, 12 dr. 4. (Le Gros.) Iodide, 1^ dr.; lard, 1 oz. OINTMENT 1175 fi. (11. P.) Todide of potnasiuin, 64 gr. ; carbonate of potnsh, 4 gr. ; distilled water, 1 dr. ; prepared lard, 1 oz. ; dissolve the carbonate and the iodide in the water, and mix thorough!; with the lard. Utes, Jj-e. As a friction in scrofula, bron- chocele, glandular enlargements, indurations, &c.; as a dressing to scrofulous ulcers, as an application in scrofulous ophthalmia, and in most of the other applications in which the eniploymiut of iodine is indicated. The last formula has been successfully employed by M. Le Qros in itch. Ob», The strength of this ointment, as prescribed by different parties varies greatly, the proportions of the iodide ranging from 9*1 to -^ of the whole, to adapt it to particular eases. When other ingredients are added, the iodide must be used in a perfectly dry state, and in fine powder, instead of being dissolved in water. This is particuliirly necessary when it is to be mixed with morcurial ointment. Ointment of Iodide of Sulphnr. St/n. Un- OUBNTCM BULPurillS lODlDI (B. P., Ph. L., L. I'rep. 1. (Ph. L.) Iodide of sulphur (in fine powder), 4 dr.; lard, 1 oz.; mix by tritu- ration. 2. (Cazenave.) Iodide of sulphur, 12 to 15 gr. ; lard, 1 oz. 3. (B. P.) lodideofsulphur. l;lard, 16. Mix. Usrs, cfc. As a local stimulimt and altera- tivi' in the chronic forms of lepra, lupus, por- rigo, psoriasis, itch, &c. ; also a remedy for acne punctata. A few drops of oil of cloves or nutmeg are commonly added. Ointment of Iodide of Zinc. S^n. Unoiten- TUM ZINCI lODiiJi, L. Prep. 1. From iodide of zinc, 12 gr. ; simple ointment, 1 oz. In scrofulous excoriations, and in the chronic oph- thalmia of scrofulous subjects, arising from a ruliixwl stiitc of the tissues and vessels. 2. (Dr Ure.) Iodide of zinc, 1 dr. ; lard, 1 oz. As a friction to glandular tumours and in- durations, and as a dressing to flabby and obstinate scrofulous ulcers. Ointment of I'odiae. S^n, Ungttenttjm lODi (B. P.), Unoubntum iodinii (Ph. U. S.J. Prep. 1.— (B. P.) Iodine, 32 gr. ; iodide of potassium, 32 gr. ; proof spirit, 1 dr. ; rub togttlier and add prepared lard, 2 oz. See OiNiMBNT OP Iodine (Compound). 2. (Ph. U. S.) Iodine, 20 gr.j rectified spirit, 20 drops; rub them together, then add of lard, 1 oz. Ointment of Iodine (Compound). Si/n. Ointment op iobuebtted iodide op potas- 8idh; unonentum potassi lodidi i0dt7ke- TUM, U. IODINII COMPOSITUM — Ph. Ij. & D., U. IODINII— Ph. E.— o. (Ph. L.) Iodine of potassium (in very fine powder), 1 dr. ; lard, 2 oz. ; mix, then add of iodine, i dr., dissolved in rectified spirit, 1 fl. dr., and mix all together. Sue Ointment op Iodine (B. P.) i. (Ph. E.) Iodine, 1 dr.; iodide of potas- sium, 2 dr. ; rub them together, then gradually add of lard, 4 oz. c. (Ph. D.) Pure iodine, i dr. ; iodide of potassium, 1 dr. ; rub them well togi tlnr in a glass or porcelain mortar, then (;rariully add of ointment of white wax, 1 ti dr., and con- tinue the trituration until a uniform ointment is obtained. Uses, Sfc. The compound ointment is an excellent frieticjn in goitre, and in enlarged or indurated glund^i or tumours, more especially those of a scrofulous character ; iu the quan- tity of i to 1 dr., night and morninir. It may be advantageously combined with extract of belladonna in the incipient bubo of scrofulous subjects, and in the early stages of cancer ; and, with an equal weight of mercurial oint- ment, as u friction in cases of enluigcd liver and spleen, and ovarian drojisy. The ximple ointment of the Ph. U. S. is generally regarded as weaker and less efficacious than the com- pound. Ointment of Iodo-chlo"ride of Mercury. Syn. UnGDENTUM HTDKAKOYRI IODO BICHLOHIDI*, Ij. I'rep. From iodochloride of .Mercury, 16 gr. ; simple ointment, 1 oz. Discutient ; probably one of the most powerful known in syphilitic cases complicated with scrofula. See Ointment of Chlokiodide of Mbb- CUET. Ointment of Iodoform (Dr Glover). 5y». UxoUENTUM lODOPOBMi. Prep. Iodoform 1 to 1 dram, ."imple cerate 8 drams. Mix. Ointment, lodo-hydrar'gyrate of Fotassa. Si/n. Ungdkntum potasse iodo-utdeakgt- KATI8, L. JPrep. 1. (Lamothe.) lodo-hydrar- gyrate of potassa, 20 gr. ; lard, 1 oz. 2. (Puche.) Red iodide of mercury and iodide of potassium, of each 8 gr. ; lard, 1 oz. As a powerful stimulant discutient; in tumours, inflammatory sore throat, &c. Ointment, lodonarcot'ic. Syn. Unquen- TUM lODO-NAECOTICUM, L. Frep. (Purvis.) Iodine, 20 gr. ; iodide of potassium, 2 dr. ; oil of tobacco (by infusion), H dr.; lard, 3 dr. To relax rigid muscles. Ointment of IpecacuanTia. Si/n. Uugpen- TUM iPECACDANHa;, L. Frep. (l)r. Turnbull.) Ipecacuanha (iu fine powder), 2 dr. ; olive oil, 2 fl. dr. ; lard or simple ointment, 4 dr. Counter-irritant ; when frequently employed as a friction, it occasions an eruption, but one of a milder character than that from either croton oil or tartar emetic. Ointment, Is'sne. Si/n. iNOUFNTrM ad- PONTICULOS, L. Frep. (Golding Bird.) Oint- ment of cantharides (Ph. L.), li oz. ; tartar emetic (in impalpaple powder), 8 gr. ; sperma- ceti ointment, 2oz. As a stimulating applica- tion to issues, to promote the discharge. See Elbmi ointmest, Cebate, Plastee, &c. Ointment, Itch. Syn. Uhguentum anti- PSOEicrM, L. Several excellent formulae fur itch ointments will be found under the names of their leading ingredients. The following are additional ones, including some nos- trums : — 1. (Bailey.) From alum, nitre, and sulphate 1176 OINTMENT of zinc, of each, in very fine powder, IJ oz. j vermilion, i oz. ; mix, add gradually of sweet oil, i pint ; triturate together until perfectly mixed, then further add of lard (softened by heat), 1 lb., with oils or aniseed, lavender, and origanum, q. ». to perfume. 2. (Bateman.) Carbonate of potassa, ^ oz. ; rose water, 1 fl. oz. ; red sulpliuret of mer- cury, 1 dr. ; oil of bergamot, i fl. dr. ; sub- limed sulphur, and hog's lard, of each 11 oz. ; mix them. (Bateman, ' Cutaneous Diseases.') The nostrum vended under the name is made as follows : — Carbonate of potash, 1 oz. ; vermilion, 3 dr. ; sulphur, 1 lb. ; lard, IJ lb. ; rose water, 3 fl. oz. ; oil of bergamot, Udr. 3. (French Hosp.) Chloride of lime, 1 dr. ; rectified spirit, 2 fl. dr. ; sweet oil, -^ fl. oz. ; common salt and sulphur, of each 1 oz.; sofb soap, 2 oz. ; oil of lemon, 20 drops. Cheap, effectual, and jnotfensive. 4. (De la Harpe.) Sulphur, 2 oz. ; pow- dered white hellebore, i oz. ; sulphate of zinc, ^ do. ; soft soap, 4 oz. ; lard, 8 oz. 5. (Jackson.) From palm oil, flowers of sul- phur, and white hellebore of each 1 part; lard, 2 parts. 6. (Nugent.) From white lead, 2 oz. ; orris root, 1 oz. ; corrosive sublimate, in very fine powder, i oz. ; palm oil, 4 oz. ; lard, li lb. 7. (Ph. E., 1744.) Elecampane root and sharp-pointed doclc {Bumex acatus — Linn.), of each bruised, 3 oz. ; water, 1 quart ; vinegar, f pint ; boil to one half, add of water-cress, 10 oz. ; lard, 4 lb. ; boil to dryness, and stain with expression ; to the strained liquid add of beeswax and oil of bays, of each 4 oz. ; and stir the mixture until nearly cold. 8. (Un&. a. comp.— Ph. E. 1744.) To each lb. of the last add of strong meicurial ointment, 2 oz. 9. (Robertson.) Soft soap, 1 oz. ; rum, 1 table-spoonful; chloride of lime (dry and good), k oz. ; mix, and add of lard, 2 oz. 10. (Swediaur.) Stavesaere (in powder), 1 oz.; lard, 3 oz. ; digest with heat for 3 hours, and then strain. The formula of the Ph. Bruns. is nearly similar. Very useful in itch ; also to destroy pediculi. 11. (Thomson.) Chloride of lime and com- mon salt, of each, in fine powder, 1 dr. ; soft soap, 1 oz. ; rectified spirit, 2 fl. dr. ; mix, add of lard, 1 oz. ; and, lastly, of strong vinegar, 3 fl. dr. Very cleanly and effective ; but should not be made in quantity, as it does not keep well. 12. (Vogt.) Chloride of lime (dry), 2 dr ; burnt alum, 3 dr. ; lard, 9 dr. To be mixed with an equal quantity of soft soap at the time of fusing it. Oba. The products of the preceding for- muliB are used by well rubbing them into the part affected, night and morning, as long as necessary, the number of applications required depending greatly on the manner in which this is done. Ointment of I'vy. Syn. TJir&UBifTTrM hb- DBEiE, L. Prep, From the leaves of common ivy, by infusion, as ointment of henbane. Used as an application to soft corns, in itch, and as a dressing to indolent ulcers and issnes. Ointment of Jatropha (Physic-nut). The milky juice of the English Physic nut {Ja- tropha eurcas) mixed with half its weight of lard. In piles. Ointment of Juniper. St/n. Dkchjemtuji JUNIPEBI. Prep. Juniper leaves, 1 part, resin ointment, 6parts; boil gently and strain. Ointment of Ju"mper-tar. Si/n. Unocen- TUM OLEI PTEOLIONI JUNIPEBI, U. CADINUM, L. Prep, (Eras. Wilson.) Lard and suet, of each 6 parts; beeswax, 4 parts; liquefy by heat, and add of pyroligneous oil of juniper ('huile de cade') 16 parts ; with a few drops of any fragrant essential oil, to conceal the smell. In ringworm, and as a stimulant ointment in some other skin diseases. Ointment, Eirkland's. See Lead ointhest (Compound). Ointment of Lahdanum. (Qnincy.) Si)«. UNOtTEifTiTM CEiNiscuM. Prep. Labdanum, 6 dr. ; bears' grease, 2 oz. ; powdered southern- wood, 3 dr. ; oil of mace, ] dr. ; balsam of Peru, 2 dr. Ointment of lard. St/n. Unottentttm adi- pis, L. Prep, (Ph. L. 1788.) Prepared lard, 2 lbs. ; melt, add of rose water, 3 fl. oz ; beat the two well together, then set the vessel aside, and when the wliole is cold, separate the con- gealed fat. A simple emollient. See OlHl- MENT, Eldeb. Ointment of Lau'rel. Syn. Lattehiie oikt- MENT; UKaUBNTUM lAUEINUM, XT. lAUEI NOBIMS, L. Prep. 1. (Ph. Lusit.) Suet (softened by heat), 8 oz. ; laurel oil (expressed oil of bay), 1 lb. ; oil of turpentine, IJ oz. This is the ' nervine balsam ' and ' nervine ointment ' of the shops in the Peninsula, and in some other parts of Southern Europe. The Ph. Bat. 1805 added i oz. of rectified oil of amber. 2. (P. Cod.) Fresh bay leaves and berries (bruised), of each 1 lb. ; lai d, 2 lbs. ; as hem- lock ointment — Ph. L. Highly esteemed on the Continent as a stimulating friction, in bruises, strains, slifl' joints, &c. ; and in deaf- ness. 3. (Trade.) From fresh bay leaves, 2 lbs. ; bay berries, 1 lb. ; neat's-foot oil, 5 pints ; boil as last; to the strained oil add, of lard suet, 3 lbs., true oil of bay, J lb., and allow it to cool very slowly, in order that it may 'grain' well. Sold for laurel ointment and common oil of bay. Ointment of Lavender (Baume). Syn. Oleum Lavandula. Prep. Lard, 2^ lbs. ; lavender flowers, 10 lbs.; white wax, 3 oz. Melt the lard, digest with 2 lbs. of the flowers for two hours, and strain; repeat this with fresh flowers till all are used ; melt the oint- ment and leave it at rest to cool ; separate the OINTMENT 1177 tnoisturc and dregs, and melt the (nntment with the wnx. Ointment of Lead. 5y». (UjrotrENTCM FtiruBi, U. tiTHABOTEI — P. Cod.) Prep. 1. Litharge, 3 oz. ; distilled vinegar, 4 oz.; olive oil, 9 oz. ; mix with heat, and stir until they combine. Camphor, morphia, and opium are common additions to lead ointment, when an anodyne effect is desirable. 2. (Compound ; Neutbal ointment, His- oin's o.. Kibifands' o.; Unouentum nbti- tbalb, u. plumbi compositum — ph. l.) Lead plaster, 2 lbs. ; olive oil, 18 fl. oz. ; mix by a gentle heat, and add of jprepared chalk, 6 oz. ; lastly, add of dilute acetic acid, 6 fl. oz., and stir well until the mass hss cooled. As a dressing in indolent nlcers, " but its utility is doubtful." (Dr Garrod.) Ob». It will bo observed that the College has already modified the old formula of this ointment. The vinegar is now the last ingre- dient added to the mass. " Gradually add the clialk, separately mixed with the vinegur, the effervesctiice being finished, and stir," &c. (Ph. L. 1836.) 8l'(! Acetate op Lead, Cab- BONATE OP L., CmOBIDS OP L., lODIDE OP L. ; Eye, Godlabd's, Lb Moet's, and other ointments contulning lead. Ointment, Le Mort's. Carbonate of lead, corrosive sublimate, lithsrge, and Venice tur- pentine, of each 1 oz. ; alum, \ oz. ; lard, \ lb. ; vermilion, q. s. to colour. Ointment of Ln'puline. Syn. Unguentcm HTPUlJNiE, L. Frep. (Soubeiran.) I.upu- line, 1 part; lard, 3 parts; digest by the heat of a water bath for 5 or 6 hours, and strain. As an anodyne dressing to cancerous niceis, and as a friction to swollen and painful joints. Ointment of Lycopo'dinm. Syn. Unouen- tum LTCOPODII, L. Prep, Lycopodium, 1 dr. ; balsam of Peru, \ dr. ; simple ointment, 1 oz. In chaps aud excoriations. Ointment of Mace. Syn. Unouentum ma- CI0I8, L. Pref. From nmce (beaten to a paste) and jiiilm oil, of each 1 lb. j purifitd beef marrow, 3 Ihs. ; gently melted together, and strained. Emollieiit and stimulant; chiefly used as a pomade for the hair. Sold for ' common oil of miice.' Ointment of Marshmariow. Syn. Un- ouentum aitbje;e, DiAiTHisa;, L. Prep. 1. (Ph. L. 1746.) Oil of mucilages, 2 lbs. ; bees- wax, i lb. ; yellow resin, S oz. ; melt them together, then aild of Venice turpentine, i oz. ; and stir the mixture until it concretes. 2. (Wholesale.) From palm oil, i lb. ; yel- low re>in, \\ lb.; beeswax, 2^ lbs.; pule lin- seed oil, 9 lbs. (sny 1 gall.) ; melt together and stir until it is nearly cold. Use%, ifc. Emollient and stimulant ; seldom used in regulnr practice, but in great repute umouff^t the common people. Linseed oil is now almost universally substituted for the oil of murilnges. Ointment of Uaster-wOTt. Syn. Pommade ANTI-CANCtluasE BB MiLIUS ; UnOUENTUM iMPEEiTOHia;, L. Prep. (Beasley.) Pow- dered master-wort {Imperatoria Ostruthium), 1} oz. ; tincture of muster-wort, 1 oz. ; lard, 2oz. Ointment of Katlco (Mr Young). Syn. Unouentum matico. Prep. Powdered matico, 3 drams ; opium, 3 gr. ; lard, 1 oz. Ointment, Merca"rial. Syn. (.Strung meb- CUEIAL ointment, BlUE O., NEAPOLITAN o.; Unouentum htdbaeotei — B. P., Ph. L. E. & D., U. H. FOETIUS, U. CiEEULEUM.) Prep. 1. (B. p.) Mercury, 16; prepared lard, 16; prepared suet, 1; rub together until me- tallic globules cease to be visible. See slso Ointment, Meecueiai (Compound). 2. (Ph. L. & E.) Mercury, 1 lb.; lard. Hi oz. ; suet, i oz. j rub the mercury with the suet and a little of the lard, until globules are no longer visible ; then add the remaining lard, and triturate altogether. 3. (Ph. D.) Pure mercury and lard, of each 1 lb. ; as before. Pur., ifC. The ' stronger mercurial oint- ment' of the shops is usually mude with a less quantity of mercury than tlmt ordered by the Colleges, and the colour is brought up with finely ground blue black or wood char- coal. This fraud may be detected by Its Infe- rior sp. gr., and by a portion being left undis- solved when a little of the ointment Is treated first with ether or oil of turpentine, to remove the fat, and then with dilute nitric acid, to remove the mercury. When made according to the instructions of the Ph., its sp. gr. is not less than 1-781 at 60° Fahr. It " is not well prepared so long as metallic globules may be seen in it with a magnifier of 4 powers." (I'h. E.) When rubbed on a piece of bright copper or gold, it should immediately give it a coating of metallic mercury, and a silvery appearance. The Vng. hyd. fort, of the wholesale houses is generally made of mercury, 12 lbs., suet, li lb., and lard, 16J lbs. It thus con- tains only \ instead of \ its weight of mer- cury. That of the same bouses labelled 'Ung. hyd. partes aquales ' is prepared with mercury, 12 lbs. ; suet, li lb.; lard, 134 lbs. Uses. This ointment is chiefly used to intro- duce mercury into the system when the sto- mach is too irritable to bear it ; in syphilis, hepatic affections, hydrocephalus, &c. For this purpose, i to 1 dr. is commonly rubbed into the inside of oneof the thighs until every particle of the ointment disappears. This operation is repeated night and morning until the desired effect is produced, and should be, if possible, performed by the patient himself. During its administration the patient should avoid exposure to cold, and the use of fer- mented or acidulous liquors, and his diet should consist chiefly of toast, broth, gruel, milk-and- water, and other inoffensive matters. This ointment has been employed to prevent the ' pitting' in smallpox ; and, diluted with 3 or 4 times its weight of lard, in several skin dis- 1178 OINTMENT eases, as a dressing for ulcers, to destroy pediculi, &c. Camphor is often added to this ointment to increase its activity. With the addition of a little extract of belladonna, or hydrochlorate of ammonia, it forms an excel- lent anodyne and resolvent friction in painful syphilitic tumours and glandular enlarge- ments. Obs. The preparation of mercurial ointment according to the common plan is a process of much labour and difficulty, and usually occu- pies several days. The instructions in the Pharmacopoeias are very meagre and unsatis- factory, and, so far as details go, are seldom precisely carried out. Employers grumble, and operatives become impatient, when they find the most assiduous trituration apparently fails to hasten the extinction of the globules. To facilitate matters, various tricks are re- sorted to, and various contraband additions are often clandestinely made. Among the articles referred to, sulphur and turpentine are those which have been longest known, 9nd, perhaps, most frequently employed for the purpose ; but the first spoils the colour, and the other the consistence, of the ointment ; whilst botli impart to it more or less of their peculiar and respective odours. On the Con- tinent, oil of eggs was formerly very generally used for the purpose, and is even now occa- sionally so employed. Nearly half a century ago Mr W. Cooley clearly showed that the difficulty might be satisfactorily overcome by simply triturating the quicksilver with -j to i of its weight of old mercurial ointment, before adding the lard ; and that the effective power of this substance was in direct proportion to its age, or the length of time it had been ex- posed to the air. His plan was to employ the ' bottom' and ' scraping' of the store pots for the pnrpose. At a later period (1814-15) Mr Higginbotto'ti, of Northampton, repeated this recommendation, and at length the plan has been imported into the Pharmacopoeia Borus- sica. About twenty years since, *' we re- opened an investigation of the subject, which extended over several months, during which we satisfied ourselves of the accuracy of the assertion of M. Roux, that the mercury in mercurial ointment exists entirely, or nearly so, in the metallic state, and not in the form of oxide, as was generally assumed. We suc- ceeded in preparing an excellent sample of mercurial ointment by agitating washed suet and qui(^ksilver together in vacuo. The quan- tity of oxide present at any time in this oint- ment is variable and accidental, and is largest in that which has, been long prepared ; but in no case is it sufficient to materially discolour the fat after the metallic mercury is separated from it. We were led to conclude that the property alluded to, possessed by old ointment, depends solely on the peculiar degree of con. sistence or viscidity of the fat present in it, and on the loss of much of the thoroughly greasy, 'anti-attritive' character, possessed by the latter in a receut state. In practically working out this idea we obtained pure fats (MAQ-HEIIO ADEPS; SBVUM PBiEPABAIUM), which, without any addition, were capable of reducing, in a few minutes, 8, 16, 32, and even 48 times their weight of mercury. We also found that the formula of the Pharmacopoeia might be adopted, and that a perfect ointment might be readily obtained by skilful manage- ment in from half an hour to an hour, even without these resources. All that was necessary was to employ a very gentle degree of heat by either performing the operation in a warm apartment or by allowing the mortar to re- main filled with warm water for a short time before using it. Suet or lard, reduced either by gentle warmth or by the addition of a little almond oil to the consistence of a thick cream, so that it will hang to the pestle without run- ning from it, will readily extinguish 7 or 8 times its weight of running mercury by simple trituration. The exact temperature must, however, be hit upon, or the operation fails. This fact was afterwards noticed in the ' Ann. de Chim.,' and some other journals." (A. J. Cooley.) M. Pomonti has proposed a method of pre- paring strong mercurial ointment, which, modified to suit the English operator, is as follows : — Fresh lard, 8 parts ; solution of nitre (see below), 1 part; mix by trituration, add of mercury, 32 parts, and again triturate. The globules disappear after a few turns of the pestle, but reappear in a few minutes, and then again disappear to return no more. When this happens, the trituration is to be continued for a few minutes longer, when lard, 24 parts, is to be rubbed in, and the ointment at once put into pots. It is said that the globules are so completely extinguished as to escape detection, even when the ointment is examined by a microscope of low power. The Solution. — Nitre, 100 gr. ; water, 1 fl. oz. ; dissolve. This quantity is sufficient for a kilogramme of mercury. M. Lahens strongly recommends for the rapid preparation of mercurial ointment the application of oil of almonds in the following proportions : — Mercury, 1000 parts j oil of almonds, 20 parts ; lard, 980 parts. The mercury is first triturated with the oil for about fifteen minutes, after which its globules are said to be no longer discernible by the naked eye; 200 parts of the melted lard are now added, and the trituration continued to the complete extinction of the metal, which is generally accomplished within an hour. The ointment is then mixed with the remainder of the lard. See Ointment op Oxide op Mebcukt. Ointment, Mercurial (Milder). Mildeb blub OINTMENT, TeOOPEE'S O., UNOTION; UhSTTEN- XUM HTDBAEGTBI MITIUS, U. CJEBTTLEUM MiTius. Prep. 1. Stronger mercurial oint- ment, 1 lb. ; lard, 2 lbs. Dose, S(e. In the itch and several other OINTMENT 1179 cutaneous diteanes, as a dressing to syphilitic ulcers, to dctroy pcdiculi on the body, &c. Each drnchm contains 10 gr. of mercury. That of theshops generally contains considerably less. 2. (With 80APJ Unocentum hydbaeqtei BAPOMACEtTM ; Savon mbecueikl). — o. (Dra- per.) Mercurial ointment (softened by a gentle heat), 1 oz. ; hydrate of potassa, 1 dr., dissolved in water, J fl. oz. ; triturate them together until the mass solidiRes. 4. (Swedinur.) Milder mercurial ointment, 8 parts ; soft soap, 2 parts ; camphor, 1 part. In periostitis, engorgements of the testicles, soft corns, 4 c. See Ointmbkt op Niteate op Mebocry, &c. Ointment, Mercurial (Compotuid), B. P. Mer- curial ointment, 6; yellow wax, 3; olive oil, 3; camphor, 1). Melt the wax and oil, and when the mixture is nearly cold, add the cam- phor in powder and the mercurial ointment, and mix. Ointment, Mercurial, with Hydrochlorate of Ammonia. Dupuytren. Syn. Unoukntdm IIYDIIAEGYEI CUM AMMONIA; MUEIATE. Prep. Stronger mercurial ointment, 2 oz. ; hydro- chlorate of ammoni!!, 1 dr. Ointment, Mercnrial, with Soda. (F. H.) Sj/n. UnGUENTDM nYDEAEOYEI CUM SODA, Savon MKncuHiEL. Prep. Mercurial ointment, 3^ oz. ; solution of soda, 3 oz. ; triturate until they combine. Ointment of Mercury, Oleate of. (U. C. Hosp.) til/n. LlNIMENTDM HYDEAUOYHI OLEATIS, UnOPENTITM BYDKABGYRI OLBATIS. (10 per cent.) Prep. Yellow peroxide of mercury, 1 dr. ; pure oleic acid, 10 dr. To the oleic acid kept u^;itated in a mortar, sprinkle in tlie peroxide gradually, and triturate fre- quently during 24 hours, until the peroxide is dissolved, and a gelatinous solution is formed, 20 per cent, as above, using double the quan- tity of yellow oxide. To be applied with a brush, or spread lightly over the part with the linger. In persistent inflammation of the joints. Professor Marshall adds to 3j of the above preparation, 1 gr. of morphia — the pure alkaloid — not one of its salts, which are inso- luble in oleic acid. In the preparation of ointment of oleate of mercury it is of the utmost importance that the mercurii' oxide should be thoroughly dry, and filrtlicr that it should be sifted in small portions at a time upon the surface of the oleic acid, each fresh portion being well incorporated before another is added. Solution should be promoted by frequent stirring, at ordinary temperatures, since experience has shown that all heating is positively injurious.' Ointment of Hercnry, Yellow Oxide of. (U. S. Ph.) Syn. Unquentum hydearoyei, OxYDi FLAvr. Prep. Yellow oxide of mer- cury, 1 dr. ; simple ointment, 420 gr. Ointment of Uete'reon. Syn. UNQUENTtTM MEZEBKi, L. Prep. 1. (Hamb. Cod.) Alco- holic extract of mezereon, 2 dr. ; dissolve in ' C. Rice. rectified spirit, q. s. ; add it to white wax, 1 oz. ; lard, 8 oz., and mix by a gentle heat. 2. (P. Cod.) Mezereon (dried root-bark), 4 oz. ; moisten it with rectified spirit, bruise it well, and digest it for 12 hours, at the heat of boiling water, in lard, 14^ oz. ; then strain with pressure, and allow it to cool slowly ; lastly, separate it from the dregs, remelt it, and add of white wax, \\ oz. Used as a stimu- lating application to blistered surfaces and in- dolent ulcers. 3. (P. Cod.) Eihereal extract of mezereon, 176 gr. ; lard, 9 oz. ; white wax, 1 oz. ; recti- fied spirit, 1 oz. ; dissolve the extract in the alcohol, add the lard and wax, heat moderately, stir until the spirit is driven olf, strain and stir till cold. Ointment of Monesia. Syn. UsorENTUn MONESI^. Prep. Oil of almonds, 4 parts ; white wax, 2 parts ; extract of monesia, 1 part ; water, 1 part. Ointment of Mustard. t 21 hours, and add of melted lard, 1 oz. Ointment of Oxide of Lead. See Ointment, Lea«. Ointment of Oxide of ]IIan"ganese. Syn. Unocentum masoanesii oxtdi, U. m. bin- OXIDI, L. Prep. 1. Black oxide of manga- nese (levigated), 1 dr. j lard, 1 oz. j mix by patient trituration. As a friction in scrofu- lous swellings and indurations; and in itch, scald-head, chilblains, &c. 2. (W. Cooley.) Binoxide of manganese, 1 dr. ; sulphur, 2 dr. ; lard, 9 dr. ; cajeput oil, 16 drops. As the last; also as a friction in rheumatism, swelled joints, &c., and in porrigo, and some other skin diseases. Ointment of Oxide of Mer'cnry. Under this name the two ointments noticed below are often confounded, owing to the different opinions held respecting the atomic weight of mercury : — 1. Ointment of Grey Oxide of Mer'cury. Syn. Ointment op suboxide of mkecitet, 0. op peotoxide op M.t ; XJnouentum hy- dbaeqybi oxtdi, U. h. stjboxydi, U. h. o. oiNEBKr, L. Prep. 1. (Ph. E. 1817.) Grey oxide of mercury, 1 oz. ; lard, 3 oz. ; triturate together. Formerly proposed as a substitute fdr mercurial ointment, but in practice it has been found useless as a friction, owing to the unctuous matter only being absorbed, whilst the oxide is left on the surface. This objection does not apply to the following prepara- tions : — 2. (Donovan.) Grey oxide of mercury, 20 gr. ; lard, 1 oz. ; mix, and expose them to the temperature of 320° Fahr. for 2 hours, con- stantly stirring. Grey coloured. It may also bo made from the nitric- or red-oxide in the same way, by keeping the ointment heated to about 300° for some hours. Cleaner and stronger than Ung. hyd. fort. — Ph. L. 3. (Tyson.) Black oxide of mercury (pre- pared by decomposing precipitated calomel with liquors of potassa and ammonia), 2 oz. ; lard, 1 lb.; triturate together. Inferior in activity to the last. It closely resembles in appearance a fine sample of mercurial oint- ment. 2. Ointment of Red Oxide of Mercury. Syn. UnGUENTUM HYDEABOYBI BINOXIDlf, U. H. OXYDI BUBKI, L. Prep. (Cazenave.) Red oxide of mercury, 30 gr. ; camphor, 5 gr. ; lard, 1 oz. Closely resembles ointment of nitric oxide of mercury, over which it, per- haps, possesses some advantage from the oxide being in a more minutely divided state. Ointment of Oxide of Sil'ver. Unouentum ABOENTl OXYDI, L. Prep. (Serre.) Oxide of silver, 16 to 20 gr. ; lard, 1 oz. As a dressing for scrofulous and syphilitic sores, &c. Ointment of Oxide of Zinc. Syn. Zinc oint- ment; NIHIL ALBUM OINTMENT+ ; UxaUEN- tum zinci (B. p.. Ph. L., E., & D.), U. oxtdi ZINCI, L. Prep. 1. (Ph. L.) Oxide of zinc, 1 oz. ; lard, 6 oz. ; mix them together. 2. (Ph. E.) Oxide of zinc, 1 oz. ; simple liniment (Ph. E.), 6 oz. 3. (Ph. D.) Ointment of white wax, 12 oz. ; melt it by a gentle heat, add of oxide of zinc, 2 oz. ; and stir constantly until the mixture concretes. 4. (B. P.) Oxide of zinc, in very fine pow- der, 1 ; bf nzoated lard, 5i ; mix. 1182 OINTMENT Uses, Sfc. Astringent, desiecative, and stimu- lant; in excoriationSf biirns, various skin dis- eases attended by profuse discharges, in chronic inUammation of the eyes depending on relaxa- tion of the vessels, in sore nipples, indolent sores, ringworm of the scalp; &e. It is an excellent and very useful preparation. See OiNTMBNT, Ttjttt (beloie). Ointment of Pep per. Syn. UxsuENTUM PiPEBis NiaEl, L. Prep. 1. Black pepper (bruised), 1 oz. ; lard, 2 oz. ; suet, 1 oz. ; di- gest together in a covered vessel, bythe heat of a water bath, for six hours, then strain, with pressure, add of expressed oil of mace, 2 dr., and stir until the mixture concretes. In piles, itch, as a friction in rheumatism, &c. 2. (Ph. U. 1826.) Black pepper (in fine powder), 4 oz. ; lard, 1 lb. ; mix. In scald- head, &c. Ointment of Phosphor'ic Acid. Si/n. Uir- GUENTUM AOIDI PHOSPHOEICI, L. JPrep. (Soubeiran.) Phosphoric acid, 1 dr.; lard (softened by he:it), 1 oz ; triturate carefully togetlier. As a friction in caries, osseous tumours, &c. Ointment of Phos'phorus. S^n. UiratrEif- TUM PH08PH0KI,U. PHOSPHOKATUM, L. Frep. (P. Cod.) Phospliorus, 1 dr. ; lard, 6 oz. 3 dr. ; uielt together (iu a wide-mouthed bottle) by the heat of a water bath, remove the vessel from the heat, and shake it briskly until the ointment concretes. As a friction in gout, chronic rheumatism, and several skin dis- eases. Ointment of Picrotox'in. Si/n. Unguentum PiCEOTOXiKji:, L. Frep. (Jajer.) Picro- toxin, 10 gr. ; lard, 1 oz. In ringworm o( the scalp, and to destroy pediculi. It should be used with care. Ointment for Piles. Si/n. Unguentum h^- MOKEHOIDAIE, U. ANTI-n.EMOEEnOIDALE, L. Prep. 1. Burnt alum and oxide of zinc, of each i dr. ; lard, 7 dr. 2. (Bories.) Acetate of lead, 15 gr. ; freshly burnt cork, i oz. ; washed h esh butter, 2oz. ; triturate well together. 3. (W. Coolcy.) Morphia, 8 gr. ; melted spermaceti ointment, .1 oz. ; triturate together until solution is complete, then add, of galls (in impalpable powder), IJ dr., essential oil of almonds (genuine crude), 12 to 15 drops, and stir until the mass concretes. In painlul piles, prolapsus, &c. It is not only very effective, but does not soil the linen so much as most other ointments. 4. (Dr Gedding.) Carbonate of lead, 4 dr. ; sulphate of morphia, 15 gr. ; stramonium ointment, 1 oz. ; olive oil, q. s. When there is much pain and inflammation. 5. (Sir H. Halford.) Ointment of nitrate of mercury and oil of almonds, equal parts, triturated together. 6. (Mazziui.) Nitrate of morphia, 15 gr. ; citrine ointment, 1 dr.; fresh butter, 1 oz. As the last. 7. (Vallez.) Extract of elder leave«, I dr. ; burnt alum, 16 gr.; poplar ointment, 1 oz. For other formulae, see the respective names of their leading ingredients. 8. (Ware.) Camphor, 1 dr. ; simple ointment, 1 oz.; dissolve by beat, add of powdered galls, 2 dr.; mix well, further add of tincture of opium, 2 fl. dr., and stir until the whole is cold. In flabby mucous and painful piles. 9. (Zanin.) Spermaceti ointment, 1 oz. ; powdered galls, 1 dr. j powdered opium, 18 gr. ; solution of diacetate of lead, 1 fl. dr. When there is both pain and inflammation, 10. (From New Kemedies.) Yellow wax, 8 parts; resin, 4 parts; lard, 12 parts; oil of sassafras, 2 parts. Melt the wax, resin, and lard, remove from the fire, add the oil of sassafras, and stir until the mass is solid. This is said to be a most excellent application for painful or itching piles. Ointment of Pitch. Si/n. Black basilicon, Ointment of black pitch ; Ung. picis (B.P., Ph. L.),U. PiciSNiGB^, L. Prep. 1. (Ph. L.) Black pitch, resin, and beeswax, of each 11 oz.; olive oil, 1 pint; melt together, strain through a linen cloth (and stir until the mass concretes). 2. (B. P.) Tar, 5; yellow wax, 2; melt together, and stir till cold. Uses, iSfc. Stimulant and detergent; very useful in indolent ulcerations, scald-head, and various foul eruptions. In itch and psoriasis, and other scaly skin diseases, a little sulphur is commonly added to it. Ointment of Plat'innm. Sm. Ungubntum: PLATINI, L. Peep. (Hcefer.) Bichloride of pla- tinum, 15 gr.; extract of belladonna, i dr.; lard, 1 oz. As a dressing for painful indolent ulcers. Ointment of Plumbago. Syn. Ointment OP GKAPHITE; UkGUENTTTM GBAPHITIS, U. PLUjiBAGiNis, L. Prep. From pure plumbago ('bl.ick-lead'), IJ dr.; lard, 1 oz. As a dressing to ulcers, and in certain skin diseases. Ointment, Plunket's. Prep. (Original for- mula.) Crowsfoot, 1 h.andful; dog's fennel, 3 sprigs; pound well, add of flowers of sulphur and white arsenic, of each 3 thimblefuls ; beat them well together, form the mass into bo- luses, and dry them in the sun. For use, pow- der them ; and mix the powder with yolk of egg, spread a little on a small piece of pig's bladder (size of half a crown), and apply it to the sore, where it must remain until it falls off by itself. Poisonous; in cancer; with great caution. Ointment, Poma'tum. See Ointment, Labd. Ointment of Pop'lar Buds. Si/n. Unguen- TUM POPULEUM, L. Prep. 1. Fresh poplar buds (bruised), 1 part; lard, 4 parts; boil until crisp, and strain. It never gets rancid. Emollient and stimulant. 2. (Compound— P. Cod.) Poplar bud*, 12 oz. ; fresh leaves of belladonna, common night- j^hade (Solanum nigrum), henbane, and poppies, of each 8 oz. ; lard, 4i lbs.; as the last. Emollient, stimulant, and anodyne. Ointment of Potas'sio-tar'trate of An'timony. OINTMENT 1183 Si/n. Antimonial ointment, Tabtae emetic O. ; UnoUEKTDM ANTIMONII TAKTABATI (U.P.), UnOUENTCM ANTIMONII POTA9SIO-TABTATEI8 (Hi. I-.). U- A- TAETAEIZATI (Ph. D.), U. ANTIMONIALE (Pll. E.), U. TA8TAEI EMETICI, li. Prep. 1. (Ph. L. & E.) Potasaic tar- trate of antimony, rubbed to a very fine powder, 1 oz. i lard, 4 oz. ; mix by trituration. 2. (Ph. D.) Tartar emetic, in very fine piiwder, 1 dr.; ointment of white wax, 7 dr. 3. (B. P.) Tartrated antimony (in fine pow- der), I ; simple ointment, 4. Mix. L'se», Jj^c. Counter-irritant; in phthisis, chronic rheumatism, certain liver atlections, and uther deep-seated pains and diseases. A portion about the size of a nut is rubbed on the skin night and morning, until a crop of pustules is produced. The part should be well rubbed with a coarse towel, so as to be reddened, before applying the ointment. The product of the Dublin formula is of only half the strength of those of the other Colleges. Obs. liuforo adding the tartar emetic to the lard it should be reduced to the state of an impalpable powder. The precipitated salt is the best for this purpose. As the pustules formed by this ointment permanently mark the skin, it should only be applied to th< sc parts qf the person which are covered by the dress. Ointment, Fur'gatlTe. See Ointment of COLOCVNTII, WoHM 0., &c. Ointment of Quinine'. Spi. UNonENTUM QUlNIiE, U. QUINIjE SULPHATIS, h. Frep. 1. Sulphate of quinine, 1 dr.; lard, 3 dr. lu the agues of children. 2. (Boasley eaAntonini.) Sulphate of qui- nine, 1 dr.; alcohol (rectified spirit), 2 dr.; sulphuric iicid, 10 drops; dissolve, and mix it with lard, i oz. In malignant intermittents ; 2 to 4 dr. at a time, rubbed into the groin or axilla. Ointment of Eed Sul'phuret of Mer'cury. jSyn. Unqukntum nYDRAKayRi BisuLpnn- USTI, U. H. BULPHOEETI EUDBI, L. frep. 1. (Alibert.) lied sulphuret of mercury, 1 dr.; camphor, 20 \zr.; simple ointment, 1 oz. In herpes, applied twice a day. 2. (Collier.) Uisulphuret of mercury, li dr.; sal ammoniac, t dr.; liird, 1 oz. ; rose water, 1 fl. dr. In several skin diseases, to diminish the itchins:, destroy pediculi, BIytlie. sago grains are already present, they often excite the contagious form of ophthalmia."' The diffusion into the atmosphere of the purulent discharge accompanying this form of ophthalmia is undoubtedly the means by which the disease is spread. Hence it is that if one ey^be affected the other may be saved from an attack by being hermetically sealed up — a method of preven- tion sometimes adopted by the ophthalmic surgeon. Mr Brudenell Carter says " that the secre- tion passes along the tear-passages into the nostrils, and is driven out with the expired air at every breath j besides the chances of direct contact that must exist when a child with oph- thaluiia is perpetually sending into the atmo- sphere what I may describe as a spray of contagious particles.'* Medical opinion is in some measure divided as to the origin of this disease ; for whilst there are authorities who believe that its propaga- tion is due to contagion assisted by insanitary environments, there are others who incline to the supposition that these latter conditions alone are sufScient to produce it. Whether this is so or not there can be no question that impure air, overcrowding, filth, and deficient water supply, which implies insufficient ablu- tion, serve to intensify and perpetuate it. So strongly and confidently impressed are Messrs Welch and Marston of the connection between unhealthy surroundings and preva- lent ophthalmia, that they regard the two as cause and effect, and state their belief " that the presence or absence of ' sago grains' affords a delicate test of the sanitary state of a school, a regiment, or any similar community." Ample and painful confirmation of these views is afforded by the prevalence of the disease amongst the children, more particu- larly those who live in very poor and crowded districts. The pitiable, blear-eyed little crea- tures that one meets with in these localities are very frequently the victims of purulent ophthalmia, and as such bear unfailing testi- mony to the insalubrity and squalor of the homes in which they dwell. Stromeyer states that he has met with the ' sago grains' in the eyelids of many domestic animals, more particularly pigs, the granules being always in proportion to the more or less dirty condition in which the animals were kept. The ahove statements plainly indicate the means by which the disease is to be combated. Of these, thorough ventilation and pure air are the most important. Stromeyer records how, by simply ventilating some barracks, he reduced to an amazing extent a number of cases of the disease, which had broken out in the Hanoverian army. Possibly this result was due to the removal, by the current of air from the apartment of the dried particles of contagious matter. » Biudenell Carter. OPIATES— OPIUM 1193 Ablution, which, carefully performed, is, in addition to ventilBtion, an important curative agent, may, through the neglect of certain precauliona, assiat to spread the disease. This it will assuredly do if the basins em- ployed by the patients for washing their eyes are not thoroughly cleansed and disinfected after bi'ing used. Furthermore, the towels may be made to spread the infection, unless they tu<> are thrown into some disinfecting solution nittT usi-, and unless a separate towel i< appro- pi iattii to each patient. The danger of rein- oculation may ensue if each towel is not changed sufficiently often. The bed-clothes of the alfeclcd persons, as well as the pillow- cases, shoiiUI he frequently renewed, the latter every day, since they collect and disseminate the discharges falling on them from the patient. Mcdiciil authorities also strongly recom- mend the isolation of the patient, and then c Taurus (Linn.), one of the rumiuantia. In its more limited sense the word is restricted to the emasculated animal. The flesh, milk, skin, horns, bones, and blood of this animal are all serviceable to man. Gold- beater's skin is prepared from the peritoneal membrane of its caecum. Its blond, fat, horns, and excrement were among the simples of the Ph. L. 1618. See Beef, Gall, Milk, and helow. Ox-Gall. Syn. Ox-bile; Fel bovinbm, F. BOVis, F. TAUBi, L. Crude ox-gall is noticed at page 774. Refined ox-gall {Fel bovinuin puri/icatum) is prepared as under : — 1. Fresh ox-gall is allowed to repose for 12 or 15 hours, after which the clear portion is decanted, and evaporated to the consistence of a thick syrup by the heat of a water bath ; it is then spread thinly on a dish, and exposed in a warm situation near the fire, or to a current of dry air, until nearly dry; it is, lastly, put into wide-mouthed bottles or pots, and care- fully tied over with bladder. In this state it will keep for years in a cool situation. For use a little is dissolved in water. 2. Fresh gall, 1 pint ; boil, skim, add pow- dered alum, 1 oz. ; boil again till the alum is dissolved, and when sufficiently cool pour it into a bottle, and loosely cork it down. In a similar manner boil and skim another pint of gall, add to it 1 oz. of common salt, and again boil, cool, and bottle it, as above. In three months decant the clear from both bottles, and mix them in equal quantities; the clear portion must then be separated from the coagulum by subsidence or filtration. Uses, S(c. Both the above are employed by artists to fix chalk and pencil drawings before tinting them, and to remove the greasiness Irom ivory, tracing paper, &e. The first is also used in medicine, OX'AIiATE. Syn. Oxalas, L. A salt of oxalic acid. The soluble oxalates are easily formed by directly neutralising a solution of oxalic acid with a metallic hydrate, carbonatn, or oxide ; and the insoluble oxalates, by double decomposition. See Oxalic acid and the respective bases. OXAL'IC ACID. HnCA- 'S'yffl. Acidum oxalioum, L. This substance was discovered by Bergman in 1776. It occurs both in the mineral and organic kingdoms, and is pro- duced artificially by the action of nitric acid on sugar, starch, woody fibre, &c. It abounds in wood-sorrel, in which it exists in combina- tion with a little potassa. With the exception of gum and sugar of milk all starchy and sac- charine substances yield oxalic acid when trented with nitric acid at a somewhat elevated temperature. Prep. 1. From sugar : — a. Nitric acid (sp. gr. 1'42), 5 parts, diluted with water, 10 parts, is poured on sugar, 1 part, and the mixture is digested at a gentle heat as long as gaseous products are evolved; the liquid is then concentrated by evaporation until it deposits crystals on cooling ; the crystals, after being drained and freed from superfiuous mois- ture, are redissolved in the smallest possible quantity of boiling water, and the solution is set aside to crystallise. The residuary 'mother- water' is treated with a little fresh nitric acid (say IJ part) at a gentle heat, after wliich it is evaporated, as before, for a second Cl'op of crystals. This process is repeated until the solution is exhausted. The brownish-coloured crystals thus obtained are allowed to effloresce by exposure to dry air, and are then redis- solved and recrystallised. By repeating this treatment they yield pure colourless oxalic acid at the third crystallisation. b. (Schlesinger.) Sugar (dried at 257° Fahr,), 4 parts, and nitric acid (sp. gr. 1'38), 33 parts, are digested together, as before, and as soon as the evolution of gas ceases the liquid is boiled down to oue sixth of its original volume, and set aside to crystallise. The whole process may be completed in about 2 hours, and iu 1 vessel, and yields of beauti- fully crystallised oxalic acid, at the first crys- tallisation, a quantity equal to 56 to 6O5 of the weight of the sugar employed. c. (Ure.) Nitric acid (sp. gr. 1-4), 4 parts, and sugar 1 part, are digested together by the heat of a water bath, and as soon as gas ceases to be extricated the vessel is removed from the heat, and set aside to cool and crys- tallise. The use of a little sulphuric acid along with the nitric acid contributes to in- crease the product. 2. From POTATO- or IiEXTEI>f-snGAB : — (Nyren.) From the washed pulp of potatoes. OXALIC ACID 1213 boileil for -ioiue hours with water, q. s., in a leaden ves.L-l, with about 23 of oil of vitriol, until the focula of the pulp is converted into •accbarine matter, shown by the liquid being no longer turned blue by iodine ; the whole is then filtered through horse-hair bags or Rtrainers, and the filtrate is evaporated until itx density is tueh that a gallon of it weighs 14 to \4ii lbs.; in this state it is converted into oxalic acid by treatment with nitric acid in the way already described. A similar pro- cess was patented some years ago by Messrs Davy, Macmurdo, and Co. 3. From sawdust : — (Roberts, Dale, & Co. Patent.) This pro- cess is the one now usually employed for the manufacture of oxalic acid on tlie large scale. It is based on Gay-Lussac's discovery, that wood and similar substances are converted into oxalic acid by fusion with caustic alkali. The practical details of the process are thus given by Dr Murray Thomson, of Edinburgh : — (1^ Hydrate of sodium and hydrate of po- tassium, mixed in the proportion of 2 equiva- lents of the former to 1 equivalent of the latter, are dissolved, and solution evaporated until of specific gravity 135 ; sawdust is now stirred in until a thick paste results. (2) This paste is then heated on iron plates, during which it is constantly stirred ; water is first given off ; tlie mass then swells ; infliimmable gases, hy- drogen and ciirburetted hydrogen, are evolved, along with a peculiar aromatic odour. When the temperature has been maintained at 400'' lor one or two hours, this stage of the process is complete ; the mass has now a dark colour, and contains only 1 to 4 per cent, of oxalic acid, and about 5 per cent, of formic acid. The bulk, therefore, of the mass at this stage consists of a substance whose nature is not yet known, but which is intermediate between the cellulnse and oxalic acid. (3) The next stage consists in a simple extension of the last, in which the muss is heated till quite dry, care being taken that no charring takes place. It now contains the maximum quantity of oxalic acid, 28 to 30 per cent. (4.) This oxalic acid now exists as oxalate of potassium and sodium in the grey powder resulting from stage 3. This powder is now washed on a filter with solution of carbonate of sodium, which seems to have the singular and unexpected power of decomposing the oxalate of potassium and converting it into oxalate of sodium. At all events, it is quite true that all traces of po- tassa are washed out with the solution of car- bonate of sodium. The only explanation that occurs to account for this unusual decompo- sition is that oxalate of sodium is a more in- soluble salt than oxalate of potassivim, and therefore may be formed by preference. (5) This oxalate of sodium is now decomposed by boiling milk of lime. Oxalate of calcium falls as a precipitiite, and soda remains in solution. This soda is boiled down, and again made use of with fresh sawdust. This recovery of alkali is also practised with thepotassinm salt which filters through in the last stage. (6) The ox- alate of calcium is now decomposed in leaden vessels with sulphuric acid. Sulphate of cal- cium is precipitated, and oxalic acid is in solu- tion, which is now evaporated, and the acid separates in crystals, which now need only to be recrystallised to make them quite pure, and fit the acid for all the purposes for which it is employed. Prod. By this ingenious process 2 lbs. of sawdust are made to yield 1 lb. of oxalic acid. Prop., S^c. Colourless, transparent, pris- matic crystals, possessing a powerful sour taste and acid reaction ; these efflDresce in warm dry air, with loss of 28g (2 eq.) of water, and then form a white powder, which may be sublimed in part, without decomposition ; the crystals are soluble in 8 parts of water (9 parts, "and form a solution ofsp. gr. 1'045," — Ure) at 60° Fahr., in their own weight or less of boiling water, and in about 4 parts of alcohol ; with the acids, it forms saltis called oxalates. Testa. — 1. Solution of chloride of barium ociMsions a white precipitate in neutral solu- tions of oxalic acid (oxalates), which is soluble in both nitric and hydrochloric acid. — 2. So- lution of nitrate of silver, under like circum- stances, gives a white precipitate, which is soluble in nitric acid, and in ammonia, and which, when heated to redness, yields pure silver. — 3. Lime water and solutions of all the soluble salts of calcium produce white pre- cipitates, even in highly dilute solutions of oxalic acid or of the oxalates, which is freely soluble in both nitric and hydrochloric acid, but is nearly insoluble in either acetic or oxalic acid, and is converted into carbonate of calcium upon ignition. — 4. Oxalic acid (or an oxalate), when heated, in the dry state, with oil of vitriol in excess, is converted into carbonate anhydride and carbonic oxide; the former produces a white precipitate with lime water, and the latter, when kindled, burns with a faint blue flame. Of the above tests, solution of sulphate of calcium (vide No. 3) is the most delicate and characteristic. — 5. It is distinguished from Epsom salt by its acid reaction, its solubility in rectified spirit, its complete dissipation by heat, and by emitting a slight crackling noise during its solution in water. See Maokbsia (Sulphate). Uses, Pais., S(c. Oxalic acid is chiefly used in the arts of calico printing and bleaching; to remove ink-spots and iron moulds from linen, and to clean boot-tops. It is extremely poisonous. The treatment, in cases of its having been swallowed, is to promote vomit- ing, and to administer chalk, whiting, or mag- nesia, mixed up with water, in considerable quantities. The use of the alkalies or their carbonates must be avoided, as the compounds which these form with oxalic acid are nearly as poisonous as the acid itself. The remain- ing treatment is noticed under Acids. In 1214 OXALURIA— OXYCHLORIDE poisoning by oxalic acid the nervous system is almost always affected, and the patients expe- rience numbness, formication of .the extremi- ties, and sometimes convulsions, so that the symptoms somewhat approach those produced by strychnia, from which it is distinguished by its corrosive action on the tissues, and its effect upon the heart and circulatory system. Concluding MemarJcs. The manufacture of oxalic acid is an important one. The process of Roberts, Dale, and Co. has so much cheap- ened the price of oxalic acid, that in 1851 it sold for 16d. per lb., and in 1864 it only cost from 8d. to 9d. per lb. More than half the amount of oxalic acid used all over the world is now made from sawdust. In manu- facturing the acid from sugar, on tlie large scale, the first part of the process is either conducted in salt-glazed stoneware pipkins of the capacity of 3 to 5 quarts each (which are about two thirds filled and set in a water batli), or in wooden troughs lined with lead, and heated by means of a coil of steam-pipe. On the small scale, a glass retort or capsule is commonly employed. The most appropriate temperature appears to be about 125° Fahr. and the best evidence of the satisfactory pro- gress of the decomposition is the free but not violent evolution of gas, without the appear- ance of dense red fumes, or, at all events, any marked quantity of them. When these are disengaged with violence and rapidity, a greater quantity of the newly formed acid suffers decomposition, and flies off in a gaseous form. Thesp. gr. of the nitric acid commonly used on the large scale ranges from 1'22 to 1'27 equivalent quantities being taken. The evaporation is preferably conducted by the heat of steam. The evolved nitrous vapours are usually allowed to escape, but this loss may he in part avoided by conveying them into a chamber filled with cold damp air, and containing a little water, when they will absorb oxygen, and be recondensed into fum- inar nitric acid. Various modifications of this plan have been patented. That of Messrs McDougall and Rawson, which is one of the simplest and best, consists in passing the mixed nitrous fumes through a series of ves- sels containing water, and connected together by tubes, so that the fumes which collect at the top of one vessel are conveyed to nearly the bottom of the next one, and then, bubbling up through the water, mix with the air, a supply of which is provided for the purpose. The nitrous fumes are thus brought alternately into contact with air and water, and by the time they reach the last vessel are reconverted into nitric acid. Another plan is to pass the mixed nitrous vapours through a vessel stuffed with some porous substance, as pumice-stone or pounded gl.iss, conjointly with a supply of steam from a boiler and a supply of ox^ gen by a blowing machine. The product obtained by skilful Tuanipu- lation are — from good dry sugar, 128J| ; from good treacle, lO^g. — " One cwt. of good treacle will yield about 116 lbs. of marketable oxalic acid, and the same weight of good brown sugar may be calculated to produce about 140 lbs. of acid." " As a general rule, 5 cwt. of saltpetre, or an equivalent of nitrate of soda, with 2i cwt. of sulphuric acid, will generate suffi- cient nitric acid to decompose 1 cwt. of good sugar, and yield, as above, 140 lbs. of fair marketable oxalic acid, free from superfluous moisture." (Ure.) On the small scale, 5 parts of sugar yield nearly 6 parts of crystallised acid. Chemically pure oxalic acid is best prepared by precipitating a solution of binoxalKte of potassium with a solution of acetate of lead, washing the precipitate with water, decom- posing it, whilst still moist, with dilute sul- phuric acid or sulphuretted hydrogen, and gently evaporating the filtrate so that crystals may form as it cools. OXALUBIA. Also known as the oxalic-acid diathesis ; is an abnormal condition of the system, marked by the presence in the urine of crystals of oxalate of lime. The crystals occur as minute transparent octahedra, and sometimes iu the form of dumb bells. They can be easily recognised under a microscope with a power of from 200 to 250 diameters, when they present a very beautiful appearance. They differ from phosphatic deposits in being insoluble iu acetic acid. Their presence is mostly indicated by the appearance in the urine of a cloud of mucus, which forms alter the urine has stood some little time. Oxaluria most generally affects persons of dyspeptic and sedentary habits and of nervous temperament ; those suffering from skin affections and neuralgia are also 'occasionally attacked by it. In ordinary cases the treat- ment consists in the administration of the nitro-hydrochloric acid, in infusion of gentian two or three times a day, or of a course of quinine and iron, aided by plenty of exercise in the open air, care being taken to avoid fatigue. If it can be borne the shower hath should also be had recourse to. Rhubarb tarts and tomatos, which contain oxalic acid, must be excluded from the diet ; so also should aerated water and too much sugar. If after a short time the oxalates should not disappear from the urine under this treatment, the patient should seek proper medical advice ; since the persistent presence of this deposit is of very serious significance, as indicating the existence in the bladder of that dangerous form of urinary concretion known as 'mul- berry calculus.' OXIDA'TION. St/n. Oxtdation. The combination of bodies with oxygen, forming oxides,; the operation or process adopted to induce or facilitate such conversion. OX'IDE. Sy». Oxtb; Oxtdum, L. A compound formed by the uuion of oxygen with another body. I OXYCHLCRIDE. Syn. Oxiohlomde; OXYCRATE-OXYGEN 1216 OXTCHIOBIDUM, L. A term often loosely applied to compounds of an oxide und chloride, whether in definite or variable proportions. See Antimokt (Oxychloride), &c. OXYCRATE. St/n. Oxyobatcm, L. The old name of a mixture of vinegar and water, dulcified with honey. OXYCRO'CEUU. See Plastebs. OXYGEN. O. Sgn. Oxtoen oas, Db- FIILOOISTIOATED AIBf, EUPyBEAL A., VlTAL A.t i OxTGENinM, L. An elementary body discovered by Sclieele and Priestly in 1774. It is remiirltRble that, although this substance forms a large proportion of our atmosphere (nearly one fourth), and confers upon it the power of supporting respiration and combus- tion, and also constitutes the principal portion or the water of our rivers and seas (eight ninths), and enters largely into the compo- sition of the majority of the various minernl bodies that form the bulk of our globe, its existence should have remnined unsuspected, or atleust undetermined, until a comparatively recent date. Oxygon is an essential con- stituent of all living organisms. It is absorbed by animals during respiration, and evolved in a free state by growing vegetables when exposed to sunlight. The oxygen gas of the atmosphere is mechanically mixed, not chemically combined, with tlie nitrogen. I'rep, 1. From red oxide of mercury, heated over a spirit lamp or a few pieces of ignited charcoal. The operation is usually performed in a small green-glnss retort, or in a short tube of hard Bohemian ghiss, closed with n perforated cork furnished with a piece of bent glass tube of small bore, to couvey the liberated gas to the vessel arranged to receive it. Pure. 1 oz. yields about 100 cubic inches. 2. From chlorate of potassium, as the lost. Pure. 100 gr. yield nearly 100 cubic inches (Brande ; 115— Ure). This is the plan adopted in the P. Cod. The decomposition occurs with both the above subatances at a heat below that of redness. 3. From a mixture of chlorate of potassium (in coarse powder), 3 parts ; powdered biuox- ide of manganese, 1 part; both by volume. Pure. 100 gr. of the mixture yield about 110 cubic inches as oxygen. This method, which has received the approval of Faraday, is exceedingly convenient. The gus is evolved with a rapidity which is entirely at the com- msnd of tlie operator by simply increasing or lessening the heat. The residuum in the iitort may be kept for another operation, if not exhausted ; or it may be at once washed out with 11 liltle warm water, and the man- ganese, which is uninjured by the process, reserved for future use. Red lead, black oxide of cuppef, red oxide of iron, and several other Bubstanres, answers nearly as well as binuxide of manganese. 4. From n mixture of bichromate of potas- sium, 3 parts; oil of vitriol, 4 parts; gently heated, as before. Yields pure oxygen very freely, and with a rapidity entirely at the will of the operator. (Balmain.) 6. From binoxide of manganese and oil of vitriol, equal parts ; as the last. 44 gr. nf pure binoxide of manganese yield 8 gr., or 24 cubic inches, of oxygen ; 1 oz. yields 88 gr., or 256 cubic inches. (Liebig.) 6. (On the large scale.) — a. From nitre ex- posed to a dull red heat in an iron retort, or gun-barrel. 1 lb. yields about 1200 cnbic inches of gas, contaminated, more or less, with nitrogen. (Ure.) b. From binoxide of manganese, as the last. 1 oz. of the pure binoxide yields 44 gr., or 128 cubic inches, of oxygen (Liebig); 1 lb. of good commercial binoxide yields from 1500 to 1600 cubic inches, or from 5 to 6 galls. c. M. Boussingault has reinvestigated a process, long known, although not usefully applied, by which pure oxygen gas may be obtained from the atmosphere at a trifling cost, so as to enable it to be collected in unlimited quantities and preserved in gas- ometers, like coal-gas, for application in the arts, manufactures, and sanitation. This process depends upon a peculiar property possessed by the earth baryta, of absorbing atmospheric oxygen at one temperature and evolving it at another; or rather, the ready conversion of hydrate of barium into peroxide of barium by a current of atmospheric air at a dull red heat, and the decomposition of this peroxide, by steam, at a lower temperature, even at 212^ Fuhr., with reproduction of hydrate of barium, the process being in reality a continuous one. The baryta is mixed with a portion of hydrate of calcium or of magne- sium, and the mixture being placed in an appropriate earthen tube heated to dull red- ness, is oxidised by passing a current of dry atmospheric air over it. As soon as the oxida- tion is complete, the tube is conuccted with the gas-holder, and a jet of steam allowed to act upon it; this reconverts the peroxide of bcirium into hydrate of barium, the excess of oxygen being given off and collected in the gas-holder. The baryta is then again oxidised by a fresh current of air and deoxidised by steam, and the whole process is repeated as frequently as required. Oue ton of baryta, thus treated, is capable of yielding 2500 cubic feet of pure oxygen every 24 hours; and this, as it does not waste or lose its properties, at tlie mere cost of the fuel and labour required in the process. d. Prom ferrate of potassium, prepared on the large scale. When exposed to moisture or thrown into water, pure oxygen is evolved. This method has been successfully adopted to maintain the air of diving-bells, and of other confined spaces, in a state fit for respiration. c. The decomposition of sulphuric acid has been recommended by JIM. Devilleand Debrfiy as a means whereby large quantities of oxygeu 1216 OXYGEN gaa may be obtained at a low price. Into a tabulated retort are put fragments of fire brick, and upon these, when raised to a full red heat, sulphuric acid is made to fall drop by drop, by passing through an iron tube, which passes through and is luted to the tubulure. The tube reaches to the bottom of the retort, and the acid is poured into it through a bent funnel. The sulphuric acid becomes decom- posed into sulphurous anhydride, oxygen, and water. The volatilised products are sent through a spiral condenser, by which the water and any undeoomposed acid become liquefied ; whilst the sulphurous acid is removed by sub- sequent washing with water, and oxygen is collected in the usual manner. f.' A process for obtaining oxygen on a large scale, and which has been made tlie subject of a patent in this country, has been devised by MM. Marechal and Tessie du Mothay. It consists in heating in a current of steam the manganatos, permanganates, chromates and ferrates of the alkalies and alkaline earths, and regenerating the residue by passing air over it at a red heat, g. Mallet procures oxygen in large quanti- ties as follows : — He puts into retorts revolv- ing on horizontal axes, a mixture of cuprous chloride, and kaolin or sand. He moistens this with water, heats it to 100° C, and passes air through the retorts for some hours. His oxygen he obtains from heating the resulting cupric oxychloride to about 400° C. ; the aqua residual cuprous chloride becomes converted into oxychloride on cooling 100 kilograms of cuprous chloride, after conversion into oxy- chloride, about 3 cubic metres of oxygen, 7. Oxygen oas at the oedinaet tem- PEBATCKE. Boettger states that when a mixture is made of equal weights of the per- oxides of lead and barium, and dilute HNOg of a strength of 9° Beaume is poured thereon, a current of pure O, free from ozone and autozone, is given off abundantly. This mix- ture of the two peroxides may be kept dry in a stoppered bottle for any length of time. Boettger also prepares pure oxygen, free from ozone, by submitting permanganate of potas- sium to a gentle heat. 8. Fleitman' has found that when chloride of lime in solution is heated with a small quantity of freshly prepared peroxide of cobalt, it is completely resolved into chloride of calcium and oxygen. A concentrated solu- tion consisting of 35 per cent, of chloride of lime, which must be previously filtered to pre- vent frotliing, yields when heated with t^th to i per cent, of peroxide of cobalt, a volume of oxygen from 25 to 30 times as great as that of the liquid, and always rather more than the calculated quantity, probably in conse- quence of the absorption of oxygen from the air. The remaining peroxide may always be employed again. A like result follows if, in- stead of the peroxide, an ordinary salt of » Walts. cobalt in small quantity be used. Fleitman seeks to explain the reaction on the supposition that there are several peroxides of cobalt, and that the effects produced depend upon the alternate formation and partial reduction of a higher oxide ; or on the formation of a cobaltic and a percobaltic hypochlorite, which is subse- quently decomposed into cobaltous chloride and oxygen. Prop. Oxygen gas is colourless, tasteless, inodorous, and incombustible; the sp. gr. is 1057 (Dumas; 1-1026— Berzelius & Dulong; 1111— Thomson); 100 cubic inches at 60° Fahr., and 36 inches of the barometer, weigh 34-29 gr. (Dumas; 34-109 gr.— Berz. ; 34-6 gr. — Brande; 33"85 gr. — Ure). Its density to that of atmospheric air is, therefore, as about 11 to 10. It is a powerful supporter of combustion, and its presence is essential to the existence of both animal and vegetable life. It forms 21§ (20-81J) by volume, and 23fl by weight, of the atmosphere. (M. Dumas.) Water dissolves about 5 per cent, by volume of oxygen, and by pressure a much larger quantity, forming oxygenated water (AQUA oxTaENii). Oxygen has recently been liquified. Tests. 1. It is distinguished from other gases by yielding nothing but pure water when mixed with twice its volume of hydrogen and exploded, or when a jet of hydrogen is burnt in it. — 2. A recently extinguished taper, with the wick still red hot, instantly inflames when plunged into this gas. — 3. A small spiral piece of iron wire ignited at the point, and suddenly plunged into a jar of oxygen, burns with great brilliancy and rapidity. Charcoal does the same. Estim. The estimation of the quantity of oxygen in an organic compound has already been described. For determining the quan- tity present in atmospheric air, and other like gaseous mixtures, Dobereiner has pro- posed the use of pyrogallic acid. The air under examination (freed from moisture) is measured intoan accurately graduated tubeover mercury, capable of holding about 30 cubic centimetres, and which it should frds fill. A solution formed of 1 part of dry hydrate of potassium and 2 parts of water, and in volume about ^^tb that of the air, is next introduced by means of a pipette with a curved point, and is gently agitated therewith in the gas for a short time ; the decrease of volume gives the proportion of carbonic anhydride present. A solution of py- rogallic acid (1 gramme in 5 or 6 centimetres of water), equal in volume to one half that of the solution of potassa already used, is then introduced by means of another pipette, and the mixed liquids are cautiously shaken to- gether over the inner surface of the tube. When absorption ceases (which it does in a few minutes), the quantity of residual gas (nitro- gen) is read off from the graduations ; the dif- ference in volume before and after the intro- duction of the pyrogallic acid indicates the proportion of oxygen. This is a mere modifica- OXYGKNAIION-OXYHYDROGEN BLOWPIPE 1217 tion of Priif. Liebijf's method. 1 grarame of n rngallic acid in combinHtion with hydrate of potiissium is cn|iiible of abBorbing about 189 cubic cciitimStrea of oxygen. (Dobereiner.) OiIkt nicthndt employi'd for the analysis of air, depending on the increase or loss of weight wlien the iiir is passed over finely divided copper heated to redness, the loss of volume when the air is exploded in a eudiometer with half its bulk of hydrogen, or when a stick of phosphorus is left in it for some hours, are well known, and described at length in every ele- mentary woi-k on chemical analysis. The last nietliod, although less accurate than the others, has the advantage of extreme simplicity. D*e». Oxygen lias been employed to in- crease the illuminative and heating power of lamps, and to render vitiated air respirable, &c. ; aud when largely diluted with atmo- spheric air, or condensed in water, as a reme- dial agent in asphyxia arising from the inhalation of carbonic acid aud carbonic oxide. Dr Ringer says that if oxygen be admin- istered at a gaseous bath for an honr or two at a time, and the bath repeated six or eight times a day, it is of groat service in senile gan)2;reno. Concluding Remarks. Oxygen gas may be coUectcil in the usual way, either over water, mercury, or in bags; or, on the large scale, in gasometers. The purity of the products of the several processes given above depends on the substances from which the gas is obtained being themxelvos pure. For particular experi- ments the Hrst portion of gas should be allowed to escape, or be received apart, as with this, as with the otiii'r gases, it is contaminated with the atmospheric air of the apparatus. Tlie gas procured from manganese or nitre may be purified by pussiiig it through milk of lime or a solution of caustic potash ; it will still, liowcver, retain some traces of nitrogen. M. Limousin' has devised an apparatus fir the preparation of oxygen by tlip attendants of hospitals, which obviates the risk of bursting of the retorts, attending its preparation by the old method. The appar-itus consists of two cast-inin hemispheres, whose edges, which are well polished and about two centimetres thick, can be fitted hermetically upon each other, and fastened by three screws. The mixture of chlorate of potash and peroxide of manganese is placed in the lower hemisphere, which rests upon a tripod ; the upper hemisphere, from w hich projects an iron tube, is now screwed on, and the iron tube connected with india-rubber and glass tubing with a Wolfs wash-bottle, from which the gas after being washed passes through a second class tube, and is thus ready for use. It may he conducted into an airtight bag, in which it will keep for several weeks. Such a bag when supplied with a tube and stop-cock will aHbrd a ready means for inha- lations. Oxysen in a condensed or compressed ' ■ Pliurm. Ceiitrallwllc,' xiv, S18. VOL, II. state is prepared by Mr Orchard, High Street, Kensington. See Oboanic substasces, OzoNK, Gases, Lkjubfaciion of, Ac. OXYGENA'TIOlf . Syn. The act or process of combining with oxygen. Formerly it w.is of more general npplication than the word 'oxidation,' with which it has been regarded as synonymous. ' Oxygenation ' is, however, at the present day practically obsolete. OXYGENI'SBD LARD. Syn. Oxygenated AXUNGE; AXUNGIA OXTQENATA, L. Prep. (Ph. Bat. 1805.) From prepared lard, 16 parts, melted over a slow fire, and then mixed with nitric acid, 1 part ; the combination being promoted by constant stirring with a glass rod, until it ceases to allect litmus paper. It should be extremely white, and should be kept in the dark. See Ointment op Nitbio acid. OXYHYDROGEN BLOWPIPE. See Blow- pipe. Ueville and Debray (' Ann. Ch. Pliys.' [3], Ivi, 385) employ the oxyhydrogen blow- pipe in the following manner for effecting the fusion of platinum and the refractory metals which accompany it. The apparatus con- sists of the blowpipe C (see below), a furnace ABD, and a crucible ORI. The blowpipe is composed of a copper tube about half an inch in diameter, terminating below in a slightly conical platinum jet about li inch long. Within this tube, which is supplied with hydrogen or coal-gas through the stop- cock H, is a second copper tube & for supply- '"? oxygen, terminated also by a platinum nozzle with an aperture of about a twelfth of an iuch in di.iineter. 77 1218 OXYMEL The furnace ABD consists of three pieces of well-burnt Hine of slightly hydraulic quality, which may be turned at a lathe with ease. The cylinder A is about 2^ inches thick, and is perforated by a slightly conical hole into which the blowpipe fits accurately, passing about half-way through the thickness of the mass. A second somewhat deeper cylinder of lime, B, is hollowed into a chamber wide enough to admit the crucible, and leave an interval of not more than a sixth of an inch clear around it. KK are four apertures for the escape of the products of combustion. Tlie outer crucible US is also made of lime, but it contains a smaller crucible / of gas coke, provided with a cover of the same material; and in this the substance to be used is placed, the crucible resting on the lime support JD'. The conical cover (? is made of lime, and its apex should be placed exactly under the blowpipe jet, at a distance from it of % to li inch. The different pieces of the furnace must be bound round with iron wire to support them when they crack. The oxygen is admitted under a pressure of a column of 16 inches of water. The temperature is gradually raised to the maximum, and in about eight minutes from this time the operaffion is complete. By employing a jet of mixed coal-gas and oxygen (-£Q, see engr.) in a furnace of lime. Deville and Debray succeeded, at an expense of about 43 cubic feet of oxygen, in melting and refining, in 42 minutes, 254 lbs. avoirdu- pois of platinum, and casting it into an ingot in a mould of gas coke j and much larger masses have since been melted by this method. Lime is so bad a conductor of heat that if a cup of lime not more than 0'8 inch thick be filled with melted platinum the exterior scarcely rises beyond 300° Fahr. (Miller's ' Elements of Chemistry,' 3rd. cd., pt. ii, p. 825.) OX'YMEI. Syn. Oxtmbl, L. An acidu- lous syrup made of honey and vinegar. There are only two oxymels in the last Ph. L. The ingredients in an oxymel should be of such a leJiaracter, and in such proportions, as to pro- duce a mixture of the proper consistence without evaporation. Oxymel of Col'chicum. Syn. Oxymel col- CHiCI COEMI, OXTMEL COICHICI, L. Frep. XFh. D. 1826.) Fresh corms (roots) of mea- dow saffron, 1 oz. ; distilled vinegar, 1 pint (wine measure); macerate for 2 days, press out the liquor, filter, add of clarified honey, 2 lbs., and boil down the mixture to the con- sistence of a syrup, frequently stirring. — Dose, 1 to 3 dr., twice or thrice a day ; in gout, rheumatism, dropsy, &c. Oxymel of Garlic. Syn. Oxymel alii, L. Prep. (Ph. L. 1746.) Sliced garlic, li oz. ; caraway seed and sweet fennel seed, of each 2 dr.; bjiling vinegar, 8 fl. oz. ; infuse, strain, and add of clarified honey, 10 oz. In hooping- cough, chronic diarrhoea, rheumatism, &c. Oxymel of Narcissus. Van Mons. Syn. Oxymel Naeoissi. Prep. Vinegar of Nar- cissus (made with 1 part of fresh flowers of daffodil to 8 of vinegar), 1 part ; honey, 4 parts. Dissolve. — Dose. A teaspoonf ul. In hooping- cough and spasmodic asthma. Oxymel, Pec'toral. Syn. Oxymel pecto- EALE, O. INULiE OOMPOSITUM, L. Prep. (Ph. Br.) Elecampane, 1 oz. ; orris root, J oz. ; water, li pint ; boil to i pint, strain, add of honey, 16 oz. ; ammoniacum, 1 oz. ; (dissolved in) vinegar, 3 fl. oz. ; lastly, boil to an oxymel. — Dose, 1 spoonful, occasionally; in coughs, humid asthma, &c. Oxymel, Sim'ple. Syn. Vineoae syeup, AoETATED honey; Oxymel (Ph. L. & D.), Oxymel simplex, Mel acetatum, L. Prep. 1. (Ph. L.) Acetic acid (sp. gr. 1-048) 7 fl. oz. ; distilled water, 8 fl. oz. ; mix, and add them to honey, 5 lbs., previously made hot. This contains only one half the acid ordered in the Plj. L. 1836. 2. (Ph. D.) Clarified honey, 1 lb. ; acetic acid (sp. gr. 1"044), 3 oz. ; as before. Stronger than the last. 3. (PI). L. 1836.) Honey, 10 lbs. ; acetic acid (1-048), li pint ; as before. This con- tains too much vinegar. (See No. 1.) 4. (Wholesale.) From honey (thick and good), 12 lbs. ; melt it by a gentle heat, add of distilled vinegar (of fully 5J), 2 quarts, and strain the mixture through flannel. No evapo- ration is required. Uses, S[c. Demulcent and refrigerant. — Dose, 1 to 4 fl. dr., either gradually sucked from the spoon or dissolved through some simple liquid. Dissolved in water, it forms a useful and pleasant cooling drink or gargle in fevers, sore throats, hoarseness, &c. ; but in some indi'- viduals it occasions griping. It is commonly used as an adjunct, in mixtures, &c. Oxymel of Squills. Syn. Honey op Squills ; Oxymel Soill«(B. P.), Mel Soill^ (Ph. L.), 0. Soilliticfm (L.) Prep. 1. (B. P.) Mix and evaporate on a water bath vinegar of squills, 1 pint, and clarified honey, 2 lbs., till the product when cold has a specific eravity of 1-32. ^ ' 2. Vineg:ar of squills, 2i pints ; gently evaporate it to 12 fl. oz., and add of honey (previously made hot), 5 lbs. 3. (Ph. L. 1836.) Strained honey, 3 lbs. ; vinegar of squills, li pint; boil to a projur OXYBRHODYNE— OYSTER 1219 consistence. The formula of the Pli. D. 1826 wa> aiinilur. fiw, S(c. Expectorant, and in large doses n«us(«nt. — Dote, J to fl. 2 dr.; in clironic coDgliB, hoarseness, humeral asthma, &c. Ozymel of Ver'digris. See Liniment of VEKDiaiiia. OXYR'RHODYNE. Syn. Oxybhhodinon. An old compound formed of 1 part of vinegar of ro>c< and 2 parts of oil of roses. OXYSAC'CHAKUM. A syrup acidulated with vinegar. See STHrp. OXYSDL'FHIDE. A name given to certain compounds or mixtures of metallic oxides and sulphides. See Antimony, Oxtbulfhide, &c. OYS'TER. Syn. OsTBEA, L. This well- known shell-flsli is the Ostrea eduUs (Linn.) " The oyster is a genus of lamellibniniliiiti' molluscs of the section with a single adductor muscle. The shell consists of two unequal and somewhat irregularly-shaped valves of lami- nated and closely foliated structure, and the hinge is without tooth or ridge, the valves being held together by a ligament lodged in a little cavity in each. The animal is in its organisa- tion among the lowest and simplest of lamelli- branchiate molluscs. It has no foot, and, except when very young, no power of loco- motii>u, or organ of any kind adapted to that purpose. Its food consists of animalcules, and also of minute vegetable particles, brought to it by the water, a continual current of which is directed towards the mouth by the action of the gills. The gills are seen in four rows wlieu the valves of the shell are sepa- rated, a little witliiu the fringed edge of the mantle. In the most central part is the addiiitor musole i and between the adductor musele and the liver is the heart, which may be recognised by the brown colour of its auricle. The month — for, as in the other lamelli- brancliiiitii, there is no bead — is situated beneath a kind of hood formed by the union of the two edges of the mantle near the hinse. It is jawless and toothless. Tlie ovaries are very larso during the season of reproduction, whieli extends over certain months when oysters are out of season for the table. Oysters are hermaphrodite"' The fecundity of the oyster is amazing. Lceuwenhoek estimated that an oyster, when full of spawn, contained frcim 3000 to 4000 of its ofFsiiring, and it has also been computed that one oyster alone produces nearly a million and a quarter of eggs. The eggs are hatched and the youni; produced within the shell and mantle of tiie parent, where they continue floating If swimming about in the vicinity of the pills in a creamy-looking kind of mucus or fluid until expelled. Their expulsion is preceded by a change of appearance in the fluid to a brownish or muddy colour ; a cir- iinustunce thnt may possibly indicate an Cli.inibprs' ' Eiicyclopttdia.* aUcration of composition in the liquid un- favorable to the infant oisU-r, and thus lead to its departure. Their departure or ex- pulsion from all the parent molluscs of the oyster-bank or bed takes place at the same time. When they leave the parent shell the yonng oysters, which in this condition are called tpat, are not more than ^^^ih of an inch in length; and two millions ot theiri when > losely packed do not occupy a space of more thiin a cubic inch. Thus cast adrift tliey are carried away by currents, their multitudinous numbers being considerably diminished by their falling a prey to numerous fish, as well as from their frequent inability to find a suitable resting- place. This obtained, the young oyster or spat attaches itself to it, and makes it the permanent home on which it eats, grows, and breeds, and, debarred of locomotion, passes its existencennless, of course, removed by external causes. Pending its obtaining a suitable locality the young oyster is provided with a powerful swimming apparatus which, it has been surmised, becomes absorbed or otherwibc disappears when its function is renchred un- necessary by the stationary life of the oyster after it has secured a habitat. The objects to which it attaches itself are numerous. The Ostrea parasitica, a species of oyster found in warm climates, fixes itself to the roots and branches o£ trees growing within rciich of and washed by the tide. Again, in some of the southern stites of North America, lar(;e oyster-beds, which are some- times of such ni!i;^nirude as to form buttresses iiirninst the force of the tides and winds, originate from the habit of young nvsters iittaehing tliemselves to the shells of old ones. Similarly the banks of some of the rivers of Georgia, which run up some few miles inland from the sea, are composed of ni.issi's of living oysters attached to each other. These banks, which are so massive as to make a channel for the river, are kuown as racoon banks, because this animal is one amongst oth'Ts which Irequents them for the sake of devourins the oysters. . . . In some of the French yarcj, or artificial oyster-beds, the y uns; oysters attach themselves to large unglazed tiles, or to fafjgots or other solid hoilies which are placed in suitable situntions for the purpose; in the English artificial beds hurdles are fre- quently employed, upon which the spat become deposited. It appears tlio young oysters select dark objects, such as slate or hiack stones, in preference to bodies of a lighter colour to fix themselves to, and that they choose, where practicable, the inner side of the object, or that portion of it away from the light. After a time the yonu!,' oys crs are removed from the breeding beds, placed in the fatteniiig beds, from whence th-^y are removed when they have attained a sufficient mzc, and sent upon the market. In England oysters are not regarded as tit to be eaten until they 1220 OrSTER are at least three years old ; whereas in France they are served up to table about a year earlier. The chief enemy of the young oyster is a species of whelk, known in France as the higourneaUi dog whelk, or piercer. These creatures, which are found in immense quan- tities in the celebrated oyster-beds at Arca- chon, near Bordeaux, cause great destruction amongst the bivalves. Part of their anatomy consists of a boring apparatus, with which tliey pierce the s-hell of the oyster; whatever of the dead oyster is left by the whelk is devoured by the crabs, which creep into the aperture in the shell made by the former. We have already alluded to the abundance of oysters in parts of Georgia, where, we may add, they are not only confined to the alluvial shores of the rivers, hut are also found in large numbers amongjt the long grass of the adjoining low lauds. In these districts it is by no means an un- common practice for the inhabitants to impro- vise a meal by picking up a bunch of oysters and roasting them over a fire kindled on the spot. In many of these localities the oysters occur in quantities so immense that a vessel of 100 tons might be loaded within three times her own length.l There are also many other parts of America in which the yield of the oyster-beds is enormous. In the State of Maryland 6000 persons are said to be employed dredging, and nearly 11,000,000 bushels of oysters were taken in 1870-71. In Baltimore as many as 10,000 persons are emplojed in tinniug this bivalve. Comparing the plenteousness of the oyster in America with its great scarcity of late years in our country, and the consequent much lower price of the foreign bivalve, we should be prepared to le.arn that considerable supplies of oysters, both alive and preserved in tius, come to us from America. The bulk of those consumed in Britain are a small variety, and come i'rom Maryland and Virginia. In 1872, owing to the diminished yield of the English oyster-beds, an attempt was made to introduce the American oyster into British waters; and we believe the dep6t for this purpose still exists at Cleesethorpes, at the mouth of the Humber, where operations in this branch of oyster culture are being carried on by the Conway Company. If, however, the opinion of an eminent pisciculturist be correct, viz. that the American oyster will not breed in our waters, we should conceive the experiment will be abandoned, since nothing will be gained by relaying them, that cannot be attained by simply importing them and sending them to the market, since it is asserted they are kept alive out of water for a month. A few years back a Select Committee ap- pointed by Parliament to inquire into the causes of the scarcity of oysters issued in 1876 a repor-t in which, endorsing the opinion of ' Cliambera* 'EncyclopBedia.' previous authorities on oyster culture, they attributed the diminished yield of our oyster- beds to continual over-dredging for them in open waters, without allowing sufScient ' close time.' The Committee found that, in France, where the stringent observances of the 'close season' was enforced, the supply of oysters had increased concurrently. The Committee, therefore, recommended the estab- lishment ' of a general close time,' extending from May 1st to September 1st, subject to certain exceptions under the supervision of the Board of Trade; the levying of penalties for buying or selling oysters for consumption during the ' close season ' being also recom- mended. The Committee further recom- mended that no oysters should be sold from the deep-sea fisheries under 2i or 3 inches in diameter. Commenting upon the above report, ' Nature ' very sensibly remarks : — " What is really wanted for the protection of the oyster is the assurance that these animals shall not be sold before they have a chance of repro- ducing their kind. Since the introduction of the railway system, the demand for oysters in distant places has become so great and the price has risen so high, that oyster culturists are tempted to send immature animals to market, and it is this fact, more than any failure of spat, that is leading to the scarcity. There are not, in consequence of the unceasing demand and consequent high price, so many full-grown oysters left to spat as there ought to be ; hence the scarcity. Any Act of Par- liament that decrees two oysters to grow where only one grew before will be greedily welcomed both by oyster cultnrists and by the public, and we hope that the issue of the present Eeport will lead to some effective measures being taken for the preservation of this delicious creature ere it be too late." Previous to 1846 the wholesale price of best English natives was £2 2s. a bushel; since then the price has risen rapidly to j64 4s. in 1865, in 18ti6 to £5, and in 1869 it had advanced to £8 ; that is, they had risen nearly 300 per cent, in 8 years, which is equivalent to an advance of from ^d. to 2d. each. At the present time they are, we believe, sold at from 3s. to 3s. 6d. a dozen by the retail dealer. Oysters are nutritious and easy of digestion when fresh, but are apt to prove laxative to those unaccustomed to their use. It is generally believed that they are in season each month of the year the name of which contains the letter R. Whitstable in Kent, and Colchester and other places in Essex, are the great nurseries or feeding-grounds for supplying the metropolis, and, indeed, the whole of England, with the most esteemed variety (natites) of this shell-fish. The shells (test^ PBEPAKAT^, T. OSTEEAUI^) were formerly used in medicine as an absorbent. Of the various species of oysters, that which holds the foremost place in the estimation of the gourmet is the 'English native;' now. OZOKEUIT— OZONE 1221 aliu! owinfif to the unwiae rapacity of the eollcctiir, nenrly dredged out of existence. The native ha» a liistoric reputation too, eincc it appears it was eagerly sought after by the old Romans, and n-as a frequent dish at their tables. The enthusiasm of the celebrated Dr Kitchener for this particular oyster was very intense. He is very pariicular in directing its shell to be opened with the greatest care so that it may be eaten alive and " tickled to death by the teeth'' The green oyster of Ostend is also prized by epicures ; it acquires its colour from its food, which consists chiefly of green monads and confervffi. Some of the American oysters are excellent in flavour, and are said to be without tile copper taste occasionally to be met with in English oysters. They smack a little of the mussel. Piiyen gives the following as the composition of the oyster: — Mpan of two AnHlyseB. Nitrogenous matter . . 14'010 Fattv matter .... 1'515 Saline matter .... 2695 Non-nitrogenous matter and loss 1'395 Water 80-385 100-00 See Shell fish, Sauces, &c. Oyster, Scalloped. Pat them with crums of breud, pepper, salt, nutmeg, and » bit of butter, into scallop shells or saucers, and bake them before the lire in a Dutch oven. Oysters, Fried (to (rarnish boiled flsh). Make a batter of flour, milk and eggs, add a little seasoning to it ; dip the oysters into it, and fry them a fine yellow brown. A little nutmeg should he put into the seasoning, and a few crumbs of lireud into the flour. Oysters, Stewed. Open them, and separate the liquor from them, then free them from grit by washing, strain the liquor, and add it to the oysters with a small piece of mace and lemou pe'el, and a few white peppercorns. Simmer very gently, and add some cream and a little flour and butter. Let them be scrvcil with sippeto. Oysters, To Feed. Put them into water, unil wash them with a birch broom till quite clean. Then place them bottom downwards in on earthonwiire pan; sprinkle them with Hour, oatmeal, and salt, and then cover with water. Repeat this treatment every day, taking care to make the water pretty salt. OZOKERIT. Syn. Fossil wax, Mineeal WAX. This substance, which has within the last few years been utilised as a source of paruflin and the mineral hydrocarbon oils, is fomid in various localities in the tertiary Btrato, mostly occurring in, or in close proxi- mity to, the coal measures. But although extensive deposits of it are to be met with in Oallicia and on the slopes of the Carpathian mountains, it is by no menus an abundant body. In the Austrian empire there are many large manufactories for its conversion into paraffin and the mineral oils. In our country there is we believe only one, that of Messrs Field. Ozokerit is usually met with as a brown and compact substance, occasionally yellow; however, it is sometimes black. It melts at a temperature varying from 60° to 80° C. Nbpt-gil i^ a substance very similar to ozokerit, and is formed on the island of SwStoi- Ostrow in the Caspian Sta. According; to Rossmassler, neft-gil is treated in the follow- ing maimer : — 15 cwt. of the crude material is put into iron stills provided with a leaden worm, and submitted to fractional distilla- tion, yielding 68 per cent, of distillate, con- sisting of 8 per cent, of oil, and 60 per cent, of crude paraffin. The oil thus ob- tained is yellow, opalescent, possesses an ethereal odour, and a sp. gr. of 0-75 tn 081. Each distillation yields a quantity of a light oil boiling below 100° C, which is used for the puipnsc of purifying the paraffin. The crude parafliu obtained by the first distil- lation is tolerably pure, has a yellow colour, and can at once be treated by the hydraulic press and centrifugal machine ; the oil from these operations is again submitted to frac- tional distillation in order to obtain more paraffin. The pressed paraffin is melted an>il,6oz,- niHstic, 1 oz, ; dissolve, add of suiriir of lead, i oz., previously ground in the least possible quiintity of oil; then further add of water, q. s., gradually, until it acquires the consistcnue of cream, working it well all the time. Used by painters to cover their work when they are obliged to leave it for some time. It may le washed off with a sponge and water. PAINTING. The art or employment of laying on colour. In the fine arts, the pro- duction of a picture or a resemblance in colours on a flat surface. The artistic and me- chanical consideration of this subject does not come witliiu the province of our vohnne ; but notices of the leading materials employed by both artists and house painters are given uuder tlieris|PLMtiv(' names. Seethe various pigments, CoLODiis, Oils, Vaunishes, &c., and below. Painting, Distem'per. A method of painting generally iidupted by the ancients. Water was tlie priuci|)al medium, but various gela- tinous and albuminous 'binders ' were added to fix the pigments. Of these the most im- portant were glue, size, and white of egg. Ii\ modern distemper, as executed by the painters of theatrical scenery, panoramas, &e., spirit of turpentine l< liii-fiely employed as a medium. Fainting, Elydor'ic. A method of painting invented hyM. Vincent, ol .Montpelicr, bavin;; for its object to (unibine the I'rcsb appenraiiee and finish of water colours witli the melloH'- mss of oil paiiiiing. The liquid oiuploycd as a veh cle for the pigments is un emulsion formed of oil and \v;itorby the intervention of cerUiiu ]ioition of gum or mucilage. Fainting, Enam'el. In this variety of paint- ing, viiiili.iblc colours arc laid on thin plates of nietaU, and fused into it. The outline is first burnt in, iiltcr which the parts arc filled up jjradnally, with repeated fusions at an enamel- lei's lump, to the most niinutefinishing touches. " rile euumel painter has to work, not with actual colours, but with mixtures which he only knows from experience will produce cer- tiiii colours after the operation of the fire." ^.Vikin.) Painting, Encaua'tic. This method is very ancient, but is now seldom practised. Ac- cording to Pliny, the colours were made up into crayons with wax, and the subject being traced on the ground with a metal point, they were melted on the picture as they were used. A coating of melted wax was then evenly spread over all, and when it had become quite cold was finally polished. The art of encaustic painting, after lying dormant for ab'mt 15 centuries, was revived by Count Caylus, in 1753. In its new form, the wood or canvas to be painted on is first well rubbed over with wax, and then held before the fire, so that the wax may penetr.ite and fill up all the interstices, and form a per- fectly even surface. The coloured pigments are next mixed with the powder noticed below, which is then rubbed smooth with some thick gum water, and applied with brushes in the same manner as ordinary water colours. When the painting is finished, and quile dry, it is brushed over with pure white wax in a melted state, the surface being equalised by the skilful application of heat ; it is, lastly, polished oif, as before. The powder. — To white wax, melted in an earthen pipkin,add, in small portions at a time, an equal weight of powdered mastic, stirring continuously until the whole is incorporated ; then pour it into cold water, and afterwards reduce it to powder in a wedgwood-ware mortar. A small quantity only of this powder is used with light colours; but more is re- quired with the darker ones, until, on approach- ing black, the two may bo mixed in almost equal proportions. Fainting, Fres'co. This method of painting was known to the ancient E^r.vptians, and was commonly practised by the Greeksand Romans. It is confined to the decoration of the walls of buildings, and is executed by incorporating the colours with the still moist pla-ster, or gesso. The pigments employed are entirely mineral or vitreous. As it is extremely difficult to alter the work after the colours are once absorbed, or after the ground has hardened, the whole must be carefully designed before commencing the picture, and no more com- menced at once than can be executed during the day. Of all the varieties of painting, fresco is " undoubtedly the most virile, most sure, most resolute, andmost durable" (Vasari), and the one most adapted for the purposes of historical painting in its grandest and most exalted forms. In comparison with it, it has been said that even oil painting is " employment fit only for women and children.'' (Michael Angelo.) Painting, Glass. See Staiked glass. Fainting, Oil. This well known and much practised method of painting takes its name from the vehicle employed for the colours. The last may be any of those of a permanent character, and whose natural tint is not altered by admixture with oil. Linseed, nut, and 1226 PAINTINGS poppy oil, are those which are principally em- ployed. The first requires the addition of 'driers,' and hence is generally used under the form of ' boiled oil.' Spirit of turpentine is commonly used to thin down the prepared colours, and the finished picture is frequently covered with a coat of varnish. Painting, Por'celain. See Pottbet, Stained GLASS, &c. Painting, Vel'vet. Any of the ordinary non- corrosive pigments or liquid colours, thickened with a little gum, may be employed in this art ; preference being, however, given to those that possess the greatest brilliancy, and which dry without spreading. See Stains, &c. Painting, Water- colour. In its strictest and modern sense, ' water-colour painting' means the painting on paper with colours diluted with water. The English school of water- colour painting has produced works which bear comparison with the great masterpieces in oil, and even surpass them in the delicacy of atmospheric effects. The old practice of making the entire drawing in light and shade by washes of Indian ink or neutral tints, and then adding the various local colours in trans- parent washes, has given place to the more healthy system of painting every object in its appropriate local colour at the outset. PAINTINGS. Many valuable paintings suf- fer premature decay from the attacks of a microscopic insect, a species of acarus or mite. The best method of preventing this variety of decay, is to add a little creasote (dissolved in brandy or vinegar), or a few grains each of corrosive sublimate and sal am- moniac (dissolved in a little water), to the paste and glue used to line the picture, as well as to add a few drops of pure creasote or of an alcoholic or ethereal solution of corrosive sub- limate to the varnish, when any is to be applied. If the destruction alluded to has already com- menced, the painting should be at once care- fully cleaned and re-lined, observing to employ one or other of the remedies just mentioned. The most apropriate and only safe situation in which to keep paintings, is where there is a pure and moderately dry atmosphere. To pro- tect pictures from the effects of damp, it has been suggested to dip the canvas into a solution of silicate of potash, and afterwards dried, previous toits being used. Impureairaboundsin carbonic acid and sulpliuretted hydrogen. It is the pre- sence of the last in the air that blackens the ' lights,' and causes most of the ' middle tints' and 'shades' to fade ; and it is exposure to damp that produces mouldiness and decay of the canvas. For this reason valuable paintings should not be kept in churches, nor suspended against heavy walls of masonry, especially in badly ventilated buildings. Excess of light, particularly the direct rays of the sun, also acts injuriously on paintings, since it bleaches some colours and darkens others. The blackened lights of old pictures may be instantly restored to their original hue by touching them with peroxide of hydrogen, di- luted with 6 or 8 times its weight of pure water. The part must be afterwards washed with a clean sponge and water. The most astonishing results have been produced in this way. See Peroxide of Hydkooen. Pettenkofer observing the colours of many of the oil paintings in the Munich galleries apparently fading, discovered that the dim and grey appearance they then presented, was not really due to any decay of colour, but to a discontinuity of the molecules of the vehicle, and the resinous substances mixed with the pigments ; the effect of which was to break up and lessen the mass of transparent colour and to diminish its intensity. This separation from each other, of the alternate particles, he con- ceived was owing to the shrinking and con- traction they underwent after long years of exposure to a moist atmosphere. To remedy it Pettenkofer subjected the aft'ected picture to two simple processes, which he is said to have found absolutely successful. The first, which he terms the 'regeneration' process, consists in enclosing the picture in a flat box, where it is exposed to the vapours of alcohol, part of which being absorbed by the resinous molecules,restore them to their original volume. Hence it follows thatthe gaps between the mole- cules being thus filled up, there is presented to the eye a continuous mass of transparent co- lour, as when the picture was freshly painted. In the previous operation the resinous con- stituents only of the picture have been acted upou and restored to their normal condition. The hardened molecules of the oil which have been employed as a vehicle have likewise dimi- nished in bulk, from the same causes, and in so doing have contributed to the lessening of the brightness of the picture. In cases where it is found the increased volume of resinous particles has failed to fill up the intervals be- tween the shrunken oil molecules, Pettenkofer subjects the picture to a further process. In this, which he terms ' nourishing it,' the picture is simply rubbed over with balsam of copaiba. Oil, which was formerly employed for this purpose, is very strongly condemned by Pet- tenkofer. Oil paintings, as probably most of our readers are aware, are mostly executed either on wood (' panel') orcanvas,now principally on the latter. Both these substances have to undergo a preliminary operation known as 'priming;' the priming being, in short, the ground on which the paint is placed. This priming may consist either of a number of layers com- posed of a mixture of chalk or plaster, with paste or glue, or else of a series of coats of oil colour. When a canvas or panel is pre- pared with the former, it is called ' distemper priming;' when with the latter, 'oil priming.' The distemper is the more quickly prepared, but is open to the objection of being easily broken, and of tt liability to absorb moisture, by which it becomes liable to separate from the canvas. PAINTINGS 1227 If the priming be of oil colour it is desirable that tlift chief pi^mt'Ut used in making it •hould be white lead, and that if any other colours are added, ihcy should hu in cnnipani- tively small quantitiod. Dr R. Liebreich ci tes an example in which a departure from this precaution, persevered in from the middle of tlie 16th to that of the 17th century, by a celebrated school of Italian painters (the liologua), has resulted In the destruction in their works of all the glazing uf the picture, " »ii that those colours only ciui be recog- nised which either contain white, or are glazed on white." Furthermore, that the dark priming u>'ed by these artists bus caused the dark parts of their pictures to become still darker. This priming which was of a reddi»h-brown colour, WHS composed of a mixture of bole Ar- menian and umber ; and it is conjectured it was empldved with the object of modifying or softening tno violent contrasts of light and dark colours, and thus of easily securing effective chiaro»'uro, and of aiding rapid execution. The Dutch and Flemish painters mostly em ployed a liglit coloured priming; sometimes it was of n light oak colour. Vandyke is said to have used grey grounds for his pictures, and in some few instances dull red ones ; and since his pictures are free from tlie objection- able qualities met with in the works of the Bo logna artists, it has been surmised that in this method of working, he had recourse to impasto colouring. In tlie selection of wood, which is subse- quently to be used for thepicture, considerable judgment and experience are required, that from the toughest and soundest oaks, nut trees, or cedir, being sought after. The cutting it into boards, and seasoning it, are al-o points exacting a ^jreat amount of time and care. The backs of pictures, if made of wood, in addition to their liability to attacks from in- sects, not unfrequently warp, or fissures form in them, or they may become hopelessly rotten. When the picture warps, it should be moist- ened with water at the back, on which it should be lain for 24 hours, at the end of which time, or sometimes less, it becomes per- fectly straight. Fissures may be filled up by pieces of wood cut to the required size. Small pieces of rotten wood, if not too near the paint- ing, may be cut out and the gaps tilled up with wedge-shaped pieces of wood. Where the loss is insi^ruificant it may be stopped up with cement. When the panel is very rotten and decayed, it may be necessary to remove the picture from it altojiether, and to place it ei ther on a new panel, or upon what Dr Liebreich regards as better still, a piece of canvas. This is by no means so formidable and as- tonishing an operation as it may at first sight appear; in short, as will be directly shown, the picture may, if necessary, he freed from its primins even, wiihout any difficulty. Hacquui, of Pari", was one of the first to remove an oil painting from its base, and to place it upon a new one. He did this with one of Raphael's Madonnas, in the gallery of the Louvre; and the same treatment has since been extended to the ' Resurrection of Laza- rus,' by Sebastian del Piombo, one of the pic- tures in our National Gallery. This process is generally accomplished as follows: — " First of all the surface of the picture is pasted over with gauze and paper ; after that the wood is made straight by moistening, or, it necessary, by making incisions with the saw, into which cuneiform pieces of wood are driven. By means of a tenon-saw the panel is to be sawn into little squares, whicli must be removed by a chisel, and in this way the thickness of the wood is reduced to half an inch ; it is then planed until it becomes no thicker than paper, and the rest is removed by means of a knife and with the fingers. " The painting being thus severed Irom its basis, it can be fixed on canvas if the priminu' is sufficiently preserved. In the opposite cjse a mixture made of chalk and glue, or some- thing of the kind, must be put on first, andvery evenly smoothed after being dry. This done the new canvas has to be fixed upon it by means of a mixture of glue, varnish, and turpentine, and the substance of tlie picture pressed tightly and evenly against it by nuans of warm irons."' Defects in the priming of an oil painting, when they are confined to a slight separation of the priming of a canvas, may be remedied by pouring into the gap caused by the seve- rance a little solution of size, and then pressing the separated surfaces gently together. Sli;;ht cracks must be filled up with fresh priming. Fur paintings in which the whole of the priming seems insecure, or has extensively separated from the canvas, it is recommended to remove them entirely from the old basis and to transfer them to new panels or canvas. The property of unchangeableness, or indis- position to fade, as exemplified in the retention of its freshness of colour by a picture, is one which, it is asserted, is very much more gene- rnllv met with in the pictures nf the Italian,^ and Dutch painters of the 15th, 16th, and 17th centuries, than in those of the French and English schools of the last hundred years. Opinions have been advanced in expl.inatinn of this circumstance. One is, that the older masters used pigments and vehicles of much greater purity and freedom from adulteration than the latter generations of painters; another, that they worked by a method and prepared their colours by n process unknown since their time, in fact, that they were pos- sessed of a technical secret, which, as they never divulged it, has died with them ; a third, that tliey had choice of many colours unknown in the present day. One of the later and most valuable contri- ' Lielireich. 2 From tlie Italidn school must be exfiepted that of Boloj^ua. 1228 PAINTINGS butions to onr knowledge of tbcse points has been made by Dr R. Liebreich, io his lecture " On the Deterioration of Oil Paintings," delivered at the Royal Institution, March 1st, 187S, which also embraces the practical deductions to be drawn from the results of his investigations. The plan adopted by Dr Liebreich for unravelling the so-CHlled secret by which the old masters so generally contrived to secure permanencyfor their colours was ingenious and logical; it consisted in dis- secting the structure and chemically analysing the pigments, vehicles, &c., of the pictures of the pupils of the great masters, for "fortunately they painted with the same material and by the same methods as the masters, and thou- sands of pictures by the pupils, well preserved and in different stages of decay, may be easily secured." The third explanation previously given as a reason for the superior durability of the colour- ing of the old over the later oil paintings is thus disposed of by hira. He says : — " We meet very often with the idea that the old masters had been in posssesion of colours, that is, pigments, the knowledge of which has been lost, and that this accounts principally for the ditferencc between the oil paintings of the 15th and 16th centuries, on the one hand, and that of tlie IStli and 19th on the other. But tliis is a great mistalse. We know per- fectly well the pigments used by the old mas- ters ; we possess the same and a considerable number of new ones, good as well as bad, in addition." He adds, " In using the expression of good and bad, I am thinking principally of their durability. From this point of view the pig- ments can be placed under tliree headings : — "1. Those that are durable in themselves and also agree well with the other pigments with which they have to be mixed. "2. Such as when sufficiently isolated remain unaltered, but when in contact with certain other pigments change colour, or alter the others, or produce a reciprocal modification. '• 3. Those which are so little durable that, even wlien isolated from other pigments, the mere contact of the vehicle, the air, or the light, makes the-r in time fade, darken, or disappear altogether. " The old masters used without reserve only those hfiloiiging to the first of these three categories. For those belonging to Ihe second they imposed on themselves certain limits and precautions. Those belonging to the third they did not use at all. " That some of the modern masters have not followed these principles is not owing to a lost secret, but to the fact they disregarded those well known principles, and even con- sciously acted against them. In Sir Joshua Reynolds' "inry, tor instance, we read that in order to produce certain tints of flesh, he inixed orpivnent, carmine lake,and blue black together. "Now, orpiraent is one of the colours of the second category, carmine lake one of the third. That is to say, orpiment, as long as it remains isolated, keeps its brilliant yellow or reddish orange colour; but when mixed with white lead it decomposes, because it cansis,ts of sul- phur and arsenic, and it moreover blackens the white lead, because the sulphur combines with it. Carmine lake, even if left isolated, does not stand as an oil colour, and, therelore, has been superseded by madder lake. Unfortunately some of the most brilliant colours are perishable to such a degree that they ought never to be used ; yet it seems to me that just in one branch of art, in which of late remarkable progress has been made, I mean landscape painting, the artists, in order to obtain certain effects of colour not easy to be realised, do not always resist tlie temptation to maice use of a number of pigments, the non-durability of which is proved beyond doubt." Another point which Dr Liebreich regards as of much more importance even than the selection and treatmentof their pigments, and in which he savs the old masters exercised great discretion, was the more sparing use of the vehicles and liquids they mixed with their colours. He points out that there are certain pig- ments which when mixed with the oil impede its drying, whilst others there are which has- ten it. " Supposing now," he says, "we should add to each of the different pigments the same quantity of oil, the drying of it would progress at different rates. But in reality this difference is very greatly increased by the fact that the different pigments require very different quantities of oil, in order to be ground to the consistency requisite for painting." Fettenkofer quotes the following figures given to him by one of the colour mauulac- turers : — 100 jiarta (weight) White lead require 12 pans of oil. „ „ Zinc white „ H „ „ „ tJreeu chrome „ 16 „ „ „ Clirotfie yellow „ 19 „ „ „ Vermilion „ 25 „ „ „ Lislitred „ 31 „ „ „ Madder lake „ G2 „ „ „ Yellow oclire „ 66 „ „ u Light ochre „ 73 „ „ „ C.iniel's brown „ 75 „ „ ., Brown inaagauese „ 87 „ „ „ Terre verte „ 1011 „ „ „ Pariaian hlue „ 106 „ „ „ Burnt terre verte „ 112 „ „ Berlin hlue „ 113 „ 1, Ivory black „ 112 „ „ „ Cobalt „ li]5 „ „ „ I'lorentine brown „ 150 „ „ „ Burnt terra sKnna „ 181 „ „ ,, B^w terra sienna „ 140 „ According to this table, a hundred parts ot the quick drying white lead are ground with twelve parts of oil, and on the other hand, slow-drying ivory black requires one hundred and twelve parts of oil. It is very important that artists should have an exact knowledge of these matters. But it PAINTINGS 1229 ■eems to me tbat they nre inaufflciently known to most of thom. All, of course, know per- fectly how difforent the drying quality of ditferent colours is. But that these diflerent colours introduie into the picture so different a quiiiitity of the oil, nud how large the quantity is in the colours they buy, and, fur- tlier, that the oil as well as the mediums or siccatives they add to dry the colours are gra- dually transformed iato a caoutchouc-like opaque substance, which envelopes and darkens the pigments, and, moreover, tliat the oil undergoes, not in tlie beginning, but much later ou, when it is already completely dry, changes of volume, and so impairs the contin- uity of the picture — all this is not sufficiently known. Otherwise, the custom of painting with the ordinary oil colours, to be bought at any colonrman's, would not liave been going on for neiirly a hundred yearB, in spite of h11 the clearly shown evil results — results due chiefly to the principal enemy of oil paintiug, that is to sny, the oil. A close optical examination and accurate study of the pictures of the French and En- glish masters of the last hundred years have revealed to Dr Liebreich their principal defects, which he says are : — 1. Darkening of the opaqne bright colours. 2. Fudingof the transparent brilliant colours. 3. Darkening, and above all, cracking of the transparent dark colours. He states that these cracks ore so characteristic and distinc- live of the pictures of this period that they might be used as a test as to whether or not a picture really belonged to this school, or was only a copy. This peculiar cracking in the paint is, ac- cording to Dr Liebreich, particuliirly observ- able in GuericKUlt's ' Wreck of the Medusa ' in the Louvre, and also in Ingres' ' Portriiit of Chernbini ;' and as the same defect is not to be seen in the works of the Dutch and Italian artists, the very rational inference to bo drawn is that the methods followed by these >eliools wi>re sounder than those adopteil by their £up:lish and French successors. Dr Liebreich believes the cracks were owing to the practice of painting over one colour with another before the first was perfectly dry. " The study of the alterations," says Dr Liebriiili " already fully developed within the last hundred years only, and their comparison with the works of the old masters would sug- gest the foUowing rules for the process of painting : — " 1. That the oil should in all colours be re- duced to a minimum, and under no form should more of it than absolutely necessary be introduced into a picture. " 2. All transparent colours which dry very slowly should be ground, not with oil at all, but with a resinous vehicle. " 3. No colour should be put on any part of a picture which is not yet perfectly dry, and above all, never a quick -drying colour upon a slowly-drying one which is not yet perfectly dry. 4. White and other qnick-drying opaqne colours may be put on thickly. On the con- trary, transparent and slowly-drying colours should always be put on in thin layers. If the effect of a thick layer of these latter is required, it must be produced by laying one thin layer over another, taking care to have one completely dry before the next is laid on. If transparent colours are mixed with sufficient quantity of white lead they may be treated like opaque ones." Dr Liebreich concludes his interesting lec- ture with some judicious advioe on the sub- ject of picture cleaning, and points out that, since ditferent pictures require to be differ- ently operated upon, all nnlversal agents and methods suggested for the purpose are open to suspicion and should be discarded. For pictures the varnish of which has be- come cracked or dim he recommends Petten- koter's treatment with alcoholiscd vapour, already described. For those in which the varnish may have become dark yellow, brown, or dirty, he advises its removal altogether, being very careful to specify the conditions under which this should be accomplished, ami the risk the picture may run of being spoiled if entrusted to an unintelligent and ignorant manufacturer. " If a picture," he says, "is thronghout painted in oil, if its substance has remained sound and even, and it has been varnished with an easily soluble mastich or lummar varnish, there will be neither difficulty nor danger in removing the varnish. This can, in such a case, be done either by a dry process, that is by rubbing the surface with the tips of the fingers and thus reducing the varnish by degrees toa fine dust, or by dissolving the varnish by application of liquids which, when brought only for a short time into con- tact with ttie oil painting, will not endanger it. We have, however, sien that the w orks of the old masters are not painted witti oil colours like those used by modern painters, but, on the contrary, that certain pigments, and espe- cially the transparent colours used for glazing, were ground only with resinous substances. These latter have in the course of time been so thoroughly united with the layer of var- nish spread over the surface of the picture that there no longer exists any decided limit between the picture and the varnish. It is in such pictures that a great amount of exi)e- rieuce and knowledge of the process used for the picture, as well as precaution, are required, in order to take away from the varnish as much only as is indispensable, and without inter fering with the picture itself. " Numberless works of art have been irrepa- rably injured by restorers, who, in their eager- ness to remove dirt and varnish, attacked the painting itself. They then destroyed just that last finishing touch of the painting without which it is no longer a masterpiece." 1280 PAINTS— PALLADIUM "The cleaner is, tlien, reminded that if the removal from the pictures of their varnish, when this is known to consist of a spirituous solution of the gums inastich or dammar, re- quires the amount of discretion and judgment before specified, still greater care and pru- dence are necessary when dealing with pictures whose surfaces have been covered witli oil, oil varnish, or oleo-resinous varnish. All these substances, which in time more or less obscure the picture, form on its face a darlc and opaque film, and this frequently requires for its removal the application of some agent, which, in dissolving the layer of varnish, is very liable at the same time to dissolve the substance of the picture also." As a recent instance of the injurious effects of injudicious picture cleaning, Ur. Liebreich mentions the case of a valuable picture in the Pitti Palace, at Florence, the 'St John of Andrea del Sarto.' The softness of the out- line of the face of the figure, which he remem- bers previous to its attempted restoration, had been entirely destroyed, which disastrous result Dr Liebreich conceived had been caused by the entire removal of the glazing. A new method for cleaning pictures is de- scribed by E. Von Bibra in the ' Journal fiir Praktische Cbemie.' A very indistinct oil- painting was freed from dust with a feather, waslied with a sponge and water, and then covered for eight minutes with a layer of shaving soap. The soap was then washed off with a brush and then left to dry. It was next thoroughly cleaned with linen cloth soaked in uitro-benzol. The picture was now distinct, hut the colours dull. Finally, it was treated with olive oil, and a coating of quick- dryius varnish laid on. (Academy, May 6th, 1878.)' FAINTS. In trade, this term is commonly applied to pigments ground with oil to a thick paste, ready to be ' thinned down' with oil or turpentine to a consistence adapted for appli- cation witli a brush. Paints are prepared on tho small scale by grinding the dry pigments with the oil by means of a stone-and-muller ; on the hirge scale tliey are ground in a colour mill. There are several pigments, as King's yellow, Scheele's green, verdigris, white lead, &o., which from their poisonous character cannot be safely ground by hand, except in very small quantities at a time, and then only by the exercise of extreme caution. In mixing or thinning down paints for use it may be useful to mention that — for out- door work, boiled oil is principally or wholly employe-d, unless it he for the decorative parts of houses, when a portion of turpentine and pale liii.^eed oil is often added. — For in-door work, linseed oil, turpentine, and a little * In givinff insertion to tlie above, we do not venture to give an opinion as to its value or the reverse. We would recotunietiil it to be read side by side with Dr Liebreicli's advice on picture cleaning, given aljove.— Ed. ' driers,' are generally used in tho same way. The smaller the proportion of oil employed for the purpose, the lees will be the gloss, and the greater the ultimate hardness of the coating. For 'flatted white,' &e, the colour being ground in oil, requires scarcely any further addition of that article, as the object Is to have it ' dead' or dull. The best driers are ground litharge, and ground sugar of lead; the first for dark and middle tints, and the last for light ones. To preserve mixed paints in pots from 'skin- ning over' or drying up, they should be kept constantly covered with water; or, what is better, with a thin film of linseed oil. Brushes, when out of use, may be preserved in a similar manner to mixed paints. When dirty, or required for a paint of another colour, they may be cleaned with a little oil of tur- pentine, which may be either preserved for the same purpose another time, or may be allowed to deposit its colour, and then used to thin down paints as usual. In no case, however, should it be thrown back into the cistern or pan with the pure ' turps.' Paints, Flex'ible. Prep. Take of good yellow soap (cut into slices), 2i lbs. ; boiling water, 1 J gall.; dissolve, and grind the solution whilst hot with good oil paint, li cwt. Used to paint canvas. Paints, Vitrifi'ahle. See Enamel, Glaze, Stained Glass, &c. FALLA'DIUM. Pd. A rare metal discovered by Dr WoUaston in the ore of platinum, in 1803. Prep. 1. A solution of the ore of platinum in aqua regia, from which most of the metal has been precipitated by chloride of ammo- nium, is neutralised by carbonate of sodium, and then treated with a solution of cyanide of mercury; the white insoluble precipitate (cyanide of palladium) is next washed, dried, and heated to redness; the residuum of the ignition (spongy palladium) is then submitted to a gradually increased pressure, and welding at a white heat, so as to form a button, in a similar manner to that adopted with platinum. Prod. Columbian ore of platinum, 1^ ; Uralian do., -252 to -ysg. 2. The native alloy of gold and palladium (from the Brazils) is submitted to the opera- tions of quartation and parting, the nitric acid employed being of the density of 1-3 ; the silver is next precipitated from the solution by means of a solution of common salt or di- lute hydrochloric acid, and the decanted super- natant liquid, after evaporation to one half, is neutralised with ammonia, and concentrated so that crystals may form ; these (chloride of palladium and ammonium) are cautiously washed in a little very cold water, dried, mixed with borax, and exposed in a crucible to the strongest heat of a powerful blast fur- nace, when a solid button of pure palladium is fiirmed. Prop., S[e. Palladium closely resembles pla- tinum in appearance, fusibility, malleability, PAL5IITIC ACID— PANCREAS 1231 nnd ductility ; bat it is leu dense, and has a rather mure silvery colour than that metal ; it is freely soluble in aqua ref;ia, and is slowly attacked by nitric acid, but tlie other acids exert little or no uction on it ; heated to red- ness in the air, a very superScial blue or purple film of oxide forms on the surface, which is again reduced at a white heat. It melts at 156°— WiMlgwood. Sp. ^r. 11-3 to 12-1 (11-8 — \V xillaston; 12 14 — Vauquelin). It readily unites with cupper, silver, and some other metals, by fusion, Tetlt. 1, The neutral solutions of palla- dium are precipitated in the metallic state by ferrous sulphate, dark brown by sulphuretted hydroiien, olive by ferrocyanide of potassium, and yellowish white by cyanide of mercury. — 2. A drop of tincture of iodine placed on the surface of metallic palladium, and then evapo- rated by the heat of a spirit lamp, leaves a black spot. By the last two teets palladium is readily distinguished from platinum. Uaei. It has been employed to form the scales of mathematical and astronomical in- struments, nnd is used in dentistry. Its alloy with silver is a very valuable white metal. It is also used for making the smaller divisions of grain and gramme weights. Palladium is not tarnished by sulphuretted hydrogen. An alloy of 1 part of palladium and 100 parts of steel is well adapted for cutting instruments which re- quire to be perfectly smooth on the edge. PALMITIC ACID. HC,fH,fi,. Prepared from palinitin {»ee next article), by saponifii'a- tion, as stearic acid is prepared friim stearin. It forms pearly scales, and melts at 140° Fahr., like mariiuric acid, which it closely resembles. PAL'MITIN. Sgn. Tbipaxmitin. CjHs (C|8H3iOj)s. The solid portion of palm oil, puriKed by crystallisation from hot ether. White; soluble in ether and slightly so in hot alcohol; melts at 118° Pahr.; by saponitication it is converted into palmitic acid. (See above.) PALPITA'TION. %«. Palpus, Palpitatio coBDia, L. A violent and irregular beating or action of the heart, either temporary or occasional. When it does not arise from sud- den or violent agitation or distress of mind, it may be regarded as a symptom of a disturb- ance of the nervous functions by disease, in which case attention should be directed to the removal uf the primary affection. PAL'Sy. See Paralysis. PANACE'A. A term formerly applied to th se I emedies which were supposed to be capable of curing all diseases, and still applied to some quack medicines. FANA'DA. See Bbead jellt (under Jklly). PAH'ART PEXMEHTA'TIOIT. The vim)U8 fermentation as developed in the dough of bread. PAN'CAKES. These are essentially fried batter, variously enriched and flavoured, ac- cording to the tiste of the cook. Wluii they contain Irnit, fish, meat, or poultry, or are highly seasoned or ornamented, they are com- monly called FBITTKKS. Prep. (M. Soyer.) Break 2 to 4 eggs into a basin, add 4 small table-spoonfuls of flour, 2 teaspoonfuls of sugar, and a little salt; beat the whole well together, adding, by degrees, i pint of milk, or a little more or less, depend- ing on the size of the eggs and the quality of the flour, so as to form a rather thick batter ; next add a little ginger, cinnamon, or any other flavour at will; lastly, pnt them into the pan, and when set, and one side brownish, lay hold of the trying-pan at the extremity of the han- dle, give it a sudden but slight jerk upwards, and the cake will turn over on the other side ; when this is brown, dish up with sifted sugar, and serve with lemon. See Feitteks. PAKCREAS. This gland, popularly known as the sweet-bread, secretes a colourlci^s and slightly viscid fluid, which p"S^esse.s the pro- perties of — 1. Converting starch into sugar; 2. Of emulsifying fats and oils. And since it is necessary that the starchy and the fatty ingredients of the food should undergo this preparatory cliange before they are in a con- dition to become assimilated by the animal economy, itwill be seen that^ancrea^ta (as the secretion from the pancreas is called) performs an important function in bodily nutrition. With a knowledge of these facts before them, it is not surpri>ing that the employ- ment of pancreatin in disease should have been recommended by therapeutists. Dr Harley, we believe, first brought this remedy tu the notice of medical men in 1S5S, since which time its principal advocate has been Dr Horace Dobell, whose method of pre- paring an emulsion from it, as well as for procuring the pancreatin pure and simple, are given below. Bernard, correctly divining that the pan- creatic fluid was concerned in the process of digestion, conceived that it aided the assimila- tion of the fatty and oily portions of the food, by saponifying them. Subsequent physiolo- gists have, however, shown, " that the action of the pancreatic secretion is evidently to break up the large granules, crystals, and globules of oil and fat into myriads of minute particles of from TiAns"* '° Huiiiith of an inch in dia- meter. In this way the fat is emulsified and converted into a milky liquid, which mixes freely with water, and passes through the tissues of the intestines into the lacteals."' Pancreatin has an alkaline reaction, and putrefies very quickly. It seems to contain a nitrogenous organic principle, resembling ptyalin or diastase in properties. It is coagu- lated both by heat and nitric acid', and is one of the few secretions in which albumen is present in a soluble condition. Even when rendered acid, pancreatin does not lose its power of emu!>ifying fatty bodies. At the moment of food being introduced into the stomach the pancreas gives out this secre- ^ Letheby. 1232 PANCEEATIN— PAPEE tiou, which is not very abondnnt at first, but gradually continues to increase for about four hours, when it as gradually diminishes for .three hours more, and then ceases altogether. £idder and Schmidt give the following as the composition of the pancreatic fluid or pancrea- tin: — Water .... 900-76 Organic matter (pancreatin) 90-38 Chloride of sodium . 7'36 Free soda .... 0-32 Phosphate of soda 0-45 Sulphate of soda 0-10 Sulphate of potassa . 0-02 r Lime 0-54 Combinations •< Mnguesia . 005 L Oxide of iron 002 1000-00 PANCREATIN. S^n. Panceeatinum. 1. (Pereira.) Cut the fresh pancreas of the pig, freed from fat and all foreign matters, into small pieces, and digest with ether. If the ether be afterwards distilled off from the filtered liquid, the pancreatin will be left as an oily product. 2. (Griffith.) It is obtained from the pan- creas of recently killed animals by treating the colourless, viscous juice with alcohol, and drying the precipitate in vacuo. Pancreatin is given for stimulating the digestion of fatty compounds. The ordinary dose is 10 grains, taken in a glass of wine or water after a meal. Dr Dohell's " Crude Pancreatic Emulsion" is prepared as follows : — After freeing from fat and all foreign matters the pancreas of a freshly-killed pig, 2i lbs. of purified pancreas are bruised in a marble mortar, and to it are added 2i lbs. of lard ; these are well beaten together, and then to the mixture 3 lbs. of water are added, very gradually, so as to ensure tile perfect absorption of the latter. The pancreatised (at is prepared by shaking up one part of the ' crude emulsion ' with three parts of ether, allowing the mixture to stand, drawing off the ethereal solution, and carefully distilling off the ether. The pan- creatised fat remains. Dr Dobell says that pancreatised fat, unlike the crude fat, has no tendency to putrefy. His ' purified pancreatic emulsion ' is made by mixing very carefully together 5 parts of pancreatised fat, 7i parts of distilled water, and 2^ parts of rectified spirit, and flavouring with oil of cloves. (3.) SaCCHAEATED PiUOEEATIir.) Mr Mattison' adopts the following process for the preparation of this substance : — The pancreas is dissected and macerated in water acidu- lated with hydrochloric acid for about forty- eight hours, then separated, and the acidulated solution of pancreas passed through a pulp filter until it is perfectly clear. To this clear 1 ' Aniericiin Journal of Pharmacy.* solution is then added a saturated solution of chloride of sodium, and allowed to stand until the pancreatin is separated. This is carefully skimmed off and placed upon a muslin filter, and allowed to drain, after which it should be washed with a less concentrated solution of sodium chloride, and then put under the press. When all the salt solution has been removed, and the mass is nearly dry, it is rubbed with a quantity of sugar of milk, and dried thoroughly without heat, after which it is diluted until ten grains emulsify two drachms of cod-liver oil. PANIFICA'TION. The changes which occur in fljur-dough under the influence of the fer- mentative process and heat, by which it is converted into bread. PAPA'VEKINE. Syn. Papaveeina. An alkaloid discovered by Merck in opium. It crystallises in needles; is insoluble in water; is slightly soluble in cold alcohol and in ether; and forms crystallisable salts with the acids which possess little solubility. The hydro- chlorate, one of the most characteristic of these compounds, crystallises in beautiful colourless prisms, which possess a high re- fractive power, and are only very slightly soluble in dilute hydrochloric acid. Fluckiger states that papaverine is much less active than thebaine, that it is not soporific either with men or animals, that it does not aiTest diarrhoea, and is but slightly analgesic. PALAMOND. Chocolate 1 oz.; rice flour, 4 02. ; potato arrowroot, 4 oz. ; red sanders, in fine powder, 1 dr. Mix. (In the above, by chocolate is meant the cacao beans roasted and pulverised without addition. Indian arrow- root, or Tous les mois, may be substituted for the potato arrowroot.) PAPEE. Sj/n. Chabta, Paptetis, L. ; Papiee, Pr. The limits of this work preclude the introduction of a description of the manu- facture of this well-known and most useful article, which is now almost exclusively made by machinery of an elaborate and most inge- nious description. We must, therefore, con- tent ourselves with a short notice of a few of the preparations of the manufactured article. (See below.) Good white paper should be perfectly devoid of odour, and when burnt it should leave a mere nominal amount of ash ; digested in hot water, the liquid should be neutral to test paper, and not affected by sulphuretted hydro- gen or the alkaline sulphurets, or by tincture of iodine. Coloured papers should not contain any deleterious matter. Paper, Antirheumatic. S^». Chaeta AJf- TiEHEUMATiCA. (M. Berg.) Euphorbium 30 parts; cantharides, 15 parts; alcohol, 150 parts. Digest eight days, filter, and add resin, 60 parts; and turpentine, 50 parts. Thin paper is to be brushed over two or three times with this varnish. Paper, Atropine. %». Chabta ateopi^;. Paper is impregnated by steeping in solution of sulphate of atropia in such a manner that a PAPEB 1233 piece |th of nn inch square shall cnntnin f Igth iif a grain of the salt j a square of -j'^th of uu inch the yj^jj*'' °^ " R™'"- Tliis square inserted between the eyelid will dilate the pupil. Paper, Atropine, Gelatinised. Tablets of gelatin are impregnated with sulphate of alropia. us above. Paper, Anti- asthmatic. (P. Codex). Si/n. Chaktafcmiveea, L. Cabtonanti-asthma- TIQ0E, I'r. Unsized grey filtering paper; 12 oz.; nitre, 6 oz, ; belladonna, stramonium, digitalis, lobelia inflata, phellandriuni, all in powder, i "z. of each; myrrh and olibanum, in powder, 1 oz. tufili. Tear the paper in pieces and soak it in water till quite soft; drain off the trriiiter piirt of the water, and beat it into a paste; iniorpnrate with it the powders pre- viously mixud. Then put into tinned iron moulds, and dry by a stove. Paper, Blistering. See Vestoants. Paper, Cloth. This is prepared by cnverii^g gMuze, calicn, canvas, &c., with a surface of pupor pulp in a ' Poudrinier manbine,' and then finishing the compound sheet in a nearly similar manner to that adopted for ordinary paper. Paper, Col'oured. For those papers which are merely coloured on one side tlie pigments, ground up with gum water or size, or the stains thickened with a little of the same, are applied witli a brush, after which the sheets are suypeuded on a line to dry. For paper coloured tliroughout its substance the tinctorial matter is usually mixed with the pulp in the process of manufacture; or the nianuf;u'tured paper is dipped into a bath of tlie colouring substance, and then hung up to dry. Paper, Cop'ying. i¥«p. Make a stiff oint- ment with butter or lard and black lead or lamp black, and smear it thinly and evenly over soft w ritiug paper by means of a piece of lliinncl; the next day wipe off the superfluous jioi tion with a piece of soft rag. f/'vf, \c. Placed on wliite paper and writ- ten on with a style or solid pen, a copy of the writing is left on the former. By lepeating the arrangement, 2, 3, or more copies of a letter may be obtained at onee. This paper, set up in a case, forms the ordinary ' manifold writer' of the stationers. The copying or transfer paper used for obtaining fac-siiiiiles of letters written with 'copying-ink' is merely a superior quality of bank-post paper. Paper, Em'ery. See Emebt. Paper, Glass. Prep. From powdered glass, as emery paper. Used to polish wood, ic. See Glass (Powdered). Paper, Gout. 5y». Charta anti-aethei- tica. Ij, ; Papier FAYAEr, Fr. Prep. 1. Eu- pliorbiuni, 1 part; cantharides, 2 parts (both in powder); rectified spirit, 8 parts; ether, 3 parts; di^'est in a stoppered bottle, with fre- quent agitation, for a week; to the strained tincture add ul Venice turpentine, 1 part; VOL. II. lastly, dip thin white paper into it, and dry the sheets in tlie air. 2. (Molir.) Euphorhium, 1 dr. ; cantharides, 4 dr. ; rectified spirit (strongest), 5 oz. ; make a tincture, to which add of Venice turpentine. It oz., previonsly liquefied with resin; 2 oz. ; and spread the mixture, whilst warm, very thinly on paper. Used as a counter-irritant in gout, rheumatism, &c. Paper, Hydrograph'ic. An absurd name given to paper which may be written on with simple water or with some colourless liquid having the appearance of water. Prep. 1. A mixture ofnnt-galls, 4 parts, and calcined sulphate of iron, 1 part (both perfectly dry and reduced to very fine powder), is rubbed overthe surface of the paper), and is tiien forced into its pores by powerful pressure, alter wliinh the loose portion is brushed olf. Writes black with a pen dipped in water. 2. From persulphate of iron and ferroey- anide of potassium, as the last. Writes blue with water. 3. As the last, but using sulphate of copper instead of sulphate of iron. Writes reddish brown with water. 4. The paper is wetted with a colourless solution of ferroeyanide of potassium, and after beini; dried is written on with a colourless solu- tion of persulphate of iron. Writes blue. Ohs. 'I'be above applications, we need scarcely say, are more amnsing than useful. Se Sympathetic ink. Paper, Incombus'tihle. See Incombustibib FABRICS. Paper, Irides'cent. Prep. ( Beasley.) Sal aiiinioniae and sulphate of indigo, of each 1 part; sulphate of iron, 5 parts; nut-galls, 8 parts; gum Arabic, ^th part; boil them in water, and expose the paper washed with the liquid to (the fumes of) ammonia. Paper, Issue. Syn. Chabta ad ponti- OTTLOS, L. Prep. (Soubeiran.) Elemi, sperma- ceti, and Venice turpentine, of each 1 part; white wax, 2 parts ; melt them together by a gentle beat, and spread the mixture on paper. Used to keep issues open. Paper, Li thograph'ic. Prep. 1. Starch, 607,. ; gum Arabic, 2 oz. ; alum, 1 oz. ; miike a strong solution of each separately, in hot water, mix, strain through gauze, and apply it whilst still warm to one side of leaves of paper, witli a clean painting-brush or sponge ; a second and a third coat must be given as the preceding one becomes dry; the paper must be, lastly, pressed, to make it smooth. 2. Give the paper 3 coats of thin size, 1 coat of good white starch, and 1 coat of a solution of gamboge in water; the whole to be applied cold, with a sponge, and each coat to be allowed to dry before the other is applied. The solutions should be freshly made. TJse, S;c. Lithographic paper is written on with lithographic ink. The writing is trans- ferred by simply moistening the back of the paper, placing it evenly on the stone, and then 78 1234 PAPER applying pressure a reversed copy is ob- tained, which, when printed from, yields cor- rected copies resembling the original writing or drawing. In this way the necessity of executing the writing or drawing in a re- versed direction is obviated. See LiiHO- SEiPHr, Ink, &o. Paper, Paste. Boil white paper in water for five hours ; then pour ofE the water, and pound the pulp in a mortar ; pass it through a sieve and mix with some gum water or isinglass glue. It is used in modelling by artists and architects. Paper, Oiled. Prep. Brush sheets of paper over with 'boiled oil,' and suspend them on a line till dry. Waterproof. Extensively em- ployed as a cheap substitute for bladder and gut skin to tie over pots and jars, and to wrap up paste blacking, ground white lead, &c. Paper Parch'ment. %». PAPrHiN, Veoe- TABLE PARCHMENT. Frep. 1. (Poumarfede and Figuier.) Dip white unsized paper for half a minute in strong sulphuric acid, sp. gr. I'8i2, and afterwards in water containing a little ammonia. 2. (W. E. Gaine, Patent 1857.) Plunge unsized paper for a few seconds into sulphuric acid diluted with half to a quarter its bulk of water (this solution being of the same tem- perature as the air), and afterwards wash with weak ammonia. This process, now extensively worked by Messrs De la Rue and Co., pro- duces a much better material than does that of Poumarede and Pignier. , Prop. A tough substance, resembling animal parchment, and applicable to the same pur- poses. It is largely used for covering pots of pickles and preserves, and by the chemist for the intervening membrane in experiments in diffusion. See Dialtser, Dialysis, &c. Paper, Protective. Various attempts have from time to time been made to prepare paper which might make the fraudulent alteration of cheques and other documents difficult or impossible. These attempts have taken two different directions, which may be briefly desci'ibed. The first and best known method consists in printing, in some delicate and easily de- stroyed colour, a complicated pattern on the face of the paper. Any reagent which will remove the writing will, of course, destroy the pattern below, and so render the alteiation evident. The cheques used by Messrs Coutts and Co. are fine examples of this kind of pro- tection, the whole of the paper being printed over with the name of the firm in characters so delicate, that they can scarcely be read without the assistance of a lens. The obvious objection to this method is, that it is possible for a skilful forger to re- place the printed design before the completion of the alteration. The otlier method consists in the introduc- tion into the paper during its manufacture of «ome substance or mixture of substances which shall strike a characteristic colour when chemical agents are applied to the ink. One of the earliest attempts of this kind was that of Stephenson, who introduced ferro- cyanide of potassium into the pulp. When any acid was applied to the writing, Prussian blue was formed with the aid of the iron of the ink. In another process iodide of potas- sium and starch were introduced into the paper, the application of chlorine then pro- ducing a blue stain (iodide of starch), while in a third (Robson's) the pulp was stained with the ingredients of common writing ink. None of these methods gave, however, any very efiicient protection against fraud, for in each case it was tolerably easy to restore the paper to its original condition. But another process which followed npon the others has proved more successful, and, when properly applied, gives a paper which is practically secure. This process was patented by Barclay," and consists in the introduction into the pulp of ferrocyanide of manganese. When any acid is applied to the writing on this paper the blue stain of Prussian blue appears. This can, it is true, be removed by alkalies, but in that ease the manganese is precipitated as the brown peroxide, an effect also produced by bleaching powder. This brown stain can be removed by sulphurous acid, but in that case Prussian blue appears simultaneously, so that the forger has merely a choice between a brown and a blue stain. When such paper is printed with a delicate design in some fugitive ink (common writing ink would be best), the greatest attainable safety is obtained. Ferrocyanide of manganese is easily formed by adding to the pulp pure crystallised chlo- ride of manganese, and rather more than an equal weight of ferrocyanide of potassium, both in solution. (Heaton.) Paper, Ba"zor. Smooth unsized paper, one of the surfaces of which, whilst in a slightly damp state, has been rubbed over with a mix- ture of calcined peroxide of iron and emery, both in impalpable powder. It is cut up into pieces (about 5x3 inches), and sold in packets. Used to wipe the razor on, which thus does not require stropping. Paper, Razor-strop. From emery and quartz (both in impalpable powder), and paper pulp (estimated in the dry state), equal parts, made into sheets of the thickness of drawing paper, by the ordinary process. For use, a piece is pasted on the strop and moistened with a little oil. Paper, Ee'siu. Syn. Poor-man's piaster; Chabta kesinosa, L. Prep. 1. Beeswax, 1 oz. ; tar and resin, of each, 3 oz. ; melted together and spread on paper. 2. (Ph. Bor.) Paper thinly spread over with black pitch. Calefacient, stimulant, and counter irritant; in rheumatism, chest affec- tions, &c. PAPER 1235 Paper, Shen'matiam. See Pafbbs, Gout, and Uesin. Paper, Safe'ty. Syn. Papibb'db bubbt^, Fr. White paper pulp mixed with an equal quantity of pulp tinged with any stain ea>ily iiffected by chlorine, acids, alkulies, &c., and made into sheets as usual. Paper, Test. Syn. Chaeta exploeatoma, L. Under this head may be conveniently in- cluded all the varieties of prepared paper em- ployed in testing. For this purpose sheets of unsized paper or of good ordinary writing paper (preferably the first), are uniformly wetted with a solution of the suit, or with a cold in- fusion or decoction of the tinctorial substance in distilled water, and are then hungup to dry in a current of pure air ; they are, lastly, cut into pieces of a convenient size, and preserved in closed bottles or jars. For use, a small strip of the prepiired paper is either dipped into or muistencd with the liquid under examina- tion, or it is moistened with distilled water and then exposed to the fumes. A single drop, or even less, of any liquid may be thus tested. The following nre the principal test papers and their applications : — 1'apku, Huazil-wood. Prom the decoction. Alkalies turn it purple or violet; strong acids, red. Papee, BtrcKTHOEif. From the juice of the berries. Keddened by acids. Papke, CiiBBaT-JCiOE. As the lust. Papke, Daiilia, Gkobgina p. From an infusion of the petals of the violet dahlia {Oeorgina purpurea), Alkulies turn it gre<'n ; acids red ; strong caustic alkalies turn it jellow. Very deliciite. Paphe, Eloehueeet. From the juice of the berries. As the last. Papeb, Indioo. From a solution of indigo. Dei oloured liy chlorine. Papke, Iodine op PoTASsiust. «. From the solution in distilled water. Turned blue by an acidulated solution of starch. 4. From a mixture of a solution of iodide of potassium iiiid starch paste. Turned blue by chlorine, ozone, and the mineral acids, and by air containing them. Papeh, Lkad. From a solution of either acetate or diaeot.ito of lead. Sulphuretted hydrogen and hydrosnlphuret of ammuuia turn it black. Papee, LiTjrrs. In general, this is pre- pared from infusion of litmus, without any pre- caution, but the following plan may be adopted when a superior test paper is desired; — ». (Blue.) Triturate cumniereial litmus,! oz., in a wedgivoi Ill-ware mortar, with boilingwater, 3 or -t 11. oz. ; put the mixture into a fiask, and add more boiling water until the liquid measures fully J pint; agitate the mixture frequently until it is cold, tlien filter it, and divide the filtrate into two equal portions; stir one of these wii h a glass rod previously dipped into very dilute sulphuric acid, and repeat the operation until the litmus infusion begins to look very slightly red, then add the other half of the filtrate, and the two being mixed to- gether, dip strips of unsized paper into the liquid, in the usual manner, and dry them. Acids turn it red ; alkalies blue. The neutral salts of most of the heavy metals also redden this, as well as the other blue test papers that are affected by acids. b, ( Red.) The treatment of the whole quan- tity of the infusion (see ahove) with the rod dipped in dilute sulphuric acid is repeated until the fluid begins to look distinctly red, when the paper is dipped into it as before. The alkalies and alkaline earths, and their sulphides, re- store its blue colour ; the alkaline carbonates and the soluble borates also possess the same property. Very sensitive. An extemporaneous red litmns paper may be prepared by holding a strip of the blue variety over a pot or jar into which 2 or 3 drops of hydrochloric acid have been thrown. Papbb, Mallow. From an infusion of the purple flowers of the common mallow. Affected like ' dahlia paper.' Papee, Manganesb. From a solution of sulphate uf manganese. Ozonised air blackens it. Papee, Rhubabb. From a strong infusion of the powdered root. Alkulies turn it brown ; but boracic acid and its salts do not affect it. Very sensitive. Papee, Rose. From the petals of the red rose, as'thelast. Alkalies turn it bright green. I)r A. .S. Taylor recommends the infusion to he very sligiitly acidulated with an acid before dipping the paper into it. More sensitive than turmeric paper. Papku, Staech. From a cold decoction of starch. Free iodine turns it blue. Papee, Sulphate op Ieon. From a solution of ferrous sulphate. As a test for hydrocyanic acid and the soluble cyanides. Papek, TURMEKIC. From decoction of tur- meric (2 oz. to the pint). It is turned brown by alkalies, and by boracic acid and the soluble borates. It is not quite so susceptible as some other tests, but the change of colour is very marked and characteristic. Paper, Tra"cing. Prep. Open a qnire of smooth unsized white paper, and place it flat upon a table, then apply, with a clean * sash tool,' to the upper surtace of the first sheet, a coat of varnish made of equal parts of Canada balsam and oil of turpentine, and hang the pre- pared sheet across the line to dry ; repeat the operation on fnsh sheets until the proper quantity is finished. If not sufficiently trans- parent, a second coat of varnish may be applied as soon as the first has become quite dry. 2. Rub the paper with a mixture of equal parts of nut oil and oil of turpentine, and dry it immediately by rubbing it with wheaten flour; then hang it on a line for 2-i hours to dry. 1236 PAPER HANGINGS— PAPINS DIGESTER Obs. Both the above are used to copy draw- ings, writing, &c. If washed over with ox- gall and dried, they may be written on with ink or water colours. The first is the whitest and clearest, but the second is the toughest and most flexible. The paper prepared from the refuse of the flax-mills, and of which bank- notes are made, is also called ' tracing paper,' and sometimes 'vegetable paper.' This re- quires no preparation ; but though very flexible, it has little strength. Paper, Var'nished. Before proceeding to varnish paper, card-work, pasteboard, &c.,itis necessary to give it 2 or 3 coats of size, to pre- vent the absorption of the varnish, and any injury to the colour or design. The size may be made by dissolving a little isinglass in boiling watei', or by boiling some clean parch- ment cuttings until they form a clear solution. This, after being strained through a piece of clean muslin, or, for very nice purposes, clari- fied with a little white of egg, is applied by means of a small clean brush called by painters a sash tool. A light, delicate touch must be adopted, especially for the first coat, lest the ink or colours be started, or smothered. When the prepared surface is perfectly dry, it may be varnished in the usual manner. See Maps, Vaenish, &c. Paper, 'Wa"fer. See Waibes. Paper, Waxed. Frep. Place cartridge paper, or strong writing paper, on a hot iron plate, and rub it well with a lump of beeswax. Used to form extemporaneous steam or gas pipes, to cover the joints of vessels, and to tie over pots, &c. PAPER HANGINGS. Theornamental paper used to cover the walls of rooms, &c. Under the old system, the paper, after being sized and prepared with a ground colour, had the pattern produced on it by the common process of ' stencilling,' a separate plate being em- ployed for each colour that formed the pat- tern. To this succeeded the use of wooden blocks, the surface of which bearing the design in relief, and being covered with colour, was applied by simple hand pressure on the paper, in a precisely similar manner to that adopted in the block-printing of calicoes. The cylinder calico-printing machine has now been suc- cessfully applied to the manufacture of paper bantlings. The colours employed for paper hangings are — Blacks. — Frankfort, ivory, and blue black. Blues. Prussian blue, verditer, and facti- tious ultramarine. Beowks. Umber (raw and burnt), and mixtures. Geays. Prussian blue and blue black, with Spanish white. Gebeits. Brunswick green, Scheele's g , Schweinfurt g., and green verditer; also mix- tures of blues and yellows. Keds. Decoctions of Brazil wood (chiefly), brightened with alum or solution of tin ; the red ochres ; and, sometimes, red lake. Violets. -Decoction of logwood and alum; also blues tempered with bright red. YELL0V7S. Chrome yellow, decoction of French berries or of weld, terra di sienna, and the ochres. Whites. White lead, sulphate of baryta, plaster of Paris, and whiting, and mixtures of them. The vehicle employed to give adhesiveness and body to the colours is a solution of gelatin or glue, sufficiently strong to gelatinise on cooling. The satiny lustre observable in some paper hangings (SATIN PAPEES) is produced by dust- ing finely powdered French chalk over the sur- face, and rubbing it strongly with a brush or burnisher. The ground for this purpose is prepared with plaster. Flock and velvet papbbs are produced by covering the surface of the pattern with a mordant formed with boiled oil thickened with white lead or ochre, and then sprinkling powdered woollen flocks on it. These are pre- viously dyed, and ground to the required fine- ness in a mill. PAPIER-HACHE. Pulped paper moulded into forms. It possesses great strength and lightness. It may be rendered partially wa- terproof by the addition of sulphate of iron, quicklime, and glue or white of egg to the pulp ; and incombustible by the addition of borax and phosphate of soda. The papier- mdche tea-trays, waiters, snuff-boxes, &c., are prepared by pasting or glueing sheets of paper together, and then submitting them to powerful pressure, by which the composition acquires the hardness of board when dry. Such articles are afterwards japanned, and are then perfectly waterproof. The refuse of the cotton and flax mills, and numerous other substances of a like character, are now worked up as papier-mache, and the manufactured articles formed of them are indistinguishable from those prepared directly from paper. PAPIN'S DIGESTER is a strong, closed, iron vessel, in which water can be heated above 212° F., thereby acquiring a temperature that adds considerably to its solvent powers. This apparatus is put to many useful applications in the arts, of which one is the speedy extrac- tion of gelatin from the earthy matter of bones. The bones may be boiled for hours at 212° without any such effect being produced. The high temperature aiqiiired by the water is effected by the confinement of the steam, the internal pressure of which can be regu- lated by means of a safety valve attncbed to the vessel. By this arrangement the water may be kept at any uniform temperature above 212° at pleasure. Professor Junichen' recom- mends the use of the digester for the purpose of boiling meat and other food. It appears ' * Chemiciil News.' PAPYRIN— PARALYSIS 1237 from the nnthor'g experiments that the time for ciokiiig viirioiH iirticles of daily consuiap- tioii is much shorter when efEeeted under strong pri-ssure, while a great saving of fuel is also iffooii'il. PAPY'RIN. See Papbb (Parchment). PAR'ACHUTE. In aerostation, an instru- ment or apparatus having for its object to rutard thf descent of heavy bodies through the air. The only form of parachute which h:is been hitherto adopted with success is that of the common umbrella when extended. The m:iteriiil-i of which the apparatus is miide arc canvas and cord, both light but strong, and careluUy put together. The car to contain the adventurer resembles that of the balloon, only smaller. It is estimated that a circular parachute, to descend in safety with an adult, weighing, with the apparatus, 225 lbs., must have a dia- meter of at least 30 feet. Its terminal velo- city would then he at the rate of 12 to 13 feet per second, or about f<| miles per hour; and the shock experienced on contact with the earth would be equal to that which the aeronaut would receive if he dropped (reely from a height about 2i feet. Scvcial descents from balloons, after they have acquired a gnat elevation, have been effected without accident by means of para- chutes. Unfortunately, however, any want of iutegrity in the machine, or any accident which may happen to it after its detachment from the balloon, is irreparable and fatal. PARACYAH'OQEN. The brown solid miitter left in the retort when cyanide of mercury is decomposed by heat. It is isomeric with cya nogen. PARAFFIN. Si/n. Tau-oil steaein. This remarkable hydrocabon is one of the several substances discovered by Reichcubach in wood- tar. Prep. 1. (Prom WOOD-TAB. Reichenbach.) Distil beech-tar to dryness, rectify the oily portion of the product which is heavier than water until a thick matter begins to rise, then change the receiver, and moderately urge the heat lis long as :inything passes over; next digest tlie product in the second receiver, in an eqii.il nieiiBiire of alcohol of SSS, gradually add (i or 7 parts more of alcohol, and expose the whole to a low temperature j crystals of pnriiflin will gradually fall down, which, after being washed in cold alcohol, must be dis- solved in boiling alcohol, when crystals of pure paraffin will be deposited as the solution cools. 2. (From COAIi — James Young, Patent 1850.) The details of this process for obtain- ing piiruffin and its cniffeners by the slow dis- tilhition of coal (preferably ' Boghead') are given in our article on pabaffin oil. The solid paraffin is separated from the last pro- ducts, or 'heavy oils,' by artificial cold; it is then melted and run into moulds. 8. (From Kanqoon petboieum — Patent.) In this proccs', which is worked by Price's Candle Company, superheated steam is em- ployed as the he;itlng agent. The paraffin, or ' BELMOKTINB,' as it is called, is the last pro- duct which distils over. 4. (From peat.) The various processes which have been suc;i:ested for obtaining paraffin from peat, turf, &c., are similar in principle to Young's. The great point is to conduct the distillation at as low a temperature as possible. Prop. A wiiite, hard, translucent body, melting at 110'-' Fahr. and upwards, according to its source, and burning with a briirht white flame. It has great stability — sulphuric acid, chlorine, and nitric acid iielow 212' exerting no action upon it. Dr Anderson states tliat its composition and properties vary with the source from which it is derived. \V'ith respect to the melting point, this variation is very remarkable. Thus, Young's paraffin, from licig- head coal, melts, acconliug to the observations of Dr Anderson, at 11 1", nliile tliat from Ran- goon petroleum (' belmontine') melts at 140', and that from turf at lit)'. Use». Paraffin is now largely used for making candles, for wiiich purpose it is specially adapted, being a most elegant substance, and surpassing all other candle materials, even spermaceti, in illuminating power. Its pro- perty of n.it being acted upon by acids or alkalies renders it suitable lor stoppers for vessels holding chemical liquids; also for elec- trotype moulds. It is not acted upon by ozone, so that it has been employed with great advantages in experiments on this body for rendering air-tight the joints formed by the union of glass tubes. As it contains no oxygen, it might be employed to protect .oxydisable metals like sodium and potassium from contact with the air. One use of pa- raffin candle-ends will commend them to the ladies of the household — a small piece of paraffin added to starch will be found to give a gloss and brilliancy of surface to the starched linen that can be obtained by no other additi' n. PARAFFIN OIIi. See OiM. PARAL'YSIS. iSyn. Palsy. A loss or con- siderable diminution of power of voluntary motion, or functional action, of any part of the body. In its most usual form one side only of the body is affected. It not uncommonly seizes the lower extremities, or all parts below the pelvis; sometimes the arms only; and occasionally a part, as one side of the face, one eyelid, the tungue, or the muscles of degluti- tion. In these cases the speech frequently becomes indistinct and incoherent, and the memory and judgment impaired, whilst the distorted features assume a more or les^ revolting aspect. The causes of paralysis are various. It may be occasioned by pressure on particular parts of the brain, the spinal marrow, or the nerves ; by poisons, the long-continued use of sedatives. 1238 PARANAPHTHALIN— PA RASITES local injuries, tlie sudden suppression of pro- fuse and habitual evacuations, and by what- ever tends to greatly relax or enervate the system. It may also be a consequence of an attack of apoplexy, or it may be symptomatic of other diseases, as scrofula, syphilis, and worms. When it is of a distinctly local cha- racter it may arise from'cxcessive use or undue employment of the part or organ. That of old age is, probably, a mere consequence of the failing nervous energy of the system being unequally distributed. Palsy usually comes on with a sudden and immediate loss of the motion and sensibility ot the parts; but in a few instances it is pre- ceded by a numbness, coldness, and paleness ; and sometimes by slight convulsive twitches. If the disease affects the extremities, and has been of long duration, it not only produces a loss of motion and sensibility, but likewise a considerable flaccidity and wasting away of the muscles of the parts affected. When palsy attacks any vital part, such as the brain, heart, or lungs, it soon terminates in death. The treatment of paralysis depends upon a careful consideration of its cause. The first object should be, as far as possible, to remove any compressing force, and to gradually arouse the torpid portion of the nervous system. In general, more or less depletion will be found beneficial, together with rather active purga- tion, and nervous stimulants, as ammonia, musk, &c. Blisters to the head and neck are also appropriate. With the debilitated and aged, venesection must be avoided. Stimulant and rubefacient frictions and liniments, tlie vapour bath, and other like remedies, also fre- quently iirove useful. In local attacks of the disease, as the loss of use of one of the hands, arms, legs, &c., no agent has proved so gene- rally successful as voltaic electricity. For this purpose the current sliould be in one direction only, and continued uninterruptedly for some time daily. When the direction of the cur- rent is alternate, with slight shocks, as in the common coil machine, this agent is of doubt- ful utility, except for occasional use. In all cases medical aid should be sought as early as possible. PAEANAPH'THALIN. Si/n. Anthbacen. See Anthbacen. PAEAPEC'TIN. See Peotiw. PAE'ASITES. The parasitical animals that infest the human body are referred to under the heads Acaei and Pediculi. Parasites, Human. The following is a list of the principal parasites infesting man. It is extracted from the ' Dictionary of Hygiene,' of W.\nter Blyth, who states that he has arranged it, with some slight alterations, from a table in Dr Aitken's ' Science and Practice of Medicine.' The two first divisions include animal parasites, the third vegetable ones. No. 1, or Entozoa, are animal parasites found inside the human body; No. 2, those found outside; No. 3, consisting of vegetable para- sites, comprises Mntophyta and Epiphytal the former existing in the interior, and the latter on the exterior of the human body. Some of the principal parasites have already been described and figured in these pages. I. Entozoa. Acephalocystis endogena, liver. „ multifida, brain. Anchylostomum, sen Sclerostoma dnodenale, intestines. Anthomia canicularis, intestines. Ascaris alata „ „ lumbricoides „ „ mystax „ Bilbarzia seu Distoma hsimatobia,, portal a tid venous system. Bothriocephalus cordatus, intestines. „ latus „ Cysticercus cellulosse. seu telae cellulosse (C. of Tenia solium), muscles. Cysticercus of TseniiB marginata (C. tenui- collis), intestines. Dactylius aculeatus, urinary bladder. Diplosoma crenatus. Distoma seu Distomum crassum, duodenum. „ hepaticum seu Pasciola hepatica, gall- bladder. „ heterophryes, intestines. „ lanceolatum, hepatic duet „ oculi humani seu ophthalmobium, capsule of crystalline. Dltrachycerus rudus, intestines. Echinococcns hominis (hydatid of Tsenia echi- nococcus), livery spleen^ and omentum. Filaria bronchialis seu trachealis, bronchial glands. seu dracunculus medinensis, sJcin and areolar tissue, „ sanguinis hominis, blood. „ oculi seu lentis, eye. Hexathrydium pinguicola, ovary. „ venarum, venous system, Monostoma lentis, crystalline. Qilstrus hominis, intestines. Oxyuris vermicularis, „ Fentastroma coustrictum, intestines and liver. „ deuticulatum, intestines. Polystroma pingnicola, ovary. „ sanguioola seu verarum, venous system. Spiroptera hominis, urinary bladder. Strongylns seu Eustrongylus brouchialus,i»-o»- chial tubes. „ seu Eustrongylus gigas (Acarus renalis), kidney and intestines. Taenia acanthotrias, intestines, „ elliptica, „ „ flavopuncta, „ lophosoma, „ „ mediocanellata, „ „ nana, intestines and liver. „ solium, intestines. Tetrastoma renale, kidney. PARATAKTARIC ACID-PASTE 1239 Trichina spiralia, mutelet. Tricocepbulus dlspar, inlestinet. II. Eeiozoa. Demodox sou Acarua f'olliculorum, aehaceous nibtlanee of cutaneous follicles. Pediculus capitaa (head louse). „ corporis seu vestimenti (body lonse). I, pnlpebrarum (brow louse). n pubis, Phthirius inguinalis (crab- louso). I, tubescctiutn, phihiriasis (lousy dis- ease). Pulex penetrans (chigoS), skin, cellular tissue. Sarcoptos seu Acarus scabiei (itch insect), icabiet, III. Entophyta and Epiphyta. Achorion Lebertii (Tricophyton tonsurans), Tmea tonsurans. „ Sch5iiluinii, Tinea favosa, Chionyphe Carteri (fungus of Mycetoma), deep tissues, bones of hands and feet. Leptothrix buccalis (alga of the month). Microsporon Audouini, Tinea deoa/vans. „ Furfur, Tinea versicolor. „ mentagrophytea, follicles of hair in sycosis or meniagra. Oldium albicans (thrush fungus), mouth, mucous, and cutaneous surfaces, Puccinia favi, Tinea favosa. Sarcina vontriculi, stomach, Torula cerevisim (Cryptoeoccus cerevisiee, yeast plant), stomach, bladder, Sfc. Tricophyton sporuloi'des. Tinea polornia. PAEATAKTAE'IC ACID. See Kacemio AOID. PARCH'MENT. See Vkllcm, and Papee (Parchment). PAECHMENT PAPER. See Papkb. PAEEQOR'IC. See Tinctuke of Camphob (Compound). Paregoric Scotcli. See Tincture op Opium (Ammoniated). PAREI'EA BRA'VA. See Velvet leaf. PARE. A Hume applied to the salmon until near the end of its second year, when it loses its dark lateral bars by the superaddition of a silvery pigment. It was formerly regarded as a distinct species. PARS'IET. Syn. Petrosblinum, L. This well-known herb is the Apium petroselinmn. The root is diuretic; the fruit (seed) car- minative; the leaves are a pleasant stimu- lating salad and condiment, and iire much used to flavour broth and soup. " The fruit is u deadly poison to parrots." (Lind. ex Burnett.) PARSNIP. The root of Pastinacea sativa. The parsnip is native to England and Ire- land, but does not grow in Scotland. It is likewise met with in many parts of Europe and in nortliern Asiii. In the wild state the root is somewhat acrid, and injurious effects have been known to have followed its use as a food. By cultivation, however, it loses both its acridity and dangerous properties, and forms a table vegetable, not in universal favour. In the Channel Islands parsnips constitute the winter food of cows; and these animals when fed upon them are said to yield butter of a better quality than can be obtained from them when partaking of any other fodder. The flesh of cattle fed on the parnsip is also highly commended. In the North of Ireland the juice of the root, mixed with hops and .veast, is made into a fermented liquor. . Par- snip wiuc is an agreeable alcoholic beverage. Composition of the Parsnip. Nitrogenous matter . 11 Starch . . 96 Sugar . 5-8 Fat . 0-5 Suits . . 10 Water . . 820 1000 PASTE. Syn. Pasta, L. ; Pate, Fr. This word is very loosely applied to substances and preparations differing so widely from each other, that it would be scarcely possible to class them together. We shall, therefore, refer the reader to the individual articles. The pastes (pA.te8) of French pharmacy are eonipound medicines of the consistence of hard dough, and which do not stick to the fingers. They are formed of sugar and fjum, dis-olvod in water or in some medicated liquid. They are evaporated so as to unite these principles by degrees, and give them the pliancy and the firniness of paste. They are employed inter- nally in doses more or less variable in a similar manner to lozenges. " IMtes, properly so called, are divided into transparent, or such as are made without agitation, like jujubes of brown liquorice ; and opaque, or such as are made with agitation, like the ]iutes of mar»h- mallow, lichen, &c." (Trousseau and Revcil.) Si'C Pastes (Artificial Gems), Pastby, and beloto. Paste, Adhesive. Let 4 parts, by weight, of glue solten in 15 parts of cold water for fifteen hours, after which the mixture must be moderately heated until it becomes quite clear. To this mixture 65 parts of boil- ing water are to be added without stirring. In another vessel 30 parts of starch paste are stirred up with 20 parts of cold water, so that a thin milky fluid is obtained without lumps.. Into this the boiling glue solution is poured,, with constant stirring, and the whole is kept at the boiling temperature. When cooled the 10 drops of carbolic acid are to be added to the paste. This paste possesses great adhesive power, and may be used for leather, paper, or cardboard with great success. It must be pre- served in closed bottles to prevent evaporation 1240 PASTE of the water, and will, In this way, keep good for years. (' Dingler's Journal.') Paste, Al'mond. Syn. Pasta amtgdalina, P. amygdalaeum;, P. eeoia, L. ; Pate bot- AlE, Fr. Prep. 1. (MoiST.) — a. Take of blanched Valentia almonds, 4 oz. ; reduce them to a very smooth paste by patient pounding in a clean mortar, adding, towards the last, a little rose water, with some eau de Cologne, or 3 or 4 drops of otto of roses or ncroli, or an equivalent quantity of any other perfume, according to the fancy of the artiste. h. \ram hitter and sweet almonds (blanched), equal parts ; rose water, q. s. It requires no other perfume. c. To either of the preceding add of sper- maceti, i oz. The white of an egg, or J oz. of white soap, Is added by some makers. With about i dr. of powdered camphor to each oz. of the above it forms tlie * camphorated almond puste' of the shops. d. Take fine Narbonne honey and white bitter paste (see helow), of each 1 lb. ; beat tliem to a smooth paste, then add, in alternate portions, of oil of almonds, 2 lbs. ; yolks of 5 eggs ; and reduce the whole to a perfectly homogeneous pasty mass. Much esteemed. It is commonly sold under the name of * honey paste,' * pdte royale,' &c. In a similar manner are made nosegay, orange, rose, vanilla, and other like pastes having almonds for a basis, by merely adding the respective perfumes. 2. (PtTLVBEULENT.) — a. (Gray.) Prepared from the cake of bitter almonds from which the oil has been thoroughly expressed by drying, grindinsT, and sifting it. b. (Bitter white.) As the last, but the almonds are blanched before being pressed. C-. (Sweet white.) As the last, but using sweet almonds. Obs. All the above are used as cosmetics, to soften and whiten the skin, prevent chaps, abiasious, chilblains, &c. The honey paste, and the sweet and bitter white pastes, are those most esteemed. (See below.) faste, Almond. (In confectionery.) Frep. 1. Take of Valentia almonds, 31bs. ; bitter do., i lb. ; blanch them, and reduce them to a very smooth paste by pounding, then put them into a clean copper pan along with white sugar and good gum Arabic, of each 1 lb. (the last pre- viously dissolved in about a pint of water;) apply a gentle heat, and stir until the whole is mixed and has acquired a proper con- sistence, then pour it out on a smooth, oiled, marble slab, and when cold cut it into squares. 2. As the last, but when the mixture has acquired the consistence of thick honey, set- ting it aside to cool ; when nearly cold, the whites of 6 eggs are to be added, and heat being again gradually applied, the whole is to be stirred until it acquires the proper consist- ence, as before. 3. Blanched sweet almonds and white sugar, of each 1 lb. j blanched bitter almonds and powdered gum, of each 3 oz. ; beat them, in the cold, to a, perfectly smooth paste, with orange-flower water or rose water, q. s., so that it may be sufficiently stiff not to stick to the fingers, and then cut the mass into squares, as before. The above aie eaten as confections. Paste, Ancho'vy. Prep. Remove the larger bones from the fish, and then pound them to a smooth p»ste in a marble mortar, adding a little bay-salt and cayenne pepper at will; next rub the pulp through a fine hair sieve, and about 3-4ths fill the pots with it; lastly, cover the surface of each to the depth of about J inch with good butter in a melted state. It should be kept in a cool situation. Other fish pastes, as those of bloaters, lobsters, shrimps, caviare, &c., are made in a similar manner. Paste, Araen'ical. See Caustics, Patent MEDICINES, and POWDEES. Paste, Baudry's. See Paste, Pectobal {beloio). Paste, Bird. See Gbeman paste. Paste, Black Currant. As black currant lozenges, but simply cutting the mass into dice or square. Paste, Car'rageen. Prep. From Irish moss, as the lichen paste of the P. Cod. (see below). Paste, Chinese'. Prep. From bullock's blood, 10 lbs., reduced to dryness by a gentle heat, then powdered, and mixed with quicklime, also in fine powder, 1 lb. It is used as a cement, made into a paste with water, and at once applied. Paste of Chlo"ride of Zinc. See Caustics. Paste of Dates. fiy». Pasta dacttlifee.e, P. dacttloeum, L. ; Pates i>e dattes, Fr. From dates (stoned), as jujube paste. Pec- toral, and slightly astringent. Paste of guin Senegal is usually sold for it. Paste, De Handel's. Prep. From opium, J dr. ; camphor, 1 dr. (both in powder) ; ex- tracts of belladonna and henbane, of each 1 dr.; oil of cajeput and tincture of cantharides, of each 10 or 12 drops; distilled water of opium (or of lettuce), q. s. In toothache. Paste, Depii'atory. Syn. Pasta epilatoeia, Ii. Several preparations of this character are noticed at pages 552 — 3. 1. A mixture of slacked lime, 2 parts, and water, 3 parts, satu- rated with sulphuretted hydrogen, is said to be so powerful, that " a layer a line in thick- ness denudes the scalp in three minutes." (Beasley.) 2. (Payan.) Powdered sulphate of copper made into a soft paste with yolk of egg. Paste of Figs. Syn. Pasta caeicabum, P. PICAEIA, L. Prep. 1. From fig.i, as jujube paste. 2. (Soubeiran.) Pulp of figs, 1 part; press it through a sieve, mix it with powdered sugar, 4 parts, concentrated by a gentle heiit (if necessary), roll the mass out, and cut it into squares or lozenges. PASTE 1241 Paste, Flonr. Sgn. Collb sb Tkus, Fr. From wheiiten flour. I'aper-hangerg, shoe- makers, &e., usually add to the flour ^ to 1 of its weight of finely powdered resin. It is then t^oinetimcs Ciilltd 'hard paste.' The addition of n few drops of creasote or oil of clovt's, or a little powered caraplior, colocynth, or corrosive sublimate (especially the first two and the last), will prevent insects from attack- ini: it, and preserve it in covered vessels for years. Sliiiiild it get too hard, it may be soft- ened with water. See Cbmbnis. Paste, Fruit. Prep. 1. To each pint of the strained juiie add of gum Arabic, 1 oz., gently cv.iporate to the consistence of a syrup, and add an equal weight of bruised white sugar; as soon as the whole is united, pour it out on an oiled slab, and, when cold enough, cut it into pieces. 2. Citric acid, f oz. ; gum Arabic, 6 oz. ; white sugar, } lb. ; water, q. s. ; dissolve, and flavour witli any of the fruit essences. It may be coloured with any of the stains used for confectionery or liqueurs. 3. As fruit lozenges. Paste, Far'niture. See Polish. Paste, Glove. See Ganteine. Paste of Gum Arabic. St/n. Pasta qummi, L. ; Pate db qommk, P. de a. Aeauique, Fr. Prep. 1. As marsh-mallow paste, omitting the mallow roots. 2. Gum Arabic (picked), 1 lb. j water, 1 pint ; dissolve, add of white 8\igar, 1 lb. j eva- porate by a gentle heat to a very thick syrup, then add the whites of 3 eggs, previously beaten up with oninge-flowcr water, 1 fl. oz., and strained through muslin, and continue the heat with constant stirring, until of a proper consisteuce on being cooled. The hist two are coniniouly sold for marsh-mallow paste (pate de guimauve). 3. (Transparent.) From gum Arabic (picked), 1 lb. ; cold water, 1 pint j white sugar, li lb. ; proceed as the last, adding orange-flowerwater 1 fl. oz., towards the end. Often sold under the name of ' white jujubes.' Paste of Gum Senegal. Si/n Pate de OOMME 8ENE0AL, Fr. As jujube paste, with- out the fruit. Paste, Hon'ey. See Paste, Almond. Paste, Jn'jnbe. Si/n. Jujcbes, Jujube lo- zenges ; Pasta jujube, L. ; Pate de ju- jubes, Fr. Prep. (P. Cod.) Jujubes (the fruit), 1 lb.; water, 4 lbs.; boil i hour, strain with expression, settle, decant tlie char por- tion, and clarify it with white of egg; add a strained solationof gum Arabic, 6 lbs., in water, 8 lbs., and to theSuixture add of white sugar, 5 Ills. ; gently evaporate, at first constantly stirring, and afterwards without stirring, to the consistence of a soft extract, then add of orange-flowerwater, 6 fl. oz., and place the pan in a ve-sel of boiling water. In 12 hours care- fully remove the scum, pour the matter into sliglitly oiled tin moulds, and finish the evapo- ration (hardening) in a stove heated to 104°, Fahr. It is commonly coloured with beet-root, cochineal, or s.iffron. Expectorant; in cough', &c. Paste of gum Arabic is usually sold for it. Paste, Li'clien. Si/n. Pasta lichexis, L. ; Path de lichen, Fr. Prep. (P. Cod.) Ice- land moss, 1 lb.; water, q. s. ; heat them to nearly the boiling-point, strain wi:h pressure, reject the liquor, and boil the moss in fresh water, q. s., for 1 hour; strain, press, add of gum Arabic, 5 lbs. ; while sugar, 4 lbs., and evaporate to a proper consistence, as above. Pectoral. With the addition of i gr. of ex- tract of opium to each oz„ it forms the opiated lichen paste. (P. Cod.) Paste, Liquorice. Syn. Ltquobice jrjuBES ; Pasta gltcieehiz^, L. ; Pate de eeolisse, P. DE B. noire, Fr. Prep. 1. (P. Cod.) Re- fined juice and white sugar, of each 1 lb.; gum Arabic, 2 lbs.; water, 3 quarts; dissolve, strain, evaporate considerably, and, of finely pow- dered orris root, i oz. ; oil of aniseed or essence of cedrat, a few drops, and pour the paste upon an oiled slab, or into moulds, as before. 2. (Brown; PAsTA G. FUSCA ; Pate de b. BEUNE.) Rpftned juice, 4 oz.; white sugar, 2 lbs. ; gum Arabic, 3 lbs. ; water, 4 pints; pro- ceed as last. 3. (Opiated ; Pate de k. ophce.— P Cod.) To the last add of extract of opium, 15 gr. 4. (White; Pate de EioLissE blanche.) As No. 2, substituting the powder of the de- corticated root for the extract. All the above are pectoral ; the second is also sliiihtly ano- dyne. They are useful in tickling coughs, hoarseness, &c. Paste, London. Syn. Pasta londinensis. Equal parts of caustic soda and unslaked lime. Reduce to a fine powder in a warm mortar, and mix intimately. Keep it in well closed bottles, and when required for use take as much as is sufficient, and make it into a paste with water. Paste, Marsh-mallow. Si/"- Pastaalth.es, L. ; Pate de guimauve, Fr. Prep. (P. Cod. 1816.) Decorticated marsh-mallow root (French), 4 oz. ; water, i gall. ; macerate for 12 hours, strain, add white sujar and gum Arabic, of each 2i lbs.; dissolve, strain, eva- porate without boiling to the thickness of honey, constantly stirring, and add, gradually, the whites of 12 eggs, well beaten with orange- flower water, 4 fl. oz., and strained ; continue the evaporation and constant stirring uutil the mass is so firm as not to adhere to the fingers, then proceed as before. Obs. It should be very white, light, and spongy. In the P. Codex of 1839 the marsh- mallowroot is omitted.and the name is changed to that of ' pate de gomme,' a compound long sold for it in the shops. Both are agreeable pectorals. See Paste op Gum Ababic. 1242 PASTE Paste, Odontal'gio. Syn. Pasta odoktai.- GIOA, L. Frep. 1. Pellitory (in powder), 1 dr.; hydrochlorate of morphia, 3 gr. ; tri- turate ; add, of honey, 2 dr. ; and oil of cloves, 6 drops. 2. Powdered mastic, pellitory, and white sugar, of each 1 dr. ; chloroform, q. s. to form a paste. It must he kept in a stoppered bottle. See Toothache, and below. Paste, Or'ange. Prep. From orange flowers, 2 lbs. ; bitter and sweet al monds, of each blanched, 2i lbs. ; beaten to a perfectly smooth paste. An agreeable cosmetic. See Paste, Almond. Paste, Or'geat. Frep. Prom blanched Jordan almonds, 1 lb. ; blanched bitter a. and white sugar and honey, of each i lb. ; beaten to a paste, with orange-flower water, q. s. (or neroli, a few drops), and put into pots. As a cos- metic or to make orgeat milk. For use, rub 1 oz. with i pint of water, and strain through muslin. Paste, Pec'toral. Syn. Pasta pectoealis, Ii. Prep. 1. (Pate peotobalb db Batidet.) Take of gum Arabic and white sugar of each 7 lbs.; water, q. s. ; dissolve, add of extract of liquorice, 3 oz. ; evaporate, add of extract of lettuce, 2 dr. ; balsam of tolu, li oz. ; orange-flower water, 4i fl. oz. ; white of 4 eggs ; oil of citrons, 5 or 6 drops. 2. (Pate pectoeale balsamiqub de Reg- nauit.) Pi'om the flowers of coltsfoot, cudweed, marrow, and red poppy, of each, 1 oz. ; water, 1 quart; boil, strain; add, of gum Arabic, 30 oz. ; white sugar, 20 oz. ; dissolve, concentrate, add of tincture of tolu, 3 fl. dr., and pour the mixture on an oiled slab. 3. (AnISATED coltsfoot PASTE; PatE DE TussiLAGE A l'anis.) From a strong decoc- tion of coltsfoot flowers, 1 quart ; Spanish juice, ^ lb.; dissolve, strain, evaporate as before, and towards the end add of oil of aniseed, 1 dr. All the above are uselul in hoarseness, coughs, &c. Paste, Pho'sphor. See Eats. Paste, Pol'ishing. Frep. 1. (For copper and brass.) See Brass Paste. 2. For iron and steel). From emery (in fine powder) and lard, equal parts. 3. (For pewter.) Prom powdered Bath brick, 2 parts ; soft soap, 1 part ; water, q. s. to make a paste. Used with a little water, and afterwards well rinsed off. 4. (For furniture.) See Polish. Paste, Ea"zor. Frep. 1. From jeweller's rouge, plumbago, and suet, equal parts, melted together and stirred until cold. 2. Prom prepared putty powder (levigated oxide of tin), 3 parts; lard, 2 parts; crocus martis, 1 part ; triturated together. 3. Prepared putty powder, 1 oz. ; powdered oxalic acid, ^ oz. ; powdered gum, 20 gi-s. ; make a stifl' paste with water, q. s., and evenly and thinly spread it over the strop, the other side of which should be covered with any of the common greasy mixtures. With very little friction this paste gives a fine edge to the razor, and its action is still further in- creased by slightly moistening it, or even breathing on it. Immediately after its use, the razor should receive a few turns on the other side of the strop. 4. Diamond dust, jeweller's rouge, and plumbago, of each 1 part; suet, 2 parts. Powdered quartz is generally substituted for diamond dust, but is much less effective. 5. (Mechi's.) Emery (reduced to an im- palpable powder), 4 parts ; deer suet, 1 part ; well mixed together. 6. (Pradier's.) From powdered Turkey stone, 4 oz. ; jeweller's rouge and prepared putty powder, of each 1 oz. ; hard snet, 2 oz. Obs. The above (generally made up into square cakes) are rubbed over the razor strop, and the surface being smoothed ofF with the flat part of a knife or a phial bottle, the strop is set aside for a few hours to harden before being used. Paste, Eegnault's. See Paste, Peotoeai. Paste, Ilubefa"cient. Syn. Pasta eubepa- ciens, L. Prep. (Clarus.) Prom acetate of lead, 1 oz. ; bisulpbate of potassa, 3 oz. ; water, q. s. It acts powerfully and quickly on the skin. Paste, Bust's. Frep. From powdered opium and extract of henbane, of each 10 gr. ; powdered pellitory and extract of belladonna, of each 20 gr. ; oil of cloves, 10 drops. In toothache. Paste, Sha"Ting. Frep. 1. Naples soap (genuine), 4 oz.; powdered Castile soap, 2 oz. ; honey, 1 oz. ; essence of ambergris and oils of cassia and nutmegs, of each 5 or 6 drops. 2. White wax, spermaceti, and almond oil, of each i oz. ; melt, and, whilst warm, beat in 2 squares of Windor soap previously re- duced to a paste with a little rose water. 3. White soft soap, 4 oz. ; spermaceti and salad oil, of each J oz. ; melt them together, and stir until nearly cold. It may be scented at will. When properly prepared, these pastes produce a good lather with either hot or cold water, which does not dry on the face. The proper method of using them is to smear a minute quantity over the beard, and then to apply the wetted shaving-brush, and not to pour water on them, as is the common prac- tice. Paste, Styptic, of Gntta Fercha. Syn. Pasta GnTT.s) peechje bttptica. (Mr Beardsley.) Gutta percha, 1 oz. ; Stockholm tar, li or 2 oz. ; creosote, 1 dr.; shellac, 1 oz., or q. s. to render it sufficiently bard. To be boiled together with constant stirring, till it forms a homogeneous mass. For alveolar haemorrhage, and as a stopping for teeth in toothache. To be softened by moulding with the fingers. Paste, Swediaur. See Chilblain. Paste, Tooth. Syn. Pasta bentifexoia, PASTES 1243 Elbctttibium dentipbicttm, L. Various preparations are known under this name. They consist, for the most part, of the ordi- nary substances used as dentifrices, reduced to the state of a very fine powder, and mixed with sufiioient honey, sugar, or capillaire, to give them the required consistence. Honey of roses is often used for this purpose, with some agreeable perfume at will, A little eau de Cologne or rectified spirit is a useful addition. The following are a few examples: — 1. (CaKBOM pasts j OpIAT CAEBONKjrS.) The cliippiiigs of Turkey stone, cylinder char- coal, and prepared chalk, of each 2 oz. ; co- chineal and cloves, of each 1 dr. ; honey, 5 oz. ; eau de Coloi^uc, q. s. It should not be put into the pots until the next day, and should be afterwards well preserved from the air. Much prized by smokers, and by per- sons troubled with a fetid breath from rotten teeth. 2. (COBAL PASTK; OpIAT DENTIFBIOEEOITOB.) From prepared coral, 8 oz. : cuttle-fish bone, 4 oz. ; mustic, 2 oz. ; cochineal, i oz. ; honey, i lb. ; essence of ambergris, 1 11. dr. ; oil of cloves, i fl. dr., dissolved in rectified spirit, 1 11. oz. As the last. Cleanse the teeth ra- pidly. 3. (Dyon'a Chabooal paste.) From ohlo- rnte of pota»sa, 1 dr.; mint water, 1 fi. oz. ; triturate until dissolved, then add, of pow- dered cliarcoul, 2 oz. ; honey, 1 oz. 4. (Maoio paste.) From white murblc dust 4 nz. ; pumice stone (in impalpable powder), 3 oz. ; rose pink, 1 oz, ; honey, i lb. ; otto of roses, 15 drops, llapidly whitens the teeth, but it should not be used too freely, nor too fri'quently. 5. (P. Cod.) Prepared coral, 4 oz. ; bitar- trnte of potasss, 2 oz. ; cuttle-fish bone and cochineal, of each 1 oz. ; alum, J dr. ; Nar- honne honey, 10 oz. ; with essential oil, q. s. to aromatise the mixture. 6. (Pelletier's OcOHTlNE.) This is stated to be a mixture of pulverised sepia-bone, butter of cacao, and honey, with essential oil 7. (Rose PASTE.) Coral paste scented with roses, or the following : — Cuttle-fish bone, 1 oz. ; prepared chalk, 2 oz. ; cochineal, ^ dr.; honey of roses, 3 oz. ; otto of roses, 6 drops. 8. (SoiATBLB PASTE, Saline dbntifbioe.) Fiom bitiirtrate of potassa or sulpliate of po- tossa (in fine powder), 3 oz. ; honey of roses, 2oz. 9. (Spanish ijentifhice, Castiiian tooth CBEam.) From Cnstile soap (in fine powder) and cuttle-fi»h bone, of each 2 oz. ; honey of roses, 5 ' iz. An excellent preparation. It is superior to all the other pastes for removing tiirtiir unil animalcnlee from the teeth. 10. (Vanilla PASTE.) From red cinchona bark, 2 dr. ; vanilla, 1 dr. ; cloves, i dr. (the last two reduced to powder by tritura- tion with^ ; white sugar, 1 oz. j cuttle-fish bone and marble dust, of each t oz. ; syrup of salTron, q. s. 11. (Violet paste.) From prepared chalk and cuttle-fish bone of each 3 oz. ; powdered white sugar, 2 oz. ; orris root 1 oz. ; smalts, i oz. ; syrup of violets, q. s. to mix. 12. (Winckler's UossATE dentipbice.) From cuttle-fish bone, 1 part ; conserve of roses (Ph. L.), 3 parts; white otto of roses, 2 drops to the oz. 13. Chalk, 8 oz. ; myrrh and rhatany roof, of each 2 oz. ; orris root, 1 oz. ; honey of ruses, q. s. to mix. In foul and spongy gums. Paste, Tooth'aclie. See Paste, Ubontalola. Paste, Tor'mentil. Si/n. Pasta toumen- TILL£, L. Frep, (Morin.) Powdered tor- mentil root made into a paste with white of egg. In whitlow; applied on linen. Mixed with an equal weight of simple syrup, it has also been recommended in dysentery and diarrhcsa. Paste, Vienna. See Caustic potassa with LiUE. Paste, Vohler'B. Trep. From dragon's blood, Idr. ; powdered opium, 2 dr.; powdered gums of mastic and sandarach, of each 4 dr. ; oil of rosemary, 20 di'ops ; tincture of opium, q. s. to form a paste. In tootliache. Paste, Ward's. See Confection op Peppee. PASTES. Syn. Aetificial gems, Facti- Tiors G. ; PlEBEES PE^CIEUSKS AUTIFICI- ELLE3, Fr. Vitreous compounds made in imi- tation of the gems and precious stones. The substances which enter into their composition, and the principles on which their successful production depends, have been already briefly noticed. The present article will, therefore, be confined to giving the reader a few original formulEB, together with several others care- fully selected from the most reliable English and Continental authorities. Like enamels the artificial gems have for their basis a very fusible, highly transparent and brilliant, dense glass, which is known under the name of ' frit,' ' paste,' 'strass,' 'flux,' 'fondant,' or ' Mayence base,' and which in its state of greatest excellence constitutes the 'artificial diamond.' For convenience, this will be no- ticed here under its last synonym. (See below, also Ure's ' Dictionary of Arts,' &o.) Amethyst. 1. Paste or strass, 500 gr. ; oxide of manganese, 3 gr. ; oxide of cobalt, ■2i gr. 2. (Douault-Wi^land.) Strass, 4608 gr.; oxide of manganese, 36 gr.; oxideof cobalt,2gr. 3. (Lan<;on.) Strass, 9216 gr. ; oxide of mangauase, 15 to 24 gr.; oxide of cobalt, Igr. Aqua narina. From strass, 4800 gr. j glass of antimony, 30 gr. ; oxide of cobalt, IJ gr. See Bebxl, of which this is merely a variety. Aventnrine. 1. From strass, 500 cr. ; scales of iron, 100 gr. ; black oxide of copper, 50 gr. ; fuse until the black oxide "f copper is reduced to the reguline form, then allow the mass to cool very slowly, so that the minute 12i4, PASTES crystals of metal may be equally diffused throuKli it. Has a rich golden iridescence. 2. As the last, hut submitting oxide of chromium for the protoxide of copper. Ap- pears brown, filled with countless gold spangles; or, when mixed with more paste, of a greenish grej', filled with green spangles. Beryl. (Douault-Wieland.) Strass, 3456 gr. ; glass of antimony, 24 gr. j oxide of cobalt, IJ gr. See Aqtta Maeina. Carbuncle. See Gaenbt. Chrysolite. From strass 7000 gr. ; pure calcined sesquioxide of iron ('trocus martis'), 65 gr. Cornelian. 1. (Red.) From strass, 7000 gr. ; glass of antimony; 3500 gr. ; calcined peroxide of iron, 875 gr. ; binoxide of manganese, 75 gr. 2. (White.) Prom strass, 7200 gr. ; cal- cined bones, 250 gr. ; washed yellow ochre, 65 gr. Diamond. 1. From rock crystal (purest), 1600 gr. ; boiax, 560 gr. ; carbonate of lead (pure), 3200 gr. ; oxide of manganese, i to 1 gr. ; powder each separately, mix them to- gether, fuse the mixture in a clean crucible, pour the melted mass into water, separate any reduced lead, and again powder and remelt the mass. 2. Pure silica, 150 gr. ; pure litharge, 250 gr. ; borax and nitre, of each 50 gr. ; arse- uious acid, 21 gr. 3. (Douault-Wieland.) — o. From rock crystal, 4056 gr. ; minium, 6300 gr. ; potash, 2154 gr. ; borax, 276 gr. ; arsenic, 12 gr. b. From rock crystal, 3600 gr. ; ceruse of Clichy (pure carbonate of lead), 8508 gr. ; potash, 1260 gr. ; borax, 360 gr. 4. (Fontanier.) Pure silica, 8 oz. ; salt of tartar, 24 oz. ; mix, bake, cool, treat the fused mixture with dilute nitric acid until efferves- cence ceases, and afterwards with water as long as the washings affect litmus paper; next dry the powder, add to it of pure carbonate of lead, 12 oz ,aud to every 12 oz. of the mixture add of borax, 1 oz. ; triturate in a porcelain mor- tar, melt in a clean crucible, and pour the fused ma-s into cold water ; dry, powder, and repeat the process a second and a third time in a clean crucible, observing to separate any revived lead. To the third frit add of nitre, 5 dr., and again melt. The product is per- fectly limpid and extremely brilliant. 5. (Laii(;on.) Litharge, 100 gr.; pure silica, 75 gr. ; white tartar or potash, 10 gr. 6. (Loysel.) Pure silica, 100 parts; red oxide of lead (minium), 150 parts; calcined potasli, 30 to 35 parts; calcined borax, 10 parts; arsenious acid, 1 part. This produces a paste which lias great brilliancy and re- fractive and dispersive powers, and also a similar specific gravity to the oriental dia- mond. It fuses at a moderate heat, and ac- quires the greatest brilliancy when remelted, and kept for 2 or 3 days in a fused state, in order to expel the superabundant alkali, and perfect the refining (' Polytcch. Journ.'). The products of the above formulie are not only employed to imitate the diamond, but they also form the basis of the other factitious gems. (See above.) 7. (Yellow DIAMOND.) Strass, 500 gr. ; glass of antimony, 10 gr. Eagle Marine. From strass, 3840 gr. ; copper stain, 72 gr. ; pure zafBre, 1 gr. Emerald. 1. From strass, 7000 gr. ; car- bonate of copper, 65 gr. ; glass of autiraon^, 7gr. 2. Paste, 960 gr. ; glass of antimony, 42 gr. ; oxide of cobalt, 3i gr. 3. (Douault-Wieland ) Paste, 4608 gr. ; green oxide of copper, 42 gr. j oxide of chrome, 2gr. 4. (Lancjon.) Paste, 9612 gr. ; acetate of copper, 72 gr. ; peroxide of iron, li gr. Garnet. 1. Paste or strass, 1200 gr.; glass of antimony, 580 gr. ; purple of cassius and binoxide of manganese, of each 3 gr. 2. (Douault-Wieland.) Paste, 513 gr. ; glass of antimony, 256 gr. ; purple of cassius aud oxide of manganese, of each 2 gr. 3. (ViNEQAK GABNET.) From paste, 7000 gr. ; glass of antimony, 3460 gr. ; calcined peroxide of iron, 56 gr. Lapis Lazuli. From paste, 7000 gr. ; cal- cined horn or bones, 570 gr. ; oxides of cobalt and manganese, of each 24 gr. The golden veins are produced by painting them on the pieces with a mixture of gold powder, borax, and gum water, and then gently heating them until the borax fiuxes. Opal. 1. From strass, 960 gr. ; calcined bones, 48 gr. 2. (Fontanier.) Paste, 1 oz. ; horn silver, 10 jir. ; calcined magnetic ore, 2 gr. ; absorbent earth (calcined bones), 26 gr. Kuby. 1. Paste, 45 parts; binoxide of man- ganese, 1 part. 2. Paste, 1 lb. ; purple of cassius, 3 dr. 3. (Douault-Wieland.) — a. From paste, 2880 parts ; oxide of manganese, 72 parts. b. Topaz-paste that has turned out opaque, 1 part; strass, 8 parts; fuse them together for 30 hours, cool, and again fuse it in small pieces before the blowpipe. Very fine. 4. (Fontanier.) Strass, 16 oz. ; precipitate of cassius, peroxide of iron, golden sulphide of antimony, aud manganese calcined with niti-e, of each 168 gr. ; rock crystal, 2 oz., or more. 5. Paste and glass of antimony, of each 8 oz. ; rock crystal, 1 oz. ; purple of cassius, li dr. Turns on the orange. Sapphire. 1. From strass, 3600 gr. j oxide of cobalt, 50 gr. ; oxide of manganese, 11 gr. 2. (Douault-Wieland.) Paste, 4608 gr.; oxide of cobalt, 68 gr.; fuse in a little Hessian crucible for 30 hours. 3. (Fontanier.) Paste, 8 oz. ; oxide of cobalt, 49 gr. Topaz. 1. From strass, 1050 gr. ; glass of antimony, 44 gr. ; purple of cassius, 1 gr. 2. (Douault-Wieland.) Paste, 3456 gr. j calcined peroxide of iron, 36 gr. PASTELS— PASTIL 1245 Torqaoise. From blue paste, 20 to 24 parts ; calcined bones, 1 part. Concluding remark*. It in absolutely neces- sary for the successful application of the pre- ceding; foi-mulffl that the substances employed should be perfectly free from impurities, more particularly those of a mineral kind. The iiilinrge, oxide of lead, and carbonate of lead, above all thinj^s, must be entirely free from oxide of tin, as the smallest particle of that substnuce may impart a ' mlllsiness' to the paste. All the ingredients must be separately reduced to powder, and, after being mixed, sifted through lawn. The fusion must be care- fully conducted and continuous, and the melted miiBs should be allowed to cool very slowly, after liaviiig been left in the fire from 24 to 30 hours, at the least. Hessian crucibles are pre- ferred for this purpose, and the heat of an ordinary pottery or porcelain kiln is sufficient in most casis ; but a small wiud-fnrnace, de- voted exclusively to the purpose, is, in general, more convenient. It is found that the more tranquil, continuous, and uniform the fusion, the denser and clearer is the paste, and the greater its refractive power and beauty. All the coloured vitreous compounds noticed under Glass may be worked up as ornamental stones, iu the same way as those just referred to. The following method of obtaining artifi- cial rubies and emeralds, first pointed out by BoSttg-cr, is exceedingly simple and inex- pensive, and deserves the serious attention of those interested in this ingenious art : — Re- cently precipitated and well-washed hydrate of alnmiuuni is nioisteued with a few drops of neutral ehroniate of potassium, and kneaded so that the mass assumes a tinge scircely pir- ceptihle ; it is then rolled up into small sticks, about the thiekness of a filnger, and slowly dried, taking the precaution to fill the fissuns (if any) that form during desiccation with fresh hydrate of aluminum. When perfectly dry, and alter having been submitted to a gentle hiaf, one end of these sticks is brought into the termination of the fiame of an oxy- hydrogen blowpipe, until a portion of the mass is fused into a small globule. After the lapse of a few minutes, several minute balls form, liaving a diumeter of some millimetres, and of such intense hardness that quartz, glass, topaz and granite, may be easily and perceptibly scratched with them. These, when cut and polished, appear, however, slightly opaque, Uy employing nitrate of nickel in lieu of cliro- niate of potassium, green-coloured globules, closely resembling the emerald, are obtained. By the substitution of oxide of chromium for chromate of potassmm, Mr Cooley pro- duced factitious gems of considerable hard- ness and beauty, though sliglitly opaque iu some portion of the mass. The addition of a very little silica prevented, in a great measure, this tendency to opacity. It may bo observed that the beauty of pastes of factitious gems, and especially the brilliancy of mock diamonds, is greatly de- pending upon the cutting, setting up, aud the skilful arrangement of the f'ul or tinsel behind them. See Enambl, Foils, Gems, Glass, &c. PAS'IELS. [Fr.] Coloured crayons. PAS'TIL. Syn. Pastille; Pastu.lus, Pas- TlLLUM, L. A lozenge or confection. The pastilles (PASTILLI) of French pharmacy, are merely ' confectionery drops' aromatised or medicated. The name is also given to mix- tures or odorous substances made up into small cones aud burnt as ineeuse. (See belom). PastUs, Ezplo'sive. Fumigating pastilles, containing a little gunpowder. U-ed to pro- duce diversion, but they often prove far from harmless. Pastils, Fumiga'ting. Syn. Abomatio pas- tilles, Incensk P.J Pastilli fdmasies, P. ODOBATI, L. Prep. 1. Benzoin, 4 oz. ; cas- carilla, i oz, ; nitre and gum Arabic, of each 3 dr, ; myrrh, 1 dr. ; oils of nutniig and cloves, of each 25 drops ; charcoal, 7 oz. ; all in tine powder; beat them to a smooth ductile mass with cold water, q. ». ; form it into small cones with a tripod b ise, and dry them in the air. 2. (Henry and Guibourt.) Powdered gum benzoin, 16 parts; balsam of tolu and pow- dered sandal wood, of each 4 parts ; a light charcoal (Linden), 48 parts ; powdered tnga- canth and true labdanum, of each 1 part; powdered nitre and gum Arabic, of each 2 parts ; cinnamon water, 12 parts ; as above. 3. (P. Cod.) Benzoin, 2 oz. ; balsau) of tolu and yellow snndal wood, of each 1. dr.; nitre, 2 dr. ; labdanum, 1 dr. ; charcoal, 6 oz. ; mix with a solution of gum traga- canth, and divide the ni.jss into pastilles, as before. 4. (Pastilles a la elette D'OBiNas.) For powdered roses in the next (brniula substitute pure orange powder, and for the essence of roses use pure neroli. 5. (Pastilles A la eose.) Gum benzoin, olit>anum (in tears) and styrax (in tears), of each 12 oz. ; nitre, 9 oz. ; charcoal, 4 lbs. ; powder of pale roses, 1 lb. ; essence of roses, 1 oz. ; mix with 2 oz. of gum tragacanth, dis- solved in rose water, 1 quart. 6. (Pastilles k la Vanillb.) Gum ben- zoin, styrax, and olibanum (as last), of eai h 12 oz. ; nitre, 10 oz. ; cloves, 8 oz. ; powdered vanilla, 1 lb. ; charcoal, 4J lbs. ; oil of cloves, J oz. ; essence of vanilla, 7 or 8 11. oz. ; as before. Obs. The products of the above formula are all of excellent quality. They may be varied to please the fancy of the artiste, by the addition or substitution of other perfumes or aromatics. Cheaper pastilles may be made by simply increasing the quantity of the char- coal and saltpetre. The whole of the ingre- dients should be reduced to line powder bctorc 1246 PASTRY mixing them. The use of musk and civet, so often ordered in pastilles, should be avoided, as they yield a disagreeable odour when burned. The addition of a little camphor renders them more suitable for a sick chamber. The simplest and most convenient way of forming the mass into cones is by pressing it into a mould of lead or porcelain. Pastilles are burned either to diffuse a plea- sant odour, or to cover a disagreeable one. For this purpose they are kindled at the apex and set on an inverted saucer or a penny piece to burn. Persons who use them fre- quently employ a small china or porcelain toy (' pastile house') sold for the purpose. Pastils, Mouth. Si/». Bbeath pill, Ca- CHOU LOZENOEB ; PaSXILLI COSMETICI, L. ; ^Cachoc abomatise, C. aeomatique, C. de BoLoaNA, Gbains de oaohotj, Fr. Prep. 1. Soft extract of liquorice, 3 oz. ; gum catechu and white sugar, of each 1 oz. ; gum traga- canth (powdered), J oz. ; oil of cloves, 1 dr. ; oil of cassia, i dr. ; essence of ambergris and oil of nutmeg, of each 12 drops ; make a firm mass with rose or orange-flower water, q. s., and divide it into one-grain pills ; when ttiese are dry, cover them with gold or silver leaf. 2. Solazzi juice (dried by a gentle heat and powdered), 4 oz. ; lump sugar, 3 oz. ; pow- dered catechu, 2 oz. ; powdered tragacanth, 1 oz. J oil of cloves, 2 fl, dr.; oil of cassia, 1 fl. dr. ; white of egg or rose water, q. o. to form a piU-mjtss ; as before. 3. Powderptl catechu, 1 oz.; Salazzi juice, 4 oz. ; lump su^'ar, 12 oz. ; oils of cloves, cassia, and peppermint, of each 1 fl. dr.; mucilage of tragacanth, q. s. to mix; as before. 4. Extract of liquorice (soft), 2 oz. ; white sugar, 3 oz. ; powdered tragacanth and casca- rilla (or orris root), of each J oz. ; oil of cloves, i fl. dr. ; oil of cassia, 12 drops, water, q. o. ; as before. 5. (Chevallier.) Powdered cofi'ee, chocolate and sup;ar, of each 1^ oz. ; powdered vanilla, and freshly burnt charcoal, of each 1 oz. ; mucilage of tragacanth, q. s. 6. CliloriJe of lime (dry and good), 1 dr. ; white 8Ui:;ar, 3 oz. ; powdered tragacanth, 1 oz. ; oil of cloves, 30 drops ; rose water, q. s. To disinfect tlie breath. Ois. Almost every maker employs his own forms for these articles. The objects to he aimed at are the possession of rather power- ful and persistent odour, and a toughness to prevent their too rapid solution in the mouth. The original Italian formula included liquorice, mastic, cascarilla, charcoal orris root, oil of peppermint, and the tincturesol' ambergris and musk, hut is now seldom employed in this country. The flavour of peppermint does not, indeed, appear to be approved of by English smokers. Sometimes, instead of being made perfectly spherical, they are flattened a little. Cachou X l' Ambke Geis, Cachou A la Canelle, Cachou a la Flbub d'Oeange, Cachou Mttsque, Cachou A xa Rose, Ca- chou A LA Vanille, Cachou A la Violette, &c., are merely flavoured and scented respec- tively with the essences or oils of ambergris, cinnamon, neroli, musk, rose vanilla, violets, &c. See Breath, Cachou Abomatise, Lo- zenoes, Pills, &c. PA"STEY. Articles of food made of ' paste' or dough, or of which ' paste' forms a principal and characteristic ingredient. The word is popularly restricted to those which contain puff paste, or such as form the staple pro- duction of the modern pastrycook ; but it is, in reality, of much more general signification. Several varieties of paste are prepared for different purposes, of which the following are the principal : — Pupp Paste. The production of a first class puflf paste is commonly regarded as a matter of considerable difficulty, but by the exercise of the proper precautions it is, on the contrary, an extremely simple affair. This paste, before being placed in the oven, consists of alternate laminae of butter or fat and ordi- nary flour dough, tjje latter being, of course, _the thicker of the two. During the process of baking, the elastic vapour disengaged, being in part restrained from flying off by the but- tered surfaces of the dough, diffuses itself between these laminse, and causes the mass to swell up, and to form an assemblage of thin membranes or flakes, each of which is more or less separated from the other. Individually, these flukes resemble those of an ordinary rich unleavened dough when baked ; but, collec- tively, they form a very light crust, possessing an extremely inviting appearance and an agreeable flavour. The precautions above referred to are — the use of perfectly dry flour, and its conversion into dough with a light hand, avoiding un- necessarily working it, — the use of butter free from water or buttermilk, and which has been reduced to precisely the same degree of plas- ticity as the dough between which it is to he rolled, — conducting the operation in a cool apartment, and, after the second or third folding of the dough, exposing it to a rather low temperature before proceeding further with the process ; and, lastly, — -baking the paste in a moderately smart but not too hot an oven. The following are examples : — 1. (Rich.) Take of flour, 1 lb. ; butter, J lb. ; cold spring water, q. s. ; make a mode- rately soft flexible dough, then roll in (as described above) of dry fresh butter, i lb. 2. (Ordinary.) Take of flour, 1 lb. ; cold water, q. s ; make a dough, and roll in, as before, of butter, 6 oz. 3. (Rundell.) Take i peck of flour, rub into it 1 lb. of butter, and make a ' light paste' with cold water, just stiff enough to work well) next lay it out about as thick as a crown-piece; put a layer of butter all over it, sprinkle on a little flour, double it up, and roll it out again; by repeating this «ith fresh PATENT MEDICINES 1247 Inyers of butter three or four times, or of tener, a very liglit paste will be formed. Bake it in a moderately quick oven. 4. (Soyer.) Put 1 lb. of flour upon your paatry slab, make a hole in the centre, into which put a tenspoonful of salt, mix it with cold water into a softish flexibfe pa»te with the ri^ht hand, dry it off a little with flour until you have well cleared the paste from the ■lab, but do not work it more than yon can possibly help ; let it remain for 2 or 3 minutes upon the slab, then take 1 lb. of fresh butter from which you have squeezed all the butter- milk in u cloth, and brought to the same con- sistency as the paste, upon which phice it ; press it out flat with the hand, then fold over the edges of the past so as to hide the butter, and reduce it with the rolling-pin to the thick- ness of about i an inch, when it will be about two feet in length ; fold over one third, over which again pass the rolling-pin ; then fold over the otlier third, thus forming a square; place it with the ends top and bottom before you, shaking a little flour both under and over, and repeat the rolls and turns twice iigiiin as before ; flour a ' baking-sheet,' upon which lay it, on ice, if handy, or otherwise, in some cool place, for about half an hour ; then roll it twice more, turning it as before, and again place it upon ice or in the cold for i of au liour; next give it two more rolls, making seven in all, and it is ready for use. " You must continually add enough flour while rolling to prevent your paste sticking to the slab." Half-i>i'fp Pastb. As the preceding, using only one half the quantity of butter, and giv- ing the paste only 3 or 4 folds. Shobt Paste, Suoet Cebst. — 1. Flour (dry and warm), 1 lb.; sugar, 3 oz. ; butter, i lb. ; 2 eggs ; water, i pint; make a light dough. If one half of • Jones's patent flour be used, no eggs will be required. 2. (Soyer.) Put on the ' paste slab ' or ■ pie board ' 1 lb. of flour, 2 oz. of pounded sugar, 6 oz. of butter, I egg, 4 teaspoonf ul of s-ilt, and i pint of water; mix the sugar and water well together, adil them with the water by degrees to the flour, and form u paste, but firmer than puft" paste. PiB Paste. That commonly used is ' short paste,' varied at will ; hut at good table* the upper crust of the pie is generally made of *pnir paste,' and the remainder of ' short paste.' Podding Paste. This for baked puddings may resemble the last. For boiled puddings (or indeed lor any), the paste may be either ordinary 'short paste,' or one made with 2 to 6 oz. of butter or lard, or 3 to 8 oz. of chopped beef suet, to each lb. of flour, with or without an egg, and a litile sugar, according to the means of the parties. The first is most appro- priate fur those containing fresh Iruit, and that with suet for meat puddings, and those containing diied fruit, as grocers curnmts, plums, &c. Jlilk or milk-and-water is often used instead of simple water to make the dough. Ginger, spices, savory herbs, &c, are common additions to the crusts of puddings. Where economy is an object, and especially among the lower classes, kitchen fat is fre- quently substituted for suet, and lard for butter. When ' Jones's patent flour' is em- ployed, an excellent plain pudding paste may be made by simply mixing it up with very cold water, and immediately putting it into the water, which should be boiling, and kept in that state until the pudding is dressed. PA'TENT MED'ICIHES. Syn. Mbdioa- MENTA abcana, L. The majority of the pre- parations noticed undei this bead are the nostrums popularly termed ' quack medicines,' and which are sold with a Government stamp attached to them. A few other secret or proprietary remedies are also, for convenience, included in the list. An alphabetical arrange- ment, based on the names of the reputed inventors or proprietors of the articles, has been adopted, as being the one best suited for easy reference. The composition of a number of them is given from careful personal inspec- tion and analysis (by Mr Cooley), and that of the remainder on the authority of Gray, Grif- fith, Paris, Redwood, the members of the Philadelphia College of pharmaiy, and other respectable writers. A variety of articles, not included in the following list, is noticed along with other preparations for the class to which they belong, or imder the names of their pro- prietors. See Balsam, Cekate, Drops, Eb- BE.NCE, TiNCTUEE, OINTMENT. PlI,L9, &C. Ahernethy's Fills. See Abeenbthy jMbdi- OINES. Albinolo's Ointment. See Holi.owat'8 Ointment (below). All Ahmed's Treasures of the Desert. There are three preparations included under this name : — a. (Antiseptic Malagma.) From lead plaster, 3 parts ; gum, thus and sahid oil, of each 2 parts; beeswax, Ipart; melted to- gether by a gentle heat, and spread upon calico. b. (Pectohai, Antiphthisis, or Cough Pills.) From myrrh, 8i lbs.; squills and ipecacuanha, of each 1 lb. (all in powder) ; white soft soap, 10 oz. ; oil of aniseed, 1^ oz ; treacle, q. s. to form a pill mass. e. (Sphairopbptic or Antibilious Pitts.) From aloes, 28 lbs. ; colocynth pulp, 12 lbs.; rhubarb, 71bs. ; myrrh andscammony, of each 3 J lbs. ; ipecacuanha, 3 lbs. ; cardamom seeds, 2 lbs. (all in powder) ; soft soap, 9 lbs. ; oil of juniper, 7 fl.oz.; treacle, q. a. This, as well as the last, is divided into 3i gr. pills, which are then covered with tin foil or silver leaf. An eNcellent aperient pill, no doubt, and one likely to prove useful in all those ca^es in which the administration of a mild diaphoretic and stomachic purge is indicated. Unlike many of the advertised nostrums of the day, theie is nothing in their compo-ition that cm 1248 PATENT MEDICINES by any possibility, prove injurious ; but beyond this they are destitute of virtue. Anderson's Scot's Pills. See PiLia. Atkinson's Infant Preservative. From car- bonate of magnesia, 6 dr. ; white sugar, 2 oz. ; oil of aniseed, 20 drops j spirit of sal volatile, 2i dr. ; laudanum, 1 dr, ; syrup of saffron, 1 02.; caraway water to make up 1 pint. Balm of Kackasiri. Hee Balsam. Balsam of Life. St/n. Baume de tib, Fr. Several compound medicines of this name are noticed on page 261. The following are well- known nostrums : — 1. (Hoffman's) — a. Of the oils of cinnamon, cloves, lemon, lavender, and nutmegs, and bal- sam of Peru, of each 2 dr. ; essence of amber- gris, oil of amber, and oil of rue, of each 1 dr. ; cochineal, 12 gr. ; strongest rectified spirit, 3i pints ; mix. b. (Ph. Dan. 1840.) Oils of cinnamon, cloves, lavender, and nutmegs, of each 20 gr. ; puri- fied oil of amber, 10 drops ; balsam of Peru, 30 gr. ; rectified spirit (tinged with alkanet root), 10 oz. 2. (Gabius's.) Kearly similar to Hofl'- mann's. 3. (Turlington's.) Benzoin and liquid sty- rax, of each 12 oz. ; balsam of tolu and ex- tract of liquorice, of each 4 oz. ; balsam of Peru, 2 oz. ; aloes, myrrh, and angelica root, of each 1 oz. ; highly rectified spirit of wine, 7 pints ; digest, with frequent agitation for 10 day.i, and filter. Externally, the above are rubefacient and corroborant; internally, sti- mulant, cordial, and pectoral. Betton's British Oil. From oil of turpentine, 1 pint ; Bavbadoes tar, 4 lb. ; oil of rosemary, 1 fl. oz. Blake's Green-mountain Ointment. We are. told that the active ingredient in this com- pound is Arnica woM^awa, with a basis of soap cerate. It is very useful as an external appli- cations in several affections. The chief ob- jection to its use is that it is a secret prepara- tion. Blake's Toothache Essence. From alum, in fine powder, 1 dr. ; sweet spirit of nitre, 5 dr. Boerhaave's Odontalgic Essence. From opium, 4 dr. ; oil of cloves, 5 dr. ; powdered camphor, 5 dr. ; rectified spirit, 1^ fi. oz. Bouchardat's Tasteless Aperient. From phosphate of soda, | oz., placed in a soda-water bottle, which is then filled up with carbonated water, at the bottling machine. For a dose. Brand's Tooth Tincture. From pellitory of Spain (bruised), 1 oz. ; camphor, f oz. ; opium, \ oz. ; oil of cloves, 1 dr. ; digested for 10 days in rectified spirit, i pint. Brodnm's Nervous Cordial. Frep. 1. "Ori- ginally it consisted simply of an infusion of gentian root in English gin, coloured and fla- voured with a little red lavender (compound spirit of lavender.). After a time the doctor added a little hark to the nostrum, and subse- quently made other additions." (' Anat. of Quackery.') 2. (Paris.) Tinctures of gentian, calumbai cardamoms, and cinchona, compound spirits of lavender, and steel wine, of each equal parts. " It is tonic, stomachic, and stimulant ; but, beyond these, possesses no curative properties." (' Anat. of Quackery.') CtaloTodyue. This nostrum, which was first introduced as "a combination of perchloric acid with a new alkaloid," has become a popu- lar anodyne and sedative. Several prepara- tions are sold under this name, and the claims of the rival makers have occasioned some expensive lawsuits. The name was undoubt- edly invented by Dr J. Collis Browne, but Mr Freeman, pharmaceutical chemist, claims to be the inventor of the preparation. Whether Browne's and Freeman's ' chlorodynes ' are essentially the same, we are not able to deter- mine, but we know that there is not the slightest foundation for the statements made by each manufacturer respecting the new vegetiible principle contained in his medicine. Chlorodyne, in every one of its forms, is simply a mixture of certain well-known materials, some of which are rather dangerous ingre- dients for a popular nostrum. According to the analysis of Dr Odgen, Browne's chloro- dyne is composed as follows : — Chloroform, 6 dr.; chloric ether, 1 dr.; tincture of capsicum, J dr. ; oil of peppermint, 2 drops; hydrochlorate of morphine, 8 gr. ; Scheele's hydrocyanic acid, 12 drops ; per- chloric acid, 20 drops; tincture of Indian hemp, 1 dr.; treacle, 1 dr. ' Towle's chloro- dyne ' is prepared according to this formula, the ingredients being named on the label. Clarke's Conglutinum. See Conglxttinum. Cochrane's Congh Bemedy. Acidulated syrup of poppies. Corn Nostrums. See Corn. Cottereau's Odontalgic Essence. A nearly saturated ethereal solution of camphor, mixed with about -r-jth of its volume of strong liquor of ammonia. Curtis's Anti- venereal Lotion. A mixture of Beaufoy's solution of chloride of lime, 2 fl. oz., with cold soft water, 8 fl. oz. For use, 1 to 2 table-spoonfuls are put into a wine-glassful of water. Dalby's Carminative. 1. (Dr Paris.) Car- bonate of magnesia, 40 gr. ; tincture of castor and compound tincture of cardamoms, of each 30 drops ; tincture of assafoetida, and spirit of pennyroyal, of each 15 drops ; laudanum, 5 drops ; oil of aniseed, 3 drops ; oil of nut- meg, 2 drops; oil of peppermint, 1 drop; peppermint water, 2 fl. oz. — Dose, J to 1 tea- spoouful. The bottle should be well shakea before pouring it out. 2. (Wholesale.) Carbonate of magnesia, 1 oz. ; tincture of castor, 5 fl. dr. ; tincture of assafoetida, 3 fl. dr. ; oils of aniseed and penny- royal, of each J fl. dr. ; oil of nntmeg, 15 drops ; syrup of poppies, 7 oz. ; rectified spirit, 34 fl. oz. ; peppermint water, i pint ; as before. PATENT MEDICINES 1249 Davidson's Cancer Kerned;. A mixture of arsenions acid and hemlock, both in powder. (Dr Paris.) Baria's Calorific. The 'liquid' is com- mercial acetic acid (sp. gfr. 1048), diluted with about an equal volume of water, and coloured with burnt sugar or spirit colouring. The * BUIELD ' consists of a piece of red flannel backed with oil sldn, to prevent evaporation. A few drops of calorific are sprinkled on the flannel, which is then bound over the ftlTertiid part. The heat of the body gradually volatilises the acetic acid, and the escape of the vapour being prevented by the oil skin, a strongly counter-irritant action is set up. Derbyshire's Embrocation. From opium and mottled sonp, of each a oz. ; extract of henbane, 2 dr. J and mace, 4 dr. j boiled for 30 minutes, in water, 3 pints ; to the cold liquor, rectified spirit, 1 quart, and liquor of ammonia, 1 fl. oz., are added, and, after repose, the clear portion is decanted. A preventive of sea-sickness. Deshler's Cerate. Yellow basilicon. Duncan's Oout ffledicine. See Gout. Dutch Agne Remedy. A mixture formed of Peruvian bark and cream of tartar, of each 1 oz. ; cloves, J dr. ; reduced to fine powder. — Dose, li dr., every 3 hours. (Dr Paris.) Godfrey's Cordial, 1. (Original formula.) Opium (sliced), i oz. j sassafras chips 1 oz. ; English brandy, 1 quart ; macerate for 4 or 5 days, then add, of water, 1 quart, treucle, 3i lbs., and simmer the whole gently for a few minutes j the next day decant the clear portion. 2. (Dr Paris.) Aniseed, caraways, and eori- nndcrs, of oach, bruised, 1 oz. ; sassafi'as chips, 9 oz. ; water, 6 pints ; simmer gently until reduced to 4 pints, then add of treacle, 6 lbs.; and when nearly cold, further add of tincture tt opium, 3 fl oz. 3. (Phil. Coll. of Phar.) Carbonate of potnssa, 21 oz. ; water, 26 pints (old wine measure) ; dissolve, add of sugar-house molasses (treacle), 16 pints (o. w. m.) ; simmer the mixture, re- move the scum, and when it has considerably cooled, add of tincture of opium, 24 fl. oz. ; oil of sassafras, J fl. oz. ; (dissolved in) recti- fied spirit, 1 quart (o. w. m.) It contains about 16 drops of laudanum ( = l^gr. of opium) in each fl. oz. The following forms are also current in the wholesale trade : — 4. Prom molasses, 16 lbs.; distilled water, 2} galls.; oil of sassafras, 1 fl. oz.; (dissolved in) rectified spirit, i gull.; bruised ginger, J oz. ; cloves, i oz. ; laudanum, 8 fl. oz. ; macerate for 14 days, and strain through flannel. 5. Sassafras chips, lib. ; ginger (bruised), 4 ox. ; water, 3 galls. ; simmer until reduced to 2 gulls. ; tnen add of treacle, 16 lbs. ; rectified spirit, 7 lbs. ; laudanum, 1 pint. 6. Opium, J oz.; treacle, 7 lbs.; boiling water, 1 gall.; dissolve, and add, of rectified spirit, 1 quart ; oil of sassafrass, i dr. ; cloves TOL. II. and mustard seed, of each J oz. ; coriander and caraway seeds, of each 1 dr. ; digest for a week. 7. Caraways, corianders, and aniseed, of each 1 lb. ; water, 6 galls. ; disti I 5 galls., and add, of treacle, 23 lbs. ; laudanum, 1 quart ; and oil of sassafras, 1 fl. oz., previously dissolved in recti- fied spirit, 1 gall. Ob». This preparation is anodyne and nar- cot'c, and, amongst the lower classes, is com- monly given to children troubled with ^ind or colic. Its frequent and excessive use has sent many infants prematnrely to the grave. Gray says, " It is chiefly used to prevent the crying of children in pain or starving." The dose is i teaspoonful and upwards, according to the age and susceptibility of the child. Grave's Gout Preventive. A tincture pre- pared by steeping, for a week, dried orange peel and hiera picra, of each 1 oz., and rhu- barb, i oz., in brandy, 1 pint. Grinrod's Remedy for Spasms. From ace- tate of morphia, 1 gr. ; spirit of sal volatile and sulphuric ether, of each 1 fl. oz. ; camphor julep, 4 11. oz. ; for a mixture. It should be kept closely corked, in a cool place, and should be well shaken before use. — Dose. A tea- spoonful in a glass of cold water or wine, lis required. It is ■■ really valuable prepa- ration. Herrendschwand's Specific. A mixture of giimboge, 10 gr., with carbonate of potassa, 20 gr. (Dr Paris.) Holloway's Ointment. The original formula of Albinolo's ointment, of which this pre- tends to be a reproduction, contained the " graisses der serpent et de vip&re," and other pharmaceutical curiosities. The principal in- gredients, however, in the Hollovtay's oint- ment of the present day are very homely substances. In the case of Silleu v. HoUoway, tried at the Court of Common Pleas in Jan\iary, 1863, the plaintifE's counsel asserted that, on the ointment being received by the agent in Paris, it was submitted to the authorised government chemists to be analysed, in accord- ance with the laws of France prohibiting the sale of secret remedies, and was found by them to contain butter, lard, Venice turpentine, white wax, yellow wax, and nothing else. In a letter to the 'Times' Mr Holloway stated that the French analysis was incorrect, for three of the ingredients named were not in the ointment, while there were other components which the analysts had not discovered. The formula adopted by those who prepare an imi- tation ointment on the large scale, and wbiih closely resembles, if it be not actually identical with, "that employed by Mr Holloway, is as follows : — Fresh butter (free from water), Jib.; beeswax (good), 4 oz.; yellow resin, 3 oz. ; melt them together, add of vinegar of eantha- rides, 1 fl. oz., and simmer the whole, with constant agitation, for 10 or 12 minutes, or until the moisture is nearly evaporated ; then add of Canada balsam, 1 oz. j expressed oil of 79 1350 PATENT MEDICINES mace, i dr. ; balsam of Peru or liquid styrax, 10 or 12 drops ; again stir well, allow the mixture to settle, and wheu it is about half cold (not before) pour it into the pots, pre- viously slightly warmed, and allow it to cool very slowly. The label will do the rest. No two samples of Holloway's ointment are pre- cisely of the same colour or consistence. Holloway's Fills. From aloes, 4 parts; jalap, ginger, and myrrh, of each 2 parts ; made into a mass with mucilage, and divided into 2-grain pills, of which about 4 dozen are put into each Is. IJd. box. Jackson's Bathing Spirit. A species of soap liniment, made of soft soap, 1 lb. ; camphor, 6 oz. ; oils of rosemary and thyme, of each f fl. oz. ; rectified spirit, 1 gall. Kaye's Infant's Preservative. A preparation partaking of the joint properties of Atkinson's nostrum and Godfrey's cordial, but more pow- erful than either, as indicated by the doses in which it is directed to be given during early infancy, viz. " two, three, or more drops." Keating's Cough Lozenges. These are said to be composed of — Lactucarium, 2 dr. ; ipe- cacuanha, 1 dr.; squills,! dr.; extract of liquo- rice, 2 oz. ; sugar, 6 oz. ; made into a mass with mucilage of tragacantb, and divided into 20-gr. lozenges. King's Sarsaparilla Pills. Prom the com- pound extract. "Instead of two pills being equivalent to 4 fl. oz. of the concentrated decoc- tion or essence of sarsaparilla, as asserted, it takes about 32 of them to represent the given quantity, and about 4 of them to be equal in strength to the common decoction of the Phar- macopoeia." " Instead of one 2s. 9d. box of these pills being equal to a pint of the costly concentrated fluid preparation, it would take nearlylj lb. of them for that purpose." ('Med. Circ.,' ii, 493.) Kitchener's Peristaltic Persuaders. See Pills. Lambert's Asthmatic Balsam. The active ingredients in this compound are said to be squills and aqueous extract of opium. Lemaznrier's Odontalgic Essence. From ace- tate of morphia, 1 gr. ; dissolved in cherry- laurel water, 1 oz. For use, a teaspoonful is added to half a wine-glassful of warm water, and the mouth well rinsed out with the mix- ture. Leroy's Purgative. — a. (No. 1.) Vegetable turbith, 6 dr. ; scammony, li oz. ; jalap, 6 oz. ; brandy, 10 pints ; digest for 24 hours, and add a syrup made of senna, 6 oz. ; water, 14 pint ; sugar, 32 oz. b. (No. 2.) As the last, only one third stronger, c. (No. 3.) Twice as strong as No. 1. Lewis's Electnarium. A liquid nostrum,'said to bo alterative and to contain a small quantity •of both antimony and mercury. Lewis's Balsamic Ointment. This prepara- tion, which is declared by its proprietor to be " utterly unsurpassable," for the most part resemble Holloway's ointment. ('Med. Circ.,' ii, 493.) Lewis's Silver Cream. This nostrum is said to depend for its efficacy on white precipitate and a salt of lead. Locoek's Pulmonic Lozenges. See Wafbes. Mahomed's Paste. See Eleotuaet. Mardant's Norton's Drops. A mixture of the tinctures of gentian and ginger, holding in •solution a little bichloride of mercury, and coloured with cochineal. Marriott's Dry Vomit. A mixture of equal parts of tartar emetic and sulphate of copper. Marsden's Drops. A coloured solution of corrosive sublimate. (Dr Paris.) Matthien's Vermifuge. — a. (To destroy the worms.) Tin filings, 1 oz. ; male fern root, 6 dr. ; worm seed, 4 dr. ; resinous extract of jalap and sulphate of potassa, of each 1 dr. ; honey, q. s. to form an electuary. — Dose. A teaspoonful, repeated every third or fourth hour for 2 or 3 days, when the following is to be substituted, and continued until the bowels are well acted on. 6. (To expel the worms.) Jalap and sul- phate of potassa, of each 40 gr. ; scammony, 20 gr. ; gamboge, 10 gr. ; honey, q. o. as before. McKinsey's Golden Cerate. This appears to resemble Poor Man's Friend. McKinsey's Katapotia. This notorious nos- trum is compounded of aloes, 5 oz. ; soap, 1^ oz. (both in powder) ; beaten up with syrup of saffron and a little essential oil, and divided into pills varying in weight from 2 to 2^ gr. each. (' Med. Circ.,' iv, 86). McKinsey's Medicinal Powder. Sy». Rev. T. Smith's m.p. From dried lavender flowers and rosemary tops, of each 2i oz. ; asarabacca, 1 oz. ; reduced to powder, and further dis- guised with a little perfume. A very small quantity of subsulphate of mercury is also most probably added. Two or three pinches of this powder, taken 3 or 4 times a day as snufE, is said by the proprietor to be sufficient to cure almost every known disease. See Asaba- BACCA. Morison's Aperient Powder. A mixture of cream of tartar and lump sugar, in nearly equal proportions, with sufficient powdered cassia to give it an aromatic flavour. See Pills. Morison's Adhesive Paste. See Plaster. OUivier's Biscuits. Take of the white of 2 eggs; water, f pint; beat them together, strain the mixture, and add to it a solution of bichloride of mercury, 76 gr. ; collect the precipitate, wash, dry, powder, and carefully weigh it; next add to it such a quantity of flour, &c., that each 2-dr. biscnit may contain exactly f gr. Papier Fayard, See Papee (Gout). Pate Arseuicale. A powder composed of arsenious acid, 8 gr.; dragon's blood, 22 gr.; cinnabar, 70 gr. It is to be made into a paste PATENT MEDICINES 1251 with the saliva at the time of applying it. A favourite remedy in caacer on the Continent. (Dr ParU). Ferry's Balm of Syriacnm. From Engiiah gin, 1 pint; moist sugar, } lb.; (dissolved iu) water, 4 oz. j mix, and add of paregDric (Tinct. Camph. Co.— Ph. L. 1836), 1 oz j tinctjire of tolu, ) oz. ; tincture of cantbarides, q. s. ; to- getlier with a few drops each of the oils of aniseed and spearmint; agitate well together, and the next day filter, or decant the clear portion. Ferry's Preventive IiOtion. This is said to be a soluticjn of sal alembroth, 2 dr., in water, 1 pint. For use, it is diluted with 4 or 5 times its bulls of water. Fieste's Toothache Essence. From liquor of ammonia, 2 parts; laudanum, 1 part. It is applied on lint. Pilules Angiliqnes. Si/n, Oeainb de bant£. Take of aloes and juice of roses, of each 4 oz. ; juices of borage and chicory, of each 2 oz. ; beat them together, and when they are re- duced to the consistence of a soft plll-masx, add of powdered rhubarb, 2 dr., powdered agBric,l dr., and divide the mixture intoli-gr. pills. A goodpurgative. — Dose, 4 to 12. Poor Man's Friend (French). See OiKi- MENT (Brown). Poor Man's Friend (Dr Roberts'). This consists chiefly of ointment of nitric-oxide of mercury. Fringle's Remedy for Typhus. (Dr Paris.) Palo cinchona (bruised), i oz. ; water, 12 H. oz.; boil them together for 10 minutes, adding, towards the end,Virginiiinsualie-root (bruised), 2 dr. ; macerate for an hour iu a covered vessel, and to the stiained liquid add of dilute sulphuric acid, 2 9. dr., and when the mixture is cold, further add of spirit of cinnamon, 1 fl. oz. The dose is 2 table-spoonfuls every six hours. Reynolds' Gout Specific. Wine of colchi- cum disguised by some unimportant additions. Eighiui's Odontalgic Drops. A solution of creasiite in an equal weight of tlie strongest rectified spirit, coloured with cochineal, and diBgui^:ed by the addition of a few drops of oil of peppermint. Rnsplni's Styptic. A strong solution of Kallic acid in spirit of roses. Dr A. T. Thomson says that it also contains sul^ hate of zinc. Rust's Toothache Paste. See Paste. Scott's Drops. Syn. Tinctukb op Soot. From wood-suot, 2 nz. ; assafcetida, 1 oz. ; brandy or proof spirit, 1 pint. — Dose, 1 to 2 tabl«-8poonfuls; iu hysteria, &c. Smith's Powder. See McKinsey's Powder. Solomon's Auti-impetigines. A solution of bichloride of mercury disguised by the addition of a little flavouring and tiuetorial matter. ('Med. Circ'ii, 69, 70). Standert's Red Mixture. Tsbe of carbonate of magnesia, 1 oz. ; powdered Turkey rhubarb, i oz. ; tincture of rhubarb, 3 ti. oz. ; tincture of opinm, 2 fl. dr. ; oils of aniseed and peppermint of each \ dr. ; (dissolved in) gin or proof spirit, 5 fl. oz. ; agitate tlie whole together, then fur- ther add of soft water, li pint. In colic and diarrhoea. — Dose. A wine-glassful. The spirit is frequently omitted, but then the mixture soon spoils. Standert's Stomachic Candy. Take of lump sugar, 1 lb. ; water, 3 fl. oz. ; dissolve by heat ; add cardamom seeds, ginger, and rhubarb, of each 1 oz. ; and when the mixture is com- plete, pour it out on an oiled slab or into moulds. Storey's Worm Cakes. Take of calomel and cinnabar, of each 24 gr. ; powdered jalap, 72 gr. ; ginger, 1 dr.; white suijar, Ij oz.; syrup, q. 8. ; mix and divide into a dozen cakes. Re- semble 'Cliing's lozenges' in their action. (See page 1007). Struve's Lotion. See Lotion, Hooping- cough. Succession Powder. A mixture of powdered quartz and diamond dust, chiefly the first. Used as an escliarotic. Tasteless Ague Drops. A solution of arse- nite of potassa. It is the common ague medi- cine in the fen counties of England. Turlington's Balsam. See Balsam: op Life (above). Talangln's Solution of Solvent Mineral. From arseuious acid, ^ dr., di>solved iu hydrochloric ncid, W dr., and the solution diluted with dis- tilled water, IJ pint. Iu ague, &c. It has rather less than half the strength Of the solu- tion of arsenite of potassn, Ph. L. Vance's Cream. See CniLBLAix. Wahler's Ointment. See CaiLBtAnf. Ward's Purging Powder. A mixture of jalap and cream of tartar, equal parts, coloured with a little red bole. — 2)o«e. A teaspoonful, or more, in broth or beer, twice or thrice daily ; in dropsy. Webster's Diet Drink. A sweetened decoc- tion of betony, dulcamara, <;uaiacum wood, liquorice root, sarsaparilla, sassafras, thyme, and turmeric. Wilson's Gout Tincture. This is said to be wine of colchicum. Wright's Pearl Ointment. Take of white precipitate, 8 oz. ; Goulard's extract, 1 pint ; rub them to a cream, and add the mixture to white wax, 7 lbs., and olive oil, 10 lbs., pre- viously melted together by a gentle heat ; lastly, stir the whole until it is nearly cold. (' Pharm. Jnurn.') Young's Aperient Drink. From carbonate of soda, 2i dr.; bitartrate of potassa, 3 dr, (both in cr \ stals) ; throw them into a soda- water bottle containing cold water, 8 fl. oz., and immediately cork it down securely, and keep it inverted, in a cool place, until required for use. Zanhetti's Bohemian Restorative Tincture. From crushed raisins, | lb.; hay saffron, 2 oz. ; aqueous extract of opium, 3 dr. ; pow- dered cochineal, 3 dr. ; capillaire and orange- 1252 PAULLINIA— PEARL flower water, of each i pint ; proof spirit, 3 pints ; digested together for a week, and then strained, with expression. PAULLIN'IA. See Guahana. PAYAH'IZIlfG. The name given to Mr Payne's process for preserving and mineralising wood. See Dbt-bot. PEACH. St/n. Peesicum, L. The fruit of Ami/ffdalus Persica. Two varieties are known in our gardens — CLiNasTOHE peach and TKEESTONB PEACH, terms which explain them- selves. Tiie fruit is wholesome; but the flowers and kernels contain prussic acid, and are poisonous. The peach, the original habitats of which were Persia and the North of India, is now very generally grown in the South of Europe, in many parts of the East, and very largely in the more temperate portions of North and South America; more particularly in Penn- sylvania, New Jersey, and Maryland, where there are extensive orchards of peach trees. This fruit is also extensively cultivated by the Mormon community at Utah. The fruit of the Nectakine, which is a variety of the peacli, differs from that of the latter in having a smooth skin. When stewed, the fruit of the peach is said to be useful in habitual constipation. Dr Fresenius has analysed this fruit, and found its composition to be: — Soluble mattei — Large Butch. Sugar 1-580 Free acid (reduced to equivalent in malic acid) . . . 0612 Albuminous substances . . 0463 "I Fectous substances . . . 6°313 J Ash 0-422 Insoluble matter — Seeds 4-629 Skins \ Pectose J [Ash from soluble matter included in weights givenj . . . 0-042] Water 84-990 100-000 )-991 It will he seen from the above that the peach contains a very small amount of sugar. PEACH'WOOD. The produce of a species of Casalpinia, now extensively used in calico- priiitin». PEAE. Syn. Pyetts, L. The fruit of Pyrus communis (Linn.), one of the rosacese. Its general qualities resemble those of the apple. Composition op the Peae. Soluble matter — Sugar 7-000 Free acid (reduced to equiva- lent in malic acid) . . 0-074 Albuminous substances . 0-260 Pectous substances, &c. . 3-281 Ash 0-285 Insoluble matter — Seeds 0'390"l Skins 3-420 J PectKJse .... 1-340 [Ash from insoluble matter included in weights given] 0-050] Water 83-950 lOO-OOO (Feesenius.) PEARL. Syn. Maeoabita, Maeoaeiifm, Pbeia, Ukio, L. The most beautiful and costly pearls are obtained exclusively from the pearl oyster {Meleagrina margaritifera) of the Indian Seas. The principal fisheries are on the coast of Ceylon, and at Olmutz, in the Persian Gulf. An inferior description of pearl is procured from n fresh-water shell-fish ( Tlnio ma/rgaritifera) in the neighbourhood of Omagh, county of Tyrone. A similar quality is also procured from the river Ythan, Aberdeenshire, It is probable that pearls from this source col- lected by the ancient Britons may have given rise to the statement by Tacitus, in his 'Life of Agricola,' of pearls " not very orient, but pale and wan," being among the indigenous pro- ducts of Great Britain. Pearls are composed of membrane and carbonate of calcium ; or, in other words, of substances similar to bladder and chalk, in alternate layers. The cause of the production of pearls is highly curious and interesting. When any foreign body gains a, permanent lodgment within the shells of any of the moUusca which are lined with pearly matter, or nacre, the pearly secretion of the animal, instead of being spread in layers on the inside of its habita- tion, is accumulated around the offending particles in concentric films of extreme tenuity, and more or less spherical, farming a pearl. Pearls were formerly used in medicine as absorbents or antacids ; and among the an- cients they were occasionally taken, dissolved in acid, both as a remedy and for the purpose of displaying the careless opulence and luxury of their possessors. A perfect pearl, large, truly spherical, highly iridescent, and reflecting and decomposing the rays of light witli vivacity, claims to rank with the most costly of the gems, and in some parts of the East is, with justice, more highly prized than even the diamond. In Europe, however, the present estimation of their value is somewhat different, " A handsome necklace of Ceylon pearls, smaller than a large pea, costs from £170 to £300; hut one of pearls about the size of peppercorns may be had for £15. The pearls in the former sell at a guinea each, and those in the latter at about Is. 6d." (Milburn.) Seed pearls are of little value, however beau- tiful. Pearl, Artificial. These are hollow spheres or beads of glass, perforated with two holes at opposite sides to permit of their being strung PEARLA8H-PEAS 1253 into necklaces. A amall portion of epsence d'orient is introduced into cacli, by suction, and i« then aiirenJ over the inner surface o( the glass. When this has become dry and hard, the globe is filled up with white wax, spermaceti, or gum Arabic. Tlie glass of which the beads are formed is slightly bluish and opalescent, aud very thin. The latest improve- ment consists in removing the glassy appear- ance of the surface of the prepared bead by exposure to the fumes of hydrofluoric acid, highly diluted. Pearl, mother of. Si/n. UNiotftrM concha;, L. ; Nacbe db feble, Fr. This is the in- ternal or nacreous layer of those shells which produce the pearls for ornamenting the per- son ; hence the term ' mother of pearl ' is by no means inappropriate. It is also derived from several other species known in trade as ear-shells, green siiail-sbclls, Bombay-shells, The brilliant hues of mother of pearl do not depend so much upon the nature of the substance iie on its structure. Its surface is covered by minute corrugations or furrows, which give a chromatic appearance to the reflected light. Sir David Brewster was the first to show that this substance is capable of imparting its iridescent appearance to fusible metal or flue black wax. Mother of pearl is cut and wrought with nearly similar tools to those used lor ivory, but its treatment, owing to its more fragile nature and delicate structure, requires con- siderably greater care. It is polished with eolcothar or putty powder. The numerous applications of mother of pearl, for buttons and knile-handles, boxes, inlaying work, Ac, are well known. PEAEl'ASH. This is prepared by calcining crude potashes on a reverbcratory hearth, dissolving the calcined mass in water, and, alter repose, decanting the clear solution, and evaporating it to dryness in flat iron pans, the product being constantly stirred towards the end to reduce it to a semi-granular state. Although purer, its richness in absolute alkali is less than that of the potashes from which it is prepared, being only from 47§ to 51§. This exists almost entirely under the form of car- bonate. The commercial value of this sub- stance is determined by the ordinary processes of ALKAIIMBTKT. FEASL BARLET. See Bablet. PEASL FLAVOUB. See Esbenos. PEAKL WHITE. This is a subchloride of bismuth ; hut the name is now commonly applied to trisuitrate of bismuth, which is sold for it. FEASLS (SoBe). Syn. Robe beads. The petals of red roses beaten in an iron mortar for some hours, until they form a smooth, black paste, then rolled into beads and dried. Hard ; very fragrant ; take a fine polish. Pearls, to Polish. Take very finely pulverised rutten i,t'd, and of diijsolving, as Tnson has shown, calomel and other mineral Bub<.tance9. Prep. 1. (Henle, ' Med. Times A Gaz..' Feb- ruary lOlh, 1872, p. 152.) "The raucous membrane of a perfectly fresh pig's stomach is carefully dissected from the muscular coat, and placed on a flat board. It is then lightly cleansed with a sponge and a little water, and much of the mucus, remains of food, &c. care- fully removed. ' With the back of a knife, or with an ivory paper-knife, the surface is scraped very hard, in order that the glands may be squeezed and their contents pressed out. The viscid mucus thus obt-jined contains the pure gastric juice with much- epithelium from the glands and surface of the mucous membrane. It is to be spread out upon » piece of glass, so as to form u very thin layer, which is to be dried at a temperature of 100° over hot water, or in vacuo over sulphuric acid. Care must be taken that the tempera- ture does not rise much above 100 F°., because the action of the solvent would be completely destroyed. When dry the mucus is scraped from the glass, powdered in a mortar, and transferred to a well-stoppered bottle. With this powder a good digestive fluid m.iy be made as follows : Of the powder .... 5 grains. Strong hydrochloric acid . 18 drops. Water 6 ounces. Macerate it at a temperature of 100° for au hour. The mixture may be filtered easily, and forms a perfectly clear solution very convenient for experiment. " If the powder is to be taken as a medicine, from two to five grains may be given for a dose, a little diluted hydrochloric acid in water being taken at the same time. The pepsin powder may be mixed with the salt at a meal. It is devoid of smell, and has only a slightly salt taste. It undergoes no change if kept perfectly dry, aud contains the active principle of the gastric juice almost unaltered. "The method of preparing this pepsin was communicated to Mr liuUuck, of the Hrm of Messrs Bullock and Company, 8, Hanover Street, Hanover Square, who at cuce adopted it for the preparation of medicinal pepsin, and soon improved upon it in some particulars. The dose is from 2 to 4 or 5 grains. — Test, fths of a grain of this pepsin, with 10 drops dilute hydrochloric acid and an ounce of distilled water, dissolve 100 grains of hard-boiled white of egg in from twelve to twenty-four hours. In the body probably twice this quantity of white of egg or even more would be dissolved in a comparatively short space of time. The digestive powder prepared from the pig's stomach retains its activity for any length of time if kept dry. I had some which had been kept in n bottle for upwards of five years, and still retained its active power unimpaired. The solution made with this pepsin and hydro- chloric acid was nearly tasteless and inodorous. One pig's stomach, which costs sixpence, will yield about 45 grains of the powder prepared as above described " Gradually the usefulness of this prepara- tion of pepsin of the pig was found out, and it 1260 PERCENTAGE— PEECOLATION had to be prepared in increasing quantities. I should be afraid to say how many pigs' stomachs have been used of late years during the winter season. " In 1857 Dr. Pavy carefully examined the pepsin prepared and sold by many different firms, and found that this dried mucus of the pig's ptomach was the most active of them all (' Medical Times and Gazette,' 1857, vol. i, p. 336). In 1870 Professor Tuson instituted a still more careful comparative examination, and with a similar result (' Lancet,' August 13th, 1870) ; for he found that this prepara- tion was twenty-jive times stronger than some others that he obtained for examination." 2. (Scheffer, ' Pharm. Journ.,' March 23rd, 1872, p. 761.) " Of the well-cleaned fresh hog stomach the mucous membrane is dissected off, chopped finely and macerated in water acidu- lated with muriatic acid for several days, during which time the mass is frequently well stirred. The resulting liquid, after being strained, is, if not clear, set aside for at least twenty-four hours in order to allow the mucus to settle. To the clarified liquid the same hulk of a saturated solution of sodium chloride is added, and the whole thoroughly mixed. After several hours the pepsin, which, by the addition of chloride of sodium, has separated from its solution, is found floating on the surface, from whence it Is removed with a spoon and put upon cotton cloth to drain ; finally it is submitted to strong pressure, to free it as much as possible from the salt solu- tion. " The pepsin, when taken from the press and allowed to become air-dry, is a very tough substance, andpi'esents, according to thickness, a different appearance, resembling in thin sheets parchment paper, and in tljick layers sole leather ; its colour varies from a dim straw yellow to a brownish yellow. Besides a little mucus, it contains small quantities of phos- phate of lime and chloride of sodium, which, however, do not interfere with its digestive properties, as they are found also in normal gastric juice. " In order to get a purer article I redissolve the pepsin, as obtained after expression, in acidulated water, filter the solution through paper and precipitate again with a solution of sodium chloride ; the precipitate, after drain- ing and prefsing, is now free of phosphate of lime and mucus, but still contains salt. In the freshly precipitated state the pepsin is very readily soluble in water, and cannot therefore be freed from adhering salt by washing. " By allowing the pressed sheet of pepsin to get perfectly air-dry — whereby it becomes coated with a white film and small crystals of chloride of sodium — and by immersing it then in pure water for a short time, the greater part of sodium chloride can be extracted, but it has to be done very rapidly, as the pepsin swells up considerably and loses its tenacity. By operating in this matter I have obtained a pepsin which dissolves in acidulated water to quite a clear colourless liquid, but as it still contains traces of salt, I prefer to call it purified pepsin." 3. (B. Ph.) A preparation of the mucous lining of a fresh and healthy stomach of the pig, sheep, or calf. The stomach of one of these animals, recently killed, having been cut open and laid on a board with the inner surface upwards, any adhering portions of food, dirt, and other impurity, are to be re- moved and the exposed surlace slightly washed with cold water ; the cleansed mucous mem- brane is then to be scraped with a blunt knife or other suitable instrument, and the viscid parts thus obtained is to be immediately spread over the surface of glass or glazed earthenware, and quickly dried at a tempera- ture not exceeding 100° F. the dried residue is to be reduced to powder, and preserved in a stoppered bottle. — Dose, 2 to 5 grains. Pepsin, Saccharated. To work it into saccharated pepsin ('American Journal of Pharmacy,' January, 1871) the damp pepsin, as it is taken from the press, is triturated with a weighed quantity of sugar of milk to a fine powder, which, when it has become air-dry, is weighed again, the quantity of milk sugar subtracted, and so the amount of pepsin found. The strength of this dry pepsin is now ascertained by finding how much coagu- lated albumen it will dissolve at a temperature of 100° F. in five or six hours, and after this sufiicient milk sugar is added to result in a preparation of which ten grains will dissolve one hundred and twenty grains of coagulated albumen, and this preparation I have called saccharated pepsin. Pepsin with Starch. Pepsin mixed with starch is the medicinal Pepsine of M. Boudault ; the Poudre nutrimentive of M. Corvisart. PEUCENTAGE. Literally, "by the hun- dred." In commerce the term is applied to an allowance duty or commission on a hundred. (Webster.) PEECHLC'EATE, Syn. Pebohloeas, L. A salt of perchloric acid. The perchlorates are distingnished from the chlorates by their great stability, and by not turning yellow when treated with hydro- chloric acid. Like the chlorates, they give off oxygen when heated to redness. They may be prepared by directly neutralising a solution of the acid with a, solution of the base. See Potassium (Perchlorate of), and Chloeine. PEECHIC'EIC ACID. See Chloeine. PERCOLA'TION %». Method op dis- placement. A method of extracting the soluble portion of any substance in a divided state, by causing the menstruum to filter or strain through it. The 'sparging' of the Scotch brewers is an example of the applica- tion of this principle on the large scale. In PERCOLATION 1261 fiarmacy, the ' method of displacement ' is frequently adopteil for the preparation of tiucturea, infusions, &c., and is, in some re- spects, superior to digestion or maceration. " The solid materials, usually in coarse or mo- derately fine powder, are moistened with a sufficiency of the solvent to form a thick pulp. In twelve hours, or frequently without delay, the muss is put into a cylinder of glass, porce- lain, or tinned iron, open at both ends, but obstructed at the lower end by a piece of calico or linen, tied lightly over it as a filter ; and the pulp being backed by pressure, ranging as to degri'B with different articles, the re- mainder of the solvent is poured into the upper portion of the cylinder, and allowed gradually to percolate. In order to obtain the portion of the fiuid which is absorbed by the residuum, an additioijal quantity of the solvent is poured into the cylinder, until the tincture which has passed through equals in amount the spirit originally prescribed. The spirit employed for this purpose is then recovered, for the most part, by pouring over the residuum as much water as there is spirit retained in it, which may be easily known by an obvious calcu- lation in each case. The method of percolation is now preferred by all who have made suffi- cirut trial of it to apply it correctly." (Ph. E.) The first portion of liquid obtained by the method of displacement is always in a state ol' high concentration. In general it is a simple solution of the soluble ingredients of the crude drug in the fluid employed. But sometimes the solvent, if compound, is resolved into its component parts, and the fluid which passes through at any given time is only one of these, holding the soluble parts of the drug in solution. Thus if diluted alcohol be poured over powder of myrrh, in the cylinder of the percolator, the fluid which first drops into the receiver is a solution of an oily consistence, chiefly composed of resin and volatile oil, dis- solved in alcohol. In like manner, when the powder of gall-nuts is treated in the same way by hydrated sulphuric ether, two layers of fluid are obtained, one of which is a highly concen- trated solution of tannin in the water of the ether, and tlie other a weak solution of the same principle in pure ether. In all cases, therefore, in which it is not otherwise directed it is absolutely necessary to agitate the several portions of the liquid obtained by percolation together, in order to ensure a product of uni- form strength or activity. Several forms of displacement apparatus are employed by different operators. A simple and useful one is that figured in the margin. It has also the advantage of being inex- pensive, and may be made by any worker in tin plate. In operating on some substances it is found advantageous to hasten the process by pressure. This may be effected by any of the methods adopted for that purpose, and already de- scribed under Filteation. An ingenious little apparatus, which is well adapted for small quantities, is shown in the engr. By pouring 0. Percolator. i. SUnd. e. Receiver. d, Meiistruom. c. Substance operated on. /. Calico strainer. mercury or water through (tf), into the bottle (c), the air in the latter sutlers compression, and acts in a corresponding manner on the percolating liquor in (o). The whole of the joints must be made air-tight. a. Percolator. b. Tube connecting it with — c. A double-necked buttle containintc — d. Mercury. e Fi-eding-tube. /. Receiver. g. Stop-cock to regulate or arrest tlie pressure of air on the contents of the c>liu(Jer (a). The method of displacement, although ap- parently simple, requires for its successful application no inconsiderable amount of ex- perience and skill in manipulation. Tlie principal points to be attended to are — the reduction of the substance to the proper state of comminution (neither too coarse nor too fine), — the due regulation of the period of maceration according to the hardness, density, and texture of the substance; and, more important still, — the proper packing of the ingredients in the cylinder. On the correct performance of the last the success of the process mainly depends. Sume substances re- quire considerable pressure to be used, whilst others, when even lightly packed, scarcely permit the fluid to pass through them. When the material is too loosely packed, the men- struum passes through quickly, but without exerting its proper solvent action ; when too great pressure is employed, percolation either progresses very slowly or not at all. . On the whole, the firmness of the packing should be inversely as the solvent and softening power of the menstruum upon the solids exposed to its action; hut to this rule there are many exceptions, and each substance may be said to require special treatment. An excellent plan, applicable to all substances, and espe- cially to those of a glutinous or mucilaginous nature, is to mix the powder with an equal hulk of well-washed siliceous sand before 1262 PERCUSSION— PERIODIC ACID rubbing it up witb the menstruum. In re- ference to the coarseness of the powder it must be observed that substances which readily become soft and pappy wlien wetted by the menstruum, should not be used so fine as those that are more woody and fibrous, and not of a glutinous or resinous nature. The ' method of displacement ' has the ad- vantage of expedition, economy, and yielding products possessing considerable uniformity of strength ; but the difficulties attending its application by the inexperienced are serious obstacles to its general adoption in the labora- tory. It answers admirably for the prepara- tion of all tinctures that are not of a resinous nature, and for most infusions of a woody and fibrous substances, as roots, woods, barks, leaves, seeds, insects, &c., and particularly when cold or tepid water is taken as the solvent. It is also especially adapted for the prepara- tion of concentrated infusions and essences, as they may thus be obtained of any required strength without loss, or requiring concentra- tion by heat, which is so destructive to their virtues. " When (ordinary) tinctures are made in large quantities, displacement is never likely to supersede maceration, on account of any practical advantages it may possess. If the prescribed directions be duly attended to, the process of maceration is unexceptioniible. The process is moi'e simple than the other ; the mode uf operating is more uniform, it is, in fact, always the same ; it requires less of skill and dexterity in conducting it; it re- quires less constant attention during its pro- gress which, in operating on large quantities is a consideration ; and, finally, the apparatus required is less complicated. When, however, only small quantities of tincture are made at a time, and kept in stock, the adoption of the process of displacement will often be found convenient and advantageous. It offers the means of making a tincture in two or three hours, which, by the other process, would require as many weeks." (Mohr and Redwood.) Another useful application of the method of displacement is to the manufacture of extracts on the large scale. Here it is superior to any other plan. By the simple and inexpensive forms of apparatus in block-tin, stoneware, or glass, which have recently been designed for the purpose, not merely a first-class product is ensured, but a great saving in fuel and labour is at the same time effected. The reader is referred to the lust edition of the 'United States Pharmacopoeia,' and to papers by Messrs Sanndersand Schweitzer in the 'Pharmaceuti- cal Year Book for 1873,' and by Mr Camp- bell in the same publication for 1874, for additional information in the subject of " Per- colation." See BitEwiua, Extract, Tihctuee, &c. PEECUS'SION. Syn. Peeoussio, L. In medicine, the act of striking any part of the body with the fingers, or any instrument, to ascertain its condition. F££CUS'SION CAPS. The composition em- ployed to prime these articles is noticed under PULMINATIHG MEEOUET. PEK'FECT LOVE. See Liqttettb (Parfait amour). PEB'FUME. A substance that emits or casts off volatile particles which, when dififnsed through the atmosphere, agreeably affect the organs of smelling. The term is also applied to the volatile eflliuvia so perceived. The principal source of perfumes is the Vegetable Kingdom. Its flowers, bceds, woods, and barks furnish a' rich variety, (rom which the most fastidious connoisseur may select his favourite bouquet. A few perfumes, as musk, ambergris, and civet, are derived from the Animal Kingdom ; but none of these evolve an aroma comparable in freshness to that of the rose, or in delicacy to that of the orange- blossom, or even the unpretending jasmine. The Inorganic Kingdom yields not a single perfume, so called; nor has the science of chemistry yet been able to produce a single odoriferous compound from matter absolutely inorganic. PEKi'U"]IIEET. Peifumes in general; also the art of perfuming them. In its commercial application, this word embraces not merely pel fumes, but also cosmetics, and other articles of a closely allied character employed at the toilet, the manufacture and sale of which constitute the trade of the modern perfumer. Formulae for the preparation of all the more valuable perfumes, as well as of others met with in trade, both simple and compound, will be found under the heads Cosmetics, Dbpi- lATOEY, Essence, Haie dyes. Oils, Pastes, Pastils, Pomade, Spieit, Watees, &c., to whicli we refer the reader. Perfumes, Ace'tic. See ViNEaAB. Perfumes, Ammo"niated. These may be prepared by simply adding a sufficient quan- tity of ammonia to the liquid perfumes. When the articles are to be distilled, a cheaper plan is to add about 5 dr. of sal ammoniac and 8 dr. of carbonate of potassa to each pint of the article just before distillation. Ammoniated Cologne water is now a fashion- able substance for spirit of sal volatile. PERIODIC ACID. Syn. Hydeio peeiodatb. (H.IO4).) 1. By passing a current of chloiine gas tlirougii a solution of sodic iodate, contain- ing caustic soda, in the proportion of 3 atoms of tlie latter to one atom of sodic iodate. The hydrated basic sodic periodate, which crystal- lises out, is dissolved in diluted nitric acid, and precipitated by the addition of argentic Titrate; a normal argentic periodate crystal- lises as the liquid cools, and tliis salt being treated with water, is decomposed into a basic argentic periodate, which is insoluble, and periodic acid, which is dissolved. By evaporating the solution, the periodic acid may be obtained in deliquescent, oblique. PERISTALTIC PERSUADERS— PETROLEUM 1263 rhombic prisinn, which are somewhat soluble in alcohol mid in ether. 2. From perclilorie acid by the action of iodine. See Iodine. PEEISTAL'TIC PERSUADERS. See PiLts (Kitchener's). PER'MANENT WHITE. See Bamum (Sul- phate) and WUITE FIGMENTS. PEENAMBU'CO WOOD. Syn. Peach wood. The wood of Cceialpinia echinata. It consti- tutes the paler variety of Brazil wood used by the dyers. PE&'BT. 8i/n. PrBAOEUM, L. A fermented liquor prepared from pears in the same way as cider is from, apples. The red rough-tasted sorts are principally used for this purpose. Tile best perry contains about 9% of absolute alcohol ; ordinary perry from 5 to 7g. Perry is a very pleasant-tasted and whole- some liquor. Wiieu bottled ' champagne fashion,' we have seen it frequently passed off for champagne without the fraud being suspected. PER'SIAir BER'RIES. See Fbsnch beb- BIBS. PERSPIRA'TION. The liquid or vapour secreted by the ramifications of the cuticular arteries over the surface of the body. The perspiratory apparatus consists of a gland deeply seated in the corium, cominumcating by means of tubules (pores) with the surface of the scarf-skin. The uses of the perspiratory functions appear to be to preserve the suppleness and sensiliility of the skin, to maintain the tem- perature of the body at a uniform standard, and to remove from the system a number of coonpounds noxious to animal life. The per- spiration " is a fluid whose regularity and continuance of exlialation are not merely con- ducive, but absolutely necessary, to health ; without such regularity the animal tempera- ture would run riot, and substances of an injurious quality would be allowed to per- meate the finest and most delicate of the tissues of the body." (Eras. Wilson.) " From the constriction or constipation of the cuta- neous pores by the ambient air, especially when the body, beforehand put into a heat, is suddenly exposed thereunto, the serous par- ticles which used to fiy off continually in vapour, being now pent in, excite an intense and feverish etfervescence; till, finding some other passage, either by the kidneys or by the glandules of the nose and windpipe, they are discharged by way of a catarrh ; or, missing this separation, still keep up the ebuUitiou, very often to the hazard of life, by suH'ocat- ing the vital fiame. And this is the natural consequence of obstructed insensible perspira- tion, which, in the vulgar phrase, is the same with what they mean by catcliing cold, and of which, give me leave to remark, that as fevers make two thirds of diseases infesting mankind, according to the computation of the judicious Sydenham, so two thirds of fevers very probably may take their rise from per- spiration hindered." (Daniel Turner.) Sup- pressed perspiration is also one of the com- monest causes of diarrhoea. PERU'VIAN BALSAM. See Bamam op Pbec. PERU'VIAN BARK. See Cinchona. PES'SARY. %n. Pessitm, Pessabium, L. An instrument made of caoutchouc, gutta percha, box-wood, or ivory, inserted into the vagina to support the mouth and neck of the uterus. They are variously formed, to meet the prejudices of the party or the necessities of the case. The cup, conical, pjlobe, and ring pessaries (pessi) are those best known. Medicated pessaries are prepared by adding the active ingredients to a hard cerate, and pressing the mixture into the desired form. Astringents (various), belladonna, acetate of lead, mercury, &c., have been thus applied by Dr Simpson and others. The different formula are piven below: — Pessary, Alum. St/n. Pessits alfminis. Alum, catechu, wax, of each 1 dr. ; lard, 5J dr. Pessary, Belladonna. Sgn. Pessits sella DONNiB. Extr.ict of belladonna, 10 gr. ; wax, 22i gr. ; lanl, lidr. ; in each pessary. Pessary, Mercurial. Syn. Pesscs htdbab- GTBi. Strong mercurial ointment, i dr. ; wax, i dr.; lard, 1 dr. Mix. Pessary, Lead. Si/n. Pessus phtmbi. Ace- tate of lead, 7i gr. ; white wax, 22J gr. j lard, lidr. Pessary, Iodide of Lead. St/n. Pessus PLUMBI lODiDi. Iodide of lead, 5 gr. ; wax, 25 gr. ; lard, li dr. Pessary, Tannin. Syn. Prssrs tannini. Tannin, 10 gr.; wax, 25 pr. ; lard, IJ dr. Pessary, Zinc. iyn. Pessus zinoi. Oxide of zinc, 15 gr. ; while wax, 22i gr. ; lard, lidr. PEST'ILENCE. See Plagpe. PESTILEN'TIAL DISEASES. All those diseases wliieh are epidemic and malignant and assume the character of a plague. See CnoLKEA, &c. PET0N6'. Same as packfong. PET'ROLENE. The pure liquid portion of mineral tar. It has a pale yellow colour, a penetrating odour, and a high boiling point; is lighter than water, and is isomeric with the oils of turpentine and lemons. In its general proportions it resembles rectified mineral naphtha. PETRCLEUM. Syn. Rock oil. Liquid BITUMEK, Oil of petbe; Oleum peteje. Bitumen liquidum, L. Petroleum is an oil found oozing from the ground or ob- tained on sinking wells in the soil. To a li- mited extent it is met with in most countries of Europe and in the West India islands, but occurs in abundance in Pennsylvania and other parts of the United States and in 1264 PEWTEE— PHARMACY ACT Canada. It varies in colour from slight yellow to brownish black, in consistence from a thin mobile liquid to a fluid as thick as treacle, in specific gravity from 800 to 1100 (water being 1000) and is either clear and transparent or turbid and opaque. Petroleum is essentially a volatile oil, and when submitted to distillation yields gases homologous with light carburetted hydrogen of marsh-gas (Ronalds obtained three), liquids of similar constitution (Pelouze and Cahours isolated twelve), and solid pa- raffin-like bodies. Commercially petroleum is distilled so as to yield petroleum-spirit or mineral naphtha used as a substitute for tur- pentine and for burning in sponge-lamps and costermongers' barrow-lamps ; petroleum oil used all over the world as mineral lamp oil for illuminating purposes; and a heavy oil em- ployed for lubricating machinery. The value of a sample of rock-oil is determined by thus distilling a weighed quantity in a small glass retort and weighing the products. The petro- leum or middle product must be of such a character as to have a specific gravity not higher than 810 or 820 and to contidn so little petroleum spirit that it only evolves inflam- mable vapour when heated to 100° Fahr. in the manner prescribed in the Petroleum Act, 1871 (see beloio). Any petroleum product or mineral oil which will not stand this test, and which is kept in larger bottles than one pint, and in larger total quantity than three gallons, cannot be stored or sold except by licence of the local authorities. Directions for Testing Petroleum to ascertain the temperature at which it gives off in- flammable vapour. The vessel which is to hold the oil shall be of thin sheet iron; it shall be two inches deep and two inches wide at the opening, tapering slightly towards the bottom; it shall have a flat rim, with a raised edge one quarter of an inch round the top ; it shall be supported by this rim in a tin vessel four inches and a half deep and four and a half inches in diameter; it shall also have a thin wire stretched across the opening, which wire shall be so fixed to the edge of the vessel that it shall be a quarter of an inch above the surface of the flat rim. The thermometer to be used shall have a round bulb about half an inch in diameter, and is to be graduated upon the scale of Fah- renheit, every ten degrees occupying not less than half an inch upon the scale. The inner vessel shall be filled with the petroleum to be tested, but care must be taken that the liquid does not cover the flat rim. The outer vessel shall be filled with cold, or nearly cold water ; a small flame sliall be applied to the bottom of the outer vessel, and the thermometer shall be inserted into the oil so that the bulb shall be immersed about one and a half inches beneath the surface. A screen of pasteboard or wood shall be placed round the apparatus, and shall be of such di- mensions as to surround it about two thirds and to reach several inches above the level of the vessels. When heat has been applied to the water until the thermometer has risen to about 90° Pahr.,a very small flame shall be quickly passed across the surface of the oil on a level with the wire. If no pale blue flicker or flash is produced, the application of the flame is to be repeated for every rise of two or three degrees in the thermometer. When the flashing- point has been noted, the test shall be repeated with a fresh sample of the oil, using cold, or nearly cold water as before ; withdrawing the source of heat from the outer vessel when the temperature approaches that noted in the first experiment, and applying the flame test at every rise of two degrees in the thermometer. See Naphtha, Oils (Mineral), &e. PEW'TEK. This is an alloy of tin and lead, or of tin with antimony and copper. The first only is properly called pewter. Three varieties are known in trade : — Frep. 1. (Plate pewteb.) From tin, 79g; antimony, 7^; bismuth and copper, of each 2§ ; fused together. Used to make plates, teapots, &c. Takes a fine polish. 2. (Triple pewtee.) From tin, 79§; anti- mon, 15% ; lead, 6j ; as the last. Used for minor articles, syringes, toys, &c. 3. (Let pewteb.) From tin, 80g; lead, 20§. Used for measures, inkstands, &c. Ois. According to the report of the French commission, pewter containing more than 18 parts of lead to 82 parts of tin is unsafe for measures for wine, and similar liquors and, in- deed, for any other utensils exposed to contact with our food or beverages. The legal sp. gr. of pewter in France is 7'764; if it be greater, it contains an excess of lead, and is liable to prove poisonous. The proportions of these metals may be approximately determined from the sp. gr. ; but correctly only by an assay for the purpose. See Beass, Gebmak siltee. Lead, and Tin. PHAEAOH'S SERPENTS. 1. The chemical toy sold under this name consists of the powder of sulphocyanide of mercury made up in a capsule of tin foil in a conical mass of about an inch in height. Ignited at the apex an ash is protruded, long and serpentine in shape. The fumes evolved are very poisonous. 2. (Noir-POISONOUS.) Bichromate of potas- sium, 2 parts; nitrate of potassa, 1 part; and white sugar, 3 parts. Pulverise each of the ingredients separately, and then mix them thoroughly. Make small paper cones of the desired size, and press the mixture into them. They will then be ready for use, but must be kept from light and moisture. PHARMACY 'ACT. The following are the principal clanse.s of the Pharmacy Act of 1860 (31 and 32 Victoria, cap. cxxi). We have separated and placed last, those provisions of the Act which relate to the sale of poisons : — PHARMACY ACT 1265 Wlieroas it is expedient for the safety of the public that persons keeping open eliop fur the retailing, iliapeusing, or compouniling of poiaonn, niid persons known as chemists and draggists should possess a competent practical kni>wled£re of their business, and to that end, that Irom and after the day herein named all persons not already en;:aged in such business should, before commencing such business, be duly examined as to their practical knowledge, and that a n'gi^tt'r should be kept as herein provided, and also that the Act passed in the i5th and 16th years of the reign of her pre- sent Majesty, intituled ' An Act for Regulating the Qualification of Pharmaceutical Chemists,' hereinafter described as the Pharmacy Act, should be amended: Be it enacted, by the Queen's most excellent Majesty, by and «ith the advice mid consent of the Lords Spiritual and Temporal and Commons in this present Parliament assembled, and by authority of the same, as follows : — From and after the Slst day of December, 1868, it shall be unlawful lor any person to sell or keep open shop lor retailing, dispensing, or compounding poisons, or to assume or u^e the title ' Chemist and Druggist,' or chemist or druggist, iir pharmacist, or dispensing chemist, or druggist, in any part of Great Britain, unless such person shall be a pliarma- ceuticul chemist, or a chemist and druggist, within the meaning of this Act, and be re- gistered under this Act, and conform to such regulations as to the keeping, dispensing, and selling of such poisons as may from time to time be prescribed by the Pharmneeutical Society with the consent of the Privy Council (Clause 1). Oliemists and drui-'gists within the meaning of this Act shall consist of all persons who at any time before the passing of this Act have carried on in Great Britain the business of a chemist and druggist in tlie keeping of open shop for the compounding of the preser-ptions of duly qualified medical practitioners, also of all assistants and assneiates, who liefore the pissing of the Act shall have been duly regis- tered under or according to the provisions of the Pharmacy Act, and also of all such per- sons as may be duly registered under this Act (Clause 3). AH such persons as shall from time to time have been appointed to conduct examinations under the Pliarmacy Act shall be, and are hereby declared to be, examiners for the pur* poses of this Act, and are hereby empowered and required to examine all such persons as shall tender themselves lor examination under the provisions of this Act,' and every person who shall have been examined by such exa- miners, and shall have obt:iiued from them a certificate of competent skill, and knowledge, and qualification, shall be entitled to be regis- tered as a chemist and druggist under this Act, and the examination aforesaid shall be ' Sue abuve. TOL. II. such as is provided under the Phnrmney Act for the purposes of a qualification to be veijis- tered as assistant under that Act, or as the same may be varied from time to time by any bye-law to be made in accordance with the Pharmacy Act as amended by this Act, pro- vided that no person shall conduct any exami- nation for the purposes of this Act until his appointment has been approved by the Privy Council (Clause 6). No name shall be entered in the register, except of persons authorised by this Act to be registered, nor unless the registrar be satisfied by the proper evidence that the person claim- ing is entitled to be registered ; and any ap- peal from the decision of the regi-trar may be decided by the council of the Pliarmaceutical Society ; and any entry which shall be proved to the satisfaction of such council to have been fraudulently or incorrectly made niiiy be erased from or amended in the register, Ity order in writing of such council (Clause l\i). " The registrar shall, in the month of January in every year, cause to be printed, published, and sold, a correct registei- of the names of :ill pharmaceutical chemi>t«, and a correct register of all persons rcunstered as chemists and druggists, and in such retzisters, respectively the names shall be in alphabetical order, according to the surnames, with the respective residences, in the tnrm set forth in schedule (B) to this Act, or to the like effect, of all persons appearing on the register of pharmaceutical chemists, and on the register of chemists and druggists, on the 81st day of December last preceding, and such printed registers shall be called ' The Registers of Pharmaceutical Chemists and Chemists and Druggists,' and a printed copy of such regis- ters for the time being, purporting to be 80 printed and published as afores.nd, or any certificate under the hand of the saiil registrar, and countersigned b^ the president or two members of the council of the Pharmaceutical Society, shall be evidence in all courts and before all justices of the peace and others, that the persons therein specified are rei.'i>tei"ed according to the provisions of the Pharmacy Act or of this Act, as the case may be, and the absence of the name of any person from such printed register shall be evidence, until the contrary shall be made to appear, that such person is not registered according to the pro- visions of the Pharmacy Act or of this Act (Clause 13). Prom and after the 81st day of December, 1868, any person who shall sell or keep an openi shop for the retailing, dispensing, or com- pounding poisons, or who shall take, use, or exhibit the name or title of chemist and druggist, or chemist or druggist, not being a duly registered pharmaceutical chemist, or chemist and druggist, or who sliall take, use, or exhibit the name or title pharmaceutical chemist, pharmaceutist, or pharmacist, not being a pharaiaceutical chemist, or shall fail 80 1266 PHARMACY ACT to conform with any regulation as to the keep- ing or selling of poisons, made in pursuance of this Act, or who shall compound any medi- cines of the British Pharmacopoeia, except according to the formularies of the said Phar- macopceia, shall for every such offence be liable to pay a penalty or sum of £5, and the same may be sued for, recovered, and dealt with in the manner provided by the Pharmacy Act for the recovery of penalties under that Act ; but nothing in this Act contained shall prevent any person from being liable to any other penalty, damages, or punishment to which he would have been subject if this Act had not been passed (Clause 15). Clauses of the Pharmacy Act relating to the sale of Poisons. It shall be unlawful to sell any poison either by wholesale or retail, unless the box, bottle, vessel, wrapper, or cover in which such poison is contained be distinctly labelled with the name of the article and the word poison, and with the name and address of the seller ot tlie poison ; and it shall be unlawful to sell any poison of those which are in the first part of schedule (A.) to this Act, or may hereafter be added thereto under section II of this Act, to any person unknown to the seller, unless introduced by some person known to the seller ; and on every sale of any such article the seller shall, before delivery, make or cause to be made an etitry in a book to be kept for that purpose, stating, in the form set forth in schedule (F) to this Act, the date of the sale, the name and address of the purchaser, the name and quantity of the article sold, and the purpose for which it is stated by the purchaser to be required, to which entry the signature of the purchaser and of the person, if any, who introduced him, shall be affixed; and any person selling poison otherwise than is herein pro- vided, shall, upon a summary conviction before two justices of the peacejn England or the sheriff in Scotland, be liable to a penalty not exceeding £5 for the first offence, and to a penalty not exceeflinij £10 for the second or any subsequent offence ; and for the purposes ot this section the person on whose behalf any sale is made by any apprentice or servant shall be deemed to be the seller, but the provisions of this section, which are solely applicable to poisons in the first part of the schedule (A) to this Act, or which require that the label siiall contain the name and address of the seller, shall not apply to articles to be exported from Great Britain by wholesale dealers, nor to sales by wholesale to retail dealers In the ordinary course of wholesale dealing, nor shall any of the provisions of this section apply to any medicine supplied by a legally qualified apothe- cary to his patient, nor apply to any article when forming part of the ingredients of any medicine dispensed by a person registered under this Act, provided such medicine be labelled in the manner aforesaid with the name audaddress of the seller, and the insredients thereof be entered, with the name of the person to whom it is sold or delivered, in a book to be kept by the seller for that purpose, and nothing in this Act contained shall repeal or affect any of the provisions of an Act of the Session holden in the fourteenth and fifteenth years in the reign of her present Majesty, intituled ' An Act to regulate the Sale of Arsenic' (Clause 17). SCHEDUIE (A). Part 1. Arsenic and its preparations. Prussic acid. Cyanide of potassium and all metallic cyanides. ' Strychnine and all poisonous vegetable alka- loids and their salts. Aconite and its preparations. Emetic tartar. Corrosive sublimate. Cantharides. Savin and its oil. Ergot of rye and its preparations. Part 2. Oxalic acid. Chloroform. Belladonna and its preparations. Essential oil of almonds, unless deprived of its prussic acid. Opium and all preparations of opium or of poppies. By virtue and in exercise of the powers vested in the council of the Pharmaceutical Society of Great Britain, the said council do hereby resolve and declare that each of the following articles, viz. — Preparations of prussic acid. Preparations of cyanide of potassium and of all metallic cyanides. Preparations of strychnine, Preparations of atropine. Preparations of corrosive sublimate. Preparations of morphine. Red oxide of mercury (commonly known as red precipitate of mercury), Ammoniated mercury (commonly known as white precipitate of mercury). Every compound containing any poison within the meaning of ' The Pharmacy Act, 1868,' when prepared or sold for the destruc- tion of vermin. The tincture and all vesicating liquid pre- parations of cantharides, — ought to be deemed a poison within the meaning of the ' Pharmacy Act, 1868 j' and also that of the same each of the following articles, viz. — Preparations of prussic acid. Preparations of cyanide of potassium and of all metallic cyanides. Preparations of strychnine. Preparations of atropine, — ought to bo deemed a poison in the first part of the schedule (A) to the said 'Pharmacy Act, 1868.' PHENOL— PHLORIDZIN 1267 And notice is hereby also given, tliat the mid Society have Buhiuitt'd the gnid resoluti'm | lor the approval of the Lords of Her Majesty's ] Council, and that such approval has been given. [ By order, I Elias Bkkubidoe, Seorelaty and Segutrar of the Pharmaceutical Society of Qreat Britain. And whereas the council of the Pharmn- cetitical Soriety of Qreat Britain did, on the 17th day of November, 1877, resolve and de- clare in the virords following : — " That by virtue and in exercise of the powers vested in the council of the Pharma- ceutical Society of Great Britain, the said council does hereby resolve and declare that Chloral Hydrate and its preparatwnt ought to be deemed poi'ons within the meaning of the ' Pharmacy Act, 1868,' and ought to be deemed poisons in the second part of the schedule (A) of the said ' Pharmacy Act, 1868.' " And whereas the said Society have submitted the said resolution for the approval of the Privy Council, and the Lords of the Privy Council are of opinion that the said resolution should be approved. Now, therelbre, their Lordships are hereby pleased to signily their approval of the said resolution. C. L. Pjiel. Tardieu states that of late years the cri- minal administration of phosphorus has in- creased consideralily in France. For example, from 1851 to 1872, in 793 cases of poisoning, 287 or 36'2 per cent, were due to arsenic, and 267 or 31'1 per cent, to phosphorus ; whilst in the years 1872 and 1874, in 141 criminal poi- sonings by arsenic and phosphorus, only 74 were due to arsenic. Tlie explanation of these facts may reasonably be ascribed to the much greater facility with which phosphorus, in the form of matches or vermin pastes, can be procured than arsenic. PHE'NOL. CsHjO. See Carbolic acid. PHEHYL. CjHs. The hypothetical com- pound radical of the phenyl-series. Carbolic acid is said to be its hydrate. PHENYL'AMIHE. C.HsHjN. Aniline is sometimes so named on account of its relation to the phenyl series. PHIALS. The ordinary green moulded phials used by the pharmaceutist are made of a glass obtained from common river sand and soapboilers' waste. In the manufacture of the gla-s for the white phials purer materials (and these as free from iron and alumina as possible) are used. Decolourising agents are also employed. The following is given as the composition of a white glass for apothecaries' phials in 'Cliemistry i Theoretical, Practical, and Analytical :" Mackenzie and Co. 100 lbs. white sand. 30 — 26 „ potash, impure. 17 „ lime. 110—120 „ ashes. •25 — '5 lbs. binoxide of manganese- cullet. Fhials, Bologna. Small flasks or phials of unannealed glass, which fly to pieces when their surface is scratched by a hard body. Thus, if a small piece of flint be dropped into theu] they are shivered; whereas if a ballet be used they remain uninjured. FHILO'NIUU. The ancient name of an aromatic opiate, reputed to possess many vir- tues invented by Philo. See Confection of Opidm. PHILOS'OPHEE'S STONE. Syn. Lapis PBIL080PHOB0M, L. A Wonderful substance, the discovery of which formed tlie day dreams of the alchemists. It was supposed to be ca- pable of converting all the baser metals into (;ol(l, and of curing all diseases. Some of the alchemists appear to have laboured under the delusion that they had actually discovered it. The last of these enthusiasts was the talented and unfortunate Dr Price, of Guildford. Speak- ing of the age of alchemy, Liebig says : — " The idea of the transmutability of metals stood in the most perfect harmony with all the observa- tions and all the knowledge of that age, and in contradiction to none of these. In the first stage of the development of science, the alche- mists could not possibly have any other notions of the nature of metals than those which they actually held. . . . We tiear it said that the idea of the philosopher's stone was an error; but all our views have been developed from errors, and that which to day we regard as truth in chemistry may, perhaps, before to-morrow, he regarded as a fallacy." PHILOSOPHIC CANDLE. An inflamed jet of hydrogen gas. PHILOSOPHIC WOOL. Flowers of zinc. PHIL'TKE. Syn. FHiLTBaM, L. A charm or potion to excite love. The ancients had great faith in such remedies. Nothing certain is now known respecting their composition; but there is sufficient evidence that recourse was frequently had to them by the ancients, and that " their operation was so violent that many persons lost their lives and their reason by their means." The Thessalian philtres were those most celebrated. (Juv., vi, 610, &c.) At the present day the administration of preparations of the kind is interdicted by law. PHLOEE'TIN. CisHkOj. A cry stall! sable, sweet substance, formed along with grape sugar, when phloridzin is acted on by dilute acids. PHLORID'ZIN. Cj,Hj40,„. Syn. Phlo- EiziNB ; Phloeidzisum, L. Prep. By acting on the fresh root-bark of the apple, pear, or plum tree, with boiling rectified spirit; the spirit is distilled off, and the phloridzin 1268 PHOCENIC ACID— PHONOGRAPH crystallises out of the residual liquor as it cools. Prop,, S(o. Pine, colourless, silky needles, freely soluble in rectified spirit and in hot water, but requiring 1000 parts of cold water for its solution; its taste is bitter and astrin- gent. When its solution is boiled with a little dilute sulphuric acid or hydrochloric acid, it is changed into grape sugar and phloretin. Phloridzin hears a great likeness to salicin. It is said to be a powerful febrifuge. — Dose, 3 to 15 gr. PHOCE'NIC ACID. See DBLPHrsio acid. PHffiNIC'IlfE. See Indioo pueple. PHONO'GRAPH. Some years back Prof. Paber, of Vienna, constructed and exliibited in the chief cities of Europe ' a talking ma- chine,' which was able to articulate simple words and sentences with considerable dis- tinctness. The complex mechanism by which this WHS effected was contrived upon the principles of the human organs of speech, as the machine possessed an india-rubber tongue and lips, and an artificial larynx, made out of a thin vibrating tube of ivory. Paber's auto- maton, although of much greater scientific interest than the automatic flute and flageolet players of Vancanson, the trumpeter of Droz, and similar exhibitions of curious workman- ship, was, like these, only a mechanical curi- osity, without any promise of a useful applica- tion. Entirely distinct from Paber's machine, not only structurally and in the method by which it produces its effects, but also in the end designed for it by its inventor being an essen- tially practical one, is the ' speaking machine or phonograph ' of Mr Edison. The first impression that will occnr to those who having heard Mr Edison's instrument speak have subsequently made themselves acquainted with its construction, will probably be one of surprise that an effect so apparently startling as that which it has been able to produce should be accomplished by means so simple. B is a brass cylinder, through whose centre passes a metal shaft, the arms of which rest on upright supports, one of which is shown in the engraving. The arm of the shaft, obscured from view, corresponding in length with the partof it which is visible, is screw-turned,and it works in anutboredoutofthesupport. Attached to the screw-end of the shaft or axle is a crank c, by turning which a double movement, viz. a rotatory and a horizontal one, may be simultaneously imparted to the cylinder. Round the surface of the cylinder is cut a spiral groove corresponding in dimensions with the threads of the screw part of the shaft. Covering the whole of the cylinder is a sheet of tin-foil, which is secured to its edges by means of shell-lac varnish. In front of the cylinder, resting on a proper support, is a mouth-piece. A, at the bottom of which (the end nearest the cylinder) is a very thin plate or diaphragm of metal, and to this diaphragm is attached a round steel point, which when not in use does not touch the foil. Previously to using the apparatus' this steel point has to be accurately adjusted opposite to that part of the foil lying over the spiral groove. If PHONOQUAPH 1269 now the lips be applied to the month-piece, and any sentence be spoken, the crank being at the same time turned, the vibrations im- parted to the metal plate by the voice will cause the steel point to come into contact with that part of the foil overlying the groove in the cylinder, and to mnlie on the foil a number of indentations, as it revolves, and is carried forward laterally before the mouth-piece. Furthermore these indentations will be found to vary in depth and sectional outline accord- ing to the nature of the vibrations which have produced them ; and as experiment proves, are the specific and infallible caligrapby of those vibrations. " It might be said that at this point the machine has already become u complete phono- graph or sound writer, but it yet remains to translate the remarks made. Now, there is no doubt that by practice and the aid of a mag- nifier it W(mld be poasiljle to read phonetically Mr Edison's record of dots and dashes,' but he saves us that trouble by literally milking it read itself. The distinction is the same, as if. Instead of peruBing a hook ourselves, we drop it into a machine, set the latter in motion, and behold ! the voice of the author is heard re- peating his own composition. The reading mechanism is nothini,' but another diaphragm, held in the tube u, on the opposite side of the machine, iiud a point of metal, which is held against the tin-foil on the cylinder by a delicate ipriiig. " It makes no difference as to the vibrations produced, whether a niiil moves over a file or a file moves over a miil, and in tlie present in- stance it is the foil or indented foil-strip which moves, and the metal point is caused to vibnite as it is afi'ected by the passage of the indenta- tions. The vibrations, however, of this point nmst be precisely the same as those of the other points which made the indentations, and these vibrations transmitted to a second membrane, must cause the latter to vibrate similar to the first membrane, and the rosiilL is a synthesis of the sounds, which in the beginning we saw, »s it were, analysed. "^ In some of the later instruments, that section of the apparatus, shown at s is dis- pensuil with, and the reproduction of the spoken words or sentences is effected by bringing the cUinder back to its original starting point, opposite to the little steel projection attached to the metal disc nt the end of the mouth- piece A. The steel point is then brought by means of a screw into contact with the foil, > According to llie ' Pi»lytcclinic Review,' Mr Edison doi-9 noi Hppeur to liave yei solved the probleni of re)i(lin^ the |ili'>noi£rHpli record by sight. He stHtes ttiat ;dt1iou^u B npcnfic form exisls fur eacit artiniliiied simnd. the chief dillli uliics arise Irom the vurvin^ indenluliuns or marlis caused l>y the s very j^ratifying, and that the material of which it may be made should be either stout felted paper (to be varnished on the outer surface when used for speaking) or drum head moistened and pressed into a concave form before using."' The crank (shown in the figure) by which the cylinder is turned is very frequently sup- planted liy an apparatus consisting of weights and wlicc Is, or else by clockwork, wliereby the cylinder is put in motion. The advantage of the working of these arrangements over that of the crank arc, that instead of an inequality a regularity of movement of the cylinder is ensured, and it is thus made to ad- vance nt the same rate whilst the words are being reproduced as when they are being spoken. One of the efl'ects of this uniformity of the rotatiiin of the cylinder under its two modes of action is to reproduce the exact pitch or tone of the voice of the speaker, although a departure from it would in no way affect the delivery of the exact words. Accordingly, therefore, to the difference in the rate of movement of the cylinder during the reception and reproduction of speech, will he the divergence in tone between the original and the reproduced voice. If the cyliniler were moved more quickly in redeliver- ing the words the result would be that they would be in a higher, and, in the opposite case, in a lower key. ProbaWv, as one writer has suggested, the "curious effect might be pro- duced of a child's voice being converted into a man's deep base, or vice versa. lu view of the results of previous scientific 1 Puhhshcd in ' Mature.' rebruary 4th, 1878. 1270 PHOSGENE GAS— PHOSPHORUS discoveries, we should not be justified in re- fusing to admit the possibility, at any rate, of the realisation of some of the applications to which its inventor believes the phonograph will, in the course of time, be put. It must be admitted tljat these predictions as to iti ultiiiiiiie capabilities are sufficiently wondrous. They are that — the phonograph will be able to record and reproduce at a future time any air sung to it, so that the vocal triumphs of some of our most accomplished singers may be preserved and resung after tlieir death; that by its means may also be conserved and respoken, likewise after de ' Morth American Review,' May, 1878. PHOSPHORUS 1271 with cold wntiT, nnd, if convenient, hentcl in a Icmlen pan or boiler until it baa entirely lost iti granular elmracter; it ia now trans- ferred to one or a series of tall casks (accord- ing to tbe extent of the batch), :ind further diluted with a large quantity of water; after repose, the elear liquid is decanted, the sedi- ment washed with water, and the ' washings ' and 'decanted liquor' evaporateil in a leaden or copper boiler until the white calcareous deposit (gypsum) becomes considerable ; tlie whole is then allowrd to cool, the clear por- tion deciinted, and the sediment thoroughly drained on a filter; the liquid thus obtainid is evaporated in an iron pot to the consistence of a thick syrup (say 4 parts), when dry char- coal (in powder), 1 part, is added, and the desiccation continued until the bottom of the pot becomes nearly red hot, after which it is covered over and allowed to cool; the dry mixture, when cold, is put into one or more earthen retorts well covered with 'luting' and properly dried, and beat is applied (sideways rather thnn at the bottom) by means of a good air-furnace ; after a short time the beak of the retort is connected -with a copper tube, the other end of which is made to dip about one fourth of an inch beneath the surface of some lukewarm wiiter placed in a trough or wide-mouthed bottle. The distilled product is gurified by squeezing it through chamois leather under warm water, and is then moulded for sale by melting it under water heated to about 145° Fahr., and sucking it up to any desired height in slightly tapering, but perfectly straight, glass tubes, [ireviously warmed and wetted. The bottom of the tube being now closed with the finger, it is withdrawn, and transferred to a pan of cold water to congeal the phosphorus, which will then commonly fall out, or may be easily expelled by pressure with a piece of wire. Prop. S[c, Phosphorus in its normal con- dition is a pale yellow, semi-transparent, and highly combustible solid ; soft and flexible at common temperatures ; it becomes wnxy at about 75° Fiihr. ; melts at about 111°, and boils at 550° Fahr. ; it takes fire in the air at 165°, and oxidates at all temperatures above 32°. Exposed to the air below 60°, its surfiice is slowly converted into phosphorus acid. It is apparently insoluble in water, but it conveys its peculiar flavour and odour to that fluid when agitated with it j it is slightly soluble in ether, naphtha, and the fixed and volatile oils, and more freely so in bisulphide of carbon. It unites with oxygen, f ormingoxides, and with oxygen and hydrogen, forming acids, and with the metals, forming phosphides. Phosphorus is remarkable for assuming se- veral allotrophic forms. In one of these lorms (amorphous phospho]^u»),j^ai)ropertie8 are so altered that they miglit^Hiose of a distinct element. , ^j" tJsea. The principal consusiption of phos- phorus is in the manuiactureof Inciter matches. When swallowed, it acts as a powerful corro- sive poi-on ; but small do., with water, 1 gall., and mix it with water, 4 galls., just brmiiilit to the boiling temperature in a deep open boiler, stirring until a uniform milk of lime is formed ; then add phosphorus, 1 lb., and keep up the boiling constantly, add- ing hot water from time to time, so as to pre- serve the nicasnre as nearly as may be until all the plidspliorus is oxidised and combined, and the strong odour of the gas has disap- peared; then filter the solution through muslin, wa-li out that portion retained by the calca- reous residue with water, and evaporate the filtrate til! reduced to 6 pints ; re-filter, to remove a portion of carbonate of calcium re- sulting from the action of the air upon the solution; evaporate again until a pellicle forms, and set aside to ervstallise — or continue the heat with const.mt stirring until the salt gran- ulates. Obi. As spontaneously inflammable phos- phnretted hydrogen is given off during the boiling, the process must be conducted under a hood, with a strong draught or in the open air. Smaller proportions than those given may be used. Prop. Hypophosphite of calcium is a white salt, with pearly lustre, crystallising In flat- tened prisms; soluble in 6 parts of cold water, and slightly soluble in dilute alcohol. It is the most important of these compounds, and when introduced into the stomach it is sup- posed to be converted into phosphate of cal- cium. It has been termed 'chemical food.' By decomposition it readily furnishes the other hypophosphites. Ferric Hyperphosphite of. FePOj. Prep. By precipitating a solution of hypophosphite of sodium or ammonium, with solution of ferric sulphate, washing the gelatinous pre- cipitate with care (it being somewhat soluble); and, finally, drying it into an amorphous white powder. This is freely soluble in hydrochloric and bypopbosphoroiis acids. FotasBinm, Hypophosplute of K,POj. Prep. Prom hypophosphite of calcium, 6 oz.,\di8- solved ill water, 4 pints ; and granulated car- bonate of potassium, 5J oz., dissolved in water, i pint. Mix, filter, and wash the precipitate till the filtrat« measures 5 pints. Evaporate till a pellieie forms, then stir constantly, con- tinuing the heat till the salt granulates. A white, opaque, deliquescent body, very soluble in water and alcohol. dninine, Hypophosphite of Dissolve sul- phate of quinine, 1 oz., in water, by the aid of diluted sulphuric aeid ; precipitate the alka- loid with ammonia; wash the precipitated quinine and digest it in hypophosphorous acid with heat (the quinine being in exees^); after filtering the solution, allow it to evaporate spontaneously till the required salt crystal- lises. It forms elegant tufts of soft, feathery crystals, which are soluble in 60 parts of water. Sodium, Hypophosphite of. Xa3P0.2. Prep. From hvpophosphite of calcium, 6 oz., dis- solved iu water, 4 pints; and crystallised ear- bonate of sodium, 10 oz., dissolved in water, 1^ pint. Proceed as in making hypophosphite of potassium, but allowing 6 pints as the mea- sure of the filtrate. If required in crystals, the granulated salt may be dissolved iu alco- hol sp. gr. -835, evaporated till syrnpy, and set by in a warm place. Crystallises in rec- tangular tables, with a pearly lustre; is very S'lluble in water and ordinary alcohol, and deliquesces when exposed to the air. Phosphorus, Trioxide of. P2O3. Sj/n. Phosphorous anhydkide ; Anhtdkous PHOSPHORIC ACir. Prep. By burning pbospborns in a limited supply of ail"- White flaky powder, with an odour of garlic, and rapidly absorbing water to form phosphorous acid. Phosphorous Acid. H3PO3. Si/n- Htdea- TKD PHOSPHOBOtrs ACID. Pure phosphorus is volatilised through a layer of powdered mer- curic chloride, containid in a glass tube; 1274 PHOSPHORUS terchloride of phosphorus comes over, which, on being mixed with water, is resolved into hydrochloric acid and phosphorous acid; by evaporating the mixed liquid to the consis- tence of a syrup, the first is expelled, and the residuum forms a crystalline mass of hydrated phosphorous acid on cooling. Prop., if-c. It is a powerful deoxidising agent. Heated in a closed vessel, it is resolved into hydrated phosphoric acid and pure phos- phuretted hydrogen gas. With the bases it forms salts, called phosphites, which possess little practical importance. Phosphorous Feutoxide Acid. PjOj. Si/n. AnHTDEOUB PHOSPHOBIC ACID; Phospho- EIC ANHTrEIDE ; PhOSPHOEIO OXIDE. By the vivid combustion of phosphorus in a stream of dry atmospheric air, or under a bell- jar, copiously supplied with dry air. The product is pure anhydrous phosphoric acid under the form of snow-like flakes. It must be immediately collected and put into a warm, dry, well-stoppered bottle. In this state it exhibits an intense attraction for water, and when thrown into it combines with explosive violence ; exposed to moist air for only a few seconds, it deliquesces to a syrupy-looking liqnid. Phosphoric Acid. There are three distinct acids usually grouped ouder this head, namely, Metaphosphokic acid, HPO3; Pybophos- PHOBic acid, H4P4O7; and Obihophosphobic ACID, H3PO4. Metaphosphorio Acid. HPO3. Syn. Mono- basic PHOSPHOEIO ACID; GlACIAl PHOSPHO- EIO ACID. Prep. Bones (calcined to whiteness and powdered), 3 parts, are digested for several days in oil of vitriol, 2 parts, previously di- luted with water, 6 parts, the mixture being frequently stirred during the time; a large quantity of water is next added, the whole thrown in a strainer, and the residuiil matter washed with some hot water; the mixed liquors are then precipitated with a solution of carbonate of ammonium, in sligltt excess, filtered from the insoluble, finally ignited in a platinum crucible. By acting upon the anhydride with cold water. When phosphoric acid is added to a strong solution of phosphate of zirconium, and the mixture, after concentration, is exposed to a low temperature, prismatic crystals are de- posited. These, after being strongly heated to expel their basic water, are pure metaphos- phate of sodium. Prom the solution of this salt in cold water, a solution of pure meta phosphoric acid may. he obtained, as above, by means of nitrate or acetate of lead and sulphuretted hydrogen. Ohs. This acid precipitates the salts of silver white, and is distinguished from the other modifications . of phosphoric acid by the property which its solution possesses of coagu- lating albumen. Pyrophosphoric Acid. H4P2O7. %m. Di- basic PH03PH0EIC ACID. By Strongly heating common or phosphate of sodium. The water of crystallisation only is at first expelled, and the salt becomes anhydrous; but as the tem- perature reaches that of redness the salt loses water and is decomposed, By solution of the altered salt in water, crystals of pyrophos- phate of sodium maybe obtained. A solution of this last compound, treated with nitrate of lead, and the resulting precipitate, suspended iu cold water, and decomposed by sulphuretted hydrogen, yields a solution of pure pyrophos- phoric acid. Obs. Heat resolves this into a solution of the ordinary acid. Pyrophosphoric acid pre- cipitates the salts of silver of a white colour. The salts of this acid are called pyrophos- phates. Orthophosphoric Acid. H3PO4. Syn. Tei. HTDBIC PHOSPHATE, TEIBASIO PHOSPHOBIC ACID. Ordinary nitric acid is heated in a tubulated retort connected with a receiver, and small fragments of phosphorus are dropped into it, singly and at intervals; as soon as the oxygenation of the phos- phorus is complete, the heat is increased, the undecomposed acid distilled off, and the residuum evaporated to the consistence of a s\ rup. In this state it forms the phosphoric acid of the shops. Commercial phosphate of sodium is dissolved in water and the solution precipitated with another of acetate of lead ; an abundant white precipitate (phosphate of lead) falls ; this is collected on a filter, well washed, and, whilst still moist, is suspended in distilled water, and sulphuretted hydrogen gas passed into it, in excess; a black insoluble precipitate forms, while pure tribasic phos- phoric acid remains in solution, and is easily deprived of the residual sulphuretted hydrogen by a gentle heat. By concentration in vacuo over sulphuric acid, it may be obtained in thin crystalline plates. The solution of this acid may he boiled without change, but when concentrated and heated to about 400° Fahr. it is converted into pyrophosphoric acid, and at a red heat into metaphosphoric acid. Its salts are the ordinary phosphates, or orthophosphates, and they give a yellow precipitate with nitrate of silver. Tests. The following reactions characterise the ordinary or other phosphates : — 1. Chlo- ride of barium produces in aqueous solutions of the neutral and basic phosphates a white precipitate, which is insoluble in either hydro- chloric or nitric acid, and with difficulty so- luble in a solution of chloride of ammonium. — 2. Solution of sulphate of calcium produces in neutral and alkaline solutions of the phos- phates a white precipitate, freely soluble in acids, even the acetic— -3. Sulphate of magne- sium produces in solutions of the phosphates, to which some chloride of ammonium and free ammonia has been added, a white, crystalline. PHOSPHORUS 1275 and quickly subsiding precipitate of the pbos- phnte of ammuninm and miigneBium, which is iasolublu in n solution of either ammonia or chloride of ammonium, but readily soluble ill acids, even the acetic— 4. Nitrate of silver, with neutral and basic alkaline phosphates, gives a light yellow precipitate. If the fluid in which the precipitate ia suspended con- tained a basic phosphate, it doi's not affect ti^st paper; il' it contained a neutral phos- phate, the reaction will be acid. If the phos- phate examined has been heated to redness before solution, it then, as a melaphosphate, gives a white precipitate with nitrate of silver. —5. Hydrochloric acid is added to the solu- tion to acid reaction, and afterwards 1 or 2 drops of a concentrated solution of ferric chloride ; a solution of acetate of potassium is next added in excess, when a flocculeiit, geUtinouii, white precipitate will be formed if phosphoric acid or any phosphate was present in any form or combination in the original liquor. This test is highly characteristic, and of general applicability. Obi. The insoluble phosphates must be first treated with diluted hydrochloric or sulphuric acid, and the resulting solution filtered and neutralised with an alkali, before applying the reagents. When the substance uniler ex- amination consists of a very small quantity of phosphoric acid or phosphate, with a large quantity of sesquioxide of iron, it should be fused with some carbonate of sodium, the residuum of the ignition exhausted with water, and the tests applied to the filtered solution. Arsenious acid, if present, should bo removed by sulphuretted hydrogen before applying the tests. When phosphate of alu- minum, the solution in hydrochloric acid is neutralised with carbonate of sodium i car- bonate of barium is next added in excess, followed by the addition of hydrate potas- sium, also in excess, after which the whole is boiled. An insoluble phosphate of barium is formed, which may be decomposed by sul- phuric acid, as before. See Molybdaie of Ammonium. Estim. Pure solutions of phosphoric acid roily bo tested by the common methods of acidlmetry. When in a state of combination, it may be separated and weighed in either of the forms noticed under GtlANO. Uses, Sfc. This acid is the common form, and is the compound alluded to when 'phos- phoric acid' is spoken of. It is extensively employed by the bleacher, dyer, calicn-printer, and enameller. Unlike sulphuric acid and the other strong acids, it does not coagulate al- bumen nor injure vegetable fibre, and is not decomposed by contact with organic matter. In combination with olumina and a large boracic acid, it is suid to be capable of pro- ducing a glaze for earthenware of extreme lieauty and durability, and perfectly innocuous. It is also used in medicine. PUOSPUOBIO ACID, UILnTBD. (B. Ph.) Put 6 fl. oz. of nitric acid (sp. gr. 1'42), diluted with 8 oz. of distilled water, into a tubulated retort connected with a Liebig's condenser, and having added 413 gr. of phosphorus, apply a very gentle heat until 5 fl. oz. of liquid have distilled over. Return this to the retort, and renew and continue the distilla- tion until the phosphorus has entirely dis- solved. Tr.insfer the contents of the retort to a porcelain capsule and evaporate the liquid until it is reduced to 4 fl. oz. Transfer to a platinum vessel and evaporate to about 2 fl. oz., and until orange vapours cease to form. Mix when cool in such an amount of distilled water that tiie volume shall become one pint. (It contains 10 per cent, by weight of anhy- drous acid. Sp. gr. 1'08.) — Dose, 10 to 30 minims properly diluted. PHOSPHOEUS, BALDWIN'S. Recently fused nitrate of calcium. For this purpose it must be broken into fragments whilst still warm, and at once placed in dry and well- stopped phials. After exposure for some time to the direct rays of the sun it emits sufileient light in the dark to render visible the figures on the dial-plate of a watch. PHOSPHOEUS, BOLOGNIAN. Syn. Keb- CHEB's PH08PH0BCS, BOLOONIAN BTONB. This substance was accidentally discovered by a shoemaker of Bologna, and excited much inteie-t about the middle of the 17th century. The following is said to have been the formula employed by the Logani family, who were particularly successful in its preparation, and acquired wealth by its sale to the curious throughout Europe. Prep. Reduce recently calcined native sul- phate of barium to powder, make it into a paste with mucilage of gum tragaoanth, and roll the mass into pieces about i inch thick and 1 to 2 inches long; dry these slowly by a moderate heat, and then expose them to it;iii- tiou in a wind furnace, by placing them loosely among the charcoal ; lastly, allow them to cool slowly, and at once place the pieces in well-stopped phials. Liko the preioilii;^ sub- stance, it phosphoresces in the dark after exposure to the sun's ra\8. PHOSPHOEUS, CANTON'S. Prep. From calcined oyster shells, 3 parts; flowers of sulphur, 1 part; placed in alternate layers in a covered crucible, and exposed to a strong heat for about an hour. It is preserved and used like the above. PHOSPHOEUS, HOMBERG'S. Recently ignited chloride of calcium. PHOSPHORUS BOTTLES. Prep. 1. Phos- phorus, 12 gr.; olive oil, i oz. ; mix in on oz. phial, and place the latter, loosely corked, in a basin of hot water ; as soon as the phosphorus is melted, remove the phial, cork it securely, and agitate it until neai-ly cold. On being uncorked it emits sufficient light in the dark to see the time by a watch, and will retain this property for some years if not too frc- 1276 PHOSPHORUS— PHOTOGRAPHY quently emplnyed. These are frequently called 'luminous phials.' 2. (Bbiqitets PHOSPHOEiQtTES.) — a. From phosphorus, 3 parts ; white wax, 1 part ; cau- tiously melted together by the heat of hot water J as the mixture begins to cool, the bottles are turned round, so that it may adhere to the sides. b. (Bendix.) Cork (rasped small, and dry) and yellow wax, of each 1 part ; phosphorus, 4 parts ; petroleum, 8 parts ; mixed, by fusion, as the last. Used as instantaneous-light bottles. A sulphur match rubbed against the composition immediately inflames on exposure to the air. They should be only unstoppered at the instant of introducing the match, and should be handled with caution. PHOSPHOKUS MATCHES. See Matches, and above. PHOSPHORUS PASTE. Syn. Anti-akse- NIOAL EAT-POISON, PhOSPHOB-PASTE. Prep. 1. Phosphorus, 1 oz. ; warm water, 1 pint ; place them in a bottle, cork it, and agitate them well together, until the phosphorus is reduced to a minute state of division, adding towards the end moist sugar, i lb. ; next add of lard (meltud by a gentle heat), 1 lb., and repeat the agitation until the whole is nearly cold; when cold, form it into a stiff dough with oatmeal or barley meal, and make this into small balls or cakes ; lastly, dry these in the air, without artificial heat. 2. (Simon.) Phosphorus, 8 parts; water (lukewarm), 180 parts ; mix in a mortar, and add of rye meal, 180 parts; when cold, fur- ther add of butter or lard, 180 parts ; sugar, 125 parts ; and mix the whole thoroughly to- gether. This is the formula authorised by an ordonnance of the Prussian Government, dated April 27th, 1843. Ohs. Rats, mice, &c., eat the above compo- sition with avidity, alter which they soon die. It is said that the best method of using it is to place small pieces of it in and about the holes, with some water in a shallow vessel for them to drink. It has the advantage of re- taining its efficacy for many years, and is less dangerous to human beings than compositions containing arsenic, whilst it is even more effec- tive for the purpose for which it is temployed. Some persons recommend the addition of a little oil of rhodium or oil of aniseed. See Eats, cScc. PHOS'PHURET. Syn. Phosphide; Phos- phxtketum:, Phosphidum, L. A compound of phosphorus with a metal or other basic radical. See the respective Metals, &c. PHOSPHURETTED HY'DEOGEN. Syn. PhOSPHOBETIED HYDBOaBN. See HXDEO- GBN. PHOSPHATIC DIATHESIS. Syn. White GBAVEL. A morbid condition of the system, characterised by the deposition in the urine of certain salts of phosphoric acid or phosphates. In this affection the urine, contrary to its normal condition, is always alkaline, and the nature of the phosphatic deposit is influenced by the source of the alkalinity. If, as most frequently happens, this is owing to the pre- sence of carbonate of ammonia (formed by the decomposition of the urea by the bladder mucous), the deposit will be found to consist of the triple phosphate, or phosphate of mag- nesia and ammonia, almost always associated with a small quantity of amorphous phosphate of lime. Under these circumstances the urine is pale in colour, and upon standing soon de- composes, in doing which it gives off a strong ammoniacal odour. Phosphatic diathesis is a frequent accompaniment of spinal aflcctious and of chronic inflammation of the mucous lining of the bladder. In mild attacks the best treatment consists in living rather generously, and in the admin- istration of vegetable tonics combined with proper doses of the mineral acids. PHOTOG'EAPHY. Syn. HEHoaEAPHT. The art of producing images on prepared sur- faces by means of the actinic or chemical rays of the sun's light. The principal photographic processes now in use are the positive-, negative-, and dry-collodion processes, in each of which a thin film or skin of iodised collodion forms the sensitive surface, a plate of glass being generally used as the foundation of the film. In a positive picture the 'lights' are silvery white by reflected light, and the ' shades ' are produced by a ' backing ' of black varnish or velvet, showing through the glass plate. In a negative picture the 'lights' are of a dirty yellow or brown by reflection, and being formed by opaque deposits, appear dense black by transmitted light. Xegatives are used in the various paper-printing processes ; they are placed upon prepared paper and exposed to direct light, which darkens those parts of the paper not protected by the opaque 'lights,' and thus produces positive prints with natural lights and shades. In this way the portrait ' cartes de visite' and other paper photographs are formed. Of late years there have been devised a great variety of new photographic processes, some of which are given below, together with modern formulae for the principal solutions, &c., in general request by the photographer. The Daguerreotype process, discovered by M. Dagutrre in 1839, has been entirely super- seded by the easier, healthier, and less expen- sive collodion processes described further on. It consists in submitting n plate of silver or silvered copper to the vapour of iodine and bromine irt the dark. A sensitive film of iodide and bromide of silver is thus formed on the plate, which is immediately exposed to the image of an object in the camera obscura. The latent image impressed on the plate is brought out or developed by exposing the plate to the action of the vapour of mercury. It is to be noted that in all English photo- graphic formuliE the solid and fluid measures PHOTOQEAPHY 1277 of apotliccnrieg weight are used ; but in buy- ing or selling chemical articles, the avoirdu- pois weight is employed. yUrate of Silver Bath (for Posifites). Ee- cr\'.t:illi8ed nitrate of silver, 5 dr., dissolved in lU oz. of distilled water. Filter the solution until it is quite clear, then add 3 drops of nitric aciil and 10 drops of collodion. Shake well together and filter. Blue litmus paper ahoald slightly redden in this bath ; should it turn very red, add a little ammonia, or oxide of silver ; should it not redden at all, add a little acid carefully drop by drop. It is pre- ferable to have a slight excess of acid. Developing Solution (for Positives). Pro- to>ulphate of iron, 2 dr., dissolved in 8 oz. of distilled water ; add 2} dr. of glacial acetic acid, 2i dr. of alcohol, and 5 minims of nitric acid. Filter, and pour into a well-stoppered bottle ; do not expose to the air. Fixing Solution (for Positives). 50 gr. of cyanide of potassium dissolved in 5 oz. of dis- tilled water ; that is to say, for every fluid oimce of solution required, mix 10 gr. of cya- nide of potassium in 1 oz, of distilled water. Filter and keep in a well-stoppered bottle, and label " Poison." Positive Paper. Plain paper requires pre- paring or salting before it is ready ibr use, or it may be purchased already salted. Procure some sheets of plain Saxe paper, and immerse them for five minutes (removing air-bubbles) in the following solution : — Chloride of ammonium , . 100 gr. Chloride of barium . . . 100 fir. Citrate of soda ... 20 ^r. Water 20 oz. Hang the sheets up to dry. For portraits and most other uses the paper is albuminised on one side. When photographs are printed to be afterwards coloured, unalbuminised paper is used. Albuminieed Paper. There are several well-known papers sold; Sive's, which is a French paper, has a high glaze and fine sur- face ; the Sajce, which is more uniform in its tcxtnre, is made in Germany. Another maker is Touigood. Positive paper is albuminised by placing it in u mixture composed of white of eggs and i-alt. To the white of each moderate- sized egg use 15 gr. of common salt reduced to a fine powder ; whisk until the albumen is all white froth. Leave this froth in a glazed earthen pan for about 12 hours, by which time most of it has settled into clear albumen ; pour the clear portion into a flat porcelain tray. This tray should be somewhat larger than the sheets of pupcr to be albuminised. Lift the paper up by the ends and lay it corefuUy on the albumen, keeping the side marked as " inferior" uppermost and dry. Tl]> piiper should be slightly damp before it is thus treated, as it then takes the albumen more regularly, and is not so liable to air- bubbles. Tlie paper must be lifted at each end, and should any air-bubbles appear, brush them off with a card or small brush, replacing the paper in the bath. Wherever the albumen does not come into actual contact with the paper, a white mark will appear in the print. Eemove the paper from the bath and place it to dry on a cardboard frame, or suspend it at the corners by clips. Paper glazed with pure albumen acquires too brilliant a glaze for portraits; the albumen may be diluted with from a i to i its bulk of water. It should be kept in tin or zinc cases. Plain Paper. Albuminised paper may bo used as plain paper if, instead of sensitising the glazed side, the plain side is placed in the seusitising solution. Nitrate of Silver Bath (for Negatives). Eecrystallised nitrate of silver, i oz. ; distilled water, 7 oz. ; collodion, 7 drops. .Shake well together until the crystals have dissolved, then filter. The purity of the negative bath is a matter of great importance, hence the necessity of employing the very best nitrate of silver, and also of excluding all foreign matters of every kind. When the bath gets out of order, it should be diluted with au equal bulk of dis- tilled water, and exposed to the sun for a feiv days, in a white glass bottle, then filtered, and sufiicient nitrate of silver added to restore the strength to 35 grains an ounce, as indicated by the argentometer. The Argentometer. This instrument is for ascertaining the strength of the nitrate of silver solution, which becomes weakened to a certain extent, after the immersion of every plate. Developing Solution (for Negatives). Proto- sulphate of iron, 75 gr. ; glacial acetic acid, 2 dr.; alcohol, 2 dr.; distilled water, 5 oz. Dissolve the crystals in the water, then add the acid and alcohol, and filter. In hot weather a little more acetic acid may be added, and if it does not flow rcadilv, the alcohol may be increased. Intensifying Solution, No. I (Negatives). Pyrogallic ncid, 10 gr.; citric acid, 10 gr. ; dis- tilled water, 5 oz. Wlien it becomes brown it is useless. No. 2. Eecrystallised nitrate of silver, 40 gr. ; distilled water, 1 oz. ; dissolve and filter. This latter will keep for any length of time in the dark. Another Intensifiiing Bath (Negatives). A saturated solution of bichloride of mercury in water. Place the uej:ative plate in a bath of the solution, remove when the film assumes a milky-white appearance, wash, and then plunge into a solution of 1 oz. of liquid ammonia to 10 oz. of water. Eemove the plate, wash, and place to dry. This mode of intensifying may be regulated by leaving the plate in the bichloride of mercury a shorter time, when it will require a weaker ammonia bath than that above given. Fixing Solution (for Negatives). Hyposul- phite of soda, 5 oz. ; distilled water, 5 oz. ; dissolve and filter. 1278 PHOTOGRAPHY Sensitising Solution {for Paper). Nitrate of Bilver, 5 dr. ; distilled water, 5 oz. j nitric acid, 2 drops ; kaolin, 1 oz. Dissolve the nitrate of silver in the water, and then add the acid and kaolin ; the kaolin will not dissolve, its use being to prevent the solution becoming dis- coloured alter using. This solution will not require filtering ; it must be allowed to become quite clear, and when required for use must be carefully decanted. This solution should be occasionally tested with the argentometer, and sufficient nitrate of silver added to restore it to its original strength. Another Negative Collodion. Ether, i oz. ; gun-cotton, 7 gr. ; bromide of cadmium, i gr. ; bromide of ammonium, li gr. ; iodide of cal- cium, 1 gr. ; iodide of potassium, 1 gr. ; iodide of ammonium, 1 gr. For intensifying, flood with chloride of gold, 1 gr. ; water, 15 oz. ; then wash, and flood with pyrogiillic acid, 2 gr. ; water, 3 oz. Toning Batlis. 1. Chloride of gold, 4 gr. ; acetate of s-oda, i oz. ; distilled water, 10 oz. ; dissolve and filter. 2. To produce black to bright sepia tones, according to length of immersion. T^ke carbonate of soda sufficient to cover a threepenny piece, dissolve it in a teaspoonful of cold water in a cup, add 2 gr. of chloride of gold, theu add 3 oz. of boiling water; use in 15 minutes. This will suit Hart's albuiniuised paper. Fixing Solution {for Paper Prints). Hypo- sulphite . 2i oz. White of eggs . . . 10 oz. Iodide of potassium . . 50 gr. Bromide of ammonium . 10 gr. Strongest solution of am- monia .... 120 minims. Introduce these materials with some pieces of broken glass into a bottle capable of holding twice the quantity, and agitate till the whole forms a Iroth, and then, when settled, it is ready. A piece of camphor placed in the solution will help to preserve it. It must be filtered before using. After the plate has been coated with the above it is finished by drying before the fire. In this pi-ocess all the above operations mav be performed in ordinary white light. To nnider the plate sensitive, heat it as hot as the hiind will bear, and when cool immerse it again in the following aceto-nitrate of silver bath for one minute, using only a yellow light, then wash thoroughly in clean water, and dry in the dark. Nitrate of silver . . ,30 gr. Distilled water . . . 1 oz. Olacial acetic acid . . i dram. The development may be commenced by either plain or alkaline pyro ; Mr M odd gives the preference to the plain, and intensifying after with acid silver. Dr Rtlet's Modified Collodio-albumen Dry Process. In this method the plate has to be sensitised as usual, and washed thoroughlv. When the plate has been well drained, and while still wet, it is coated with the following solution : Albumen . . . . 1 oz. Water 2 oz. Ammonia . . . .30 minims. Tlie solution is beaten to a froth, allowed to cettle, and filtered before usin^'. Pour suffi- cient over the plate to cover it, letting it flow backwards and forwards so as to "oak into the film. Pour the albuminous solution away and thoroughly wash the plate, the last rinsing being with distilled water. Let the plate dry ; when perfectly dry, moisten the plate with distilled water, and pour over the following solution : Gallic acid . . . . 2 pr. Water 1 oz. Filter the solution before using. Pour it on and oH' the plate to well permiate the film, then set the plite up to drain, and dry without washing off the gallic acid solution. When the surface is dry finish by the heat of a dull fire. Bromide of Silver, Wet Process. To every ounce of good collodion 'add 8 t;r. of bromide of cadmium. The nitrate bath must be made 80 gr. to the oz., and slightly acidu- lated with nitric acid. The plate must remain in the bath the full time it recjuires to form a dense opaque film. When the plate is ready (it must not be removed from the bath until the film is much denser than in the ordinary wet process) it must be washed thoroughly to remove all silver. It must then have poured over it a 3-grain solution of gela- till made slightly alkaline with carbonate of soda, or diluted albumen (albumen, 1 oz. ; water, 4 oz., well beaten together). When the plate is in this condition it may be exposed wet, or it may be allowed to dry. Prior to development it must be well washed, and the alkaline method must always be adopted. If the plates are used dry, a preliminary coating of dilute albumen is necessary, but if used wet, this is not necessary. Bromide of Silver, Emuhion Process. By this method the nitrate bath is not necessary, as the sensitive material is contained in the collodion. The purchase of the material ready-made for working this proce.«s is recom- mended in preference to its direct manu- facture, as its preparation demands the use of considerable technical skill, together with the employment of a gun cotton not usually 1280 PHOTOGRAPHY attainable. Mr Hughes says the 'Liverpool Dry Plate Company' supply an excellent emulsion. It is only necessary to pour the emulsion on to a plate and to allow it to dry, when the plate is ready for use. The develop- ment is by the alkaline process. Qelatino-hromide of Silver, Emulsion Pro- cess. In this process the use both of the nitrate bath and of collodion are abolished. The material employed is very troublesome to prepare, and oti this account, as well as because of the risk of failure attending the use of home-made articles, it is far preferable it should be purchased. It may he obtained under the name of ' Kennett's Sensitised Pellicle.' This pellicle consists of shreds of dry gela- tin containing the sensitive salts. Fresh directions accompany each packet of the " Sensitised Pellicle." 2%e Honey Process. Let the plate be cleaned, coated, and sensitised in the usual manner ; then place it in » bath of distilled water, washing it more or less, as it may be required to be kept for a longer or shorter time. Pour on the plate a solution made of equal parts of honey and distilled water in the same manner as when using collodion ; throw away the first portion, and repeat the operation, letting the solution soak in for one or two minutes ; pour back the honey solution into its bottle ; drain the plate on blotting paper, and keep it in the dark free from dust. The time required for exposure of the plate is about double as long as in the ordinary wet process. The plate should be soaked in distilled water previous to being developed, in order to soften or remove the film of honey j the older the plate the longer it will require to be soaked, afterwards dip the plate in the silver bath, and develop in the usual manner. The Carbon Process. In this process, the Adoption . of which is daily increasing, the material employed consists of a layer of gela- tin containing carbon, or some other permanent pigment, spread on paper. In this condition the paper is not sensitive to light, but if it be treated with a solution of bichromate of potash, dried in the dark, and afterwards exposed to sunlight under a negative, those portions of the paper which have been acted upon by the light will become insoluble, whilst those parts that have been prote<:ted from it will be soluble. When, therefore, after sufficient exposure, the pre- pared paper is removed from the negative, a picture the reverse of the negative will have been formed, in which the pigmented gelatin alone remain, and performs the part of the reduced silver in the ordinary photograph. If the film, after exposure to light under a negative, is soaked in warm water, all the parts which have been protected from the action of the light can be dissolved, and a relief is formed which, when dry, is sufficiently hard to transmit its shape to lead, from the mould or plate thus obtained a com- paratively large number of impressions can be taken, either with coloured gelatin or with fatty colours, the well-known Woodbury-type being the most successful of the several pro- cesses b.ised on the fact. Photographic Varnlsli. See Vaekishes. Miscellaneous eeoipes ; To Clean Glass Plates. (Mr Mayall.) Shake up together alcohol, 30 parts; strong liquid ammonia, 10 ; water, 40 ; and fine tripoli, 30 parts. The plates are to be rubbed hard and evenly with balls of cotton wool dipped in this mixture. Eub again, when dry, with a clean ball of cotton ; lastly, dust the back and edges with a clean hog-hair brush. To Clean off Collodion Pictures. This may be done, whether they have been varnished or not, by means of a tuft of cotton wool dipped in wood spirit. To Colour Photographic Prints. This may be done variously in water and oils. A simple way is to rub in slowly with a small camel-hair brush a minute piece of dry colour laid upon the part, as of flesh tint for the face, &c. When properly distributed, the paper may be breathed upon, and the tint will not easily be rubbed off. Or it may be carefully coated with gelatin. M. Minotto has described a plan of colouring on the back of the paper. The picture, being held up to the light, is first faintly outlined, on the reverse side ; colours are then laid on, of water or oil, as preferred, on this side. When dry the paper is rendered transparent by a varnish, and the colours will then appear through it with all the delicacy and effect of a miniature on ivory. Good strong writing paper is best for this purpose ; the colours must he vivid; and the varnish may consist of Canada balsam dissolved in turpentine, or a mastic vai-nish may be used, or turpentine and wax, or oil. To Semove Stains from the Hands. The powerfully poisonous character of cyanide of potassium renders its employment for the above purposeanoperationattended with considerable danger. Iodide of potassium and iodine may both be subotituted, but the first is expensive, and the second requires considerable nicety in its applicatiim, lest a coloured stain be left on the skin. Instead of the above substances, M. Fortin recommends to wash the hands with a concentrated solution of either sulphate or chloride of zinc, to which some acid is added at the same time. He advises the deepest and blackest stains being touched with metallic zinc, whereby the reduction of the oxide oi silver or that of the gallate of iron is pro- moted, and all metallic stains adhering to or penetrating into the skin removed. Since most of the salts of zinc are colourless, and soluble in water, the hands soon become quite clean. They should then be washed, first with pure water, and next with soap and water. The reader desirous of further inloruiation PHOTOGRAPHY 1281 on the Biibjert of photography cannot do better than consult Mr Ernest Sjmn'a valuable manual, cnlitliil • Workshop Uiceipts,' and Mr Huu'hes' ' Principle* and Practireof Photo- graphy,' to both of which we are largely in- debted. Captain Abney's work on ' Photo- graphy, cannot be too highly ci mmcnded. See COLLODIOW, PhoTOOEAPHIO. Fhotograpliio Waste Products, Kecovery of. We extract the following from the ' Ame- rican Chemi-t' for February, 1876. The contributor, Mr. 0. A. Pitkin, A. B., states t.liiit the nictliods given have been collected from the ' Philadelphia Photogrnipher,' the ' British Photographic Journal,' Hardwick's ' Photograph Chemistry,' &c., &c. ; also that they iuclude siiggestious by Professor Hill. 1. Nitrate bath, a, recovered ; j8, reno- vated. 2. Hyposulphite bath. 3. Ueduclion of silver chloride, oxide, or sulphide. 4. Qold waste, a, recovered ; /3, separated fi'om silver. ■J- Paper waste and washings from positive prints. 6. Cynnide solution, 7. Developer. I. Nitrate Bath, a, Recovered. 1. Add solution of caustic potash or lime, as long as there is a brown precipitate. Allow to settle, pour off liquid, and collect silver oxide lor reduction; vide III, below. 2. For I lb. of silver, add 1 oz. sulphuric acid and ^ Ih zinc, and allow to stand two days. Precipitate as chloride, wash eight or ten times by decnntation, aud dissolve gradually in nitric acid. NoTKS. — Test complete wnsliin? by hydro- chloric acid. Wash with water till zinc nitrate is removed. If zinc clings to silver wash with hydrochloric arid. 3. Suspend slieet of copper in bath for two or three days. 4. Acidify as nitric acid, precipitate as silver chloride by sodium chloride or hydro- chloric aciil, and reduce ns vide HI, below. 5. Immerse in bath two strips of copper attaehed to the poles of n Daniell's or Smee's cell. Silver deposited on the copper as in 3, above, 6. Add sodium bicarbonate or sodium hy- drate. Reduce as 8 below, or if pure eiiniii;h, dissolve precipitate at once in nitric acid. 7. Concentrate bath, make alkidiue by sodinm cnrhomite, and add aqueous solution of oxalic acid neutralised with sodium carbonate. Filter, dry, aud fuse with equal weight ot sodium biearbonnte. 8. De|io«it, either with or without battery,on iron. (Iron can be obtained purer than zinc or copper, and possesses the additional ad- vantage that the iron Sidts, as iodides, &c., are rot. n all quite soluble). Fuse with potassium nitrate and sodinm carbonate. /3. Benovated. 1. Dilute with three volumes of distilled water, expose to sunlight, filter, add sodium carbonate till slightly turbid. Expose to sunlight six honrs more, filter, add sodium car, bonate till silver all thrown down. Wash, precipitate by decantation, and dissolve in nitric acid. Filter again, make up to 35 grammes; neutrali.»e, expose to sun a week, and bath is ready for use. 2. Neutralise with ammonia till just alka- line; boil till black; let cool, filter, acidify with pure nitric acid, aud eviiporate to crys- tallisation, then fuse. When cool, add dis- tilled water, shake and let stand exposed to light. Filter and add drained crystals. Dissolve and make solution aeid witli pure nitric acid. Expose again to sunlight, (ilter, and bath is ready for u»c. 3. Add potassium permangnnatc, expose to sunlight, filter, acidify, put in clean bottles four-fifths full, cork, and freeze in a tray ; thaw gradually till ball of ice one-eighth size of bottle remains. This contains impurities to be reduced as III, below. Use rest lor uew bath at once. II. Hyposulphite Bath. 1. Precipitate as silver sulphide by potas- sium sulphide. Reduce as III, below, or dis- solve in nitric iicid. 2. Precipitate by hydrosulphurio acid, and reduce ns III. 3. Decompose hyposulphite by waste nitro- sulphuric acid from manuiaciure of gun- cotton for collodion. Have silver sulphide and sulphur, with sodium nitrate and sul- phate iti solution. Suspend zinc in solution, then boil two or three hours; wash on filter, dry, fuse with borax and sodium carbonate. 4. Suspend sheet copper in bath. 5. Add hydrochloric acid, which sets free sulphur aud precipitates .-ilver chloride. Oxidise sulphur by aqua regia, and reduce silver chloride as in III. 6. Add sodium hypochlorite to the alkaline solution. Wash, precipitate, and fuse with mixed carbonates. This gives sodium bisul- phate and chloride as by-products, no sulphur, no fumes. III. Reduction of Silver Chloride, Oxide^ or Sulphide. 1. Mix with one third weight of colophony. Heat moderately in crucible till greenish-blue flame ceases, then suddenly increase heat, aud obtain a button of metal. 2. Melt with alkaline carbonates enough to cover surface from air ; then mix with 75 per cent, of chalk and 4 per cent, of charcoal, aud heat. 3. Ignite with nitre on red-hot pl.iDe care- fully, and in small quantities to avoid explo- 81 1282 PHOTOMETRY sion, run down to button with borax aud sodic carbonate. 4. If chloride, reduce to oxide by boiling with strong potash, then reduce by glucose; or boil the cliloride with glucoae and sodium carbonate. 5. Add silver chloride dissolved in ammonia -to a boiling solution of one part glucose and three parts sodium carbonate in 40 per cent, of water, keeping up the boiling all the time. 6. Add to silver chloride sodium hydrate in solution and grape sugar, and expose to sun- light in open dish with occasional stirring, lleduce to dark brown oxide of silver, soluble in nitric acid, 7. Mix with five times weight of sodium carbonate. Fill hessian crucible half full, and sprinkle sodium chloride over the top. Heat slowly in anthracite fire. After half an hour increase heat till crucible is white-hot. When complete fusion has taken place, allow to cool, and break out button of silver. 8. Fuse with two parts mixed carbonates (sodium and potassium). 9. Add pure zinc and dilute sulphuric acid, and let stand two days. Wash silver off with water acidulated with sulphuric acid, to remove all ziuc ; finally fuse to a button. 10. Mix with \ialf weight dry sodium carbo- nate and one-fourth weight of clean dry sand, and ignite. IV. Oold Waste, a, Recovered. 1. Make just acid with hydrochloric acid, add solution containing 2 oz. pyrogallic acid, shake, let stand 24 hours: filter. Dissolve in aqua regia, and product after evaporation will be found better for toning than that precipitated by iron. 2. Acidify toning bath, and add sulphate of iron (2 grammes to 1 gramme chloride of gold.) /3. Separated from Silver. 1. Treat button obtained by fusing waste from hypo-toning and fitting baths with dilute nitric acid. Wash insoluble part with am- monia to remove silver chloride, if present, and dissolve in aqua regia. 2. Digest 20 grammes in flask with 1 fl. dr. hydrochloric acid, 15 m.m. of nitric acid, and 2 dr. of water. After quarter of an hour boil, add 2 oz. water; filter. Silver chloride with organic matter, &c. left undissolved. Reduced as HI, above. 3. Add excess of pure potassium hydrate, and then bull in flask with excess of solid oxalic acid. V. Paper Waste. 1. Soak paper in strong solution of salt- petre, and burn. 3. Treat with nitric acid, precipitate with sodium chloride or potassium hydrate, then put with III, above, for reduction. WasMngs from Positive Prints. Precipitate by sodium chloride, potassium hydrate, or on copper plates, &c., as above, and reduce, as in III. VI. Cyanide Solution. 1. Dilute with water, precipitate by (1) potassium sulphide, (2) sodium chloride, and reduce as 3. 2. Decant bath into iron kettle, warm, add ferrous sulphate slowly till slight precipitate of oxide. Make alkaline, and add solntion of grape sugar till brownish-yellow colour. Allow to settle, syphon oflT liquid. Wash sediment on filter, and ignite to recover silver. Note. — Ferrous sulphate forms ferro- cyanide, therefore no free alkaline cyanide should be present. VII. Developer, 1. Vide II. (3, 4, 5, 6), with hypo bath; (1) and (2) not applicable, for sulphide of iron would be formed. 2. Reduced by its own iron (if ferrous sulphate). PHOTOM'ETET. The art of determining the relative intensities of different lights. Various methods have beenadopted,atdiff'erent times, for this purpose, among which, how- ever, a few only are sufficiently simple for general application. The principle adopted by Bouguer and Lambert depends on the fact that, though the eye cannot judge correctly of the proportional force of different lights, it can generally distinguish with great precisian when two similar surfaces or objects presented together are equally illuminated, or when the sh.adows of an opaque object produced by different lights are equally dark. Now, as light travels in straight lines, and is equally diffused, it is evident that its intensity will progressively lessen as the distance of its source increases. This diminution is found to be in the duplicate ratio of the distance. To apply this principle to candles, lamps, gas- lights, &c., we have only to arrange two of them so that the lighter shadow resulting from both shall be of equal intensity, after which we must caref'illy measure the distance of each of them from the surface on which the light or shadow falls. The squares of these dis- tances give their relative intensity. In general, some known light, as that from a wax candle (4 to the lb.), is taken as the slandard of cocu- parison. Dr Ritchie's ' photometer ' consists of a rectangular box, about 2 inches square, open at both ends, and blackened inside to absorb extraneous light. In this, inclined at angles of 45° to its axis, are placed two precisely similar rectangular plates of plain silvered glass, and fastened so as to meet at the top, in the middle of a narrow slit about an inch long and the eighth of an inch broad, and which is covered with a strip of tissue or oiled paper. In employing this instrument, the " lights must be placed at such a distance from PHTHISIC— PHTHISIS 1283 each other, and from the instrument between them, thHt the light from each iiball fall on the reflector next it, and be reflected to the corresponding portion of the oiled paper. The photometer is tlicn to be moved nearer to the one or the other, until the two portions of the oiled paper corresponding to the two mirrors are equally illuminated, of which the eye can judge with considerable accuracy." In Prof Wheatstone's 'pnoTOMETBB' the relative intensity of the two lights is deter- mined by the relative lirijihtness of the oppo- site sides ofa revolving silvered ball illuminated by them. In the method of photometry usually, but erroneously, ascribed to Count Rumford, the sliadows of an opaque object formed by differ- ent lights, and allowed to fall on a white wall or paper screen, are contriisted. A wire about -/jtlis of an inch thick, and about a foot in length, with the one end bent so as to form a handle, is commonly used to form the shadows. The method of proceeding is similar to that first above noticed. It is generally supposed that the equality of two shadows can be appreciated with greiitei- certainty than that of two lights. PHTHISIC. A popular name for difficnlty of breathm-^, from its supposed reseniblauce to phthisis. See BRONcniTis, and below. PHTHISIS. (A wasting away.) This is the formidable disease ordinarily or popularly known as " consumption," although, strictly speakinjj, there are points of ditroreiicu between consumption and phthisis, as well as between these and another variety of the malady known as tuberculosis. The statistics which follow, however, apply to all those diseases of the lungs accompanied by wasting, and as such include the mortality from plitliisis, tubercu- losis, and consumption. Ill the Registrar-General's returns for many years past, under the' heads ' phthisis,' or ' tubercular disease," have been included chronic bronchitis, emphysema, fibroid changes of the lungs and kindred aSections. ' It is, however, probable that the figures re- presenting the niortolity are fairly accurate, as the errors are to a certain extent compen- sating; and, indeed, tubercles are often found even in the diseases above mentioned.' The following table, taken from the Regis- trar-General's retnrns for 1848—75, shows the annual number of deaths in England from phthisis, during a period of 28 years : — 1848 . . 51,663 1862. . 60,962 1849. . 50,299 1863. . 51,072 1850. . 46,618 1864. . 53,046 1851 . . 49,166 1865. . 53,734 1852 . . 50,594 1866. . 65,714 1853 . ■ 54,918 1867. . 65.042 1854. . 51,284 1868 . . 51,423 1855 . . 52,290 1869. . 52,270 1856. . 48,950 1870. . 54,231 1857 . . 50,106 1871. . 5:i,;i7(: 1858. . 50.142 1872 . . ^^..-isy 1859. . 50,149 1873. . 51,355 1860. . 51,024 1874 . . 4;i,:i7'.l 1861 . . 51,930 1875. . 52,'ji;j Dr Farr in his letter to the Resistrar-Oene- ral on the causes of death in England in 187.T, writes, " Phthisis is a most faial di>ea8e, al- though it has declined within the last twenty- five years." According to the same authority, the mean rate of mortality from this disease was 2 81 1 per 1000 in the five years from 1850 to 1854. and 2L'8;5 in the live years from 1870 to 1874 One of the most prominent facts revealed even by a cursory study of the statistics cm phthisis, is the large share which the breath- ing ot impure or tainted air has in the origin and dissemination of the disease. Hence it follows that thickly populated and overcrowded localities suffer nmfh more from its raviin^es than those which are less densely inhabited. This is exemplified in the follow- ing table : — Proxiniitv Avernge Inuuul Mortuliiy to 100,000 living. or iioinicas i Pensity of Fursuus ton Sq, Mile. ot Person to Persou. Flilliiais. Other diseuBes of the Respiratory Organs. 1 YUTOS. 15 to 25 25 to 35 35 to 45 15 to 25 25 to 35 35 to 45 Healthy dis- tricts . . 135 163 336 398 330 34 45 67 London . . 19,470 14 264 395 493 45 69 148 Lancashire . 1,008 60 419 475 484 46 86 195 England and Wales . . 808 108 362 438 407 38 61 113 In the very badly ventilated Leopoldstadt, in Vienna, 378 prisonersout of 4280 died between the years 1834 to 1847, or at the rate of 86 per 1000 ; and out of these as many as 220, or 51-4 per 1000, died from phthisis. Con- 1 Dr Wynler Blyth. 1284 PHTHISIS trasting with this the rate of mortality from the same disease in the well-ventilated House of Correction in the same city, we learn that out of 3037 thei'e died in five years (from 1850—1854) 43, or 14 per 1000, and of these 24, or only 79 per 1000, died from the same disease. The great prevalence of phthisis that used to prevail, not only in our army, but in the principal European ones, has been clearly shown to have been referable to the overcrowd- ing and defective ventilation of the barracks. And this applied equally to the barracks of military stations possessing such mild and genial climates as Gibraltar, Malta, Ionia, Jamaica, Trinidad, Bermuda, &c.' The sanitary Commissioners appointed some years back to inquire into the prevalence of consumption amongst our soldiers, came to the conclusion that the foul atmosphere of the barracks was the cause of it. The correctness of our decision has been corroborated by tlie greatly diminished number of deaths which have followed the improved ventilation in our barracks, recommended by the Commissioners. At the present time, owing to those hygienic improvements, the mortality from phthisis is not more than half what it was in our army prior to 1867. The same satisfactory results have been obtained by the introduction into the French barracks of similar sanitary im- provements. Animals are affected in precisely the same manner as human beings. Thus, it Is that phthisis attacks monkeys when shut up in badly ventilated buildings, and cows confined in close sheds. After these statements we shall be prepared to find that indoor trades and occupations swell the hills of mortality from phthisis much more than those carried on in the open air. That this is the case is shown by the following table : — Deaths from Phthisis at Victoi ia VarTc Hospil al, showing the influence of Occupation. Cmse of Death. Ages undee Totals. Not staled. 20. 25. 30. 35. 40. 45. 50. 55. 60. 65. Female lives 45 41 25 15 12 3 1 1 143 Indoor occupation 32 31 30 24 15 9 5 4 150 Malps/^'^'*'^ occupation ^^'"^n Outdoor „ The same reduced to a 10 7 7 5 4 3 4 1 41 9 96 21 21 13 12 11 8 2 i 2 100 100 83 57 43 26 18 3 1 7 434 per centage. Female lives 32 28 18 10 8 2 1 1 100 Indoor occupation . 21 21 20 16 10 7 3 ... ... 2 100 ,, , ' Mixed occupation ^"l^n Outdoor „ 24 17 17 l-J, 10 7 10 3 100 9 86 21 87 21 76 13 51 12 40 11 27 8 22 2 3 i 1 2 100 7 400 The influence of occupation in developing phthisis is forcibly illustrated in the following table : — The above figures may he supplemented by the others, which show the difference between the deaths from phthisis and other lung dis- eases occurring amongst the agricultural and the manufacturing populations, and are ano- ther illustration of the nature of the toiler's occupation upon his liability to consumption. Thus, for every 100 deaths by phthisis and other lung diseases that take place amongst the men in various agricultural districts of England between the ages of fifteen to fifty- five, there are in Coventry 163 deaths; in ' DrParkes. Blackburn and Skipton, 167; in Congleton and Bradford, 168 ; in Leek, 182 ; in Maccles- fitld, 184; in Bolton, 190; in Nottingham, 192; in Rochdale, 193; in Derby, 198; in Salford and Ashton-underLyne, 203; in Leeds, 218; in Preston, 220; and in Man- chester, 263.2 As bearing directly upon the above portion of our subject, we may quote the sixth report of the medical officer of the Privy Council, who therein states — " In proportion as the people of a district are attracted to any collec- tive indoor occupation, in such proportion, other things being equal, the district death-rate by lung diseases will be increased." ' Quoted by Dr Wynter Blyth. PHTHISIS 1285 Dulrict. Nature oi priocipal Induitry in the Dijtrict. Suttli-rate by Fhlliisis and other Lung Diseases at between 15 and ih years ot age, per lUd.UOO of each class referred to. Berkhampstend . liL'ii;luiin Huzziird Newport Pugiicll Towci'ttter . , , , Yeovil . . . .1 1 Leek Coiigleton .... Macclesfield Standard Northern District "I Extensive female employment in f J straw-plaiting \ l Extensive female employment in f lace-making \ ("Extensive female (with some"] ■j males) employment in glove- l making J 1 Extensive employment (more F V, female than male) in silk- J work Agriculture .... Male. 219 319 301 •SM 280 437 5fi6 693 631 Temale. 578 531 615 577 409 85« 7^0 80O 1 333 ! 1 The much larger numher of cases of lung disease amongst those who pursue indoor call- ings than amongst others whose occupations are carried on out of doors, arises principally from the defective ventilation of the work- shops or rooms in which the labour is carried on. When indoor occupations are practised in large and efficiently ventilated apartments, or existence is passed in healthy houses, as in the dwellings of the rich and upper classes, who have also tho additional advantages of good food and warm clothing, the liability to phthisis becomes immensely diminished, Tho much greater immunity from the dis- ease which the richer enjoy over the poorer classes has been carefully pointed out by Dr Guy, who, writing on this subject in the ' Journal of the Statistical Society,' says — " The ratio of deaths from consumption fol- lows the same order as the average age at death, being lowest where the average age is highest, and the reverse. Thus the average age at death of the class of gentlemen is 68 61, and the ratio of deaths from consumption 1 to 260 ; while in the class of artisans the average age is 4806, and the proportion from consump- tion is 1 to 2-29. " Again, the class of gentry presents a i . Number of K DcaUis. 1 c 15 20 80 40 50 60 70 Under Under ■3 -" Condition. to to to to to to to 30. 40. 1: Ratio. a .2 S 20. SO. 40. 60. 60. 1 i 70. 80. ■s. (5 ! •3 S 1 Gentlemen, 1 &c. . . 10-84 18-67 27-11 19-27, 15-06, 6-03 3-01 29-51 56-62 39 1 to 5-00 166 835 Tradesmen 8-lfi 24-34 26-98 20-111 12-70 6-35 1-06 3280 69-78 38 1 „ 2-60 189 491 Artisans . 7-:;5 23-69 26-24 22-79 13-34 6-20 0-43 30-94 1 57-18 384 1 „ 2-29 2318 6308 smaller proportional number of deaths under thirty and forty than either of the other classes. It is also worthy of observation that the pcr-centage proportion of deaths from consumption under thirty and forty is higher in the class of tradesmen than in that of the artisan and labourer, although the ratio of cases of consumption is greater in the latter class. This is doubtless accounted for by the fact already established, that the strong exer- tion which a considerable portion of the la- bonring class employed within doors use in their occupations, and the large number em- ployed out of doors, has the effect of retarding the effect of pulmonary consumption. The tradesman, it will be seen, occupies the inter- mediate place between the indoor and outdoor labourer — between the artisan using little ex- ertion and the aitisan using much exertion. . . . . Another point attracts attention, viz. the great proportion of deaths from consumption occurring in the class of gentry from fifteen to twenty years of age. Does not this show that the liability to the disease is greater in this class than in the two others, and does it not tend to strengthen the position that the 1286 PHTHISIS excess of the deaths from consumption in the other classes is due to the unfavorable circum- stances in which they are placed ? " The ratio of deaths from consumption in the class of gentry, low as it is, would have been still lower if the medical men, who are included in it, were omitted. The number of cases of pulmonary consumption occurring in members of that profession is very remark- able, and it is a subject of regret with the author that they were not made a separate class." Much less clearly and satisfactorily esta- blished is the question as to whether consump- tion is or is not contagious. The instances which have occurred of its extensive and rapid spread in overcrowded barracks, prisons, men- ot-war, merchant vessels, large workshops, &c., not unreasonably seem to lend weight to the opinion that the germs of the disease might have been conveyed by the atmosphere charged with them from an unhealthy to ii healthy subject, on whom they might develop the malady. " But," as Dr Blyth writes, " it must be remembered that, in all crowded localities, there is direct vitiation of air, and it is difficult to say whether tiie foul air or actual contagion have most to do with the propagation of the malady." He adds " that consumption, under ordinary conditions, is certainly not conta- gious; but, under special insanitary influences, certain forms of consumption may be conta- gious, althougii it is still a matter not proven." Dr Guy bases his objection to the doctrine of the generally contagious nature of consump- tion upon the fact of the small fluctuations in the annual number of deaths caused by it. The lowest rate of mortality for phtliisis for a million of inhabitants in London was, he states, for any one of the fifteen years from 1840 to 1854 inclu-ive, 2645, and the fluctua- tion was very slight. The figures in three consecutive years were— 1849, 2777; 1850, 2645 ; 1851, 2970. " If, then," Dr Guy s«js, " any one were to assert that this disease is contagious, which is tantamount to saying that it may be epidemic, the figures I have quoted would in themselves furnish an answer in the negative. They are suggestive of a domestic disease, influenced, as is bronchitis, by the seasons and the weather." The statistics before quoted as to the corre- lation between the prevalence of consumption and unhciilthy surroundings, lead to the belief, that before this connection between the two was so well defined, cases of phthisis were often erroneously referred to hereditary taint, when tliey may simply have arisen from the patient having been environed with the same unfavorable hygienic conditions as his parents ; these unfavorable conditions, including not only polluted air, but bad food, deficient apparel, and want of exercise. Hence it is that most of the later patiiologigts, without denying the existence of the transmitted form of tlie dis- ease, believe the hereditary influence has been greatly over estimated. " As regards the origin of tubercle," writes Dr Douglas Powell, " opinions are extremely various, and indeed irreconcileable; but the tendency of modern research — the experiments of inoculation in animals, and the very powerful advocacy of Prof. Niemeyer, ia certainly to show that tubercles is much more commonly a secondary disease than has until lately been suspected — that people are, in fact, only exceptionally, if ever, born to die of tuberculosis. '*A due appreciation of this doctrine, so diffe- rent from that even now accepted by many, is of almost national importance in giving en- couragement to those hygienic and other mea- sures of prevention, the neglect of which has too often been sanctioned by a foregone con- clusion. " It would I tliink be extremely injudicious to deny hereditary predisposition to tubercles altogether. Moreover, when we come to the question of hereditary predisposition to the forms of consumption which originate in ca- tarrhal pneumonia, it is freely admitted that the oifspriirg of consumptive parents have a tendency to this form of pulmonary phthisis, that the scrofulous have a like tendency (Nie- meyer), and that scrof ulosis is sometimes here- ditary." As allied to this portion of the question may be mentioned the opinion of some pathologist, that phthisis may be either caused or pro- moted by habitual drunkenness; and that a drunkard may transmit it to his off'spring. The proneness to consumption is greatly modified by sex and age, the influences of which upon the disease are very defined and unmistaltable. Thus, women are more liable to its attacks than men, and young and mid- dle aged persons of botii sexes than old ones. "In Edinburgh the ratio of deaths from phtliisis was found to decline from '285 at twenty years to -052 above sixty years ; at Nottingham, from •416 to '017 in the same period of time; at Chester, from -245 to -054; at Carlisle, from '290 to '097 ; and in Paris, according to Louis, from -325 to -042 ; while the general average decline was from "285, or 28-5 per cent., at twenty to thirty, to -078, or -780 per cent., above 60."' Amongst other conditions unfavorable to the consumptive patient, in addition to the breathing of a polluted atmosphere, may be named insufficiency of nourishing food and apparel, variable weather, and a damp soil. This latter is particularly inimical to plithi- sical sufferers. Indeed so closely is dampness of soil associated with the spread of phthi- sis, that the disease has been conclusively showu to have diminished in localities in pro- portion as these have been properly drained. Dr Andrews, of Chicago, says that consump- tion is most prevalent near the sea, and 1 Blyth. PHYLLOXERA VASTATRIX 1287 tliat it diminishea iu proportion to the distance of the inland locality from the ocean. A dump atmosphere also provokes the disease. Phthisis seems to be a malady peculiar to temperate climates. As to the influence of the season upon the disease, Dr Haviland says, "In England we learn from the statis- tical returns that the spring is the most fatal to consumptive patients, whether male or fe- male, but with regard to the other seasons there is considerable variability. For instance, suppose we take the seasons of 1838 in the order of their fatalityto males, they would stand thus — spring, 1187; winter, 1048; summer, 968 ; autumn, 904. Tu females — spring, 972 ; summer, 937; winter, 896; autumn, 825. Then again, although the spring invariably takes the lead, the other seasons change places with each other from year to year; and what is remarkable, this inconsistency docs not seem to be dependent upon the temperature, as we shall presently see. In the returns for 1853, the following statistics in deaths from con- sumption appear: — Winter, 1872 ; spring, 1971; summer, 1745 ; autumn, 1914. The order of fatality in the years above quoted would there- fore be : — l8SS.—MaUt. 1. Spring. 2. Winter. 8. Summer, 4. Autumn. WiH—Ftmalet. 1. Sprmf(. 2. SummtT. 8. Winter. 4. Autumu. IMO—Tolal. 1. Spring. 2. Wiiiicr. S. Sumniur. 4. Autumu. Ih:a.— Total. 1. Spring. 2. Autumn. 8. Winter. 4. Summer. " So far, therefore, as seasons are concerned, the above table proves that spring, i.e. April, May, June, ia the most inimical quarter to phtliisical patients, and probably Autumu — October, November, December, the least so. In London at h a»t, if not throughout Eng- land generally, the spring is undoubtedly the most olmoxious to consumptive cases; and this statement is in accordance with the expe- rience of those physioiaiis wlio have opportu- nities of seeing the rise, progress, and cud of many hundreds of phthisical patients during the year. Dr Richard Quain observes that the cold easterly wind of spring completes the work, winch the winter had left undone."' That greater or less destruction of the lungs, which is cliiiruotenslic of pulmonary phthisis, originates iu the presence in them of a dis- eased (iroM til, consisting of very minute masses or grains, which are sometimes grey, and at others \ellnw or clicosilike in appearance. These little bodies are either diffused uni- formly through the substance of the Inngs, or are collected toj;ether in them in larger or smaller masses. In the latter case, each little mass generally sets up iu the surrounding tis-ue of the limgs, inflaiiimalxon and suppuration, wh^cb, although only prqcessis by which nature endeavours ti expel the alien siiKstunce from the Iniig, may, by constant repetition, cause the destruction of the greater part of the res- pinitiiry organs. * 'ClimHte, Weatlitr, and Diseuse,' by Dr Iliivilund. PHYILOXEEA VASTATRIX. In 1866 M. Delorme, of Aries, in the South of Prance, whs the first to suggest that a peculiar disease which had manifested itself the previous year amongst the vines growing in the plateau of Pujaut on the west bank of the river Rhone, in the Department of the Card, was of a new and speciQc character. Shortly afterwards a commission appointed by the Herault Agricultural Society visited Qne of the infested localities, and one of its members, M. Planchon, confirmed JI.Dclorme's conjectures, by discovering the catise of the vine malady. This he conclusively showed was due to the presence of a peculiar and hitherto unknown description of Aphit, be- longing to the genus Phglloxera, which, as illustrative of its devastating qualities, be named P. vus/atrix. A full-grown Phylloxera va.ttnirix does not exceed more than the 33rd or 40th of an inch in length. Examined under a microscope, in addition to short pointed legs, it is seen to be furnished with a proboscis nearly half as long OS its body. Upon examination this proboscis seems to be composed of three tongues, of whi<^h the centre one is the longest, and these are united at their base into a kind of flat, sharp-pointed blade, which is the boring or puncturing apparatus, by the aid of which the insect pierces into the roots, from which it sucks the juices that constitutes its food. About half the proboscis or sucker is inserted into the bark of the root, and the creature can not only attach itself to the root by means of it, but can also turn on it, as on a pivot, when engaged in the depredations. Mnle Pliylloxera; dot in circle showing natural size. These are continued from April to October, by which month the insect has lost the yellow colour that ili-tina, dorsal view; /, winged female, dorsal view, greatly enlarged. d by their punctures; le largtr routs, natural in which patches of a vineyard have continued unaffected amidst the surrounding devasta- tion, owing to the absence in those particular parts of the soil, of tlie argillaceous element. A forcible illustration of this malijiu iu- iiuencc of clay in the soil is afforded by tlie following analyses of two specimens of ertrth taken from the same vineyard. The specimen marked " healthy " w:is from a small plot of ground in which the vineswere perfectly sound; that distinguished as " unhcaltl-.y" formed by far the greater portion of tlie soil of the vineyard, the plants i;rowiug in which were all suffering from the ravages of the parasite : — Henllhy. Unhealthy Water . 2-25 . . 3-20 Nitrogen .... . 0-11 . . 0-12 Sulphate of calcium 002 . . 042 Chloriile of sodium 1-15 . . 018 Carbonate nf calcium 49-00 . . 42-00 .■siliceous sand . 23-50 . . 10 20 Chiy 17-75 . . 37-50 Organic substances ' and error of analysis. 5-62 . . 6-38 lOU-00 10000 From the locality already inclicoted, where it Imd first developed Itself in 1805, the vine disease *;rnduHlly extended until, in the ycur 1873, it was ravaginf;r the viney!»ul•^ of the Card, V:nu-In«e, Tsere, Heranlt, I)r6me, Boiiches du Khone, Ardeehe, Hiis.-^e-J-Alpes, Var, the Gironde, and tlie Charentes, since which time it has gradually continued to spreiid into the adj;icent districts. " We may train a inore precise idea than can be afforded by a mere observation of the pfeoirruphical extension of the disease, of tlie di'^astrous nature of the ravajjes of the Phylloxera, by the examination of some of the statistics of the crape-cnip in sncccs.sive years, in some of the departments attacked. Thus, in the Department of Vauclnse, where the disease showed itself in 186H, there were in 1866, according to the results obtained by the departmental commission institutedat Avignon to observe on the new vine-disease, 6000 hectares absolutely dead or dying, and a much larger number alrendy attacked, which have since succumbed to tlie parasite. Out of the 30,000 hectares of viney;irds comprised in tlii« department, 25,000, or five sixths of the tota.1 1290 PHYSIC BALLS— PICKLE area, have been destroyed. In the Gavd, where the vine flourishes better than in the above-mentioned department, the rava£es of the disease are yet most terrible ; for in 1871, in the Arrondissement ot Uzes, but one half of the average crop was produced, and in the Arron- dissement of Nismes a tenth part of the crop was destroyed. These proportions, moreover, have increased since that year. " If we examine the mischief done in the less extended areas of the communes, we shall obtain a still clearer idea of the rapid spread of the disease ; — " CosmTTNE or Gbavbson. 6-67 mean crop 10,000 hectoli 1868 „ 8,500 1869 2,200 1870 400 1871 205 1872 100 1873 50 tres. " In the Commune of Maillanne the crop in 1868 was only 40 per cent, of the average of the three preceding years, while in 1869 it was only 10 per cent. In the Commune of Eyragues the crop in 1868 was about 33 per per cent, of the average of the three preceding years, and in 1869 there was a further falling off of about 10 per cent. In 1870 the crop in the three above-named communes was almost entirely destroyed. From instances such as these, faiily selected from many others equally tragic in their stern figures, we may form some idea of the magnitude of the disaster. In- deed, it is difficult to see, so rapid is the ex- tension of the disease, how, unless some potent and effective remedy can be soon applied, any vine-bearing district in France can escape the visitation of the Piiylloxera."' The French Government, fully alive to the peril threatening the staple product of their country, shortly alter the appearance of the Phylloxera in the vineyards of France, offered through their Minister of Commerce and Agri- culture a reward of 300,000 francs for the discovery of a means of nrresting and stopping its ravages ; and in 1871 the Academy of Sciences, at Paris appointed a commission, presided over by the celebrated chemist M. Dumas, to investigate the biology, habits, &c., of the parasite, together with the nature of the injuries it inflicted upon the vine, the area of its depredations, &c. From amongst the members of this commission three gentlemen were chosen to visit the infected districts, so as to be afforded an opportunity of studying the Phylloxera at its destructive work, and its environments of soil, situation, tempera- ture, &c. The delegates selected by the Commission were MM, Balbiani, Cornu, and Duflaux, re- spectively amongst the most distingu'shed living representatives of zoology, botany, and chemistry in France, and the results of their ' 'Sature.'TOl. I. labours was the issue, some few years back, of a most exhaustive and valnable report to the Academy of Sciences on the subject of the Phylloxera. Tlie vines of other countries besides those of Prance have also suffered from the attacks of the Phylloxera. Thus it has made its appear- ance in the vineyards of Algiers, Italy, Ger- many, Spain, Portugal, Switzerland, Australia, and North America, on all of which it has been productive of more or less serious injury to the vintage. Amongst the numberless remedies that have been suggested and tried, with varying but by no means uniform or satisfactory results, for the destruction of the Phylloxera, may be men- tioned sulphur, the sulphites, tobacco, caustic soda, and potash, bisulphide of carbon, coal- tar, soft soap, lime, the immersion of the vine in sulpho-carbonate of potassium, and the application around the roots of sand. A certain amount of success, it has been said, has attended the employment of the sulpho-carbonate of potassium and sand. An American botanist, Mr Riley, recom- mends the importation into French vineyards of the American vines, which he suggests should be employed as stocks on which to graft the French ones. The American plant being of a hardy nature, he believes its incorporation with the more susceptible French ones, would give rise to a vine sufficiently vigorous to resist, or at any rate not to be injured by the ravages of the parasite. PHYSIC BALLS. See Veteeinaet medi- cines. PHYSOSIIGMATIS FABA. See Caiabab BEAN. PrCA. Depraved appetite. PIC'AMAK. One ot the peculiar principles discovered by Reichenbach in beech-tar, and described by him as a viscid, colourless, oily liquid, only feebly odorous, but intensely bitter; insoluble in water; freely soluble in alcohol, ether, and oils; boiling point 520° Fahr. ; sp. gr. I'OaS. See Kbbasote. PICCALIL'LI. See Pickles. PICK'LE. The liquor in which subst'tnces used as food are preserved. That for flesh is commonly brine ; that for vegetables, vinegar ; both of which are commonly flavoured with spices, &c. Prep. 1. (Foe meat.)— o. From bay salt, 3 lbs. ; saltpetre, 2^ oz. ; moist sugar, 1 lb. ; allspice and black pepper, of each (bruised) 1 oz. ; water, 9 pints ; simmer them together in a clean covered iron or enamelled vessel for 7 or 8 minutes ; when the whole has cooled, remove the scum, and pour it over the articles to be preserved. Used for hams, tongues, beef, &c., to which it imparts a fine red colour and a superior flavour. i. From bay salt and common salt, of each 2 lbs.; moist sugar, 1 lb. ; saltpetre, J lb. ; all- spice (bruised), -joz. ; water, 1 gall.; as belore. PICKLES 1201 Used chiefly for iwrk and hania. Common Rait may be substituted for bay salt, but it is less )>nwerfully antiseptic, and the fluvoiir is less gmteful. 2. (For TE0ETABLB8.) — a. Strong distilled vinegar, to eacli quart of which li oz. of good salt has been added. h. Gnod distilled vinegar, 4 pints; common fftlt, 2i oz. ; black pepper, \ oz. j unbleached Jamaica K>nger, 2^ oz. (the laat two bruised, but not dusty) ; mace (shredded), \ oz. ; sim- mer in an enamelled iron or stoneware vessel, as above, and strain through flannel. Some- times a little capsicum is added. Used either hot or cold, according to the vegetable it is intended to preserve. Fickle, Lemon. See Sacces. PICKLES. These well-known articles are easily prepared of the finest quality. The vetretiibles and fruit, selected of the proper quality and at the proper season, after being well cleansed witii cold spring water, are steeped for some time in strong brine; they are then drained and dried, and transferred to bottles or .jars J the sjiiec (if any) is then uHdeil, the bottles filled up with hot, stronjr, pioklinK vinegar, and at once securely corked down and tied over with bladder. As soon as the bottles are cold the corks are dipped into melted wax, the more surely to preserve them air-tight. Good wood or distilled vinegar is commonly used for this purpose ; but tlie best malt or white wine vinegar of the strength known as No. 22 or 24 is exclusively employed for the finer pickles whieh are not spiced. In those for early use the ' steep' may be made in hot or boiling brine, by which the product will lie ready for the tible in a much shorter period ; but wiih substances of a succulent and fliibl)y nature, as cabbage, cauliflower, some fruit, &e., or in which crispness is es- teemed a murk of excellence, this is inadmis- sible. To such articles the vinegar should also be added cold, or, at furthest, should be only slightly warmed. As a general rule, the softer and more deliente articles do not require so long soaking in brine as the harderand coarser kinds; and tliey may be often advantageously pickled by simply pouring very strong pickling vinegar over them "ilhout applying heat. It must also be observed that beetroot, and other like substances which are sliced, as well as cer- tain ilelieate fruits, must not be steeped at all. Tiie spice is commonly added whole to the bot- tles ; but a more economical plan is to steep it (bruised) for some time, or to simmer it in the vinegar before u-ing the latter, as in the forms given under Pickle {above). The spices and flavouring ingredients em- ployed lor pickles are— allspice, black and white pepper, capsicums or red pods, cloves, garlic, ginger, horseradish, lemon peel, mace, mustard, shallots, and turmeric. These are chosen with reference to the particular variety of the pickle, or the taste of the con- sumer. A good SPICED VINEOAB for pickles gene- rally is the following: — Bruise in a mortar 2 oz. of black pepper, 1 oz. of ginger, \ oz. of allspice, and 1 oz. of salt. If a hotter pickle is desired, add i dr. of cayenne, or a few cap- sicums. For walnuts, add also 1 oz. of shal- lots. Put these into a stone jar, with a quart of vinegar, and cover them with a bladder wetted with the pickle, and over this place a piece of leather. Set the jar on a trivet near the fire for 3 days, shaking it 3 times a day, then pour it on the walnuts or other vegetables. For walnuts it is used hot, but for cabbage, &c., cold. To save time it is usual to simmer the vinegar gently with the spices; which is best done in an enamelled saucepan. In the preparation of pickles it is highly necessary to avoid the use of metallic vessels, lis both vinegar and brine rapidly corrode brass, copper, lead, ic, and thus become poisonous. These liquids may bo best heated or boiled in a stoneware jar by the heat of a water bath or a stove. Common glazed earthenware should be avoided, either for making or keeping the pickles in, as the glazing usually contains lead. Pickles should also be kept from the air as much as possible, and should only be touched with wooden or bone spoons. They are also belter prepared in small jars, or bottles, than in large ones, as the more frequent opening of the latter exposes them toil much. Copper or verdiffris is fre- quently added to pickles to imp.irt a green col lur, or the vinegar is boiled in a copper vessel until sufficiently 'greened' before pour- ing it on the vegetables. This poisonous ad- dition may be readily detected by any of tlie tests mentioned under Coppeb. If a green colour be desired, it may be imparted to the vinegar.and ultimately to the pickles, by steep- ing vine leaves, or the leaves of parsley or spinach, in it. A teaspoonful of olive oil may be advantageously added to each bottle to keep the pickles white, and to promote their pre- servation. *,* The following list includes the leading pickles of the shops, and some others : — Barberries. Fiom the ripe fruit, without heat. Beans. From the young green pods of the scarlet bean, and the French or kidney bean, with beat. Beetroot. From the sliced root, without steeping in brine, and with cold spiced vinegar. When wanted for immediate use the vinegar may be used boiling hot. Broccoli. As CAULiFLOWEita. Cabbage. This, either red or white, ia cut into thin slices, and steeped in strong brine or sprinkled with common salt, and allowed to lie for 1 or 2 days ; after which it is drained for 10 or 12 hours in a warm room, and then put into jars or bottles, with or without a little mace and white peppercorn^, and at once covered with cold, strong, white vinegar. — Another plan is to steep tiie sliced rabbige in 1292 PICKLES alum water for 10 or 12 hours, and, after draining and drying it, to pour the vinegar upon it as before. The product of the last formula eats very fresh and crisp, but takes longer to mature than that of the other. Some persons add a little salt with the vinegar ; and others mix slices of red beet with the cabbage. Capsicums. As geekkii^s. Cauliflowers. As CiftBAGE (nearly). Or, they may be steeped in hot brine for 1 or 2 hours before pouring the vinegar over them. Cherries. From the scarcely ripe fruit, bot- tled, and covered with strong and colourless pickling vinegar. Codlins. As beans. Cucumbers. As eHEEEiNS. Elderflowers. From the clusters, just before they open, as BSD cabbaoe. A beautiful pickle. English Samhoo. From the young shoots of elder, denuded of the outer skin, pickled in brine for 12 or 14 hours ; then bottled with a little white pepper, ginger, mace, and allspice, and pickled with boiling vinegar. Excellent with boiled mutton. Eschalots. With boiling spiced vinegar, or spices added to each bottle. French Beans. Sck above. Garlic. As esohaiots. Gherkins. From smnll cucumbers (not too young), steeped for a week in very strongbrine; this last is then poured off, heated to the boil- ing point, and again poured on the fruit ; the next day the gherkins are drained on a sieve, wiped dry, put into bottles or jars with some spice (ginger, pepper, or cayenne), and at once covered with strong pickling vinegar, boiling hot. Several other pickles may be prepared in the same way. Gooseberries. From the green fruit, as either OABBAQE or CAULIFLOWEKS, Indian Mango. From green peaches. (See helow.) Indian Pickle. Syn. Piccalilli. This is a mixed pickle which is characterised by being highly flavoured with curry-powder, or tur- meric, mustiird, and garlic. The following form is commonly used : — Take 1 hard white cahbnge (sliced), 2 cauliflowers (pulled to pieces), some French beans, 1 stick of horse- radish (sliced), ahont 2 dozen small white onions, and 1 dozen gherkins ; cover them with boiling brine ; the next day drain the whole on a sieve, put into a jar, and add, of curry- powder or turmeric, 2 oz. ; garlic, ginger, and mustard seed, of each 1 oz. ; capsicums, i oz. ; fill up the vessel with hot pickling vinegar, bung it up close, and let it stand for a month, with occasional agitation. See Mixed pickles (ieloio). Lemons. From the fruit, slit half way down into quarters, and cored, put into a dish, and sprinkled with a little salt; in about a week the whole is placed in jars or bottles with a little turmeric and capsicums, and covered with hot vinegar. Limes. As the last. Mangoes. As lemons, adding mustard seed and a little garlic, with spices at will. Eng- lish MANGOES are made from cucumbers or small melons, split and deprived of their seeds. Melons. As lemons (nearly). Mixed Pickles. From white cabbage, canli- fiowers, French beans, cucumbers, onions, or any other of the ordinary pickling vegetables, at will (except red cabbage or walnuts) treated as geeb£INS ; with raw ginger, cap- sicum, mustard seed, and long pepper, for spice, added to each bottle. A little coarsely bruised turmeric improves both the colour and flavour. Mushrooms. From the small button mush- rooms, cleansed with cold spring water, and gently wiped dry with a towel, then placed in bottles, with a blade or two of mace, and covered with the strongest white pickling vinegar, boiling hot. Myrobalans. The yellow myrohalan pre- served in strong brine. Gently aperient. D^asturtlnms. From the unripe or scarcely ripe fruit, simply covered with cold strong vinegar ; or, as cabbage or gherkins. Onions. From the small button or filbert onion, deprived of the outer coloured skin, and either at once put into bottles and covered with strong white pickling vinegar, or previously steeped for a day or two in strong brine or alum water. When required for early use, the vinegar should be poured on boiling hot. Peaches. From the scarcely ripe fruit, as GHEBEINS. Peas. As beans or cahliploweeS. Piccalilli. See Indian pickle. Sadish Pods. As beans or gherkins. Samphire. From the perennial samphire (JBrythmuTn maritimwm), covered with strong vinegar, to each pint of which J oz. of salt has been added, and poured on boiling hot. Said to excite the appetite. Tomatoes. From the common tomato or love apple, as gherkins. Walnuts. From the young fruit of Juglans regia, or common walnut : — 1. Steep them in strong brine for a week, then bottle them, add spice, and pour on the vinegar boiling hot. 2. On each pint of the nuts, spread on a dish, sprinkle 1 oz. of common salt ; expose them to the sun or a full light for 10 or 12 days, frequently basting them with their own liquor; lastly, bottle them, and pour on the vinegar, boiling hot. ■ 3. (Dr Kitchener.) Gently simmer the fruit in brine, then expose it on a cloth for a day or two, or until it turns black ; next put it into bottles or jars, pour hot spiced vinegar over it, and cork down immediately. In this way the pickle becomes sniTiciently mature for the table in half the time required for that piepared by the common metliod. Dr Kit- PICOLINE— PIES 1293 chener aliio recommends this parboiling pro- ci'»8 for sevi'ral other pickles. Some persons pierce the fruit with an awl or stocking-needle, in several places, in order to induce early ma- turation. The spices uisually employed are mustiird seed, allspice, and ginger, with a little uiace and garlic. FIC'OXiINE. An oily substance, discovered by l)r Anderson, associated with aniline, chinoline, and some other volatile bases, in certain varieties of coal-tar naphtha. PICRIC ACID. }iCfU,(tiO,)fi. Si/n. C'abbazotio agio, Niteophenisic acid, Tki- NITUOPUENISIC ACID. A peculiar compound formed by the action of strong nitric acid on indigo, alues, wool, and several other sub- stances. I'rep. 1. Add, cautiously and gradually, 1 part of powdered indigo to 10 or 12 parts of hot nitric acid of the sp. gr. 1-43; when the reaction has moderated and the scum has fallen, add »n adililioual quantity of nitric acid, and boil the whole until red fumes are no lunger evolved ; redissolve the crystals of im- pure picric acid deposited in boiling distilled water, iind remove any oily matter Ibund float- ing on the surface of the solution by means of bibulous piiper ; a second time redissulve in boiling water the crystals which form ns the liquid cools, saturate the new solution witli carbonate of potassa, and set it aside to crys- tallise ; the crystals of picrate of potassium tliua obtained must be purified by several re- solutions and re-crystallisations, and next decomposed by nitric acid; the crystals depo- sited as the liquid cools yield pure picric acid by again dissolving them in boiling water, and ru-i'i-ystHllis>itii)n. 2. Disxilve the yellow resin of Xanihorrhoea haalilia (Botany Bay Gum) iu a snfficiencv of strong nitric acid. Kcd vapours are evolved, accompanied by violent frothing, and u deep red solutinn is produced, which turns yellow after boiling. Evaporate this solution over a water bath. A yellow crystalline mass is de- posited, which consists of picric acid with small quantities of oxalic and uitrobenzoic acids. The picric acid is purified by neutralising the yel- low mass with potassa, and crystallising t» ice out of water. The pure picrate of pota.ssium thus obtained is decomposed by hydrochloric acid, and the liberated picric acid is puritied by two crystallisations. This process, devised by Sleiihouse, is one of the best, and yields a quantity of the acid amounting to 5U|; of the resin cm|do^ed. Prop., tfc. Brilliant yellow scales, scarcely soluble in cold water, but very soluble in boil- ing water, and in alcohol and ether; fusible; volatile ; taste insupportably bitter, and very permanent. It forms salts with the bases (picrate-;, carbazolates), mostly possessing a yellow colour, and exploding when heated. The picrate of lead has been proposed as a f ul- mlnat ng powder for percussion caps. The picrate of potassium has been given with advantage in intermittent fevers. A solution of picric acid in alcohol is an excellent test for potassa, if there be not too much water pre- sent, as it throws down a yellow crystalline precipitate with that alkali, but forms a very soluble salt with soda. Most of the picrates may be made by the dirci t solution of the car- bonate, hydrate, or oxide of the metal, in a solution of the acid in hot water. The picrate of silver forms beautiful starry groups of acicular crystals, having the colour and lustre of gold. The principal use of crude picric acid is for dyeing yellow. It is said to be lorgely em- ployed for the adulteration of beer. It is, however, highly poisonous. According to Prol. Rapp, it acts deleteriously both when swal- lowed and applied to the unsound skin. Five grains seriously affected a lai ge dug, and killed it within twenty-four hours. It induces vomit- ing, feebleness, and geneial loss of nervous tone. The tissues of animals poisoned by it (even the white of the eyi) were tinged of a yellow colour. See 1'ohteu, &c. PICROTOX'IN. C.jHuOj. Syn. PiCEO- TOXINE.PlCTBOTOXIA, PiCKOTOXINA. A [.oisou- 0U8 principle discovered by Boullay in the fruit of Anamirta paniculuiat or Cocculus indicus. Prep. 1. Precipitate a decoction of Coc- cuius indicus nitha solution of acetate of lead, gently evaporate to dryness, redissolve the residuum in alcohol of '817. and crystallise by evaporation; repeat the solution and crystal- lisation a second and a third time. Any adher- ing colour may be reniovcd by agitating it with a very little water ; or by animal charcoal, in the usual manner. 2. (Kane.) Alcoholic extract of Coeculus indicus is exhausted with the smallest possible quantity of water, and the mixed liquors fil- tered ; to the filtrate hydrochloric acid is added, and the whole set aside to crystallise. The product may be purified a-' before. trap., S(c. It forms small, colourless, stel- lated needles ; soluble in alcohol, ether, and acetic acid, and feebly so in water; boiling water dissolves it freely ; taste of solutions in- expressibly bitter ; reaction neutral. It does not combine with acids, as formerly asserted, but it forms feeble couibinations with some of the bases. It is a powerful intoxicant and narcotico-acrid poison. It acts powerfully on the spinal cord and nervous system generally, occasioning an increase of the animal tempe- rature, and peculiar movements, similar to those described by Flourens as resulting from sections of the cerebellum. It is frequently present in malt liquors, owing to their com- mon adulteration with Coeculus indicus. PICTURES, OIL. To clean. See Paiktikgs, Oil. PIERRE DIVrSTE. Syn. CcPKrM alu- MINATUM. See Lapis ditixus. PIES. Alexis Soyer gives the following instructions for making pies : — 1294 PIG-PILES To make - pie to perfection, — when your paste (half -puff or short) is carefully made, and your dish or form properly full, throw a little flour on your paste-boai-d, take about ai lb. of your paste, which roll with your hand until (say) an inch in circumferenee ; then moisten the rim of your pie-dish, and iix the paste equally on it with your thumb. When you have rolled your paste for the covering, or upper crust, of an equal thickness throughout, and in proportion to the contents of your pie (5 inch is about the average), fold the cover in two, lay it over one half of your pie, and turn tlie other half over the remaining part ; next press it slightly with your thumb round the rim, cut neatly the rim of the paste, form rather a tiiiclc edge, and mark this with a knife about every quarter of an inch apart j observing to hold your knife in a slanting direction, which gives it a neat appearance ; lastly, make two small holes on the top, and egg-over the whole witli a paste-brush, or else use a little milk or water. Auy small portion of paste remaining may be shaped to fanci- ful designs, and placed as ornaments on the top. " For meat pies, observe that, if your paste is either too thick or too thin, the covering too narrow or too short, and requires pulling one way or the other, to make it fit, your pie is sure to be imperfect, the covering no longer protecting the contents. It is the same with fruit ; and if the paste happens to be rather rich, it pulls the rim of the pie to the dish, soddens the paste, makes it heavy, and, there- fore, indigestible as well as unpalatable." Meat pies require the addition of either cayenne, or black pepper, or allspice ; and fruit pies, of enough sugar to sweeten, with mace, ginger, cloves, or lemon peel, according to taste and the substance operated on. See Pastry, &c. PIG. The pig or hog (Szis scrofa—hmn.), one of the common pachydermata, is now do- ' mesticated in all the temperate climates of the world. Its flesh constitutes pork, bacon, ham, &c. ; its fat (lard) is officinal in the Pharma- copoeias. Tlie skin, bristles, and even the blood and Intestines of tliis animal, are either eaten as food or turned to some useful purpose in the arts. See Poek, Leather, &c. PIG'MENTS. These are noticed under the respective colours. PIG-STYE. In order tliat a pig-stye may not become a nuisance and a danger to health it is essential that the liquid excrement of the pig should be carried oft: by means of an effec- tive and well-covered drain, and that the solid matters should he frequently removed. Should it come to the knowledge of the sanitary inspector of the district that a pig- stye is deficient in this particular, the inspec- tor has power to cora))el the owner of the stye to construct proper drainage. Urban authorities have full powers in the matter of pig-styes, since under section 26 of the Public Health Act it is enacted "that the owner of any swine or pig-stye kept in a dwelling-house, or so as to be a nuisance to any person, is liable to a penalty of 40s. or less, and to a further penalty (if the offence is continued) of 5». a day. The authority can also, if they choose, abate the nuisance them- selves, and recover the expenses of such action from the occupier of the premises in a sum- mary manner. A rnral authority has power to deal with the matter under provision 3, section 91, of the Public Health Act, which defines as a nuisance "any animal so kept as to be a nuisance or injurious to health." PIKE. The &0X lucius (Linn.), a fresh- water fish. It is remarkable for its voracity, but is highly esteemed by epicures. Various parts of it were formerly used in medicine. The flit (OLEITM 10011 piscib) was one of the simples of the Ph. L. of 1618, and was es- teemed as a friction in catarrhs. It is even now used in some parts of Europe to disperse opacities of the cornea. PIL'CHAED. The Clupea pilchardus, a fish closely resembling the common herring, than which, however, it is smaller, but thicker and rounder and more oily. It abounds on the coasts of Devon and Cornwall, where it is not only consumed as food, but pressed for its oil. PILES. Si/n. Hemoeehotds; H^moe- EHoiDES, L. A painful disease occasioned by the morbid dilatations of the veins at the lower part of the rectum and surrounding the anus. Piles are principally occasioned by costive- ness and cold ; and, occasionally, by the use of acrid food. They have been distinguished into — BLIND PILES, or a varicose state of the veins without bleeding, — mucous piles, when the tumours are excoriated, and mucus or pus Is discharged, — PLEEDiifo piles, when accom- panied with loss of blood, and — excees- CENTiAii piles, when there are loose fleshy excrescences about the verge of the anus and within the rectum. The treatment of piles consists in the admi- nistration of mild aperients, as castor oil, or an electuary of sulphur and cream of tartar. When there is much inSammation or bleeding, cold and astringent lotions, as those of sulphate of zinc or alum, should be applied ; and when the pain is considerable, fomentations of de- coction of poppy heads may be used with advantage. To arrest the bleeding, ice is also frequently applied, but continued pressure is more certain. When the tumours are large and flaccid, the compound ointment of galls is an excellent application; and if there is a tendency to inflammation, a little liquor of diacetate of lead may be added In confirmed piles the internal use of copaiba, or, still better, of the confection of black pepper, should be persevered in for some time, together with local applications. In severe cases the PILL COCHU— PILLS 1293 protruded tumoiirs are removed by surj^eons, by the knife or ligature. See Ointments, E1.KCTUARIK8, &e. PILL COCUIA. See Compound Coi-oorNxn Pills (below). PILL EUFI. See Pills of Aloes with Mtiikii (below). PILLS. Sgn. PiLCLs; (Ph. E. & D.), PiLCLA (Ph. L ), L.; Pilules, Sacchaboles soLiDES, Fr. Pills are little balls, of a eemi-solid con- sistcnci', composed of various medicinal sub- stances, and intended to be taken whole. The facility with which they are made and admi- nistered, their comparatively little taste, their )iowi'r of preserving their properties for a con- siderable length of time, and, lastly, their portability and inexpensiveness, have long rendered them the most frequently employed and the most popular form of medicine. Tlie rapid and skilful preparation «t pills, from all the numerous substances of which they are composed, is j'lstly considered to demand the highest qualifications in the practical dis ]iciisiT. The medicinals employed must be nuide into a consistent and moderately firm ma«s, BuiBciently plastic to be rolled or moulded into atiy shape, without adhering to the fingers, knife, or slab, and yit sufficiently solid to retain the globular form when divided into pills. A few substances, ns certain ex- tnut", &('., are already in this condition ; but the otluTs require the use of an excipient to give tliim tlio requisite bulk or consistence. As a general rule, all the constituents of a pill which can be pulverised should be reduced to fine powiler before mixing them with the soft ingredients which enter into its composition j and these last, or the excipient, should next be gradually added, and the mixture triturated and beaten until the whole forms a perfectly homogeneous muss. It is then ready to be divided into pills. This is effected by rolling it on a slab, with a pill or bolus knife, into small pipes or cylinders, then dividing these into pieces of the requisite weight; and, lastly, rolling them between the thumb and fiuger to give them a globular form. A little powdered liquorice-root or starch is commonly employed to prevent the pills adhering to the fingers, or to each other, after they are made. Magnesia, so frequently used for this purpose, is unsuited for pills containing mecallic suits or the alka- loids, or other remedies, which are exhibited in very small doses. Instead of forming the mass into pills by hand, in the manner just referred to, a con- venient and simple instrument, called a * pill- machine," is now generally used by the drug- gists for the purpose. This consists of two pieces. The first (see fig. 1) is divided into tliree compartments: — c is a vacant space to reass (pill-mass), which it is not intended at once to divide into pills, it should be preserved in a piece of bladder or gut-skin placed in a covered stoneware or earthenware pot. In this state it may be occasionally moistened with u little weak spirit to prevent its getting hard. The weight (size) of pills varies from i gr. to 6 gr. If heavier than this, they are called ' boluses.' Formerly, as a general rule, they were made of 5 gr. each; but pills of this weight are, in general, so large that some persons find a difficulty in swallowing them. Another disadvantage of large pills is the trouble of nicely apportioning the dose, — one pill bein^, perhaps, too small a quantity, and two pills the reverse. Hence, 2 to 3-gr. pills are now the favourite size with both pill-takers and dispensers, notwithstanding that 5-gr. ' ' Pharmaceutical Year Book.' TOI,. II. pills are still ordered in one of the authorised Pharmacopoeias. Pills are occasiomilly coated with gold, silver, and other substances, to render them more agreeable to the eye, or to prevent the taste of nauseous ingredients affecting the palate during deglutition. They are gilded and sil- vered by placing them, in the moist state, on a leaf or two of the metal in a small iiallipot, and covering them in a similar manner with another leaf of metal ; over the mouth of the gallipot is laid a piece of smooth writing paper, and on this the palm of the hand ; a sudden and rapid circular motion i< then given to the whole. If the pills are not sufficiently moist or sticky, they should be rendered so by rolling them between the fingers very slightly moist- ened with mucilage, before proceeding to silver them. Another method is to shake them in a similar manner with a little gold or silver dust. llr Haselden recommends a varnish com- posed es follows : — Kesin ' of tolu, 3 parts ; rectified spirit, 6 parts; methylated ether, 2 parts. Well shake until all that will is dis- solved. Use the clear solution. MrHasleden says iodide of iron pills are well preserved by this coating, and also granules of secale cornutum. When pills are to be covered with gelatin, each pill, being stuck on the point of a very thin wire four or five inches in length, is dipped into a solution of gelatin, so as to coat it com- pletely, and the wire is then inserted into a pin-cushion, or a vessel containing fine sand, and left until the gelatin is firm, which oceurs in about a quarter of an hour; the pins may then be easily removed by simjily warming them, by placing the centre of each wire for a second or two in the flame of a spirit lamp or candle. 'Sugar-coated pills' are prepared in nearly the same way, but substituting hot and highly concentrated svrup, to which a little gelatin has been added, for a simple solution of gelatin. The following details for coating pills with sugar are taken from the ' Chemist and Druggist :'■•—" The pills are first varnished with the following liquids — Ether . . .100 parts, lials. tolu . . . 10 „ Colophonium , . 1 „ Absolute alcohol . , 10 „ By first rolling them in a mortar with this ethereal solution, and then transferring to a sheet of writing paper with the sides bent upwards, shaking being continued till they are perfectly dry. Then to a small' quantity of the saccharated albumen (see next recipe) add a few drops of water, at the same time beating for a short while, so that a thick paste will be formed. Into this mass the pills are stirred, and when moistened on all » TMs is the substance wliich ia left in the preparation of Bvrnp of tolu. > Dec. 15th, 1871. 82 1298 PILLS sides, quickly poured into a wooden pill-box, which has been previously filled about one third with the finest powdered sugar obtain- able, and immediately shaken, or rather rolled in a lively way with great force, separating from time to time those cohering. When no more sugar will adhere they are dried over a gentle fire, taking care not to bring them too near the stove lest they should craelc. Shak- ing, of course, must be continued till dryness is effected." Albumen cum Sacchaxo. Take the white of an egg, and in an evaporating dish beat with it as much powdered sugar, passed through a very fine sieve, as will make rather a thick fluid. Then place it in a water bath and evaporate to dryness, stirring constantly, that no sugar may be deposited. Pulverise and set aside for further use. M. Burden covers pills with collodion. Others have recommended for this purpose a solu- tion of gntta percha in either chloroform or bisulphide of carbon. The ready solubility in the stomach of pills thus covered has, with justice, been questioned. Gelatin, or, still better, gelatin mixed with a little sugar, is unexceptionable in this respect ; whilst it un- doubtedly excludes the taste of nauseous medi- cines more effectually than any other sub- stance. Mr Furley employs a thin coating of albumen to render pills tasteless. As pill-masses arc likely to get hard and brittle by keeping, an excellent plan is to keep the dry ingredients powdered and mixed to- gether in well-corked bottles or jars, when a portion may at any time be beaten up with syrup, conserve, soap, &c. ; according to the formula, and as wanted for use. The mixed ingredients in this state are technically known as 'species' or 'powder' for the respective pills. " It is generally said that pills should be taken on an empty stomach, and at a con- siderable distance from a meal ; but for our- selves we think that it is nearly always better to take them during a meal ; first, because the stomach does not then find itself immediately under the influence of substances which, if not always dangerous, seldom fail to act more or less disagreeably; secondly, because its absorbent action is more certain; and, lastly, because they are then taken more easily." (Trousseau and Reveil.) The meal here re- ferred to should be a light one, from which acidulous and other substances likely to interfere with the action of the remedy snould be excluded. The dose should also be increased.' In the London Pharmacopoeia the singular number *(* pilala') is now very properly em- ployed to express the names of the officinal pill-masses; but in the other Pharmacopoeias the names are given in the plural form. As the latter is almost universally adopted in speak- ing of magistral formulae and riostrnms, we have used it in all cases, for the sake of uni- formity and for ease of reference. See Bolus, ExTEACT, Peeboeibing, and below. Pills, Abernethy's. See Abeenethy me- dicines (page 6). Pills of Ac'etate of lead. Si/n. Pilule PLU^iBl ACETATis, L. Prep. 1. Acetate of lead, 20 gr. ; powdered camphor, 15 gr. ; con- serve of roses, q. ». ; mix aud divide into 12 pills. 2. (Radius.) Acetate of lead and powdered mallow or liquorice root, of each i dr.; simple syrup, q. s. ; divide into 18 pills. — Dose, 1 to 5 daily, washed down with water soured with vinegar; as a powerful astringent in haemor- rhages, dlarrhcea, the night-sweats in phthisis, &c. See Opiated Lead pills. PiUs of Acetate of Mercury. Syn. Pilulje HYDEAEQTEI ACETATIS, L. Frep. 1. Sub- acetate of mercury, 18 gr. j sugar of milk (or manna), 1 dr.; mucilage, q. s. ; divide into 24 pills. — Dose. As an alterative, 1 daily ; as a sialogogue, 1 every four or five hours, or of tener ; in syphilis, &c. See Kbysee's PILLS. 3. (Opiated — Ciirmixihael.) Acetate of mer- cury, camphor, and opium', of each 30 gr. ; syrup of poppies to mix. For 30 pills. Less apt to affect the stomach and bowels than the last. Pills of Acetate of Mor'phia. St/n. Pilulje MOEPHIiE ACETATIS, L. Prep. 1. Acetate of morphia, 2 gr. ; sugar of milk, 15 gr. ; con- serve of roses, 20 gr. ; for 12 pills. Anodyne, sedative, and soporific. — Dose. One, as re- quired. 2. (Dr A. T. Thomson.) Acetate of mor- phia, 1 gr. J powdered foxglove, 6 gr. ; pow- dered camphor, 10 gr.; powdered gum Arabic, 8 gr.; syrup of tolu, q. s. ; to be divided into 6 pills. Sedative and antispasmodic. — Dose. One, every 3 or 4 hours ; in phthisis, palpita- tions, spasms, &c. The hydrochlorate of mor- phia may be used instead of the acetate, with advantage. Pills of Ac'onite. Si/n. PiLULjiE aconiti, P. EXTEACTI A., L. I>rep. (Dr TurnbuU.) Alcoholic extract of aconite, 1 gr. ; liquorice powder, 12 gr. ; simple syrup, q.s.; mix, and divide the mass into 6 pills.— Zlose. One pill, every 3 or 4, hours ; as a powerful anodyne and sedative in excessive action of the heart, acute rheumatism, gout, neuralgia, &c. The uljmost care should be taken both in their preparation and administration. Pills, Aliberf s. See Pills, Apeeient. Pills of Aloes. */». PlLULA ALOES Soco- TEINiE (B. P.), PlLFLa; ALOETlCi:, P1LDL.JB ALOES (Ph. E.), L. Prep. 1. (Ph. E.) Soco- trine aloes (in powder) and Castile soap, equal p;irts; conserve of red roses, q. ». to form a pill-mass. 2. (Ph. V. S.) Powdered aloes and Castile soap, equiil parts, beat into a mass, and divided into 4 gr. pills. 3. (B.P.) PiLULA ALOES Baebadeitsis, Frep. Barbadoes aloes, in powder, 2 oz. ; hard soap. PILLS 1290 in powder, 1 oz. j oil of caraway, 1 fluid dr. ; coiifc-ct on of roses, 1 oz. Beat all togetliei- until thoroughly mixed. Obi. " Ttiis pill muy be also correctly made with the finer qualities of East Indian alues, as the (true) Socutrino variety is very scarce ; :ind many, not without reason, prefer (pure) Barbadoes aloes." (Ph. £.) The dose, as a laxative, is 5 to 10 u:r. ; as a purgative, 12 to 20 gr., or more. Slu Pills op Aloes and Soap. Fills of Aloes and Assafoetida. 5y». Pilula ALOES ET ASSAPCETIDA (B. P.). Prep. Soco- trine alues, in powder, 1 ; assafoetida, 1 ; pow- dered hard soap, 1; conTection of roses, 1 (i confection sufficient — Squire). Mix. Catliartic Mud antiHpasmodic. — Doae, 5 to 10 gr. Pillj of Aloes (Compound). Syn. Pilule ALOETIC* COMPOSITE, PlLCLA ALOE3 CO.M- P081TA (Ph. L.), PlLULJE A. OOMPOSIT*; (Ph. U.), L. Frep. 1. (Ph. L.) Socotrine aloes (ill powder), 1 oz. ; extract of gentian, 1 oz. ; oil of carawiiy, 40 drops ; treacle, q. s. ; tlie whole tn be beiitcn together until tliey form a mass proper for radking pills. 2. (Ph. D.) Hepatic aloes (in powder), 2 oz. j extract of gentian and treacle, of each 1 oz. ; oil of caraway, 1 ft. dr. ; as tlie last. Obs. The above is a very valuable pur- gative in habitual costivcness and indigestion, in all cases in which the use of uloes is not contra-indicated. The dose is from 5 to 15 gr., or more. Pills of Aloes (Diluted). Si/n. Pilulje Ar,oi:s DILOTS, L. Prep. 1. (Dr Miirslmll Hall.) Barbadoes aloes, Castile soap, extract of liquo- rice, and treacle, equal parts ; water, q. s. ; dissolve, with heat, strain, and evaporate to the onn-iitoticeoE a pill-mass. Resembles the PILULA Aioiis orsr saponb— Ph. L. Fills of Aloes and Assafoeti'da. Si/n. Pilule AL0E9 ET assapcetida (Ph. E.), L. Prep. (Ph. K ) Aloes (Socotrine or East Indian, powdornl), asssaloetida, aud Castile soap, equal parts; beat them with conserve of red roses to a proper pill-mass. — Dose, 5 to 10 gr., once or twice daily, iis a stomachic tonic and laxa tive, in dyspepsia, flatulence, &c. ; and 12 to 20 gr., oa a purgative in similar ca~os. It is extremely useful in costivenesSjwith flatulency, occurring' in hysterical and liypocbondriacal subjects. The B. P. preparation is the same a^ this, eX'c-pt that hard soap is used instead of Castile nnap. Fills of Aloes and Gin'ger. Syn. Piiul.e ALoiia ET zi.saiBSUis, L. Pre/i. (Ph. U. 1826.) Aloes, 1 oz. ; Ca^tilL■ softp, i oz. ; ginger. 1 dr. ; oil of peppermint, i dr. ; beaten to a iiiai«s. A useful laxative in cold habits. — Dote. As the last. Fills of Aloes aud Ipecac'nanha. •.%». Dr BaILLIF.'s I>I.\.\KIl PILLS; PlLUL.E ALOES El irKCACL'AMi.F., L. Prep. (Dr Buillie.) Pow- ili'roil uliie-, ;io gr. ; powdered ginger (linest). 45 gr. ; ipecacuauli.i, 12 gr. ; syrup of orange peel, q.s. to mix. For 21 pills. — Dote. One, about an hour before dinner. Fills of Aloes and I'ron. S<^n. Pilci.e ALOES ET FEEEI (Ph. E.), L. Prep. 1. (B. V.) Barbadoes aloes, 2 ; sulphate of iron, 1^ ; compound powder of cinnamon, 3; confection of roses, 4 ; mix (6 of confection required — Squire). — Dose, 5 to 10 gr. 2. (Ph. E.) Sulphate of iron, 3 parts ; Bar- badoes aloes, 2 parts; aromatic powder, 6 parts; conserve of red ro-es, 8 parts; powder the aloes and sulphate of iron separ.itel v, beat the whole to a mass, and divide this into 5 -^m . pills. An excellent medicine in chlorosis, hys- teria, and atonic amenorrhoca. — Dose, 1 to 3 pills daily. Fills of Aloes and Uas'tic. .See Pills, DiNNEE. Fills of Aloes and tfer'cary. Si/n. Pilule ALOES COM HYDBAEOIRO, L. See PiLLS, Apeuient (8). Fills of Aloes and Myrrh. Syn. llrpus's PILLS; PlLl'LA aloes CUM MYRUUA (Ph. L. & D.). PiLOL.E RUFI or COMMUNES { I'h. L. 1720), p. ALoiis ET MtBBHi; (B. p.. Ph. E.), L. Prep. 1. (I'h. L.) Sneiitiino or hepatic aloes (in powder, i oz. ; saffron, myrrh pow- dered), and soft soap (Ph. L.), of each 2 dr. ; treacle, q. s. to form a pill-mass. 2. (Ph. D.) Hepatic aloes, 2 oz. ; myrrh, 1 oz. ; dneJ saft'ron, i oz. ; all in powder; treacle, 2i oz. 3. (I'll. E.) Aloes (Socotrine or East Indi in), 4 parts; myrrh, 2 parts; saffron, 1 part; beat tliein to a pill-mass with i.'onserve of red roses, q.s. 4. (Ph. L. 1836 and Ph. D. 1826.) Aloes (in powder), 2 oz. ; saffron and pdwilered myrrh, of each 1 oz. ; syrup, q.s. to form a pill-mass. 5. (B. P.) Socotrine aloes, 2 ; myrrh, 1 ; dried saffron, i ; ennfection of roses, 2\ (3 arc required — SjMtVe). Mix. Stimulant and cathartic. — Dose, 5 to 10 gr. Obs. This compound is a most excellent stomachic purgative and cminenagoijiie, when there are no febrile symptoms present. It is said to have been employed ever since the time of Rliazes, and is still in extensive use. — Dose, 10 to 20 gr. Fills of Aloes and Ehu'barb. Sipu Pii.uLiE ALOiia EX EH EI, P. B. CUM EHEO, L. Prep. Powdered Soci'trine or hepatic aloes, pow- dered rhubarb, and soft soap (Ph. L.), of each J dr. ; oil of chamomile, 10 drops ; for 30 pills. — Dose, 1 to 5, either as a stJiiiach tonic or laxative; especially in dyspepsia,- with loss of appetite. Fills of Aloes and Kose-juice. Si/n. PiLULiE ALOES BOSATJE, L. ; PiLULES A.NGELIQUES, UuiiNS UE SANIE, Fr. Prep. Take aloes and roscjniee, of eacb4oz.; jui.e of borage and ehicoiy, of each 2 oz. ; dissolve witli heat, evaporate to an e.Miacl; add, of rlmbarb, 2 dr.; atr-iric, 1 dr.; ami divide the mass into IJ-gr. pills. — Dose, 4 to 12, as a purge. 1300 PILLS Pills of Aloes with Soap. Syn. Vylv^m ALOES CUM SAPONB (Pli. L.), L. Frep. (Ph. L.) Powdered extract of Baibadoes aloes, soft soup, and extract of liquorice, equal parts; treacle, q. s. to form a pill-mass. — Dose, 10 to 20 gr. ; io the usual cases in which aloes is administered. It is more readily soluble in the juices of the primae vise, and is milder than most of the aloetic pills without soap. See PiLis or Aloes (Diluted). Pills, Aloes and Turpentine. (Bois.) Syn. Pilule aloes et TEEEBiUTHiKa;. Prep. Boiled turpentine, 2 dr.; aloes, i dr. Divide into 40 pills. Pills, Al'terative. Syn. PiLULas alteeantes, L. See Pills, Calomel, Meeoukial, and Plummee's, &c. Pills of Al'um. Syn. PiLULm aluminis, P. A. coMPoaiTJE, L. Frep. 1. (Augustin.) Alum, 20 gr. ; benzoic acid, 6 gr. ; powdered gum and white sugar, of each 10 gr. ; water, q. s. to form a mass. For 36 pills. In phthisis and atonic mucous discharges. The whole to be taken in the course of 2 or 3 days. 2. (Capuron.) Catechu, 1 dr. ; alum, \ dr. ; opium, 10 gr. ; syrup of red roses, q. ». ; divide into 5-gr. pills.— Z)ose, 1 to 3; in chronic diarrlicea and leucorrhoea. 3. (Radius.) Alum and catechu, equal parts ; extract of gentian, q. s. to mix; divide into 2 or 3-gr. pills. — Dose, 2 to 4, every four hours; in passive hfemorrhages, mucous discharges, and chronic diarrhoea. Pills of Ammoni'acnm. Syn. PiLULiE am- MONIACI, L. Frep. 1. Gum ammoniacum, 1 dr. ; powdered sugar, 5 dr. ; conserve of hips, q. s. In old coughs and hysterical aifec- tions. 2. (Compound.) — a. (Ainslie.) Ammonia- cum, 1 dr. ; mercurial pill, 15 gr. ; powdered squills, 6 or 8 gr. ; simple syrup, q, s. For 16 pills. In asthmatic coughs, with deranged action of the liver. — Dose. One, 2 or 3 times a day, b. (W. Cooley.) Ammoniacum and saga- penum, of each 1 dr. ; dried sulphate of iron, \ dr. ; conserve of hips, q. a. In obstructed menstruation, and in the chronic diarrhoea of hysterical subjects. Pills of Ammo"niated Cop'per. Syn. PiLULa; CUPEI AMMONIATI (Ph. E.), p. C. AMMONIU- EETI, L. Frep. (Ph. E.) Ammoniated copper (in fine powder), 1 part; bread-crum, 6 parts; solution of carbonate of ammonia, q. s. to make a mass, which is to be divided so that each pill may contain ^ gr. of ammoniated copper. In epilepsy, and in some other spas- modic diseases.. — Dose, 1 pill, night and morn- ing, gradually increased to 5 or 6. Pills of Ammoniated I'ron. Syn. Pilule FEEEI AMMONIATI, P. E. AMMONIO-OHLOKIDI, L. Frep. 1. (Dr. Copland.) Ammoniated iron, 1 dr. J aloes and extract of gentian, of each i dr. ; for 30 pills. In scrofula, chlorosis, Ameuorrhoea, &c. 2. (Radius.) Ammoniated iron and gal- banum, of each 1 dr. j assaf oetida, 2 dr. ; castor, 20 gr ; tincture of valerian, q. s. For 3-gr. pills. — Dose, 2 pills, night and morn- ing ; in atonic nervous disorders, epilepsy, &c. Pills of Ammo"nio-cit'rate of Iron. Syn. P1LUL.E PEEBI AMMONIO-OITBATIS, L. Frep. (Beral.) Ammonio-citrate of iron, 1 dr. ; white sugar, 3 dr. ; mucilage, q. s. to mix. For 3-gr. pills. — Dose, 1 to 3, or more; as a mild chalybeate tonic. Pills, Aualep'tic. See Pills, James', Ana- leptic, &c. Pills, Anderson's Scot's. Various formulse for these pills are extant, the products of which differ widely from the genuine article. Dr Paris, some years since, declared that they consisted of Barbadoes aloes, jalap, and oil of aniseed. "A careful examination of the proprietary article, with other facts that have come to our knowledge, leads us to believe that the first of the following formulae is the one now employed in the preparation of the ' Grana Angelica,' or ' Anderson's True Scot's Pills,' of the present day." (Cooley.) Frep. 1. From Barbadoes aloes, 7 lbs. ; jalap (in fine powder), 2^ lbs. ; treacle, i lb. ; soap, 6 oz. ; melted together by the heat of a warm bath, and, when partly cold, aromatised by stirring in of oil of aniseed, 1 oz. The mass is divided into about 3i-gr. pills, of which 26 or 27 are placed in each \s. \\d. box. A mild and useful aperient. — Dose, 5 to 15 gr., or more. 2. (Original formula.) Socotrine aloes, 1 oz. ; best myrrh, J oz. ; saffron, 1 dr.; separately pounded very fine ; mix them, in an earthen pipkin, with a spoonful each of water and sweet oil, by the heat of a slow fire, and form the mass into "common-sized pills." From a copy of the original document in the Chapel of the Rolls. 3. (P. Cod.) Aloes and gamboge, of each 6 dr.; oil of aniseed, 1 dr.; syrup, q. s. ; mix, and divide into 4-gr. pills. Much more power- ful than the preceding, and closely resembling Morison's ' No. 2 pills.' 4. (Phil. Coll. of Pharm.) Barbadoes aloes (in powder), 3 lbs.; Castile soap, i lb.; colo- cynth and gamboge (both in fine powder), 2 oz. ; oil of aniseed, 1 oz. ; beat to a mass with water, q. s., and divide it into 3-gr. pills. Less active than the last, but more so than the ' True Scot's Pills.' Pills, An'odyne. Syn. Piluls) anodyne, L. Frep. ] . (Hosp. F.) Qpium (in powder), 6 gr. ; camphor, 15 gr. ; conserve of roses, q. s. ; divide into 12 pills. — Dose, 1 to 3, as reqnired. 2. (A. T. Thomson.) Calomel, potassio-tar- trate of antimony, and opium, equal parts ; syrup of saif ron, q. s ; divided in SJ-gr. pills. In acute rheumatism and neuralgia. — Dose, 1 pill, at bedtime. Pills, Antibil'ioos. All the ordinary aperient PILLS 1301 and fltomnchic piMs may be (-lapsed under this lifiiil. See till" names of their proprietors or reputed inventors, or those of their leading ingredients. Pilla Antichlorofic. Si/a. Pir.ur,^ anti- CHLOBITlc*. L. Prep. 1. (Radius.) Aloes and ctirbouato of iron, of each ^ dr.; gum ara- nioniiicnm. 1 dr. j extract of taraxacum, q. ». For S-L'r. pills. — Dote, 2 to 6, ni^^ht and morn- ing ; in chlorosis, amenorrha'a, &c. 2. (Tnitissuau & Kevcil.) Porphjrised iron filings, 1 dr. ; extract of wormwood, q. n. For 36 pills. — Done, 3 or 4; as the last. FUIb, Antimonial (Componnd). Si/n. Pilu- le ANTIM0NIALI8 C0MP09IT.B, P. ANTIMONII CO., L. Prep. 1. Antimonial powder, i dr. ; calomel, camphor, and powdered opium, of each 6 gr, ; conserve of roses, q. s. ; divide into 4'-gr. pills. — Done, 2, at night; in acute rheumatism, nL'uriil'.;iii, chronic coughs, »&c. 2. (St li. Ho-ip.) Tartar emetic, 1 gr. ; guaiacum and pill of aloes and myrrh, of each i dr.; treacle, to mix. For 16 pills. As the last. Fills, Antispasmod'ic. Syn. Pilule akti- BP48MoDic^, L. Prep. (Ur A. T. Thomson.) Opium, 1 gr. ; Russian castor, 13 gr. ; pow- dered (ligiialisi, 2 gr. ; syrup, to mix j divide into 4 pills. — Dose, 1 or 2, two or three times a day ; in spasmodic asthma, difficulty of breathing, &c. Several other formulas for antispnsraralic pills will be found both above and below. 2. (Trousseau & Reveil.) Musk, 15 gr. ; extract of valerian, i dr. ; liquorice powder, q. 8. I'"or 20 pills.- — Dose, 1 eveiy two hours, until there is a marked improvement iu the symptoms ; in pneumonia, accompanied by delirium, especially in drunkards; in spaims of the uterus, and in various other spasmodic affections. Pills, Ape"rlent. Si/n. PiLULiB apebientks, L. Prep. 1. Hepatic aloes, 2 dr. ; rhubarb and Castile soap, of each 1 dr. ; scatnmony, 1 dr. (all in powder) ; essential oil (at will), 10 or 12 drops ; beaten to a smootli muss, and divided into pills. 2. Compound extract of colocynth (Ph. L. 1836), IJ dr.; extract of ^'eiitian, i dr. ; pow- dered ipecacuanha, 20 4;r. ; oil of cloves, cara- way, or cassia, a few drops. In dyspepsia, loss of appetite, &c. 3. (Abcriiethy's.) See page 6. 4. (Alibpil's.) From calomel, resin of jalap, and Castile soap, of each 1 dr.; oil of orange peel or citron, 6 or 8 drops. For 60 pills. As nn occasional mild pur^'ative, especially in bilious hai'iis and worms. 5. (Sir B. Brodie.) Compound extract of colocynth and mercurial pill, of each J dr. ; scamiiiony and Castile soap, of each 15 gr. ; oil of caraway, 6 or 7 drops. For 24 pills. Aa the last. 6. (W. Cooley.) Aloes, 1^ dr.; jalap and Castile -Clip, of each I dr. ; rhubarb and car- damoms, of each i dr. (all in powder) ; oil of juniper, 12 drops. For 3-gr. pills. A useful mild aperient, for either frequent or occasional use. 7. (Dr Copland.) Compound extract of colocynth (Ph. L. 1836), 40 gr. ; extract of henbane, 30 gr. ; Castile soap, 12 gr. ; ipeca- cuanha, 6 or 7 gr. For two dozen pills. — Lose, 2, on retiring to rest. As an aperient in nervous aflections and iiritable habits. 8. (Harvey.) Mercurial pill and powdered aloes, of each t dr. ; ginger, 20 gr. For 24, pills. Iu constipation, attended with a defi- ciency of bile. 9. (Dr Neligan.) Compound colocynth pill and soap of jalap, equal parts ; either with or without a few drops of some aromatic essential oil. For 4 or 5-gr. pilla. As an aperieut for general use. 10. (Sir C. Scudamore.) Compound extract of colocynth, 40 gr. j extract of rhubarb, i dr. ; scimmony and soap, of each 12 gr. ; oil of caraway, 5 or 6 drops. For 20 or 21- pills. 11. (Stahl's ; PlLOL^. AFEIIIKNTKS StAULII — Ph. Hannov.) Powdered aloe-', 1 oz. ; com- pound extract of eolocyutli, i oz. ; iron filings, 2 dr.; mucilage, q. s. Iu amenorrhea, low habits, and worms. 12 (Vance.) Compound extract of colo- cynth, 80 trr. ; extract of rhubarb, 12 gr. ; Castile soip, 6 or S gr. ; oil of cinnamon, 4 or 5 drops- OS*. The products of the above formula) may be divided into pills of any size deemeil most agreeable to the patient, and tliey may be aromatised by the addition of any essential oil at will. The dose varies, according to cir- cumstances, from 5 to 10 or 12 gr., or more. Those containing aloes or mercurials are beat taken at bedtime, For other formula; see the various offiemal and other pills contaiuing aloes, colocynth, gamboge, rhubarb, scummony, &c. Pills, Aromai'ic. i">.v»- Pilule abomatic.t:, L. Prep. (Ph. L. 1740.) Compound powder of aloes, 3 oz. ; balsam of Peru, i oz. ; syrup of oran;^e peel, q. s. Aperieut, sudorific, and nervine. — Dose, 10 to 20 gr. Pills of Arse"iiiate of Iron. Si/n. Pilule FEREi arseniatis, L. Prep. (Uiett ) Ar- seniate of iron, 3 gr. ; extract of hops, 2 dr. ; powdered mallow-root, i dr. ; syrup, q. s. For 48 pills. — Dose, 1 to 2, daily ; in caucerous, scrofulous, and herpetic affections. !?ee Pills, Aesenical. PiUs of Arseniate of So'da. Sj/n. 1'ilulj! SOD.E ABSBNIATIS, L. Prep. (Erasmus Wil- son.) Arseniate of soda, 2 gr.; distilled water, the smallest possible quantity to dissolve it ; powdered gum guaiacum, i dr. ; oxysulphuret of antimony, 20 gr. ; mucilHge, q. s. For 2i pills. — Dose, 1 pill, as the last ; in herpes, &c. See Pills, Absknical. Pills, Arsen'ical. S^n. Asiatic pills, Cae- NATic p.. East Indian p., Tanjoee p. ; Pi- lule aksenici, p. aesenicalis, p. Asiatice, P. ACID! AESKSiosi, L. Prep. (P. Cod.) Ar- 1302 PILLS senious aciil, 1 gr. ; black peppet (in fine pow- der), 12 gr. ; rub them together for some (considerable) time in an iron mortar, then adc|, of pondered gum, 2 gr.; water, q. s. to make a mass ; whioh is to be accurately divided into 12 pills. Each pill contains ^j gr. of white arsenic. Obs. This compound is commonly employed in the East Indies in syphilis, elephantiasis, intermittents, the bites of venomous snakes, &o. ; and as a preventive to hydrophobia. The common practice in England is to employ 16 gr, of pepper to 1 gr. of arsenious acid, and to divide the mass into 16 instead of 12 pills. The dose is one or two pills daily, taken after a meal. The use of all compounds containing arsenic demands great caution. Fills, Arsenical (Opiated). Si/n. Vilvlm ABSENIOI CUM OPio, L. Frej). (A. T. Thom- son.) Arsenious acid, 2 gr. ; powdered opium, 8 gr. ; Castile soap, 20 gr. ; simple syrup, q. s. For 34 pills. — i>ose. As the last ; in inter- mittents, herpes, lepra, psoriasis, periodical headaches, neuralgia, &c. (See above.) Pills, Asiatic. See Pills, Aksenioal. puis of Assafoet'ida, Si/n. Pilol^ assa- rcETiDA (Ph. E. & U. S ), L. Prep. 1 (Pli. E.) Assafcetida, galbanuni, and myrrh, of each 3 parts ; conserve of red roses, 4 piirts, or q. a. ; mix, and beat them to a proper pill- mass. 2. (Ph. U. S.) Assafcetida, IJ oz. ; Castile soap, a oz. ; water, q. 3. ; divide into 240 pills. Obs. The above (particularly the last) are stimuhmt and antispasmodic — Dose, 5 to 10 gr. ; twice or thrice daily; in hysterical affec- tions, &c. (See below.) Pills of Assafcetida (Compound). Si/n. Fi- ■LVLM ASSArOETIDJE COMPOSITE (B. P., Ph. D.) Frep. 1. (Ph.D.) Assafcetida, 2 oi.; gal- banum, myrrh, and treacle, of each 1 oz. ; mix in a capsule, by the heat of steam or a water bath, and stir until it becomes a uniform mass. — Dose, ifc. As the last. The B. P. directs the quantity of galbanum to be double the above. 2. (Hosp. P.) Assafcetida, 1 dr. ; soft soap (Ph. L.), 20 gr. ; ipecacuanha and squills, of each (in powder), 12 gr. ; syrup, q. s. — Dose, 5 to 10 gr. ; in chronic asthmas, coughs, &c. Pills of Assafcetida with I'ron. S^n. Pilvlm ASSAFfflTID^ C.VM PEEBO, L. Frep. (W. Cooley.) Assafcetida, 1 dr. ; extract of chamo- mile, i dr. ; mix with a slight heat ; add, of dried protosulphate of iron, 15 gr. ; oil of caje- put, 10 drops ; and divide into 36 pills. In hypochondriasis, hysteria, amenorrhcea, chlo- rosis, &c., alter an aperient. Pills, Asthma. Sj/n. Piutl^ antasthma- TICM, L. Prep. 1. (Expectorant.) From compound squill pill, 20 gr.; calomel, 5 gr. ; powdered opium, 3 gr. ; made into 6 pills. — Dose, 1 or 2, at bedtime. Expectorant, and sometimes laxative. 2. (Tonic.) From compound iron pill, 2 dr. ; extract of gentian, 1 dr. ; mix, and divide into 60 pills. — Duse, 2, night and morning, with an occasional dose of laxative medicine. Pills, Astringent. Sya. PiLULiE astrik- aENTBS, L. See PiLLS OP AoETATE OP LEAD, Alum, Gallic acid, Nitbaib op Silveh, StILPHATE OP IeON, SULPHATE OP COPPEB, Tannin, &c. Pills of Atropine. (P. Cod.) Si/n. Pilitl* ATE0PIJ3. Prep. Atropia, li gr. ; sugar of milk, 1 dr.; gum Arabic, 12 gr. ; syrup of honey, q. s. Triturate the atropia for a long time with the sugar of milk, and make into 100 granules and silver them. Granules of arsenious acid, digitalin, and strychnia, are prepared in the same way. Pills, Bacher's Ton'ic. Syn. Pilule tonics Baoheei, L. Prep.l. (Dr Paris.) Extract of black hellebore and powdered myrrh, of each 1 oz. ; powdered blessed thistle, 3 dr.; mix, and divide into 1-dr. pills. — Dose, 2 to 6, three times a day. 2. (P. Cod.) Alkaline extract of hellebore and extract of myrrh, of each 2 dr. ; pow- dered blessed thistle, 1 dr. For 4-gr. pills. — Dose, 1 to 2, as the last. An alterative tonic, hydragogue, and emmenagogue ; in debility, dropsy, amenorrhcea, &c. A favourite remedy in some parts of Europe. Pills, Dr Baillie's. Prep. (Cooley.) Aqueous extract of aloes and compound extract of colo- cynth, of each 3 dr. ; Castile soap, 1 dr. ; oil of cloves, 15 drops. For 4-gr. pills. A good occasional aperient. — Dose, 1 to 3, at bedtime, or early in the morning. See Pills, Dinner. Pills, Balsamic. (Morton.) Si/n. Pilfls balsamica. Prep. Powdered millipedes, 18 dr. ; gum ammoniacum, 9 dr. ; benzoic acid, 6 dr. ; saffron, 1 dr. ; balsam of tolu, 1 dr. ; anisated balsam of saffron, 6 dr., or sufficient. Pills, Barbarossa's. These are supposed to have been the first mercurial preparation em- ployed in medicine. They consisted of quick- silver, rhubarb, musk, and amber. puis, Rev. D. Barclay's. Prep. (Cooley.) Resinous extract of jalap, 1 dr. ; almond or Castile soap, 1\ dr. ; extract of colocynth, 2 dr. (or powdered colocynth, 3 dr.) ; gum guaiacum, 3 dr. ; potassio-tartrate of antimony, 10 gr. ; oil of juniper, 8 or 10 drops; oils of caraway and rosemary, of each 4 drops ; make a mass with syrup of buckthorn (the smallest possible quantity), and divide into 4-gr. pills. A dia- phoretic aperient. — Dose, 1 to 3, at bedtime. Pills, Dr Baron's. Prep. From compound rhubarb pill, 30 gr. ; compound extract of colo- cynth, 20 gr. ; powdered ipecacuanha, 6 gr. For 3-gr. pills. An excellent stomachic aperient.— Iloie, 1 to 3 pills, at bedtime; in dyspepsia, loss of appetite, &c. PiUs, Earthez's. Prep. Prom myrrh, 1 dr. ; aloes, i dr. ; musk, 15 gr. ; camphor, 12 gr. ; balsam of Peru, q. s. to form a mass. ForSi- gr. pills.— Dose, 2, thrice daily ; in hysteria, amenorrhcea, chlorosis, &c. Pills, Bath Digestive. Prep. (Cooley.) Rhu- barb, 2 oz. ; ipecacuanha and Castile soap, of PILLS 1303 each 1 oz. ; c;\psidiin, ginjjer, and gamboge, of ciicli J oz. (all in powder) j syrup of back- thorn, q. g. For 4-gr. pills. — Doae, 1 as a dinner pill ; 2 or 3 as an aperient. Fills of Be'beerine. Si/n. PilvlJ! bebeer- iNiE, L. Prep. From sulphate of bcbeerine, i dr. ; aromatic confection, q. s. ; oil of cajeput, 8 or 6 drops. For 18 pills. — Doae, 1 to 3, every four hours ; as an antiperiodic, instead of bark or quinine. Pills, Be'chic. Pihtl.e BKcnioa;, L. Prep. (Trousseau and Reveil.) Extract of digitalis, 18 gr. ; white oxide of antimony, 30 gr. ; ex- tract of liquorice, 40 gr.; mix carefully, and divide Into 40 pills. Expectorant and seda- tive. — Dose, 2 to 12, or more ; in cases of irri- tating coughs, catarrh of the pulmonary Ciipil- larics or bronchia, &c. See Pills, Con&ii. Pills, Beddoe's. Prep. From dried (efflo- resced) carbonate of soda, 1 dr. ; soap, ij dr. ; oil of juniper, 12 drops ; syrup of ginger, q. s. ; divide into 30 pills. In gravel, stone, &c. — Dose, 2 to 5. Pills of Belladon'na (Compound). Si/n. PiLn- L/li BKLLADONNiE C0MP03IT.E, L. Prep. 1. (Ainslie.) Extract of belladnnna, mercurial pill, and powdered ipecacuanha, equal parts. For 3-gr. pills. — Dose, 1 niglit and morning, in cancerous and glandular utfections. 2. (Debrevne.) Camphor and assafojtidn, of each 1 dr. ; extract of belladonna, 20 gr. j ex- tract of opium, 5 gr. ; syrup, q. s. For 48 pills. — Dose, 1 pill, gradually increased to 6, daily. In hysteria, ameuorrhasa, &c. Pills, Belloste's. See Pills, Mbkcurial. Pills, Bennet's. See Pills, Fulleb's. Pills, Benzoic. (Dr Paris.) Syn. Pilul.e BENZOES. Prep, Benzoic acid, 12 gr. ; ex- trnct of poppies, 18 gr. Mix, for 6 pills. — Dose, 1 pill. Expectorant. Pills of Biohlo"ride of Mercuryf. Pills of corrosive sublimate. Pills of Biclilo"rid9 of ■ Plat'innm. Syn. PlLDL.*: PLATINI BIOHLOBIDI, L. Prep. (Dr Hoefer.) Bichloride of platinum, 7i gr. j ex- tract of gnaiat'um, 1 dr. ; liquorice powder, q. o. For 24 pills. — Dose, 1 pill, twice or thrice dally ; as an alterative, in syphilis, &c. Pills, Bicker's. Prep. From rust (carbonate) of iron, 2 dr. ; aloes, myrrh, and sulphur, of each 1 dr.; ox-gall, q. s. to mix. For 4-gr. pills. — Dose, 1 to 6, morning and evening ; in debility, chlorosis, &c. Pills of Bit'tersweet. Si/n. Pilul.^ dul- OAMAsa:, L. Prep. (Radius.) Extract of bittersweet (dulcamara), 1 dr. ; crude antimony and bittersweet (iu powder), of each \ dr. For 3-gr. pills.— Dose, 6 to 12, twice or thrice a day ; in obstinate skin diseases. Pills, Bland's. Syn. PiLTTLffi; antichloro- Tic.K, L. Prep. (Trousseau and Reveil.) Sul- phate of protoxide of iron, 2 parts ; reduce it to powder, and dry it in a stove at 104° Fahr. ; add to this dry carbonate of potassa, 2 parts ; boney, 1 part; and form the mass into 80 pills. Tonic and emmenngogue. — Dose, 1 to 10, daily ; in debility, chlorosis, &c. Pills, Blue. See Pills, JIkrcdbial. Pills, Bontius's. Syn. Pilul.*: nTDROOOOJ:, P. H. BoKTii, L. Prep. (B. Cod.) Socotriue aloes, gamboge, and gum ammoniacum, of each 1 dr. ; white-wine vinei;ar, 6 dr. ; dissolve by heat at twice, press out the liciuor, evaporate to a pilular consisteuce, and divide Into 4-^r. pills. — Dose, 1 to 3 ; as a strong cathartic, in drop.sy. Pills, Brigg's Gout and Ehenmatic. This nostrum closely resembles in !ii>|ic:irauce, odour, and properties, the I'LUMSiints pill of the Pharmacopoeia ; the two are probably iden- tical. (Cooley.) Pill of Bro'mide of Iron. Syn. Pilclb FEBBI BBOMIDI, L. Prep. (Masindle.) Bro- mide of iron and powdered gum .Vniblc, of each 12 gr. ; conserve of rose^^, 20 gr. j mix, and divide Into 20 pills. They should be kept iu a dry, corked jihlal. Tonic and alterative, — Dose, 1 to 2, night and morning; in debility, especially that of scrofulous habits, in chlo- rosis, &c. Pills of Bra'cine. Syn. Pilul.e bbuch, L. Prep. (Jliigcnilie.) Brucine, 12 t,'r. ; con- fection of rose', ^ dr.; carefully niixi d and divided iuto 2-1 pills, whicli arc recommended to be silvered. 'The quantity of tlio coulectlon may be advantageously doubled. — Dose, 1 pill, night and morning; in the same affections as those for which strychnine Is administered. The acetate hydrochlorate, or sulphate of bru- cine nniy be substituted for the alkaloid in the above formula, in a slightly larger quantity. Pills of Calomel. Syn. Pilul>ecalomela- NOB, P. E CALOlIELiNK, P. nYDBAROIRI SUB- CHLORIDI, P. n. CLOHIDit, P. H. C. MITIS (Ph. U. S.), 1j. Prep. 1. Calomel, 4 dr.; powdered gum Araliic, 1 dr.; simple syrup, q. s. ; mix and divide into 240 pills. Each pill contains 1 gr. of calomel. A cimvenient form of exhibiting this drug when uncombined with other i-cmedies. — Dose, 1 to 5 pills, according to the indication. 2. (U. C. Hosp.) Calomel, 2 dr. ; rhubarb, \\ dr. ; conl'ectiou of senna, q. ^. For 4 dozen pills. An excellent alterative aperient, espe- cially in hepatic affections. Pills of Calomel (Compound), fyn. Phtm- MEu's PILLS, Red p. ; Pilula niDHAHoyRi SUBCHLOEIDI COMPOSITA, PlLCLi: CAI.OME- LANOS COMPOSlT.fi (Ph. E. & D.), PlLTTIJi PUJMMEBI, PiLtJLA HTDEABGYBI CHLOHIDI COMI'OSITA, L. (Ph. L.). Prep. 1. (Ph. L.). Chloride of mercury (calomel) and oxy>ulphide of antimony, of each 2 dr. ; rub them together, add of guaiacum (in powder) and treacle, of each 4 dr., and form the whole into a pill- mass. 2. (Ph. E.) Calomel and golden sulphide of antimony, of each 1 part; gnaiacum (in pow- der) and treacle, of each 2 parts ; beat the whole to a pill-mass, and divide it iuto 6-gr. pills. 1301 PILLS 3. (Ph. D.) Calomel and precipitated sul- phide of aniimon V, of each 1 dr. ; triturate them together, then add, of guaiacumreain (in powder), 2 dr. ; castor oil, 1 fl. dr. ; and beat the whole to a uniibriu mass. 4. (B. P.) Calomel, 1 ; sulphurated antimony, 1 ; guaiac resin (in powder), 2 j castor oil, 1 ; mix. — Dose, 5 to 10 gr. Obs. An excellent alterative pill ; very use- ful in lepra, in secondary syphilis affecting the skin, and in various other chronic cutaneous diseases ; also in dyspepsia and liver com- plaints. — Dose, 3 to 10 gr., night and morn- ing. Pills of Calomel and Opium. Si/n. Pilul.^ CAIOMELANOS ET OPII (Ph. E), L. Frep. (Ph. E.) Calomel, 3 parts; opium, 1 part; conserve. of red roses, q. s. ; divide the mass so that each pill may contain 2 gr. of calomel. — Dose, 1 or 2 pills, in rheumatism, facial neuralgia, and various inflammatory affections. They offer a convenient form for gradually introducing mercury into the system, and, if continued, induce salivation. Pills of Camphor. Syn. Ptlvlm oam- PBOEa;, P. CAMPHORATJ!;, L. Prep. Camphor and sugar, of each (in powder) 2 parts; conserve of hips, 1 part. For 3-gr. pilLs. Anaphiodisiac, sedative, diaphoretic, and nervine. — Dose, 1 to 5, twice or thrice a day. Pills of Camphor (Compound). Si/n. ViimjjM CAMPHORJE COaPOSIT.E, P. CAMPHOKAT.E u., L. Prep. 1. (Dupuytren.) Camphor, 21 gr. ; pure musk, 8 gr. ; opium, 2 gr. ; syrup, q. s. ; divide iiicn 12 pills. — Dose, 1 to 4, tliree or four times daily ; in putrescent sores, hospital gangrene, &c. 2. (Fr. Hosp.) Gum ummoniacum. 40 gr. ; camplior, 30 gr. ; musk, 10 gr. ; opium, 5 gr. ; tincture of valerian, q. s. ; divide into 4-gr. pills. — Dose, 2 to 6 pills, daily ; in nervous and hysterical affections, &c. 3. (liicord.) Camphor and lactucarium (or extract of lettuce), equal parts; divide into 4-gr. pills. — Dose, 3 to 6 pills daily ; as an anaplirodisiac. 4. (U. C. Hosp.) Camphor, 20 gr. ; assa- foetida, 1 dr. ; extract of valerian, 2 dr. JTor 30 pills. As No. 2. Pills of Canthar'ides. Si/n. PiluLjE can- THABIDIS, P. u. COMPOSURE, L. Prep, 1. Cantharides (in very fine powdfr), 8 gr. ; ex- tract of gentian, ^ dr. ; liquorice powder, lU gr. For 12 pills. — Dose, 1 to 4 daily ; as a diuretic, emmenagogue, &c. 2. (Ellis.) Cantharides (in very fine pow- der), 18 gr. ; opium and camphor, 36 gr. ; mix, and divide into 36 pills. — Dose, 1 pill, at bedtime ; as an aphrodisiac, in parties labour- ing under general debility. They should be used with extreme caution, and but seldom. Pills of Caout'chonc. Syn. Vii.vlm gummi BIASTICI, L. Prep. (Bonis.) India rubber, cut into small squares or spheres, then moist- ened with syrup of tolu, and, lastly, shaken in a box with a mixture of powdered gnm and sng.ir. In phthisis.— 2)o»e, 1 pill, three or four times a day. They pass through the primse vise unaltered, and may therefore fairly be presumed to be inert. Pills of Capsicum. Syn. Cayeunb peppeh PILLS ; PiLUt.aE OAPSICI, L. Prep. 1. (Guy's Hosp.) Ciipsicum, 1 part; rhubarb, 2 parts (both in powder); treacle, q. s. ; mix, and divide into 3i-gr. pills — Dose, 1 to 3, an hour before dinner, to create an appetite and pro- mote digestion. 2. (Radius.) Powdered capsicum, 20 gr.; extract of gentian, 1 dr. ; powdered gentian, q. s. to form a mass. For 60 fiWs.—Dose, 2 to 4 pills, thrice daily ; in clironic dyspepsia, e.^pecially in the loss of tone of the stomach arising from intemperance. Pills of Carbolic Acid. Syn. Piltjl.s acidi OAEtiOLICI. Prep. Carbolic acid, 3 drops; soap powder, '60 gram ; lycopodium, '06 gram ; powdered tragacanth, q. s. For .six pills. The two first ingredients form a semi-fluid mass, which the lycopodium does not absorb, but which is solidified by means of the traga- canth. Pills of CarTionate of I'ron. Syn. Vallet'8 PILLS ; VlhVLM FEERI CAEBONATIS (Ph. E ), L. Prep. (B. P., Ph. E.) Saccharated car- bonate of iron, 4 parts ; conserve of red roses, 1 part ; mix, and divide the mass into 5-gr. pills. —Dose, 1 to 3, or more ; as a mild chaly- beate and antichlorotic. 5 to 20 gr., B. P. For another formula, see Pills, Blaud's {above'). PiUs, Carbonic Acid. (Mr Morson). Syn. PILUL.S ACIDI CARBONICI. Prep. Mix J dr. of bicarbonate of soda and 25 gr. of tartaric acid, ciiarsely powdered, with the smallest possible quantity of syrup and mucilage to form a niHss. Divide into 12 pills. Pills, Catarrh'. Syn. PiLUL.a!; anticatae- KHALES, L. Prep. 1. (Trousseau and Reveil.) Turpentine, 4 dr. ; ammoniacum, 1 dr. ; bal- sam of toln, \ dr. ; aqueous extract of opium, 5 gr. ; liquorice powder, q. s. ; mix, and divide into 80 pills. — Dose, 5 or 6 daily ; in chronic catarrh of the bronchi and bladder. 2. (Trousseau & Reveil.) Alcoholic extract of aconite, 30 gr. ; sulphuret of calcium, 16 L'r. ; p iwdered sugar, q. s. For 24 pills. — Dose, 1 pill, three or four times daily; in chronic pulmonary catarrh. Pills, Cathar'tic. Syn. Pilul.e cathaeti- CJE, L. Prep. 1. (Dr Collier.) Calomel, 10 gr. ; powdered jalap and prepared chalk, of each i dr. ; oil of caraway, 10 drops ; syrup of buckthorn, to mix ; divide into 5-gr. pills. — Dose, 1 to 4. 2. (Dr A. T. Thomson.) Scammony, 4 gr. ; extract of taraxacum, 16 gr. ; divide into 6 pills. — Dose, 3 pills, twice daily ; in hypo- chondriasis and chronic inflammation of the liver. 3. (A. T. Thomson.) Calomel, 15 gr. ; pow- dered jalap, 45 gr ; mucilage, q. s. to mix. For 18 pills. — Dose, 1 to 3, at night, to empty PILLS 1303 tlie bowels, in bilious nlTuctiong. Other for- muliu fur cathartic pills will be found both abuve aii>l below. PlUa, Cathartic (Compound). Si/n. Pilitl£ CATHAHTIUai COMPOSITE, L. Prep. (Ph. U. S.) Compounil extract of colocynth, 4 dr.; pow- dered extract of jiilup and calomel, of each 3 dr. ; powdered gamboge, 40 gr. ; water, q. B. ; mix, and divide into 180 pills. An excel- lent purgative, ospecittlly in bilious atfections, d_\-iH'p»iii. &c. — Doae, 1 to 3 pilU. Pills of Cetrarine. (Dr Neligan.) Si/n. PlLULK CETiUttLNa:. Cetrarine, 2+ gr. j ex- tract of calumba, ^ dr.; make into 12 pills; one every four hours as a febrifuge. Fills, Chamberlain's Eestorfative. A nostrnm composed of cinnabar and milk of sulphur, e(innl parts ; benten up with conserve of hips. PiUs of Cham'omile. Si/n. PiluL/E anthe- MIDI8, P. FLOUUM CHAM^MEII, L. Prep. Extriii't of gentian, 1 dr. ; powdered aloes, i dr. ; powdered rhubarb, 20 gr. ; oil of clia- moMiile, 10 drops. A tonic and stomachic aperient. — Dose, 5 to 15 gr. This forms tiie ' chamomile pills ' of the shops. They should be kept in a corked pliiul. (See below.) Pills of Chamomile (Compound). Ht/n. PiLtt- hM ANTUKMIDIS COMPOSITES, L. Prep. 1. (Aiiislic.) Kxtract of chamomile, 1 dr. ; assa- fa'tids, i dr. ; powdered rhubarb, 20 gr. ; di- viiied intrep. (.Miiiii'ndie.) S.ida-ihlo- ride of gold, 1 gr. ; extract of mezereon, 2 dr. ; divide into 60 pills. Pills of Chloride of Lime. Si/n. Pills op CnLOBINATED LIME ; PlLCL^E CALCIS HYPO- CHLOEITIS, L. Prep. 1. Chloride of lime, 12 gr. ; starch powder, 2 1 gr, ; conserve of hips, q. s. ; divide into 36 pills. 2. (Dr Copland.) Chloride of lime, 15 gr. ; compound powder of tragiicantli, 90 gr. ; syrup, q. s. For 24 pills. — Dose, 1 to 3, twice or thricre daily ; in various putrid affections, fevers, &c. Pills -of Chloride of Mercuryf. Pills of calnmel. Pills, Chol'era. Sj/n. I'riTL.E aniichole- BIC.X, E. Prep. 1. Powdered camphor, 15 gr. ; powdered capsicum (pure), i dr, ; bicarbonate of soda, 1 dr. ; conserve of roses, q. s. For 36 pills. — Dose, 2 to 4, every 15 minutes, washed down with a wine-glassful of cold water con- taining half a teaapoonful of ether ; repeated every 15 or 20 minutes until reaction ensues. They should be freshly made. 2. (PiLULA ANTICnOLEBlCAAKABICA.) Prep. Assnfcetida, asclepias gigantea, and opium, of each li gr. in each pill. One every half or three quarters of an hour, broken down in a spoonful of brandy and water, till the sym- ptoms yield. After vomiting and purging have ceased, if prostnvti'>u iiml spiisms are urgent, give ^ or i dnses. Black pepper is snhstiluted for aselepias in this country. 3. (PiLUL-E CAMBOGIS COMPOSITiE. I!. P.) Prep. Gamboge, aloes boils, aud compound cinnamon powder, of each 1 p:irt ; soap, 2 parts ; syrup, q. s. — Dose, 5 gr, to 10 gr. Pills of Ci'trate of I'ron and Quinine'. Syn, PlLCL^K FEEEI CITBATIS CUM QUINA, L. Prep. From citrate of iron and quinine, 1 dr. ; pow- dered citric acid, 20 gr. ; conserve of hips, q. s. For 3.6 pills. An excellent tonic in debility, chlorosis, &c. — Dose, 1 to 3, twice or Jirice daily. Pills, Sir C. Clark's. See Dinner pills. Pills, Coindet's. See Pills of Iodide op Mebcubt, Pills of Col'chicnm. See Pills, Gout. Pills of Col'ocynth. Sun- Pilulje e Duonirs, P. EX COLOCYNTHIDE SIMPLICIORES, L. Prep. (Ph. L. 1746.) Colocynth and scaramony, of 1306 PILLS canh 2 oz. ; oil of cloves, 2 cTr. ; syrup of buck- thorn, q. s. All active hjdragogue cathartic. —Dose, 2 to 12 gr. Pills of Colocynth (Componnd). Syn. Pill OP COOHIA; PlLULiE OOOCIM, P. COOHIJE, PlLTJLA COLOOTNTHIDIS COMPOSITA (B. P.), P. COLOCTNTHIDIS COMPOSITE (Ph. li. & D.), P. coLOOYNTHiDis (Ph. E.), L. Prep. 1. (Ph. L.) Extract of colocynth (simple), 1 dr. ; powdered extract of aloes, 6 dr. ; powdered scammony, 2 dr.; powdered cardamoms, i' dr.; soft soap (Ph. L.), IJ dr. ; mix, and beat them altogether, so that a mass may be formed. This is intended as a substitute for the compound extract of culocyuth of the Ph. L. 1836. 2. (Ph. E.) Socotrine or East Indian aloes and scammony, of each 8 parts; sulphate of Itotiissa, 1 part; beat them together; add of colocyntl), in fine powder, 4 parts ; next add of oil of cloves, 1 part ; and, with the aid of a little rectified spirit, beat the whole to a mass, and divide this into 5-gr. pills. 3. (Ph. D.) Colocynth pulp, scammony, and Castile soap, of each (in powder) 1 oz. ; hepatic aloes, 2 oz. ; treacle, 10 dr. ; oil of cloves, 1 fl. dr. ; mix, and beat them into a mass of uniform consistence. 4. (Ph. L. 1746.) Socotrine aloes and scam- mony, of each 2 oz. ; pulp of colocynth, I oz. ; oil of cloves, 2 dr. ; syrup of buckthorn, q. s. to form a pill-mass. This is the original for- mula published by Galen for 'pilnlas cochise niinores,' and, under various slight moditica- tions, it has continued in use ever since. 5. Aloes, IJ lb.; colocynth, | lb.; jalap, 6 oz. (all in powder); oil of cloves, IJ oz. ; syrup or treacle, q. s. to mix. Trod. About 4| lbs. Tliis forms the common 'pil. coehioe ' of the druggists. A few, more conscientious than the rest, add to the above, scammony, 6 oz. It is greatly inferior to the Ph. pill. 6. (B. P.) Colocynth, in powder, 1 ; Bar- badoes aloes, in powder, 2 ; scammony, in powder, 2; sulphate of potash, in powder, i; oil of cloves, i; distilled water, a suffiiuency (about i) ; mix. Dr Gregory's favourite pill. — Dose, 5 to 10 gr. Obs. Compound colocynth pill is a cheap and excellent cathartic, more powerful than the other officinal aloetic pills, and well adapted to cases of habitual costiveness. ^ It has long been extensively used by the poorer classes, and in domestic medicine generally. — Dose, 5 to 15 gr. Pills of Colocynth and Hen'bane. Si/n. Pi- LULiiE COLOOYNTHIDIS ET HTOSCTAMI (B. P., Ph. E.), L. Frep. 1. (Ph. E.) Colocynth pill- mass, 2 parts ; extract of henbane, 1 part ; beat them up with a few drops of rectified spirit (if necessary), and divide them into 5 gr. pills. — Dose, 1 to 3 pills ; as an anodyne purgative, in irritable bowels. 2. (B. P.) Colocynth, in powder, 2 ; Bar- badoes aloes, in powder, 2; scammony, in powder, 2 j sulphate of potash, in powder, i ; oil of cloves, i ; extract of hvoscyamus, 3 ; distilled water, a sufficiency ; mix. — Dose, 5 to 10 gr. Pills of Copaita. Sgn. PiiULa; copaib.e, L. Prep. (Ph. U. S.) Pure balsam of co- paiba, 2 oz. ; recently prepared calcined mag- nesia, 1 dr. ; mix thoroughly, then set the inixture aside until it acquires a pillular con- sistence, and lastly, divide it into 200 pills. Obs. Unless the magnesia has been very recently calcined, the copaiba hardens very slowly or not at all. It is said that " lime produces the eft'ect more completely and uni- formly than magnesia," and that " specimens of copaiba which are old and contain the most resin harden qqickest." (Redwood.) For present use, the quantity of magnesia may be at least doubled. Dr Pereira orders copaiba, 1 oz. ; magnesia, 5 or 6 dr. — Dose, 10 to 30 gr., frequently ; in diseases of the mucous membranes of the urinary organs. Cubebs are often added. Pills, Dr Copland's. See Pills, Apeeient and Pectoeal. Pills of Corro'sive Sublimate. Si/n. Pills OF chloride or meecurt; P. of eichlo- KiDE OF Mt, Hoffmann's p. ; Pilttl^ sub- LIMATIS COEEOSiyi, P. HTDEARGYBI BICHLO- EIDI+, P. MAJOEES HOFFMANNI, L. Prep. 1. Corrosive sublimate, 3 gr. ; white sugar, i dr. ; triturate together in a glass mortar for some time, then add of powdered gum Arabic, 20 gr., and beat the whole to a mass with dilute hydrochloric acid, q. s. For 36 pills, each containing ^ gr. of corrosive subli- mate. 2. (Brera.) Corrosive sublimate, 3 gr. ; rectified spirit, the smallest po.'-sible quantity to dissolve it; bread-crum, q. s. to form a mass. For 24 pills, each contiiining \ gr. of the coiTOsive subliniate. 3. (Dr Paris.) Corrosive sublimate and sal- ammoniac, of each 5 gr. ; water, ^ fl. dr.; triturate together until solution is complete, then add of honey, i dr. ; liquorice powder, 1 dr. (or q. s.), and divide into 40 pills. Each pill contains | gr. of corrosive sublimate. 4. (Ph. Hannov.) Corrosive sublimate, 15 gr. ; distilled water, J fl. dr. ; crura of bread, q. s. to form a mass. For 120 pills, each con- taining ^ gr. 5. (PlVULM HTDEAEGTEl BICHLOEIDI CUM otTAiACO. Dupnytren.) Prep. Perchloride of mercury in subtle powder, 3 gr. ; extract of opium, 6 gr. ; extract of guaiacum, 12 gr. Make into 20 pills. Obs. The above formulse are among those most usually employed. Other authorities order pills containing .^th of a gr. Dzondi orders ^\; gr., and Hufeland only jL gr., in each pill. The commencing dose should not exceed 1 pill containing the ^ ot a grain, twice or thrice a day. It may afterwards be safely kept at ^th of a grain. They are chiefly em- ployed in syphilis, but are also occasionally exhibited with great advantage in glandular PILLS 1307 indurations and enlargements, and in cancer ; due caution being observed. Pills, Coagh. See PiiLS, Pectobal, Ex- PBOTOBANT, &C. Pills of Cre'aaote. Syn. Pilule cbeasoti, L. Prep. 1. (Pitsclittft.) Creasote, 6 gr. ; powdered henbane, 24 gr. ; conserve of hips, q. 1. For 2t pills. — Dote, 1 three timeii daily ; in sea-sicltness, the vomiting during preg- nancy, &c. 2. (llieche.) Crensote, 1 dr.; extract of liquorii'e and gum galbanum, of each i dr. ; powiIiTid miillow-root, 2 dr.; to be divided into 2-gr. pills. — Dote, 3 to 6, four times a day ; in acute rheumatism, bronchitis, ncu- rali;ia, phthisis, &c. Pills, Creapigny's. S e Pills, Dibneb. Pills of Cro'ton Oil. Sgn. PiluljE ceotonis, P. tiolii, L. Prep. 1. Croton oil, 3 drops ; oil of cloves, 4 drops ; bread-crum, q. s. For 3 pills, one of which is a dose. 2. (Ur Copland.) Croton oil, 6 drops; pill of aloes and myrrh, IJ ilr. ; soap, 20 gr. ; liquorice powder, q. s. For 30 pills. — Dose, 2 to 4. 3. (Dr Recce.) Croton oil, 6 drops ; Castile soap, J dr. ; oil of cuniway, 8 drops ; liquoiice powder, q. s. For 12 pills. — Dose, 1 to 3. In dropsy, visceral obstructions, &c. See CaoTON OIL. 4. (With MBRoniiY — Dr NcligNn.) Croton oil soap, 3 gr. ; exirnet of henbane and mer- curial pill, of each 24 gr. ; oil of pimento, 12 drops; divide into 12 pills. — Dose, 2 at bed- time. (See above.) Pills of Cy'anideof Mer'onry. Syn. VizxtLiE HTDUARQYHI OTANIDI, P. H. CTAHITBKTI, L. Prep, ((inibourt.) Cyiini Je of mercury, 6 (jr. ; opium, 13 gr. ; bread-crum, 60 gr. ; honey or syrup, q. a. For 96 pills. — Dose, 1 night and morning; in .syphilis, chronic iullamma- tion of the viscera, &c. Pills of Cyanide of Potas'sinm. Si/n. Pi- iVhM POTASSII CTANIDI, L. Prep. (Goliling Hird.) Cyanide of potassium, 2 gr. ; arrow- roiit, 20 gr. ; simple syrup, q. s. For 18 pills. — Dose, 1, twice or thrice a day ; as a sedative in hysteria, gastrodynia, extreme nervous excitability, &e. See Dbauqht and Mix- TUBE, HydBOCTANIO. Pills of Dandeli'on. See Pills, Taeaxa- cuu. Pills, De Haen's. Prep. (St Marie.) Gum ammoniacum and pill aloes with myrrh, of each 1 dr. ; extracts of hemlock and Castile soap, of each IJ dr. For 2-gr. pills.— Z>ose, 3 to 6 daily ; in painful Or obstructed men- sirnntion, chlorosis, &c. Pills of Del'phine. S^n. Pilfl.e bel- PHINI.E, U Prep. (DrTurnbuU.) Delphine, 1 gr. ; extracts of henbane and liquorice, of each 12 gr. For 12 pills.— Z>om, 1 to 3, twice n day j in dropsy, gout, rheumatism, &c., in- stead of veratrine. PiU», Deobstrnent. (I/. Ph., 1746.) Syn. PiLULS EcpHBAcriCA. Prep. Aromatic pill, 3 oz. ; rhubarb, 1 oz. ; extract of gentian, 1 oz. ; sulphate of iron, 1 oz. ; carbonate of potash, t oz. ; syrup of roses, q. s. Pills of Dento-iodide (Biniodide) of Mercury. Si/n. Pilul* hxdbauoybi DErro-iODiDi. (Magendie.) Prep. Deuto-iodide (biniodide) of Mercury, 7i gr.; extract of juniper, 75 gr.; powdered liquorice, q. b. for 100 pills. Fills, Diaphoret'ic. Syn. Pilule diapho- RETlca;, L. Prep. 1. Antimonial powder, i dr. ; opium, 10 gr. ; calomel, 5 pr. ; confec- tion of opium, q. 8. to mix; divide into 10 pills. — Dose, 1 at bedtime ; in coughs and bronchial irritability, after an aperient. 2. Guaiacum, 19 gr. ; emetic tartar and opium, of each 1 gr. ; simple syrup, q. s. to nii\ ; divide into Spills. — Dose, lto2, in acute rheumatism, &c. 3. Camphor and antimonial powder, of each i dr. ; opium, 10 gr. ; aromatic confection, q. e. to mix. For 12 pills. In fevers, and in some spasmodic diseases. — Dose, 1 pill. 4. Powdered guaiacum, 10 gr. ; compound powder of ipecacuanha, 5 gr. ; confection of roses, q. s. to mix ; for a dose. As a diapho- retic, in inflammatory afEectiona and rheu- matism. Pills, DiaTrhoe'a. Syn. Pilule: antidi- ABiiHtEALES, L. Prep. (Trousseau & Reveil.) Soft extract of opium, li gr. ; calomel and powdered ipecacuanha, of each 3 gr. ; conserve of hips, q. 8.; divide into 10 pills. — Doxe, 1, two or throe times daily; in chronic and chuleraic diarrhoea. Pills, Diges'tive. Under this bead are generally classed all the stomachic and milder aperient pills. See Pills, Bath ; Pills, DiNNEB, Ac. Pills of Digitaline. Syn. Pilulje dioi- TALIN.E, L. Prep. 1. IJigitaline, 1 gr. ; powdered sugar, i dr.; thick mncilape, q. s. For 24 pills. — Dose, 1 to 4 daily, watching the effects; as a sedative to reduce the tone of the circulation, in phthisis, enlargement of heart. &e. Sic Pills, Foxglove. Pills, Din'ner. Si/n. Pilule dict^; ante- ciBDJi, L. ; Grains DE SANTli, Fr. Prep. 1. Aloes, 1 dr. ; rhubarb and extract of gentian, of each i dr.; ipecacuanha and capsicum, of each 12 gr. ; syrup of ginger, q. s. to mix. For 3J-gr. pills. 2. (^Dr BaiUie's.) See oiore. 3. (Bath BiGESTiVE PILLS.) See aSorp. 4. (Pills oe aloes and mastic; Ladt Ceesfigny's pills, Lady Hesketh's p., Lady Webster's p., Digestive p.. Stomach p., P1HJI.K aloes et mastiches. P. a. cum MASTICHE, p. SIOMACBir^ MESUES; GbAINS DE VIE, GBAINS DE MESUES.) From aloes (pow- dered), 6 dr. ; powdered mastic and petals of red roses, of each 2 dr.; syrup of wormwood, q. 8. to form a pill-mass. For 3gr. pills. In small doses they excite the appetite; in larger ones tliey produce a bulky and ec pious eva- cuation. This is the formula of the old Paris 1308 PILLS Codex. Rhubarb is now frequently substi- tuted for the rose petals. 5. (Sir C. Bell's.) From sulphate of quinine, 4gr. ; mastic, 6 gr. ; rhubarb, 50 gr. ; syrup of orange peel, q. s. to mix. For 12 or, prefer- ably, 18 pills. 6. (Sir Chas. Clarke's.) From extract of chamomile, J dr. ; myrrh and rhubarb (in powder), of each 20 gr. ; powdered Socotrine aloes, 10 gr. ; oil of chamomile, 8 drops; mucilage, q. s. to form 20 pills. " These pills, which were originally prescribed by Sir Chas. Clarke, are much used in London." (Redwood.) 7. (Frank's.) From aloes and jalap, of each 4 parts ; rliubarb, 1 part; syrup of wormwood, q. s. For 3gr. pills. 8. (P. Cod.) Aloes, 6 dr. ; extract of cin- chona bark, 3 dr. ; cinnamon, 1 dr. ; syrup of wormwood, q. s. The do«e of the above is 3 to 5 gr., about an hour before dinner, to promote the appetite; or, ai a puigative, 10 to 15 gr. Pills, Dluret'ic. Syn. Pilulje diureticb, L. Frep. 1, From powdered foxglove, 12 gr. ; calomel, powdered squills, and opium, (if each 4 gr. ; conserve of hips, q. o. For 12 pills. 2. (Dr A. T. Thomson.) Mercurial pill, 1 dr.; powdered squills, 20 gr. ; coufection of roses, q. s. ; divided into 20 pills. The dose of either of the above is 1 pill, twice or thrice daily ; in dropsy, &c. Fills, Dixon's. According to Dr P.ir!s these pills consist of aloes, scammony, rhubarb, and a little tartar emetic, beaten up with syrup. ** The following formula produces a pill pre- cisely siuiiliir to this nostrum : — Take of com- pound extract of colocynth (Ph. L. 1836), 4 dr.; powdi-red rhubarb, 2 dr.; potassio- tartrate of antimony, 8 gr. ; syrup of buck- thorn, q. s. ; mix, and divide into 120 pills. Aperient and diaphoretic. — Dose, 2 or 3, at bedtime.'* (Cooley.) Although a nostrum it is really an excellent medicine, adapted for numerous case;*. Pills, Duchesne's. Prep. From aloes and gum ammouiacum, of each 30 gr. ; mastic and myri'h, 10 gr. ; carbonate of potassa and saffron, of each 3 gr. ; syrup, q. s. In the dyspepsia of hysterical patients, in engorge- ments of the abdominal viscera, following intermittent fevers, &c. Pills, Dys'entery. Syn. Pilul^e dtsekte- EIC^, L. Prep. Pure alumina and tannic acid, of each 20 gr. ; antimonial powder, 15 gr. ; castor oil, J dr. — Dose, 5 to 10 gr. ; fre- quently. Pills of Elate'rium. Syn. PiLui^ elate- BII, L. Prep. (Radius.) Elaterium, 6 gr. ; extract of gentian and Castile soap, of each 9 gr. ; mix, and divide in 12 pills. — Dose, 1 to 4 J in obstinate constipation, aud as a purge in dropsy, &c. Pills, Emet'ic. Syn. P1LITL.E EMETiOyE, P. CtrPRI SOLPHATIS COMPOSITiE, L. Prep. (Swediaur.) Sulphate of copper and ipeca- cuanha equal parts; syrup or conserve of roses, q. s. For 5-gr. pills. — Dose, 1 pill, repeated every 15 minutes, until vomiting comes on. See Emetics. Pills, Epilep'sy. Syn. Pilulje antepilep- TIC.E, P. AD epilepsiam, L. Frep. 1. (Griffith.) Powdered indigo, 75 gr. ; assa- foetida, 15 gr. ; Russian castor, 7 gr. ; mix, and divide the mass into 20 pills. — Dose, 1 every hour. 2. (Recamier.) Ox,ide of iron, 9 gr.; cam- phor and extract of belladonna, of each 6 gr. For 12 pills. — Dose, 1 to 3, every 3 or 4 hours. Pills, E/got of Eye. Syn. Pilule eb- GOT.E, P. SECALIS CORIfTJTI, L. Prep. 1. (Dewees.) Powdered ergot, J dr. ; extract of gentian, 1 dr.; divide into 15 pills. In ob- structed and painful menstruation, hsemor- rhages, &c. — Dose, 1 pill, thrice daily. 2. (L'.illemande.) Aloes, ergot, and rue, of each 8 gr. ; for 12 pills; As the last. Pills of Er'gotine. Syn. Pilttl^ EEO0Tiif.E, L. Frep. (Bonjean.) Ergotine (Bonjean's), 24 gr. ; liquorice powder, 40 gr. ; sy rtip, q. s. For 24 pills. — Dose, 3 to 6 daily ; as an in- ternal hajmostatic, &c. Pills, Everlast'ing. Syn. Perpetual pills , PiLULiE MTERTSM, P. PEEPETUjE, L. Small spheres of metallic antimony. They possess tile property of purging as often as swallowed, but have now long fallen into disuse. Pills, Expec'torant. Syn. Piluls expec- TORANTES, L. Prep. 1. Myrrh, IJ dr. ; powdered squills, ^ dr. ; extract of henbane, 2 dr. ; syrup, q. s. ; divide into 30 pills. — Dose, 2, night and morning. 2. (A. T. Thomson.) Powdered squills and extract of hemlock, of each ^ dr. ; ammoui- acum, IJ dr. ; divide into 30 pills. — Dose, 2 twice or thrice u day. In chronic coughs, asthma, &c., after an aperient. See Pills, Pectoral, &c. Pills of Extract of "Walnut Leaves. (Nes- rier.) Syn. Pilulze jdolandis. Prep. Ex- tract of walnut leaves, 1 dr. ; powdered wal- nut leaves, sufficient to form a mass ; to be divided into 20 pills, 2 or 3 to be taken in the day. Pills, Family Antibil'ions. Syn. Aloe pills ; ALOisS BOSATA, PlLUL^: ALOBS KOSAT^, L. Prep. Socotrine or hepatic aloes, 3 oz. ; juice of roses, 1 pint; dissolve by beat, strain through a piece of coarse flannel, evaporate to a proper consistence, and form it into pills. Purgative, in doses of 5 to 15 gr. Pills, Fe'ver. Syn. PiLtrL.E PEBRipuGa:, L. Of these the principal are those containing antimouials, bark, quinine, and salicine (which see). Pills, Fordyce's. An active purgative, closely resembling in composition the compound gam- boge pill of the Pli. L. Pills, Dr Fcthergill's. Prep. (Cooley ) Aloes, 4 dr.; extract of colocynth and scam- PILLS 1309 mony, of cnch 1 dr.; diaphoretic antimony, 30 gr. ; Bynip, q, s. For 3J-gr. pills. A dia- phoretic aperient. — Dose, 1 to 4 piUa at bed- time. Pills of Fox'glove and Hen'bane. Syn. Pi- LULJi DIOITALia ET HTOSCYAMF, L. Prep. (Ur A. I'. Thomson.) Powdered foxglove, 4 gr. i powdered camphor, 12 gr. ; extract of lienbiuio, 18 i,'r. For 6 pills— 2)o»e, 1 or 2 at bedtime ; as a sedative in maniacal and 8]>asmodic afTeitions, ic. Pills of Fox'glove and Sqnills. Sy». Pi- LtJUEDioiTALia KTSCILL* (Ph. E.), L. Prep. (Ph. E.) Powdered foxglove and squills, of each 1 part; aromatic electuary (Pli. K.), 2 parts ; consorvu of red roses, q. s. ; divide into 4-gr. pills. A valuable diuretic in dropsies. — Doae, 1 to 2 pills. Pills, Frankfort. These are the Pilules An- peliques noticed among PATENT MEDICINES, furnied into 2-^'r. pills, and silvered. Pills, Franks'. See Pills, Dinneb. Pills of Fuligoka'li. Si/n. Pilulji puli- OOKALI, L. Prep. (Deschaiups.) Fuligokiili, 6 dr. J stiircli, 2i dr. ; powdered tragncauth, 10 gr. ; syrup, q. s. For 100 pills, which must be covered with 2 or 3 coats of gum, and pre- served from the air. The pills of sulphuretted fuligokal (Pilulffl Fuligokali Sulphurati) are prepared in a similar manner. Pills, Fuller's. St/n. Bennet pills; Pilu- le benedict;e, L. Prep. (Cooloy.) Aloes and sulphate of iron, of each i dr.; myrrh and .'it'iina, of each 20 gr. ; nssafcetida and gal- li.iuum, of each 10 gr. ; mace and saffron, of each6gr. ; syrup, q.s.; mix and divide into 4-gr. pills. Antispasmodic, emmenagogue, and tonic, and slightly aperient. — Dose, 1 to 4, acciinling to tlio obji'ct in view. Fills, Gairthorn's Mild Provi"sioiial. Prep. (Coiiliy.) Compound gamboge pill, 60 gr. ; aqueous extract of aloes, 40 gr. ; sulphate of potassa and extract of senna, 30 gr.; compound scammony powder, 15 gr. ; balsam of Peru, 6 or 8 gr. ; emetic tartar, 3 gr. ; mix, and divide into 36 pills. Purgative. — Dose, 1,2, or more, vrhen required. Pills of Oalliannm (Componnd). Syn. Pi- LULA OALBANI COMPOSIIA (Ph. L.), PiLULiE o. COMPOSiTiE, L. Prep. 1. (Ph. L.) Myrrh and prepared siiLMpenum, of each 3 dr. ; prepared galbanum and soft soup, of each 2 dr. ; pre- pared assufoctida, 1 dr. ; treacle, q. s. to form a pill-mass. 2. (Ph. L. 1836.) As the last, omitting the soap. 3. (Ph. D. 1826.) As the Ph. L., except that troncic is substituted for syrup. Obs. These pilK are stimulant, expectorant, antispasmodic, and emmenugogue. — Dose, 10 to 20 gr. ; in hysteria, chrouic coughs, chlo- rosis, anienorrlneM, &c. Pills of Oalbanmn with Iron, Syn. Pilule OALBANI CUM FEKRO, L. Prep. (Ouy's IIo-p.) Compound galbanum pill, 2 parts ; precipi- t.ited sesqiiicixide of iron, 1 part; water, q. ». to form a mass. For 4i-gr. pills. An excel- lent tonic emmenagogue. — Dose, 10 to 20 gr. ; iu chlorosis, amenorrhoea,&c., when chalybeates are not contra-indicated. Fills of Gam'boge (Componnd). Sgn. Gam- boge pills, Fobdtce's p. ; Pilule cam- B091« COMPOSITA (Ph. L.), P. CAMBOQl* (Ph. E.), L. Prep. 1. (Ph. L.) Po^.lered Soco- triue or hepatic aloes, 3 dr. ; powdered gam- boge, 2 dr..; powdered ginger, 1 dr.; soft soap (Ph. L.), 4 dr.; mix, and beat them to a pill- mass. The formula) of the Ph. L. 1836 and Ph. D. 1826 are precisely similar. 2. (Ph. E.) Uamboge, East Indian or Bur- hadoes aloes, and aromatic powder, of each (iu powder) 1 part; Castile so.ip, 2 parts; syrup, q. s. Obs. All the above are active cathartics. — Dose, 6 to 15 gr., at bedtime ; in obstinate constipation, &c. Pills of Qen'tian (Componnd). S/in. Pilulje OENTIAN,KOOM10SIT^, L. Prep. (W. Cooley.) Extract of gentian, 1 dr. ; powdered rhuharh and cardamoms, of each ^ dr.; ipecacuanh:!, 12 gr. For 3-gr. pills. Stomachic. — Dose, 2 or 3, twice or thrice daily, to improve the appetite and digestion. Pills, Gout. Slin. I'lLULaiANTABTlIKlTICE, L. Prep. 1. (Bouchardat.) Extract of eol- chicum and compound extract of cotoeynih, of each 1 dr. ; aqueous extract of opium, 3 gr. ; mix, and divide into 3-gr. pills. — Dose, 1 or 2, according to their purgative action, us required. 2. (Sir H. Halford's.) Prom acetic extract of colchicum, J dr. ; Dover's powder and com- pound extract of colocynth, of each 18 gr. For 12 \>\\\a.—Dose, 1 pill. 3. (Lartigue's.) From compound extract of colocynth, 20 gr. ; alcoholic extract of colehi- cum seeds and alcoholic exti'aet of digitalis, of each 1 gr. For 2-gr. pills. — Dose, tfc. As the last. 4. (St George's Hosp.) Acetic extract of colchicum, 12 gr. ; Dover's powder, 30 gr. For 12 pills. — Dose, 2 pills. 5. (Sir C. Scudaniore's.) From acetic ex- tniet of colchicum, 1 dr.; powdered marsh- mallow root, q.s. to form a mass. I'or 40 pills. — Dose, 1 to 3, or more, with caution, as required. 6. (Trousseau & Reveil.) Powdered colchi- cum seeds, \ dr.; powdered digitalis and sul- phate of quinine, of each 15 gr. ; calomel and extract of colocynth, of each 8 gr. ; syrup, q. s. For 20 pills. — Dose, 1 to 4, during the diiy, at the commencement of an attnek of gout. Other furmulie for gout pills will be found under the respective names. Pills, Dr Griffith's. Powdered rhubarb, 1\ dr.; sulphate of iron, i dr.; Castile soap, 40 gr. ; water, q. s. to form a mass. For -48 pills. An excellent remedy in costiveness, with loss of tone of the bowels. — Dose, 2 to 4, at bedtime. Pills, of Gu'aiacum (Componnd.) Syn. PiLtJ- 1310 PILLS la; GFAIACI COMPOSlTiE, L. Prep. 1. Pow- dered resin of guaiacum, 1 dr. ; oxysulphide of antimony, 40 gr. ; oil of cajeput, 12 drops; extract of gentian, q. s. to form a mass. For 4-gr. pills. — Dose, 3 to 6, thrice dally ; in gout, rheumatism, secondary syphilis, various obstinate cutaneous affections, &c. 2. (St B. Hosp.) Guaiacum, 30 gr. j Ipeca- cuanha and opium, of each 3 gr. ; syrup, q. s. For 12 pills. — Dose, 1 to 3. As the last. Pills, Halford's. See Pills, Gout. Pills, Dr Hamilton's. The same as the colo- cynth and henbane pill of the Ph. E. The compound pills of gamboge, now vended under the title of 'Mobison's No. 2 Pills,' were long known in Scotland as Dr Hamilton's Pills. Pill's, Head'aohe. Syn. Cephalic pills j Pilule cephalic^, P. ANTicEPnALALOic^, L. Prep. 1. Caffeine, 15 gr. ; aloes, 20 gr. ; conserve of hips, q. s. For 12 pills. — Dose, occasionally ; when only one side of the head is affected. 2. (Bioussais.) Extract of opium, 6 gr. ; extracts of belladonna and henbane, of each 15 gr. J extract of lettuce, 30 gr. ; butter of caciio, 4 dr. For 120 pills. — Dose, 1, twice or thrice diiily; in headache, accompanying spasmodic affections, &c. 3. (Dr Wilson Philip.) Powdered nutmeg and rhubarb, of each 20 gr. ; extract of cha- momile, 20 gr. ; oil of peppermint, 10 or 12 drops. For 30 pills. — Dose, 1 to 3, thrice daily; in nervous headaches. Pills, Helvetius's. %». Pilul^e aluminis Helvetii, L. Prep. Alum, 2 dr. ; dragon's blood, 1 dr. ; honey of roses, to mix. For 48 pills. Astringent. Pills of Hem'lock (Compound). Syn. Vylvlm CONII COMPOSITA (B. P., Ph. L.), L. Prep. (Ph. L.) Extract of hemlock, 5 dr.; pow- dered ipecacuanha, 1 dr. ; treacle, q. s. Anti- spasmodic, expectorant, and narcotic. — Dose, 4 to 8 gr (B. P. 5 to 10 gr.), twice or thrice daily ; in hooping-cough, bronchitis, incipient phthisis, &c. Pills of Henbane (Compound). Syn. Pilul^e HYOSCYAMt ET ZINCI, L. ; PlLULES DE MeS- LIN, Fr. Prep. (P. Cod.) Extracts of henbane and Valerian, and oxide of zinc, equal parts. For 3-gr. pills. — Dose, 1 to 10 ; as au anodyne or sedative in neuralgia, nervous attacks, &c. Pills, Lady Hesketh's. See Pills, Uinnek. Pills, Hoffmann's. See Pills op Cobrosive sublimate. Pills, Holloway's. See Patent medicines. Pills, Hooper's Female. Prep. 1. (Gray.) Sulphate of iron and water, of each 8 oz. ; dissolve, add, Barbadoes aloes, 25 lbs.; white canella, 6 oz. ; myrrh, 2 oz. ; opopanax, 1 oz. 2. (Phil. Coll. of Pharm.) Barbadoes aloes, 8 oz. ; dried sulphate of iron, 2i oz. ; myrrh, extract of black hellebore, and Castile soap, of each 2 oz. ; canella and ginger, of each 1 oz. ; water, q. s. ; divide the mass into 2^- or 3-gr. pills, and put 40 in each box. Cathartic and emmenagogue. — Dose, 2, or more. " If we omit the soap, lessen the quantity of extract of hellebore, and increase that of the aloes, we think the form will be nearer that of the original." (Cooley.) Pills of Honnd's-tongne. (P. Cod.) Syn. PILUL.E CUM CTN0GL0SS6. Prep. Eoot-bark of hound's-tongue, 4 dr. ; henbane seeds, 4 dr. ; extract of opium, 4 dr. ; myrrh, 6 dr. ; oli- banum, 4 dr. and 48 gr. ; saffron, 96 gr. ; castor, 96 gr. ; syrup of honey, 14 dr. Mix. Contains 1 gr. of extract of opium in 10 gr. The original form of nicolans contained styrax, and seems to have been the origin of the compound styrax pill, as well as of this compound. Pills, Hnmphrey'B. See Pills, Pectoeai,. Pills, Hunter's. See Pills, Renal. Pills, Hydragogne. See Bontius's pills, &c. Pills, Hydropho'bia. Syn. PiLUL.aE ad ba- BiEM, L. Prep. (Werlhoff.) Cantharides (in very fine powder), ^ gr. ; belladonna and calo- mel, of each 4 gr. ; camphor, 8 gr. ; muci- lage, q. s. For 12 pills. — Dose, 2 to 3, twice daily. Pills of latropha. (DrBarham.) Syn. Pi- LUL.S) Iateoph^:. Prep. Decorticated seeds of Jatropha gossypifoli, 3 dr. ; gamboge, ex- tract of colocynth and scammony, of each 1 dr. Make into 90 pills. — Dose, 1, 2, or more. Pills of In'dian Hemp. Syn. PiLULiE can- nabis Indict, L. Prep. From alcoholic ex- tract of Indian hemp, J dr.; sugar of milk, 1 dr. ; mucilage, q. s. For 48 pills. An ex- cellent pill for soothing pain and quieting the system, acting without causing headache or constipation of the bowels. — Dose, 1 pill, in- creased to 2 or more, as necessary. Pills of In'digo. See Pills, Epilepsy. Pills of I'odide of Arsenic. Syn. Pilulje ABSENioi lODiDi, L. Prep. 1. ( Dr Neligan.) Iodide of arsenic, 2 gr. ; manna, 40 gr. ; mucilage, q. s. ; mix, and divide into 12 pills. 2. (Gardner.) Iodide of arsenic, 1 gr. j extract of hemlock, 20 gr. For 20 pills. — Dose, 1 pill, twice or thrice daily ; in lepra, psoriasis, and some other scaly skin diseases. Pills of lodideof Iron. Syn. PiLUL.a; fekui lODiDi, L. Prep. 1. Unoxidised iron filings (recently levigated), 20 gr. ; iodine, 40 gr. ; distilled water, ^ dr. ; mix in a cold wedg- wood-ware mortar, and triturate them together until the red colour of the mixture has en- tirely disappeared; then add, of powdered gum, 20 gr. ; powdered sugar, 1 dr. ; liquorice pow- der, q. s. to form a mass, and divide it into 48 pills. Each pill contains 1 gr. of dry iodide of iron. — Dose, 1 to 6 pills, twice or ihrice a day. 2. (B. P.) Fine iron wire, 40 gr. ; iodine, 80 gr. ; rtflned sugar, in powder, 70 gr. ; liquorice root, in povfder, 140 gr. ; distilled water, 50 minims. Agitate the iron with the iooine and the water in a strong stoppered ounce phial until the froth becomes white. PILLS 1311 Ponr the fluid upon the sugar in a mortar, triturate brisklv, and gradually add the liquorice. — Doi«, 3 to 8 gr. 3. (Ph. U. S.) Protosulphate of iron, 60 gr. ; iodide of potnuium, 80 gr. (both in fine powder) ; mix, add of powdered traga- canth, 10 gr. ; powdered sugar, 30 gr. ; and form tlie whole into a mass with syrup, q. s. For 40 pill'i. Euch pill contains nearly 2 gr. of the dry iodide, or about 2^ gr. of the common hydrated iodide of the shops. — Dose, 1 to 3, as the last. Obs. 'I he above pills are reputed alterative, tonic, nnrt emmenagogue, and are found pecu- liiirly UKcful in indurations, scrofula, chlorosis, leucorrhoea, &c., when the administration of chalybeates is not contra-indicated. Pills of Iodide of Lead. %n. VihVLS PLUMUi lODiui, L. Prep. Prom iodide of leud, 16 gr. ; powdered sugar, 1^ dr. ; muei- Ingp, q. s. For 60 pills. — Dote, 1 pill, gra- dually increased to 3, or more, twice a diiy ; in scrofuln, sciri Iiuh, &c. Pills of Iodide of Mer'cnry. Sy». Pilule nTmuuoYEi lODiDi, L. Prep. 1. (Ph. L. 1836.) Qiecn iodide of mei'cury and pow- dered ginger, of t*arh 1 dr. ; conserve of hips, 3 dr. — Duxe, 2 to 5 gr., twice or thrice daily, as an allcrutive in scrofula and scrofulous syphilis, &c, li. (Coindkt'8 Pills.) From green iodide of mercury, 1 gr. ; extract of liquorice, 20 gr. ; mix, and divide into 8 pills. — Doee, 2 to 4, a^i the last. Pills of red iodide of mercury are uiiide in the siime way, but, owing to its j:ru;\ter activity, only one fourth of tlie above quantity of iodide must enter into their com- position. Fills of Iodide of Potas'sinm. S^n. Pilule POTASSII lODiDl, L. Prep. 1. Iodide of potassium and powdered starch, of each i dr. ; conserve of hips, q. s. For 36 pills. — Dose, 1 to 6, thrice diiily ; in glandular indurations and enlargements, goiture, scrofula, &c. 2. (\\>)ft..) Iodide of potassium, 15 gr. ; burnt sponge and extract of duleamarn, of each 5 dr. ; Wiiter, q. s. For 180 pills. — Dose, 1 1" 6, twice a day, as the last. Pills of I'odine. Si/n. Pilule: iodinii, L. Prep. (Radius.) Iodine, 6 gr. ; extract of gentian, 1 dr. j powdered gnni, q. s. For 24 pills. — Dose, 1 to 3 ; in scrofula, iScc. ; also, in mercurial and scorbutic salivation. Pills of Iodide of Silver. iSyi». Pilvlm ae- OKNTI lODIUI. (Dr Patterson.) Prep. Iodide of silver, nitrate of potash, of each 10 gr., rub together iiiio a vei-y fine powder, and add, liquorice powder, i dr. j white sugar, 20 gr. ; mucilage, q. s. ; to form a mass, to be divided into 40 pills ; 1 three times a day. Pills of lod'oform. Si/n. Pilttl.^: iodo- FOBUi, L. Prep. (Bouchardat.) lodiform, t dr. J extract of wormwood (or gentian). 1 dr. ; mix, and divide into 36 pills. — Dose, 1, t« iee (ir thrice daily ; in scrofula, &c. Fills of Ipecac'aaiiha (Compound). Sj/n. Pills op ipecacttakha with SQrii-L.s, P. of I. AND OPIUM ; Pilule iPECACDASH.fi cuit SCILLA (Ph. L.), P. IPECACUANHiE ET OPH (Ph. E.), L. Prep. 1. (Ph. L.) (.ompound powder of ipecacuanha (Dover's powder), 3 dr. ; powdered aramoniacum and squills (freshly powdered), of each 1 dr. ; treacle, q. s. to form a pill-mass. Anodyne, sudorific, and expecto- rant. — Dose, 5 to 10 gr. ; in chronic coughs and asthma, &c. 2. (Ph. E.) Dover's powder, 3 parts; con- serve of red roses, 1 part; mix, and divide into 4-gr. pills. R«-embles Dover's powder in its effects. It is hence regarded by many as a useless preparation. 3. {B. P.) PlLULA IPECACrANHS CUM SciLLA. Prep. Compound ipecacuanha pow- 'leT-, 3 oz. ; fresh-dried squill, 1 oz. ; animonia- cum in powder, 1 oz. ; treacle, q. o. Hiat all tocelher. — Dose, 5 to 10 gr. Pills of I'ron (Compound). Si/n. PiluljK PEREI COMPOSITA (Ph.L.), P. F. CUM WYIIURM, L. Prep. (Ph. L.) Myrrh (in powder), 2 dr. ; carbonate of soda, 1 dr. ; rub tlieni together iu a warm mortar, then add of sulphate of iron, 1 dr., and again triturate; lastly, add of treacle, 1 dr., and beat all together, to form a pill mass. An excellent mild clialybeate tonic and emmenagogue, similar in its properties to ' GriHith's Mixture.' — Dose, 6 to 15 gr., two or three times a day. Fills, Italian Black. Sgn. Pilule Italics NIOn.E, P. ALOETIca; FEBKATJE, h. Prep. (Ph. Bor.) Powdered aloes and dried sulphate of iron, equal parts; beaten up with rectified spirit, q. s., and divided into 2- or -J-gr. pills. See Pills of Aloes and laoN. Pills of Jal'ap. Si/n. PiLULJi; jalap.*;, L. Prep. 1. (Ph. E. 1783.) Extra.t of jalap, :i dr.; aromatic powder, 1 ilr. ; syrup, q. >. 2. (Ph. Bor.) Soap of jalap, 3 parts ; pow- dered jiilap, 1 part; beat them to a pill-mass. — Dose (of either), 10 to 15 gr. Pills, James's Analep'tic. Prep. 1. Anti- monial powder, guaiacum, and pill of aloes with myrrh, equal parts; syrup, q. s. 2. (Cooley.) Autiraonial powder (James's), pill aloes with myrrh, and compound aloes powder, of each 2 parts ; powdered ammo- niacuui, 1 part; beaten up with tincture of castor, q. s., and divided into 3J-).'r. pills. A diaiihoretic purge. — Dose, 2 to 4 pills. Pills, Dr J. Johnson's. Prep. From com- pouud extract of colocynth, 2 dr.; calomel, i dr. ; potassio-tartrate of antimony, 2 gr. ; oil of cassia, 12 drops. For 4 dozen pills. An excellent alterative and diaphoretic aperient. — Dose, 1 to 3 pills. Pills, Kaye's. See Pills, Wobshell's. Pills, Keyser's. Prep. (Guibourt.) Red oxide of mercury, IJ oz. ; distilled vineftar (dilute acetic acid), 1 pint; dissolve, add to the resulting solution manna, 2 lbs., and triturate for a long time before the fire, until a proper consistence is attained; lastly, divide the mass iuto pills of l.i j.'r. each. 1312 PILLS Ols. Keyser's pills were once celebrated tbroughout Europe as a remedy possessing extraordinary virtue, and so highly were they prized that the method of preparing them was purchased by the French Government for the benefit of the nation. Richard, who first pub- lished a full account of them, concludes by ob- serving that he considers this compound to be, without exception, the most effectual remedy for syphilis hitherto discovered. In this coun- try, however, it has long sunk into compara- tive disuse with the faculty ; probably from pills of acetate of suboxide of mercury being erroneously employed under the name, whereas, according to Robiquet, acetate of protoxide of mercury (called by him the * peroxide *) forms the basis of the original preparation. The dose is 1 to 2, night and morning, as an altera- tive; and 2 to 6, twice a day, as a sialo- gogue. Pills, King's. See Patent medicines. Pills, Kitchener's. Syn. Dr Kitcheneb's PERISTALTIC PEESUADEB3 ; PlLUL^ EHiEI ET CAEUi, L. Prep. From powdered Turkey rhubarb, 2 dr.; simple syrup, 1 dr.; oil of caraway, 10 or 12 drops. For 40 pills. An admirable stomachic, dinner, or laxative pill, according to the quantity taken. — Dose, 2 to 6. " From 2 to 4 will gene?-ally produce one addi- tional motion within 12 hours. The best time to take them is early in the morning." Pills, Klein's. Prep. From anjmonisicQm and extract of centaury, of each i dr. ; Castile soap, 1 dr. ; oil of amber, 3 drops. For 2gr. pills. Stomachic, eramcuagogue, and pectoral. — Dose, 2 to 6 pills. Pills of Lac'tate of Iron. Syn. Pilulj! FEEBi lACTATis, L. Prep. (Cap.) Lactate of protoxide of iron and powdered marshmallow root, equal parts; clarified honey, q. s. For 3-gr. pills. One of the most valuable of the chalybeates. — Dose, 1 to 2, three or four times a day. Pills of Lax;tnca"rium. Syn. Pilule iac- TUCAEII, L. Prep. 1. (Brera.) Lactucarium, 18 gr. ; conserve of elder-berries and extract of liquorice, of each q. s. For 12 pills. — Dose, 1 to 2 pills, every three or four hours ; in dry asthma, obstinate coughs without ex- pectoration, &c. 2. (Dr Duncan.) Lactucarium, 12 gr. ; liquorice powder, 20 gr. ; simple syrup, q. s. For 12 pills. — Dose, 1 to 2 pills, every hour, as an anodyne, or to induce sleep. Pills, Lartigne's. See Pills, Goitt. Pills of Lead. Prep. 1. See Pills op Acetate oe Lead. 2. (Opiated; PiLULffi PLTTMBi opiATiE — Ph. E.; PlLULA PLUMBI CUM OPIO — B. P.) Acetate of lead, 6 parts j opium, 1 part ; con- serve of red roses, about 1 part ; beat them to a proper mass, and divide this into 4-gr. pills. " This pill may also be made with twice the quantity of opium." In haemor- rhages, obstinate diarrhoea, dysentery, spitting of blood, and other cases demanding the use of a powerful astringent. It has also been highly extolled in cholera. — Dose, 1 to 3 pills, twice or thrice daily, washed down with water soured with pure vinegar. Pills, lee's Antibil'ions. Prep. ('Amer. Journ.of Pharm.') Aloes, 12 oz. ; scammony, 6 oz. ; calomel, 5 oz. ; gamboge, 4 oz. ; jalap, 3 oz. ; Castile soap and syrup of buckthorn, of each 1 oz. ; mucilage, 7 oz. ; beat them together, and divide the mxss into 5-gr. pills. A powerful cathartic, and, from containing mercury, not adapted for frequent use. See Wtndham's pills. Pills, lewis's Al'terative and Liver. These " for the most part resemble Scott's bilious AND LITEE PILLS. They are, however, of a more drastic and powerful character, and fre- quently operate with considerable violence." Pills, Lockstadfs. Prep. (Phoebus.) Sul- phate of quinine, 3 gr. ; aromatic powder, 10 gr. ; essential oil of almonds, 1 drop; extract of gentian, q. s. For 10 pills. — Dose, 1 to 2, thrice daily, as a stomachic tonic ; or the whole at once, before an expected attack of an ague or intermittent. puis, lockyer's. Prep. From panacea of antimony, 6 gr. ; powdered white sugar, 4 dr.; mucilage, q. s. For 48 pills. Cathartic and emetic. — Dose, 1 to 4 pills. Pills of Lnpulin. (Magendie.) Syn. Vi- LULa; LUPULINI. Prep. The powder tritu- rated forms a sufficiently tenacious mass for pills, without any addition. Pills, Dr Lynn's. Prep. Prom pill of aloes with myrrh andcompound extractof colocynth, of each 1 dr. ; calomel, J dr. For 4 dozen pills. Aperient and antibilious. — Dose, 1 to 3 ; in costiveness, biliousness, &e. Pills of Manganese, Carbonate. (Hannon.) Syn. P1LUL.I: MANQ-ANESII CAEBONATIS. Prep. Dissolve separately, 17 oz. of crystal- lised sulphate of manganese, and 19 oz. car- bonate of soda, in water, q. s. Mix the solu- tions and add to every 17 oz. of tlie liquid, 1 oz. of syrup, and allow the precipitate to subside in a well-closed bottle. Pour off the supernatant liquid, wash the precipitate with sugared water, express, mix it with 10 oz. of honey, and evaporate rapidly to a pill consis- tence. — Dose, from 4 to 10 4-grain pilla daily, in ansemia, chlorosis, &c. Pills of Manganese, Iodide. (Hannon.) Syn. Pilule manqanesii iodidi. Prep. Iodide of potassium, 1 oz. ; dried sulphate of manganese, 1 oz. ; mix with honey, q. s. to form a pill mass; divide into 4-gr. pills.— Dose. From 1 pill daily, gradually increased. Pills of Manganese, Malate. (Hannon.) Syn. Pilule mak&anesii malatis. Malate of manganese, 15 gr. ; powdered cinchona bark, 15 gr. ; honey, q. s. for 20 pills. 3 to 5 or 6 daily. Pills of Manganese, Muriate. (Niemann.) Syn. PlLULJJ MANGANBSII MUBIATIS. Prep. Chloride of manganese, 2 scruples; gum Arabic, 2 scruples ; liquorice, 1 scruple. Mix. PILLS 1313 FilU of Uanganese, Phosphate. (Hannon.) Sy/I. Prt,CL* MANOANE8II PHOSPnATIS. Prep. Phosphttte oF inttngnnese, \\ dr.; cinchonu bark, J dr. ; syrup of catecliu, q. ». Hake into 4-gr. pills. Fills of Manganese, Tartrate. Si/n. Pit.ulx MAMOANESH TAETBATI8. As Pills of Miilate Mani^aneso. Fills of Manganese and Sulphate of Iron. (Hnnnon.) Si/n. ViLVLM manoanesii kt FEBEi suLPHATia. I'rep. Sulphate of iron, 13 oz. ; sulphate of manganese, 3^ oz. ; car- bonate of soda, 17i oz. ; honey, 10 oz. ; syrup, q. 8. to make a mass to be divided into 4-gr. pills. Pills, Mar'tial. Si/n. Pills op ikon and WOBMWOOD; I'lLULa: fekbi oitm absinthio, P. MABTiALKH, L. Frep. (Sydenham.) Levi- gated iivin filings, 1 dr.; extract of wormwood, q. s. Tonic and hsematinic. — Doae, 5 to 10 gr., twiiM- a day. Pills, Matthew's. St/n. Pilt7L.£ MATTRiEi, P. PACiFiCiK, L. Prep. 1. (Dr Paris.) lilack hellebore, Castile soap, liquorice, opium, saHVon, and turmeric, equal parts; made into pills with oil of turpentine. 2. (Ph. E. 1741.) Opium and saffron, of each 1 dr. ; castor, 2 dr. ; soap of turpentine, 3 dr.; balsam of copiiiba (or oil of turpentine), q. s. to form a mass. Alterative and anodyne. — Doae, 3 to 10 gr. Fills, McKinsey's. See McKinsst's eata- POTIA, among Patent medicines. Fills, Meglin's. Si/n. Piltjlb8 db Meolin, Fr. Sou PiLM OP Henbane (Compound). Fills, Merca"rlal. Syn. Blue piu ; PiLtTLA IITDBARGYKI (B. P.), PlLUL^ HY- DBABOYRI (Pll. L.), PIHTL.E H. (Pll. E. i D.), p. meeopbiales, L. ; Pilules mbbch- niKLLES, Vr. Prep. 1. (Ph. L.) Jlenur.v, 4 dr. ; confection of roses, 6 dr. ; rub them together until globules can no longer bo seen ; then add of liquorice powder, 2 dr., and beat tlie whole together, so that a proper mass may be formed. 2. (I'h.E.) As the last; afterwards dividing tile mass into 5-gr. pills. 3. (Ph. D.) As the Ph. L. formula, but takinj,' four times the quantity of tlio respective ingredients. 4. (B. P.) Mercury, 2; confection of roses, 3; decorticated liquorice root, in fine powder, 1 ; rub the mercury with the confection of roses until metallic globules are no longer visible, then add the liquorice, and mi.\- the whole well together. — Dose, 3 to 6 gr. as an alterative, 10 gr. ns a purgative. Obs. Th.' remarks under 'Mbbciteial oint- JIKNT ' (p. 1179), for the most part, also apply here. Tliis pill, when properly prepared, pre- sents no globules of mercury when moderately rubbed on a piece of white paper, and imme- diately communicates a white stain to a piece of bright gold or copper. It possesses con- siderable density, and has a dark blue or slate colour. It euntains l-Srd of its weight of VOL. II. mercury, which may be ascertained from its ip. gr. ; or, more exactly, by au assay for the metal. It is the mildest and the most exten- sively used of all the mercurial preparations. — Dose. A< an alterative, 1 to 3 ttr. ; as a purgative, 10 to 15 gr. ; and as a sialogogne. 5 iir 6 gr., or more, twice or thrice daily. To prevent it affecting the bowels, it is commonly combined with either rhubarb or opium. A blue pill taken ovcr-niglit, and a black draught in the morning, is a popular remedy in bilious complaints. See Abee.sethv medi- cines. 5. (Collier.) Mercury, 2 dr.; sesquioxide of iron, 1 dr.; confection of red roses, 3 dr.; triturated, as before, until the globules disap- pear. An excellent extemporaneous substitute for the common mercurial pill. The addition of only a few grs. of the sesquioxide of iron to 1 oz. of conserve, renders the latter capable of rapidly killing a large quantity of quick- silver. (). (Tyson.) Grey oxide of mercury (pre- pared by decomposing calomel with liquor of potassa to which u little liquor of ammonia has been adiled), 2 dr.; confection of roses, 6 dr. ; powdered chamomiles, 1 dr. ; mix. As a substitute for the College pill. 7. (' Pharm. Journ.') Stearin, 1 dr.; rnb it in a warm mortar till it assumes the consist- ence of thick cream, then add of mercury, 4 dr., and again triturate until the globules di...- appear ; next further add, of coufection of roses and wheaten flour, of each 3 dr., pow- dered i^um, 1 dr., and form the wliole into a pill-ma.ss. As a substitute for the College pill. 8. (PlLCLi; HYDEAEOTEOSiE — P. Cod.) Mercury and honey, of each 6 dr. ; triturate till the globules are extinguished, then add of aloes, 6 dr. ; rlmbarb, 'A dr. ; scammony, 2 dr. ; black pepper, 1 dr. ; and make a pill-mnss as before. Contains l-4th part of quicksilver. Alterative and aperient. — Dose, 5 to 10 gr. BEt.LosTE'p, Babbaeossa's, Sedillot'b, and Mobelot's PILLS are nearly similar com- pounds. See Pills op Calomel and Coeeo- siVE sublimate, &e. 9. (PlLULS UNOTTENTI HYDEAEOTEI — Biett.) Prep. Mercurial ointment, powdered sarsaparilla, 1 dr. Mix, and divide into 48 pills. From 1 to 4 daily. 10. ('Pilule bYDEAEOYEi cum saponk — P. Cod.) Prep. Mercurial ointment, 2 dr. ; soap, 1 scruples ; liquorice powder, 2 scruples. Make into 3-gr. pills. Pills, Mercurial (Arabic). Syn. PiLULiE MEBOURIALES AeabiCE, L. Prep. Take of quicksilver and coi'rosive sublimate, of each i dr. ; triturate them patiently together until the globules disappear; then add, of agaric, pellitory, and senna, of each 1 dr. ; honey, q. 8. to make a pill-mass. For 3J-gr. pills. — Dose, 2 a day. Employed in the ' traitement arabique' for the cure of obstinate cutaneous diseases. 83 1314 PILLS Fills, HerciiriEil, Hahnemann's. (F. H.) Syn. PlLUia! HTDEAKGYKI HaHNEMANNI. Prep. Hahnemann's soluble mercury, 20 gr.; gum Arabic, 30 gr. j sugar, 30 gr. Mix, and divide into 30 pills. Fills, Mitchell's. Prep. Aloes, J dr. ; rhu- barb, 1 dr. ; calomel, 6 gr. j emetic tartar, 2 gr. For 36 pills. An alterative aperient. — Dose, 2 to 4 pills. Pills, Moat's. Similar to Moeisok's pills. Pills, Morison's. Prep. — a. (No. 1 Pills.) From aloes and cream of tartar, equal parts, made into a mass with either syrup or muci- lage. A mild aperient. b. (No. 2 pills.) From colocynth, 1 part ; gamboge, 2 parts ; aloes, 3 parts ; and cream of tartar, 4 parts ; made into a mass with sviup, as the last. An active purgative, often acting with great violence. Both No. 1 and No. 2 are divided into 3-gr. pills, of which 4 dozen are put into each Is. IJd. box. The proper dose of either is 1 to 3 or 4 pills; but they are often given by the Morisons in doses of 12, 20, 30, or even more, daily. For the history of these pills and their proprietors, see'Auat. of Quackery,' or 'Med. Circ.,' ii, 9—27. Pills of Mor'phia. Syn. PiLULai morphia, L. Prep. (Magendie.) Morphine, 1 gr. ; con- serve of roses (stiff), q. o. For 6 (or, better, 8) pills. — Dose, 1 pill; as an anodyne or soporific. Fills of Morphia (Compound). (Eougier.) Sun. PiLULjE MOBPHIiE COMPOSITE. Prep. Sulphate of morphia, 2 gr. ; cyanide of po- tassium, 4 gr.; mucilage, q. s. Make into 24 pills; 1 every six hours, in neuralgia. Pills, Moseley's. Prep. Finest Turkey rhu- barb, 60 gr. ; Jamaica ginger, 30 gr. ; sugar, 20 gr. (all in powder) ; tincture of rhubarb, q. s. to (orm a mass. For 4-gr. pills. A mild and excelleut medicine, closely resembling Kitchener's peeistaltic pekscaders. Fills of Musk. Syn. Pilule moschi, L. Prep. (Dupuytren.) Opium, 2 gr. ; musk (genuine), 8 gr. ; camphor (in powdi r), 24 gr. ; syrup, q. s. For 8 pills. Antispasmodic and stimulant. — Dose, 1 to 3, thrice daily, in low nervous affections; or the whole during the day in hospital gangrene, &c. Fills of Myrrh. See Pills op Aloes and Mykeh. r Pills, Hapier's Neuroton'ic. Of these, like Moeison's pills, there are No. 1 and No. 2. The first is a simple stomachic aperient; the other, a stimulant tonic. They both owe their sale and reputed virtues to extensive adver- tising. ('Anat. of Quackery.') Pills, Napoleon's. See Peotoeal Pills. Fills, Neuralg'ia. Hyn. Pilule antineu- BiLGICiE, L. Prep. 1. (Marchal De Calvi.) Aqueous extract of opium, 4 gr. ; sulphate of ■quinine, 16 gr..; powdered cinnamon, pow- dered orange leaves, and exti act of valerian, o! each 20 gr. ; syrup of belladonna, q. s. Por 3 dozen pills. — Dose, 1, hourly. 2. (Trousseau & Eeveil.) Extracts of opium and stramonium, of each 8 gr. ; oxide of zinc, 2 dr. ; syrup, q. s. For 40 pills. — Dose, 1, every two or three hours, gradually increased in frequency until there is some considerable disorder of vision, &c. Both of the above should be used with care. See Fills, Meg- lin's, &c. Fills of Hi'trate of Bismnth. Si/n. Vilvlm BISMHTHI TEiSNiTEATis, L. Prep. From trisnitrate ot bismuth and powdered rhu- barb, equal parts ; syrup of orange peel, q. s. to form a mass. For 3-gr. pills. — Dose, 1 to 2, every two hours; as a tonic, stomachic, and antispasmodic, in dyspepsia, debility, spasms, &c. Pills of Nitrate of Mercury. Sifn. PiLtrLJE HYDEAEGYEI PEOTO-NITEATIS. PiLULESDE Saintb Maeie. Prep. Powder of proto- nitrate of mercury, 7i gr. ; extract of li- quorice, i dr. Mix accurately, and divide into 60 pills. — Dose, 1, four times a day. Fills of Nitrate of Sil'ver. Syn. Pilul^e AEGENTI NITEATIS, L. Prep. 1. (St. B. Hosp.) Nitrate of silver (crystallised), 12 gr. ; liquorice powder, 24 gr. j treacle, q. s. For 12 pills. — Dose, 1 pill, twice or thrice a day ; in chi'onic epilepsy and some other spasmodic disorders. 2. (Dr A. T. Thomson.) Nitrate of silver, 6 gr. ; crum of bread, q. s. (say \ dr.); mix, and divide into 12 pills. — Dose, 1, every six hours. Obs. To prevent the blue or slate coloured tinge of the skin, sd often produced by the continued use of the salts of silver, 8 drops of diluted nitric acid in 1 fl. oz. of water should be taken after each pill. Pills, Norton's Chamomile. Prep. From aqueous extract of aloes, 1 dr. ; extract of gen- tian, 3 dr. ; mix, and drive off the excess of moisture by the heat of a water bath ; then add of essential oil of chamomiles, 20 drops, and divide the mass into 60 pills. To preserve their aromatic properties, they should he kept in a dry glass bottle or a well-covered earthen- ware pot. — Dose, 1, as a dinner pill; or 2, night and morning, as a stomachic tonic, (' Anat. of Quackery.') Pills of Nux Vom'ica. Syn. Vi-lvlm nuois voMicffi, L. Prep. 1. Nux vomica and aloes (both in powder), equal parts ; syrup, q. s. For 3-gr. pills. — Dose, 1 to 3, twice or thrice daily, carefully watching the effects; in ner- vous derangement, general debility, impotence, paralysis, &c. 2. Alcoholic extract of nux vomica, 1 part i powdered sugar, 2 parts; beaten up with rec- tified spirit, q. s. For 2i-gr. pills. — Dose, 1 to 2 ; as the last. 3. (Mondiere.) Alcoholic extract, 6 gr. ; levigated black oxide of iron, 1 dr. ; syrup, q. s. In atonic incontinence of urine, amenoirhoea, &c. Fills, Odontalgic. Syn. Pilules odontal- aiCM, L. Prep. (Ph. Bor.) Powdered opium PILLS 1315 and extract! of belladonna and lienbane, of each 10 gr. ; oil of olivet, 20 drops ; powdered pcllitory of Spain, i dr.; bent them to a mass, ■ml divide it into 1-gr. pills; keep them in a corked phial. Fills, Opiated Lead. See Pills of Leas. Pills of 0"pium. Si/n. Anodyne pills, NionT p.. Thebaic p. ; Pilols opii (Ph. U. S.), P. o. or THEBAIC* (Ph. E.), L. Prep. 1. (Pli. E. ) Opium and conserve of red roses, of each 1 piirt; sulphate of potash, 3 parts; rub tliem together to a proper mass, and divide into 5-gr. pills. — Dose. 1 to 2 |iill9, as an aiiocljno or soporific. Each pill contains 1 gr. of opium, or double the quantity in the same pill of the previous edition of t'ne Ph. E. 2. (Ph. U. S.) Powdered opium, 1 dr. ; Castile soap, 12 gr. ; water, q. s. For 60 pills. As the last. Fillsof Ox Qall. Si/a. Bile pill; Piltjl* PKi.i.is BOVINI, P. BILIS, L. Prep. 1. From inspissated ox-gall formed into pills by the addition of any simple powder ; or the harder I'xtract beaten up with u little proof spirit. Powdered rhubarb is frequently used for the purpose. For 3-gr. pills. — Dose, 1 to 6 ; for coDitipution, flatulence, &c., arising from a defiriency of bile. 2. (Compound.) From inspissiited ox-gnll, 1 dr. ; powdered rhubarb, 4 dr. ; powdered ipecacuanha and capsicum, of each 15 gr. ; oil of cai-nw.'iy, 12 drops. For 48 pills. — Dose, 1 to 4; in loss of appetite and dyspepsia, with torpor of the bowels, &c. See Constipation, Gall, &c. Pills of Ox'ide of Gold. Si/n. Pilule; aubi OXYDi, L. Prep, (Magoiidie.) 'i'eioxide of gold, 6 gr. ; extract of mezureon, 2 dr. ; mix, and divide into 60 pills. Each pill contains ■J*! jfr. of teroxide. — Dose, 1 to 3 ; in scrofula, syphilis, malignant fevirs, &c. Pills of Oxide of Mercury. See Fills, Heucobial. Pills ofOnde of Sil'ver. Sj/n. Pilui..e ab- GKNTI OXYDI, L. Prep. From oxide of silver, t; gr. ; powdered rhubarb mid extract of gen- tiiiii, of each 12 gr. For 1 dozen pills. — Dose, 1 pill, twice or tlirice daily ; in gastralgia, hiemuri'huges, nervous nffecti'in.s, &i:. Milder than the pills of nitrate of silvir. Fills of Oxide of Zinc. Sj/n. Pilvl^s zinci OXVUI, L. Prep. From oxide of zinc, pow- dund iMsiarilla, and conserve of hips, equal pirts. Fi)r 3.J-gr. pillj. Tonic and antispas- modic. — Dose, 1 to 3, thrice daily; in dys- j>e|i-ui, gastric or spasmodic coughs, epilepsy, choi' n, ^c. Pills, Parr's Life. Prep. Aloes, 7 lbs. ; rhu- barli ;ind jidap, of each 5 lbs. (.ill in pow- doi); cviract of gentian, 3J lbs.; soft soap, I lb. ; liijuorice powder, Ireacli', iiiid moist sug.ir, ot euL'h 4i lbs.; oil of cloves, 10 oz. ; oil of caiaway. 3i oz. ; mix, and bent the whole to a proper mass with syrup lii'ioins, q. a.. :iiid divide it into 3i-!,'r. pills. " Tbin' lire :ii>out;4 dozen in each Is. IJd. box, weigh- ing (dry) barely 3 gr. each." A good stoma- chic and aperient pill, but possessing none of the exti-aordinary virtnes ascribed to it by its proprietors. "('Med. Circ.,' ii, 146, 1G7, &c.) Pills of PauUin'ia. Si/n. Gpabaxa pills; PlLUL.aE OUAHAN.E, P. PAOLLINIJE, L. Prep. 1. Faullinia mixed op with syrup of orange peel, and the mass divided into 2i-gr. pills. — Dose, 2 to 8. 2. (Dr Gavrelle.) Extract of guarann, 1 dr. ; liqnorice powder, q. s. For 40 pills. — Dose, 3 to 6, daily. Obs. These pills are highly esteemed on the Continent as a tonic and astringent, in diseases of the bowels and bladder, in chlo- rosis, debility, &o. Fec'toral Pllle. %». Breath pills ; Pi- LUL7E PECTOEALES, L. Prep. 1. Compound squill pill, 1 dr. ; gum benzoin, ^ dr. ; pow- dered ipecacuanha and extract of henbane, of each 15 gr, ; syrup, q. s. For 3 gr. pills. — Dose, 2 to 4, three or four times a day ; in asthmas, cliroiiic bronchial atFections, coughs, &c. 2. (Dr Copland.) Camphor (in powder), 10 gr. ; ipec.icuanha, 15 gr. ; extract of hem- lock, 1 dr. — Dose, 3 to 6 gr. ; in irritating and spasmodic couphs, &c, 3. (Hajrgirt.) Powdered ipecacuanha and squills, of each t dr. ; acetate of morphia, 6 pi . ; Castile soap, 3 dr. ; mix, and divide into 72 pills. A most excellent medicine, at once aoothinpand expectorant. — Dose, 1 to 2, thrice a day, or of tener, 4. (HuMPHiiiES' Couon Pills.) From pow- dered ipecacuanh:i, 15 gr, ; compound squill- pill, 1 dr, ; compound extract ofcolocynth, i dr. For 3J-gr, pills. — Dose, 2 pills, nightand morning. 5. (Ur Latham.) Coinpnnnd powder of ipecacuanha, 1 dr. ; fresh squill and gutn am- moniacuni, of each 20 gr, ; calomel, 4 gr. For 20 pills. A most valuable pectoral and expectorant. — Dose, 1 pill, thrice daily; in bi'oiichitis, coughs, &c., after the more active iiitlatntnatory symptoms have subsided. 6. (Na|ioleon's.) From ipecacuanha, 30 gr.; squills and .iinmnniacum, of each 40 gr. (all in powder); muciliige, q, s. to mix. For 24 pills. It is siiid that this was a favourite renndy with the Emperor Napoleon I for diffiinity of breathing, bronchitis, and various affections of the organs of respiration. — Dose, 2 pills, ni'.'ht and morning. 7. (I^r Paris.) Powdered squills, J dr.; powdered myrrh, li dr. ; extract of henbane, 40 gr. ; wai,Lr (or simple suuu), q. s. to mix. For 4-gr. pills. — Dose, 2 pills, night and moriiinr. As X', 2. 8. (Ph. L. 1746.) Gum ammoniacum, 4 dr.; gain bciuoiii, 3 dr.; gumm\rrh. 2 dr.; satiron, 1 dr ; anisatLd bilsam of sulphur, i dr. ; s\rup of tolu, q. s. to mix, — Dose, 5 to 15 !zr.' 9. (Richter.) Assafoetida and valerian, of 1316 PILLS each i dr. ; castor, 15 gr. ; powdered squills and sesquicarbonate of ammonia, of each 8 gr. ; extract of aconite (alcoholic), 3 gr. For 4-gr. pills. — Dose, 1 to 3 pills, night and morn- ing ; in spasmodic affections of the respiratory organs. Pills, Perpet'ual. See Pills, Eveelastins. Pills, Peter's. Prep. (Cooley.) Aloes, 3 dr.; gamboge, jaiup, and scammony, of each 2 dr. (all in powder); calomel, 1 dr. ; beaten up with rectified spirit, q. a. A powerful cathartic. — Dose, 1 to 3 pills. Pills of Phosphorus. (B. P.) Si/n. Piittl^ Phosphoki. Prep. Phosphorus, 2 gr. ; bal- sam of tolu, 120 gr. ; yellow wax, 60 gr. Put the phosphorus and balsam into a wedgwood mortar half full of hot water, and when the phosphorus has melted and the balsam become sufficiently soft, rub them together beneath the surCace of the water until no particles of phosphorus are visible, the temperature of the water being maintained at or near 140° F. Add now the wax, and as it softens mix it thoroughly with the other ingredients. Allow the mass to cool without being exposed to the air, and keep it in a bottle immersed in cold water. It may be softened with a few drops of rectified spirit when made into pills. — Dose, 3 to 6 gr. Pills of Pip'erine. /Syn. Pilule pipekinje, L. Prep. From piperine, t dr. ; extract of cinchona, q. s. For 80 pills. — Dose, 1 pill, every two hours, during the intermission of an ague; also as an aphrodisiac and a remedy in piles. Pills of Pitch. St/n. Pilulje piois nigb^, L. Prep. From black pitch and powdered black pepper, equal parts ; beaten together in ii warm mortar, and divided into 4gr. pills. — Dose, 2 pills, night and morning ; in piles, &c. Pills, Pitschaft's Eocoprot'ic. Prep. From strained aloes and disulphate of quinine, equal parts; made into 2-gr. pills. A tonic and stomachic aperient. — Dose, 2 to 4, at bedtime ; in torpor of the large intestines, the dyspepsia of the debilitated, &c. Pills of Podophyllin. S^n. Pilulje podo- PHYLLINI. Prep. Kesin of podophyllin, ^ gr. Extract of henbane. To make one pill. One or two for a dose. Pills of Prussian Blue. (Jolly.) Si/n. PiLTJLK PEHBI PEEOYAHIDI COMPOSITA. Prep. Prussian blue, 18 gr. ; sulphate of quinine, 12 gr. ; extract of opium, 1 gr. ; conserve of roses, q. s. Mix, and make into 12 pills; 1 every three hours, in neuralgia. Pills, Plnmmer's. See Pills of Calomel (Compound). Pills, Pur'gative. Sun. Pilule PunaANTES, L. Prep. 1. (Dr Robinson.) Aqueous ex- tract of aloes, 1 dr. ; powdered scammony, J dr. ; balsam of Peru, 10 or 12 gr. ; oil of car- away, 9 or 10 drops ; mix, and divide into 30 pills. A warm, stimulating aperient, highly recommended to excite the peristaltic action of the bowels of the aged, sedentary, and debili- tated. — Dose, 1 to 4 pills, as required. 2. (Trousseau & Eeveil.) Eeain of jalap, 1 dr. ; scammony, J dr. ; extract of colocynth, 6 gr. ; excipient, as required. For 20 (or, better, 24) pills. — Dose, 1, " every two hours, in the morning, fasting, until they operate." For other formulas see Pills, Apeeient and Cathaetic, and Pills of Aloes, Jalap, COLOCTNTH, &c. Pills of ftninine'. See Pills of Sulphate OF Quinine. Pills, Eeece's. See Pills, Chieatta. Pills, Ee'nal. Syn. Pilulze eenales, L. Prep. 1. Squills, myrrh, and digitalis, of each (in powder) 10 gr. ; extract of rhubarb and mercurial pill, of each 15 gr. ; powdered nitre, 20 gr. ; oil of juniper, 10 or 12 drops. For 24 pills. Alterative, diuretic, and tonic. — Duse, 3 to 6, thrice a day. Hunter's Renal Purify- ing Pills are similar.but omitting the mercurial pill. Ue Roos' Renal Pills contain a prepara- tion of copaiba. Pills, Eheu'matism. Si/n. Pilule; anti- EHEUMATlCiE, L. Prep. 1. Gum guaiacum, 1 dr. ; nitrate of potassia, 1^ dr. (both in powder) ; soft soap (Ph. L.), i dr. ; oil of caje- put, 16 drops. For 4 dozen pills. — Dose, 2 to 6, night and morning; in chronic rheumatism, and rheumatic gout. Their action is accele- rated by the copious use of lemon juice during the day. 2. (Beasley.) Extract of artichoke, i dr. ; powdered sarsaparilln, 20 gr. ; oil of sassa- fras, 1 drop. For 12 pills. — Dose, 1 pill, thrice daily. Pills of Ehu'barh. Sv«. Pilule ehei (Ph. E.),L. Prep. 1. (Ph.E.) Powdered rhubarb, 9 parts ; acetate of potassa, 1 part ; conserve of red roses, 5 parts; mix, and divide into 5-gr. pills. A stomachic and gentle aperient, parti- cularly useful in atonic dyspepsia. —Dose, 2 to 4 pills. 2. (Ph. U. S.) Powdered rhubarb, 6 dr ; Castile soap, 2 dr. ; beaten up with water, q. s., and divide into 120 pills. As the last. Pills of Rhubarb (Compound). Syn. Aeo- MATic pills. Balsamic laxative p., Edin- EUEGH p.. Stomachic p. ; Pilula ehei com- posita (B. p.. Ph. L.), PiLULiE E. composite: (Ph. E. & D.), P. stomachicje, P. aeomatice, L. Prep. 1. (Ph. L.) Powdered rhubarb, 4 dr.; powdered Socotrine aloes, 3 dr.; pow- dered myrrh, 2 dr. ; soft soap (Ph. L.), J dr.; oil of caraway, 15 drops ; treacle, q. ». to form a mass. 2. (Ph. L. 1836.) Powdered rhubarb.l oz. ; aloes, 6 dr.; myrrh, 4 dr.; Castile soap, 1 dr.; oil of caraway, J fl. dr. ; syrup, q. s. 3. (Ph. E.) Powdered rhubarb, 12 parts ; aloes, 9 parts ; myrrh and Castile soap, of each 6 parts ; conserve of red roses, 5 parts ; oil of peppermint, 1 part; mix, and divide into 5-gr, pills. The oil of peppernjiut may be omitted, when so preferred. PILT-S 1317 4. (Ph. D.) Rhubarb, li 02. ; hepntic aloes, 9 dr.; myrrh and Castile Muip, of each in fine jiowdcr, 6 dr.; oil of pcppcnniut, 1 fl. dr.; treacle, 2 oz. ; mix, and beat the whole to a uniform mans. 5. (Ph. U. S. & Ph. E. 1817 ) Rlnibnrb, 8 dr. ; aloe», U dr. ; myrrli, 4 dr. ; oil o( pepper- mint, ) 11, dr.; Byrup of orange peel, q. B.; mix, and divide into 240 ]>ill8. (1. (B. P.) Uhuliarb, in fine powder, 3 oz.; .^^ocdtrine aloes, in fine powder (some physi- cians iirifer the aqueous extnict — Squire), 2i o?.. i myrrh, in fine powder, IJ oz. ; bard soap, 11 oz. ; English oil of peppermint, IJ dr. ; treacle, by weight, 4 oz. ; reduce the soap to line powder and triturate it with the rhubarb, aloes, aud niyi rli ; add the treacle and oil, and beat into :\ ui ass. — Doae, 5 to 1 gr. 06». The above are tonic, stomachic, and f;ently laxative ; extremely useful for obviating costiveness and giving tone to the stomach and bowels.— i>o*e, 6 or 8 to 20 gr. The Lon- don pill is not only the most agreeable, but it keeps the best. Fills of Bliubarb and Car'avray. See KncuKNKii'a Pebistaltio Peksuadees (Patent inedicineB), Fills of Khnbarb and Chamo'mile. Syn. Sl'KEDIMAN'8 riLLB ; I'lLULJE UIIHI ET ANTHE- Miuis, L. I'rijK From aloes, in \rrh, rhubarb (eiich in powder), and extriict of cliauiomile, of each 1 dr.; es»euti»l oil of chnmnmile, 10 or 1'2 drops. For 4-gr. pills. An excillent tonic and stomachic aperient, particularly useful in the ilyspepsia and loss of appetite of bard driuki rs. — Vose, 1 to 3 pills, eiiber before din- ner or at bedtime. Fills of Khabarb and Copai'ba. Syn. Vi- hVLB, KHIil ET OOPAID.E, P. U. BALSAMICJE, L. Prep, (Swediaur.) Powdered rliubiirb aud itiini. equal purls; balsam of enpaiba, q. s. Pills of Bhubarb and Gin'ger. Syn. Sto- IIAIII PILLS; PitrLJJ lUlEI ET ZINGIBEH13, L. Prep. From powdered rhubarb, 1 dr. ; powdered ginger, \ ilr. Castile soap, 20 gr. ; tincture or essence of gin;;er, q. a. to form a mass. For 30 pills. — Dose, 1 to 6. Fills of Rhubarb and Ipecac'uanha. Syn. PlLlL.K RHBI ET IPKOACUANHa;, L. Frep. Fjoui rhubarb, \ dr. ; ipei'acuanha, 15 gr. ; opium, 5 gr. (each in powder); oil of cin- namon, 6 drops ; syrup, q. ». For 18 pills. — Doxe. In loss of appetite and spasmodic dys- |>ep6ia, 1 to 3 pills, twice a day ; in dysentery, diarrhce I, &c., to relieve tormina and tenesmus, 1 every two hours. Pills of Rhubarb and I'ron. Syn. Filvue KHEI ET PEBRI (Ph. E.), L. Frep. (Ph. E.) Dried sulphate of iron, 4 parts ; extract of rhubarb, 10 parts; conserve of red roses, 5 piirts ; beat them to a proper mass, and 4'vide tliis into 5-gr. pills. — Dose, 2 to 4 pills ; in the atonic dys|)cpsia of debilitated subjects,, in cbliipsi-, &c. Fills of Ehabarb and Ox-gall. Syn. Pilule mihi ET FELLis DoviNi, L. Frep. From pow- dered rhubarb, gum ammoniacum, and inspis- sated ox-gall, equal parts ; beaten up with a little tincture of ginger or proof spirit, and the mass divided into 2i-gr. pills. In dyspepsia and constipation dependent on w tdrpid action of the liver. — Dose, 2 to 6 pills. Pills of Rhubarb and So'da. Syn. Pilule nilEI ET gOD£, P. E. COMP. CUM SODA, L. Frep. (Guy's Hosp.) Dried carbonate of soda, powdered rhubarb, and extract of gentian, equal parts. For 4j-gr. pills. — Dose, 2 to 4 pills ; in acidity, heartburn, diarrhcea, loss of appetite, &c. Pills, Richter's. See Pectoral pills. Fills, Dr Robinson's. See Pills, Pchoa- TIVE. Fills, Rudins's. Syn. liroirs's exieact; PiLULJ! EDDII, EXTEACTCM KUDU, L. Prep. 1. Colocynth pnlp, 6 dr. ; aguric, Idack helle- bore, and turpetlium root, of each 4 dr. ; cin- namon, mace, and cloves, of each 40 gr. ; rectified spirit, \ pint ; digest for 4 days, ex- press the tincture, and evajjoriite it to a proper consistenceformakingpills. Formerly esteemed one of the most safe and certain cathartics in troublesome constipation. — Dose, o to20gr. 2. (Ph. E. 17.S3.) Black hellebore and colo- cynth, of each 2 oz, ; water, 4 pints (o. w. m.) ; boil to a quart, strain, evaporate to the con- sistence of bnney, and add, of aloes, 2 oz. ; scammony (powdered), 1 oz. ; next remove the vis-el from the fire, and further add if sulphate of piitassa, 2 dr. ; oil of cloves, 1 dr. ; and form the whole into a pill-mass. Resembles the last (nearly). Fills, Rufus's. See PiiLS of Aloes with Myhbh, Fills of Sahadilla, Syn. Piliti; cevadille. Prep. Equal jiarts of subadiliii aud honey; make into 5-gr. pilN. — Dose. For an adult, 4 to 6 pills ; for a child, 1 to 2, Vermifuge, Fills of Saffron. Syn. Pilule ceooi, L. Prep. 1. From buy saffron, 1 dr. ; myrrh, \ dr. ; oil of cajeput, G drops; svrup of saffron, q. s. For 36 pills. — Dose, 1 to 3 or 4, occasionally ; as a stimulant in low spirits, hypochondriasis, &c. 2, (Phoebus,) Saffron, myrrli, and sulphur, equal parts ; inspissated bile, q, s. For 2-gr. pills, — Dose, 2 to 12 daily ; as an eminena- gogne. Pills of Sagape'num (Compound). Syn. Vi- LUL^SAGArENICOMPOSIT.E, L. Prep. (Ph. L. 1836.) Siigapenum, 1 oz. ; aloes, \ dr, ; syrup of ginger, q, s. — Dose, 5 to 20 gr. ; as a stimu- lant antispasmodic laxative, in dyspepsia with flatulence, flatulent colic, &c. Fills of Sal'icin. Syn. Pilul,e SALiciNiE, L. Prep. From salicin, \ dr. ; powdered rhu- barb, 20 gr. ; extract of gentian, q. s. to mix. For 4-gr. pills. — Dose, 2 to 4, every three hours, during the apvrexia of intermittents. Fills of Sandal Wood Oil. (Ebert.) Syn. Pilule olei santali. Prep. Oil of yellow sandal wood, i oz. ; yellow wax, i oz. Melt the wax into a capsule, and weigh into it the 1318 PILLS oil of sandal wood. Mix, and stir until cold, then roll out the mass and divide it into 80 pills, by means of the pill machine or pill-tite, in the same manner as in the ordinary mass, and sprinkle with marshmallow root powder. Each pill contains about 3 gr. or abont 5 drops of the oil. The excipient is unobjec- tionable, as it is readily soluble in the juices of the stomach. Pilla of Scam'mony (Compound). Syn. Pilule: soammonii composit.e, L. Frep. 1. (St. B. Hosp.) Scammony, 24 gr.; ginger, 20 f;r. ; aloes and gamboge, of each 12 gr. ; treacle, q. s. ; mix, and divide into 12 pills. A powerful cathartic and vermifuge. — Done, 1 to 3 pills. 2. (B. P.) Resin of scammony, resin of jalap, of each 1 oz. ; curd soap, in powder, 1 oz. ; strong tincture of ginger, 1 fl. oz. ; recti- fied spirit, 2 fl. oz. Add the tincture and spirit to the soap and resins, and dissolve by the aid of a gentle heat, then evaporate the spirit over a wattr-bath until the mass has a pilular consistence. — Dose, 5 gr. to 15 gr. Pills, Scot's. Prep. From aloes, 9 lbs. ; jalap, 3 lbs.; gamboge and ginger, of each \ lb.; beaten with treacle, q. b. See PiLis, Andeeson's Soot's. Pills, Dr Scott's Bil'ions and Liver. Prep. (Cooley.) Compound extract of colocynth (Ph. L. 1836), 8 oz. ; powdered rhubarb, 4 oz. ; powdered myrrh, 2 oz. ; sort soap, \ oz. ; oil of caraway, 2i dr.; strong syrup of saffron, q. o. to form a pill-mass. " There are twenty- five 3i-gr. pills in each Is. l^d. box." " It has been stated that these pills contain a minute portion of antimony." ('Anat. of Quackery.') Pills, Sed'ative. Syn. Pilttije SEDATiva;, L. Prep. 1. Hydrochlorate of morphia, 6 gr. ; powdered sumbul, 20 gr. ; alcoholic ex- tract of Indian hemp, i dr. For 2-gr. pills. — Dose, 1 to 3, twice or thrice daily ; in exces- sive nervous iiTitability, painful menstrua- tion, &c. 2. (U. C. Hosp.) Camphor, 1 dr. ; reduce it to powder by means of rectified spirit, 3 or 4 drops; add of extract of henbane, 20 gr., and divide the mass into 20 pills. To allay pain and excitement, &c. — Dose, 1 to 2 pills. 3. To either of the above, add of powdered rhubarb and extract of gentian, of each 20 gr., and divide the mass into 4-gr. pills. — Dose, 1 to 4 pills ; when, besides the other symptoms, the stomach and bowels are disor- dered. Pills, Sedillot's Febrifage. Prep. From pow- dered opium, 3 gr. ; sulphate of quinine, 12 gr. ; confection of opium, 10 gr., or q. s. For 12 pills. — Dose, 1 to 2, every second hour, during the intermission of an ague. Pills of Sen'na. Syn. Piutl^ SEWNiE, P. S. COMPOSITiE, L. Prep. 1. Powdered senna, 1 dr. ; extract of rhubarb, i dr. ; powdered capsicum, 4 gr. ; oil of juniper, 6 or 8 drops. For 3-gr. pills. An aperient well suited for females. — Dose, 5 to 8 pills. 2. (Hufeland.) Powdered senna, 1 dr. ; ex- tract of dandelion, q. a. to mix. For 30 pills. As the last. Pills, Smith's. Prep. From powdered aloes, 4 dr. ; jalap, 2 dr. ; ginger and soft soap, of each 1 dr. ; oil of juniper, \ dr. ; emetic tartar, 6 gr. For 120 pills. Laxative and diuretic. — Dose, 1 to 4, at bedtime, or early in the morning. Pills, Dr Hugh Smith's. See Stouach Pills. Pills of Soap. Syn. Pilule: safokis, P. CFM SAPONE, L. Prep. (P. Cod.) White Castile soap, 32 parts; powdered marshmallow root, 4 parts ; powdered nitrate of porassa, 1 part; beat them to a mass, and divide this into 4-gr. pills. In habitual costiveness, cal- culary affections, &e. — Dose, 1 to 6 pills, twice or thrice a day. Pills of Soap (Compound). Syn. Pills op SOAP AND OPirM, LaUDAHUM PILLS; PlLULA SAPONIS COMPOSITA (Ph. L.), PlLUL.ffi BA- PONis CUM opio, L. Prep. 1. (Ph. L.) Opium and liquorice, of each (in powder) 2 dr.; soft soap (Ph. L.), 6 dr.; beat them to a uniform mass. 2. (B. P. & Ph. U. S.) Opium (in fine powder), i oz. ; Castile soap, 2 oz. ; distilled water, i fl. dr., or q. s. ; reduce the soap to powder, mix it with the other ingredients, and beat the whole together, as before. — T>ose, 3 gr. to 5 gr. See Pills op Opium. Obs. The above pills contain l-5th part of their weight in dry opium. The dose is 3 to 10 gr., in the usual cases in which the admi- nistration of opium is indicated. Mr Skey, the eminent surgeon of St. Bartholomew's Hospital, has sliown the great value of this pill in promoting the healing of obstinate ulcers, more especially those of the legs. Pills of Soda. Syn. Pilule; sous, caebo- NATis, L. Prep. (Ph. E. 1817.) Exsiccated carbonate of soda, 4 parts; Castile soap, 3 parts; syrup, q. s. to form a mass. Antacid and slightly laxative. — Dose, 10 to 20 gr. This pill was a great favourite of the once celebrated Dr Beddoes. Pills, Soot. (Dr Neligan.) Syn. Pilule; PULiaiNIS. Prep. Extract of soot, i dr.; compound galbanum pill, 1 scruple ; oil of valerian, 15 minims. Make into 12 pills. Take 2 three times a day. For hysteria. Pills, Speedimau's. Prep. (Cooley.) Aloes, 3 dr.; rhubarb, myrrh (all in powdei), and extract of chamomile, of each 1 dr.; oil of chamomile, 20 drops. For 4-gr. pills. An excellent aperient, tonic, and stomachic. — Dose, 2 to 4 pills, as a purgative ; 1, as a sto- machic or dinner pill. Pills, Splenet'ic. Syn. Vilvlm antisple- NETica;, L. Prep. (Saunders.) Strained aloes and gum ammoniacum, of each 3 dr.; myrrh and bryony, of each J dr. For 4-gr. pills.— 2>o««, 8 to 5. "Extolled in amenor- PILLS 1319 r1up» and liypnchondrlnsiB." (Dr R. £. Griffith.) Fills of Squill (Componnd). Si/n. Couon FILLS, PlLLB OF SQDlLLa AND OIMOKB; Pl- LUH BOILIiK COMrOSlTJI (B. P., Ph. L.), PiLUL.E sciLL* compobiTjE (Ph. D.), p. SclLL.i; (Ph. E.), L. Prep. 1. (Pli. L.) Freslily pnvvilered equilU, 1 dr. ; powdered ginger niid powiliTcd ammoniaemn, of each 2 dr.; mix, iidd of soft soap (Ph. L.), 3 dr. ; treacle, 1 dr.; and bent the whole together, so thut a uia's may be formed. 2. (Ph. !ose, 1 night and morning; in asthmas, &c. Pills of Strych'nine. St/n. Pilulje strych- SIM, h. Prep. (Magendie.) ^trichnine, 2 gr. ; conserve of hips, 36 gr. (liquorice pow- der, q. s.) ; mix very carefully, divide the mass into 24 pills, and silver them. — Dose, 1 pill night and morning; in amaurosis, impotence, paralysis, &e. Pills of Sulphate of Copper. (Brande.) Sgn. PiLULS; CDPKi SULPHATIS. Prep. Sul- phate of copper, 3 gr. ; bread cruio, 1 dr. 1320 PILLS Mix, for 24 pills; 1, three or four times a day. Pills of Snl'phate of I'ron. Syn. Pilulb TEKKi SU1PHATI3 (Ph. E.), L. Prep. 1. (Ph. E.) Dried sulphate of iron and conserve of red roses, of each 2 parts ; extract of dande- lion, 5 parts. For 5-gr. pills. A useful cha- lybeate tonic. Dose, 1 to 2, twice or thrice daily ; in dyspepsia, chlorosis, amenorrhoea, &c. 2. (Ph. E. 1817.) Sulphate of iron (dried), 1 oz. ; extract of chamomile, 1^ oz. ; oil of peppermint, 1 dr. ; syrup, q. s. As the last. 3. (Ph. U. S.) As No. 1, but substituting extract of gentian for extract of dandelion. For other fuuuulm, see Pins, Hoopeb's FEMALE, &C. Pills of Sulphate of Quinine'. Syn. Yylv- IjM QUINI^ SULPHATIS, P. Q. DISULPHATIS, L. , Frep. 1. Sulphate of quinine, 20 gr. j extract of gentian, 40 gr. For 20 pills. 2. (Ph. U. ^.) Sulphate of quinine, 2 dr.; powdered gum, i dr.; strained honey, q. s. For I'M pills. Each pill contains 1 gr. of the sul- phate or disulphate of quiuine, — Dose, 1 or 2 twice a day, as a tonic and stomachic ; 6 to 12, every two or three hours during the remissions of agues. 3. (U. P.) Mix 60 gr. of sulphate of qui- nine, and 20 gr. of confection of hips to a uniform mass. — Dose, 2 gr. to 10 gr. 06s. Various additions are often made to the above forinulaj, according to the mdica- tions, by wliich numerous other useful pills are produced. Thus, potassio-tartrate of anti- mony is frequently added in obstinate inter- niittents; iodide of potassium, in scrofulous affections ; foxglove, in the hectic fever of phthisis ; bitter tonics and aromatics, in dys- pepsia, flatulence, &q. ; carbonate of soda or magnesia, in acidity and heartburn; calomel, mercurial pill, in bilious atfections ; rhubarb and aloes, in bowelly affections ; sulphate of iron and other chalybeates, in debility, amenor- rhcea, and chlorosis ; calomel, as an alterative, «fcc., &c. Pills of Sulphate of Zinc. St/n. PiLULa; ZINOI SULPHATIS, P. Z, B. COMPOSITJJ, L. Prep. 1. Sulphate of zinc, 12 gr. ; extract of gentian, J dr. i liquorice powder, q. h. For 20 pills. In dyspepsia, epilepsy, and various convulsive diseases. 2. (Dr Paris.) Sulphate of zinc, 10 gr. ; powdered niyrrli, 1^ dr.; conserve (if roses, q s. For 30 pills. — Dose, 1 to 2, twice or thrice daily ; in hooping-cough, &c. Pills of Sulphnret of Iron. (Biett.) Syn. Pilule pekbi sulphubeti. Prep. Sulphuret of iron, i dr. ;.marshmallow powder, 10 gr. j syrup, q. s. Make into 20 pills ; 1 to 4 pills daily, in scrofulous eruptions. Pills, Syph'ilis. Syn. PilcL-E antistphi- LITICJS, L. Seethe various pills of mercury, gold, &c. The pills of corrosive sublimate commonly pass under this name. Pills, Tangore. See Pills, Aksenical. Pills of Tan'nic Acid. Syn. Pilule tan- Nlifl, P. ACIDI TANNIOI, L. Prep. From tan- nic acid or tannin and powdered sugar, of each i dr.; conserve ot roses, q. s. For 24 pills. — Dose, 1 or 2 pills, thrice daily, in diarrhoea ; or 2 every three hours, in internal haemor- rhages, spitting of blood, &c. Pills of Tar. Syn. PiLULa; picis LiQniDjE, L. Prep. From tar, 1 dr. ; powdered gen- tian, i dr., or q. s. For 24 pills. Stimulant, diuretic, and sudorific. — Dose, 1 to 4, thrice a day; in dropsies, worms, ichthyosis, and several other skin diseases, &c. . Pills of Tarax'acnm. Syn. Piiui^ taeax- ACi, L. Prep. 1. Extract of dandelion, 1 dr. ; powdered rhubarb, q. s. ; divide into 3^-gr. pills. In dyspepsia, &c., complicated with congestion of the liver. 2. (St Marie.) Extract of dandelion and Castile soap, equal parts; liquid acetate of potassa, q. s. to mix. For 4-gr. pills. As a diuretic in dropsy. 3. Extract of dandelion, 1 dr. ; mercurial pill, 20 gr. ; powdered digitalis, 15 gr. ; liquo- rice powder, q. s. For 24 pills.— Dose, 1, after- wards increased to 2 or 3; in dropsy connected with liver disease. Pills, Thomson's Stomach and Liver. Prep. From extract of dandelion, 1 dr. ; scammony aud rhubarb, of each 15' gr. For 14 pills. — Dose, 2 pills, night and morning ; in hysteria, hy])ochondriasis, and chronic inflammation of the liver or kidneys. Pills of Tobacco. (Augustin.) Syn. Pl- LULiE TABACi. Prep. Powder of tobacco, 24 gr. ; confection of roses, q. s. ilix, and form 72 pills.— Dose, 2 to 4 daily, till nausea is produced. In dropsy. Pills, Tonic. Syn. Pilul^s; tonicb, L. Prep. 1. Sulphate of iron, ginger, and myrrh (all in |iowder), equal parts ; conserve of roses, q. s. ; mix, and divide into 4-gr. pills. — Dose, 1, twice a day ; in debility, chlorosis, &c. 2. Powdered myrrh and sulphate of iron, of each 1 dr. ; disulphate of quinine, \ dr., powdered capsicum, 15 gr. ; conserve of roses, q. s. to mix. For 60 pills. — Dose, 1 or 2, twice or thrice a day ; in debility, dyspepsia, ague, &c. 3. (Dr Collier.) Tartrate of iron and ex- tract of gentian, of each 1 dr. ; oil of cinna- mon, 2 drops. For 30 pills. — Dose, 3 to 6, three or four times a day. A good stomachic tonic. 4. (Dr Collier.) Oxide of zinc, \ dr. (or sulphate of zinc, 20 gr.) ; myrrh, 2 dr.; cam- phor, 20 gr. ; confection of hips, to mix. For 40 pills. — Dose, 1 or two pills, three times a day; in epilepsy, chorea, and other nervous disorders, debility, &c. 5. (Dr A. T. Thomson.) Rhubarb and ginger, of each 4 dr. ; extract of chamomile, 1 dr. ; divide into 30 pills. — Dose, 2 or 3, twice a day; in dyspepsia and chlorosis. 6. (Dr A. T. Thomson.) Sesquioxide of iron and extract of hemlock, of each 1 dr. ; mix, and divide into 20 pills. — Dose, 1 or 2, PILOCARPINE— PIMARIC ACID 1321 twice ft day j in fluor albus, scrofula, Ac. Several other lormiilm for tonic pills will be found under the niiiiies of the leading ingie- dientx, 4c. (See above.) Pills of Turpentine. (P. Cod.) Si/n. Pi- lULS TKBKUINTHIN.U. jPrep. Venice turpen- tine, li oz. ; ciirbonate of magnesia, 1 oz. Miike into 200 pills. Fills of Vale"rian (Componnd). St/n. Pi- LVLS VALEBIAN^ OOMPOSITiE, L. Prep. (Dupuytren.) Powdered valerian, i dr.; castor and white oxide of zinc, of each 20 gr. ; eyrup, q s. ; to mix. For 18 pills. — Dose, 2 or 3, tlirice daily ; in hysteria, hypochondriasis, chlorosis, homicrania, &c. Pills of Vale"rianate of Zinc. Si/n. Pi- lULS VAtKBlANAB, L. Frep. From vale- rianate of zinc and powdered gum, of each 15 gr. ; conserve of hips, q. s. to form a mass. For 18 pills. — Dose, 1 pill, twice daily; in nervous headaclie, neuralgia, hysteria, &c. Pills, Vallet's. See Pills op Carbonate OF luoN. Pills, Vance's. See Puts, Apeeient. Pills of Vera'trine. St/n. Pilulj? vkba- TBIN^, h. Prep. 1. (Magendie.) Voratrine, J gr. ; powdered giiui Arahic nud syrup of gum, of each q. s. to form 6 pills. (See Ac/ow.) 2. (Turnbull.) Vcriitrine, 1 gr. ; extract of henbane and liquorice powder, of each 12 gr. ; mix, and divide into 12 pills. — Dose, 1 pill, every 3 hours; in dropsy, opilep'ii, hysteria, paralysis, nervous palpitations, Ac. This should be prepared aud used with great caution. Pills, Ward's Eed. 8yn. Waed's antimo- NIAL PlLLB. Prep. From glass of nntiincmy (finely levigated), 4 oz. ; dragon's blood, 1 oz. ; mountain wine, q. s. ; to form a mass. For IJ- gr. pills. Emetic. " They are recommended iu obstinate rheumatism affections, in foulness of the stomach and bowels, &c. Their action is often of a very unpleasant character." ('Anat. of Quackery.') Pills, Lady Webster's. See Pills, Diknkk. Pills, Whitehead's Essence of Mustard. Bal- sam of tolu, with resin. (Dr Paris.) PilU, Whytt's. Prep. (Radius.) Aloes, chloride of iron, and extract of horehound, of each \ dr. ; nssufoetida, \\ dr. For 2-gr. pills. — Dose, 2 to 5, thrice daily ; in leucorrboea, chlorosis, hysteria, &,c., with constipation. Pills, Worm. Si^n. Pilul.*; anthelmin- tics, P. VKHMiFUoa:, L. Prep. 1. Calomel, 1 oz. ; sugar, IJ oz. ; mucilage, q. s. ; mix, and divide into 240 pills. — Dose, 1 to 2, over- night, followed by a strong dose of castor oil early the next morning. 2. Gamboge, 6gr. ; calomel, 5 gr.; mucilngo, q. s. ; divide into 3 pills. For a morning's dose, fasting. 8. Extract of wormwood, calomel, aud pow- dered scammoiiy, equal parts. For 4-^.'r. pills. — Dote, I to 2, as the last. For ascarides, and other small worms. 4. (Bresmer.) Powdered aloes and tansy seed, of each 4 dr. ; oil of rue, 9 or 10 drops. For 12 pills.— Z)o*e, 3 to 6, in the morning, fasting, and repeated in two or three hours. 5. (Phoebus.) Iron filings, i dr. ; assafcetida, li dr.; essential oil of tansy, 10 or 12 drops; extract of wormwood, q. s. ; mix, and divide into 80 pl\h.— Dose, 6 pills, thrice daily. 6. (Peschier.) Ethereal extract of male fern, 30 drops ; extract of dandelion, 1 dr. ; powdered rhizomes of male fern, q. s. to mix. For 30 pills. In tapeworm. — Dose, 6 to 15, at bedtime ; the dose being repeated in the morning, and then followed in au hour by a strong dose of castor oil. Pills, Wordsell's (Kaye's.) Prep. (Cooley.) Powdered aloes, gamboge, and gnger, equal parts ; together with a very small qnaotity of iliapliorrtic antimony, beaten into a mass with either syrup or treacle, and divided into 2 J-gr. pills. " There are about 4i dozen pills in each Is. lid. bo^." " The do*c, as given in the directions, is from 2 to 8 pills (or even 10 to 12) daily." ('Anat. of Quackery.') They (ivqnently operate with great violence. Pills, Wyndham's (Lee's). Prep. (Cooley.) Aloes and gamboge, of each (in powder) 3 oz. ; Castile soap and extract of cow-parsnip, oi' each 1 oz. ; nitre, i oz. For 5-gr. pills. A powerful drastic cathartic. — Dose, 1 to 3 pills. Pills of Zinc. Sec PiLis OP OxiDB, Sul- phate and Valhuianate of Zino, &c. PILOCARPIHE. Prep. Exiiaust the leaves or bark of Jaborandi with 80^ alcohol, to which hydrochloric acid has been added in the proportion of 8 grains per litre; distil and evaporate to the consistence of an extract. Rcdissolve the extract with a small quantity of distilled water and filter; treat with ammonia in slight excess, and a large quan- tity of chloroform. Distil off the clihToform, dissolve the residue iu distilled water acidu- lated with hydrochloric acid, and filter. Treat afresh with chloroform and ammonia. The chloroformic solution is then shaken with water, to which hydrochloric acid is added, drop by drop, up to the quantity sufficient to satur.ite the pilocarpine. The foreign matters remain in the chloroform, and upon evapora- tion of the aqueous liquid the hydrochlorate is obtained, well crystallised, in long needles radiating from a common centre. The hydro- chlorate dissolved in distilled water, and treated with ammonia and chloroform, yieldc the pilocarpine upon evaporation of the chlo- form solution. Pilocarpine appears under the form of a soft viscous substance ; it is slightly soluble in water and very soluble in alcohol, ether and chloroform. It presents all the chemical cha- racters of an alkaloid, and rotates the plane of polarized light strongly to the right. (Paris Pliarmaceutical Societv.) PIMA'KIC ACID. A resin acid first Ob- tained by Laurent from the turpentine of 1322 PIMENTO— PIPETTE Finus maritima (Bordeaux turpentine), by the action of hot alcohol. PIMEN'TO. Si/n. Alispicb, Clotb pepper, Jamaica p.. Pimento bebeies; Pimenta (B. P., Ph. L., E., & E.), Pipeb caetophtlla- TUM, P. JaMAICENSE, P. ODOBATUM, PIMENTiE bacCjE, L. " The dried unripe berries of the allspice tree, JEugenia pimenta, from the West Indies" — B. P. "The immature fruit of Uu- genia pimenta (Myrtus pimenta, Linn)" — Pli. L. It possesses a mixed odour of cinnamon, cloves, and nutmegs, which, with its other properties, it for the most yields to alcohol, ether, and water. It is a stimulant and tonic, and is much esteemed as an adjuvant in me- dicines prescribed in dyspepsia, flatulence, gout, hysteria &c. ; and also to cover the taste of disagreeable medicines. — Dose, 5 to 30 gr., bruised or in powder. See Essence, Oils (Volatile), Spirits, and Waters. PIM'PLES. See Ebuptions (Papular). PINCH'BECK. A gold-lilie alloy of copper and zinc. See Dutch gold. PINE APPLE. Sgn. Ananas. The fruit of Ananassa sativa, a plant of the natural order BromeliacecB. It is astringent, esculent, anrt possesses a rich flavour and odour. In Europe it is chiefly used as a delicacy for the table ; but in tropical climates it is said to be valu- able in renal diseases. See Essence, &c. PI'NEY TAL'LOW. Syn. PiNET BESIN, P. SAMMAB. An oleo-resinous substance obtained from the fruit of Valeria indica, a tree com- mon in Malabar, by boiling it with water. It is intermediate between fat and wax, makes good soap and excellent candles. It melts at yS" Falir. Sp. gr. -9250 to 9265. PI'NIC ACID. The portion of common resin or colophony which is soluble in cold alcohol of sp. gr. -838. FINK. A well known shade of light red. The name is also- applied to several pigments, consisting of whiting stained with liquid dyes. See Red and Yellow pigments, &c. PINK DYE. Prep. From washed Siifflower, 2oz. ; salt of tartar, i oz. ; cold water, 1 quart ; digest for 3 hours, express the liquor, and strain it. Used as a cosmetic, and to dye silk stockings, &c., of a rose colour. The colour is brought out by afterwards applying to, or passing the articles through, water soured with lemon juice. See Satjcees (Pink). PIP'EEIN. CiyHigNOj. Syn. Pipebina. PiPEEiNUM, L. J?rep. (P. Cod.) Alcoholic extract of black pepper is treated with a weak solution of caustic potassa (1 to 100), and the residuum, after being washed with cold water, is dissolved in alcohol ; the solution is next agitated with a little animal charcoal, and the filtrate is allowed to evaporate spontaneously ; the product may he purified by the re-solution in alcohol and re-crystallisation. Prop., S;e. Colourleo, or only slightly yel- low; tasteless; inodorous; fusible; and crvs- tallisiible ; insoluble in water ; freely soluble in strong spirit, and in the acids; very feebly basic ; a few definite compounds have, how- ever, been obtained with difficulty ; reddened by oil of vitriol. It has been much employed in Italy and on the Continent as a febrifuge. — T>ose, 2 to 10 gr., frequently repeated, during the apyrexia of intermittents. 04*. An assay for its piperin is the only certain method of testing the quality of either black or white pepper. For tliis purpose a weighted quantity of the sample is reduced to powder, and is exhausted with alcohol of the sp. gr. '883 ; the mixed tinctures are then eva- porated to an extract, which is treated as above. See Peppeb. PIPES. (In confectionery.) These are formed from any of the common lozenge-masses, by rolling them into cylinders of about the thick- ness of a goose-quill. They are frequently medicated. PIPETTE. A graduated glass instrument, in frequent use in the chemical laboratory, for conveying a measured quantity of fluid from one vessel to another. The pipette mostly consists of a bulb, from each end of which proceeds a straight, slender hollow stem, communicating with the bulb, and varying in length with the capacity of the instrument. Thus constructed, the lower end of the pipette can be dipped into a vessel with a narrow and long neck, such as a flask, containing a fluid, the required volume of which can be removed from it. The pipette varies in capacity from 1 to 200 cubic centimetres. ])r Fresenius gives the following directions for its use : — " To fill a pipette with the fluid which it is intended to transfer from one vessel to another, the lower part of the instrument is dipped into the fluid, and suction applied to the upper aperture, either direct with the lips or through a caoutchouc tube until the fluid in the pipette stands a little above the required mark ; the upper, somewhat narrowed, ground orifice is then closed with the point of the index of the right hand, which to that end had always better be moistened a little, and holding the pipette in a perfectly vertical direction, the excess of over the quantity required is made to drop out by lifting the finger a little. When the fluid in the pipette has fallen to the required level, the drops which may happen to adhere to the outside of the pipette are carefully wiped off, and the contents of the tube are then fully transferred to the other vessel. In this process it is found that the fluid does not run out completely, but that a small portion of it remains adhering to the glass in the point of the pipette ; after a time, as this becomes increased by other minute particles of fluid trickling down from the upper part of the tube, a drop gathers at the lower orifice, which may be allowed to fall from its own weight, or may be made to drop off by a slight shake ; if, after this, the point of the pipette be laid against a moist portion of the inner side of the vessel, another minute portion of fluid will PISTACHIO NUTS— f ITCOAL 1323 trickle out ; and lastly, another trifling droplet or 80 limy bo got out by blowinir into the piptttf tbrongli the upper orifice. Now, sup- pnsing the operator follows nn fixed rule in tliia respect, letting the fluid, for instance, in one operiition simply run out, whilst in another operation he lets it drain afterwards, and in a tliird blows off' the last particles of it from the pipette, it is evident that the re^puctive quan- tities of fluid delivered in the several opera- tions cannot he quite equal. I prefer in all cases the second method, viz. to lay the point of the pipette whilst draining finally against H niuiit portion of the inner side of the vessel, which I liave alwiiys found to give the most accurate corresponding measurements. FISTA'CHIO NUTS. Si/n. Pibtacia nuts ; NnoES PISTACIJE, li. The kernels of the fruit of Piscatia vera (Linn.), one of the turpentine trees. They closely resemble almonds, buture sweeter, ami form >i green emulsion with water. Used in confectionery and perfumery, and also as a deisort fruit. PITCH. Syn. Bliok pitch. Boiled p., Stone p., Wood p. j Pjx (Pli. L.), Pix kiqka, L. " A dry bitumen prepared from liquid pitch." Pli. L.) The residuum from boiling tar in an open iron pot, or in a still, until the volatile and liquid portion is driven off. The volatile products principally consist of crude pyroligueous acid and oil of tar. Pitch is chietl.v employed in ship-building. As a medicine, it is stimulant and tunic, and has been used internally in some skin diseases, and in pilc^. An ointment made of it is also extensively used in cutaneous atfections of the scaly. — Dose, 10 gr. to J dr. Pitch, Burgundy. St/n. White pitch, Bun- orNur PINE KEsiN ; Fix Bubodndica (B.P., Ph. L., E., & D.), Ij. " Impure resin prepared from the turpentine o(Abie» exceha," or Nor- way spruce fir. (Ph. L.) " A concrete resi- nous exudation, probably, in a great measure, from Abies excelta." (Ph. E.) It is chiefly used in plasters. Obs. The importation of this substance has for some years past been gradually lessening in amount, in consequence of the substitution for it of a fictitious pitch, made by melting common resin with liuseed oil, and colouring the muss with annotta or palm oil. The phy- siolojjiial action of the two articles is, how- ever, considerably different, since Burgundy pitch acts upon the skin as a powerful local irritant, exciting a slight degree of inflam- mation, and not unfrequently producing a pimply eruption and an exudation of purulent matter. It is celebrated for its elt'ecta when employed as a plaster in all cases where warmth, support, and long adhesion to the skin, arc desirable; and in the latter quality no substance equals it. The fictitious Bur- gundy jiitch has similar properties, but in an immensely less degree. Pbkpahbd Bukgundt Pitch (Pix Bue- OPNUICA fs^Pabata — Ph. L.) is ordered to be obtained in the same way as that adopted for strained ammoniacum. This plan is, however, seldom, if ever, adopted in trade. Fitch, Burgundy (Facti"tioua). Syn. Fix BoEGUNDiCA factitia, L. Prep. By melt- ing good yellow resin, 1 cwt.,with linseed oil, 1 gall., and palm oil (bright), q. s. to colour. The mixture is allowed to cool considerably, and is then pulled with the hands in the same way as lead plaster is treated ; after which it is placed in ' bladders ' or ' stands ' for sale. Obs. The product of the above formula is the ' Burgundy pitch ' of the shops. The ' pulling ' or ' working ' destroys the trans- lucenc V of the re-in, and imparts to it the peculiar semi-opacity of foreign Burgundy pitch. Cold water is commonly employed to cool it down. Annotta is often substituted for palm oil as a colouring substance. The addi- tion of some of the ' droppings ' or ' bottoms ' of Canada balsam, Ohio turpentine, oil of ju- niper, &c., renders this article nearly equal to foreign pitch ; but in commerce this is never attempted, the aim being only the production of a lively colour with moderate toughness. A common melting-pan and fire (il clean, nnd carefully managed) will succeed sufficiently, but, both for safety and convenience, steam is preferable, and on the large scale, nlnio-t indis- pensable. A good workman can pull and put into stands or casks about 5 cwt. daily; or from li cwt. to 3 cwt. in bUdders, tlif hitter quantity depending on tlie size of the bladders. (See above.) Pitch, Can'ada. Sf/n. Hemlock gum, H. pitch. Similar to Burgundy pitch ; but from the Abies C'lnadenses, or hemlock spruce fir. Pitch, Jews'. Asphaltum Pitch, Min'eral. Indurated mineral bitumen. See AspiiALTUM, Bitumen, &c. PIT'COAL. Si/n. CoAL; Houri-LB, Fr. ; SteinkOHIE, Ger. This article has been truly described as the most valuable of all those niineriil substances from which Great Britain derives its prosperity, and the one which may be regarded as the main support of the whole system of British production. It fuses the metals, it produces the steam which sets our machinery in motion, and, in short, it may be said to render all the resources of this country available for use. The more important kinds of coal may be classified as follows : — I. Lignite or brown coal (?ce page 969).) — 2. Bituminonsor caking coals. The most widely diffused and valuable of English coals. They are subdivided into : a. Caking coal. Splinters on heatinu, but the fragments then fuse together in a semi- pasty mass. The chief sources of this valu- able variety of coal are the Newcastle and Wigan districts, b. Cherry coal or soft c^al. Lustre very bright; does not fuse, ignites well and burns rapidly. Glaszow, Stafpord- shire, Derbyshire, Nottingham, Lancashire, lie. c. Splint, rough, or hard coal. Black 1324 PLAGUE and glistening ; does not ignite readily, but burns up to a clear hot fire. It constitutes the bulk of the great coal fields of North and South Staffordshire, and occurs in the Glasgow district, in Shropshire, Leicestershire, War- wickshire, &e. d. Cannel or parrot cohI. Dense and compact, having a shelly fracture, and taking a poiisli like jet. Splinters in the fire, and burns clearly and brightly. Wigan and other parts of Lancashire, West Glasgow, &e. The curious deposit at Bathgate, near Edin- burgh, commonly known as • Boghead cannel coal,' ' or ' Torbanehill mineral,' differs con- siderably from the ordinary ' cannels.' — 3. Anthracite or stone-coal. The densest, hardest, and most lustrous of all kinds of pitcoal. Burns with little flame or smoke, but gives gi'eat heat. South Wales, Devonshire, &c. —4. Steam coal. Approaches nearly to anthracite. Admirably adapted for steam-vessels. South Wales, Tyne district, &c. The quality of coal may be ascertained by either directly testing its heating power or by chemical analysis. In the iqvestigations undertaken at the Museum of Economic Geology, under the directions of Sir H. De la Beche, and which furnished the materials for the celebrated ' Admiralty Reports,' three dif- ferent methods were adopted for this purpose.' These consisted in — the determination of the quantity of water which a given weight of the coal was capable of converting into steam, the quantity of litharge which it was capable of reducing to tlie metallic state, and, lastly, its ultimate analysis by combustion with oxide of copper. See Oeoanio Substances. The quantity of sulphur in coal is another matter of importance that may be determined by chemical analysis. (See Sulphuk.) The presence of more than 1^ of sulphur renders coal unfit for the economical production of good light-gas, and more than 2g of sulphur renders it objectionable for use as domestic fuel. In like manner, coals containing mineral ingredients in excess are to be avoided, not merely on account of the quantity of ashes left by them, but for their tendency to vitrify upon the bars of the furnace, and to produce what is technically called 'clinkers.' The presence of much silica or alumina, and more particularly of any of the salts of lime, in ' steam coal,' is, on this account, highly objec- tionable. For some further information connected with this subject, see Anthkacite, Chim- neys, Coke, Ppel, Gas, Lignite, Oils, (Mineral), Okganio substances, &c. PLAGUE. (Pestis). " A specific fever attended with bubo of the inguinal and other glands, and occasionally with carbuncles." Such is the definition of plague given in the 'Nomenclature of Diseases' (published in 1869), drawn up by a joint committee ap- pointed by the College of Physicians. More detailed acgounts of the diseape, ' See Watt's * Diet, of Chemistry,* vol. i, page 1033. described by other pathologists, state that it attacks the patient with great suddeness, or only after a few premonitory symptoms. These are: — Shivering, extreme prostration, intense headache and giddiness, excessive restlessness, and an overwhelming sense of anxiety. The patient's gait becomes uncer- tain, and he staggers like a drunken man. These symptoms are more or less accompanied by nausea, bilious vomiting, and frequently by bilious diarrhoea. As the disease advances, delirium very frequently sets in ; the nausea, vomiting, and diarrhoea increase in intensity, the tongue becomes swollen and covered with a dark fur, whilst the lips, teeth, and nostrils are coated with a dry fetid incrustation. Pro- vided the attack does not terminate fatally, in a very rapid manner, these symptoms are ac- companied by sharp pains (increasing in inten- sity during the progress of the malady) in the groin, armpits, and neck. These pains in the above parts precede the appearance of tlie buboes, and in many cases, of the carbuncles, which, associated with the fever, are. so charac- teristic of plague. These glandular swellings vary, in different cases, as to the time when they make their appearance. Sometimes they do so during the first day of the attack, at others, after two or throe da^'s — and in others, again, not until uear the close of the disease. With the buboes and carbuncles, small red purplish spots {petechice), frequently appear on the body. The carbuncle is by no means an invariable accompaniment of the disease. Dr Russell, out of 2700 cases, found only 490 in which it showed itself. He states that when carbuncle develops itself, it is dis- tributed over the whole surface of the body with the exception of the scalp, the palms of the hands, and the soles of the feet. " The plague may be said to assume four degrees of severity: — 1. Slight fever, without delirium or buboes. 2. Pever, delirium, and buboes. 3. Fever, delirium, or coma, buboes, carbuncles, and petechia. 4. Congestive fever, fatal on the first, second, or third day, before the appearance of buboes. The fever, though usually continued, may assume the intermit- tent or remittent type."^ There is considerable diversity of opinion as to the origin of plague. By some patho- logists it is maintained tliat it spreads solely by contagion ; by others the contagion theory is altogether repudiated, and certain local and epidemic agencies are referred to as its source; whilst others, again, adopt a medium view and, whilst not denying its contagious origin, hold that it may also be developed by endemic and epidemic causes. It hears a great resemblance to typhus. With the exception of the outbreak of plague at Veltianka, in Astrakan, in the beginning of the current year (1879), the pes- tilence has not visited Western Europe during ' Hooper's ' Vade Mecum,' edited by Messrs Guy and Harlcy. PLAGUE 1325 the present century an exemption whiili, being »o obviously due to the improve I suui- tary and liygienic coiidilions of the modern European cities uud towns, is a forcible illus- tration of how largely the power of curtailing tbo propagation and progress of tbe scourge U within the mciins of human control. There can be little, if any, doubt that the same total ab>encc of drainage, and the very possible c'utisequent contamination of drinking water, added to the narrowness of the streets, tbe overcrowded and badly ventilated state of the houses themselves, and the dirty habits of the inmaten, whicli are also characteristic of those quarturs of eastern cities and towns in which plague is always more or less occasionally pre- valent, obtained in tbe fourteenth, fifteenth, sixteeiitb, and seventeenth centuries, amongst Kuropcan communities, \Vu learn, on the authority of Mr Marshall (who gets his figures from the weekly bills of mortality of the period), that during tbe six- teenth and seventeenth centuries London was seldom free from the pestilence, and that in several yi'ars, not usually regarded by histo- rians as plague epochs, it annually slew from less than 1000 to 4O00 of the inhabitants. Between the years 1593 and 1665, five severe outbreaks of the disease occurred in London, and the number of deaths for the respective years were as follows ; — 1593, 11,003; 1603, 36,269; 1025, 35,417; 1636, 10,400; 1065, 68,596. According to Sir William Petty, the average mortality during these several attacks amounted to about a fiftli of the population. That insanitary surroundings and the spread of plague, whilst sanitary cues and its decline, follow each other like cause and eti'ect, may be emphasised by the statement of two facts: — 1. The medical commissioner lately sent by the Uuvsian government to tbe seat of the late outbreak of the malady in Astrakan, dis- covered the people dirty in their habits, living in noisome, overcrowded houses, and the atmo- sphere polluted with the smell of decaying fish, added to which the village was most miserably drained. 2. Ranken records that in Rajpootana plague propagated by tbe filthy habits of the inhabitants was for some years ahnost entirely obliterated by tlie adoption of sanitary precautious. It may here be noticed thitt the Astrakan plague was associated n itli rnttammation of the lungs, a feature which led an eminent Russian physician to adopt the opinion, that the Astrakan malady is the same as the Indian plague, which is believed to be the same disease which, under the name of ' The Black Death,' committed such appalling devastation in Kurope, Asia, and Africa, in the fourteenth century. In his ' Epidemics of the Middle Ages,' ' Hecker has told of the ravages of this ruthless pestilence, which made its appearance in ' PuUlisLed by the Sjdcalinni Socii-ly, 18 W. Europe in 1348. Its devastations at Florence have been very powerfully described by Boc- caccio in the introduction to his ' Decameron.* Boccaccio was in Naples at the time it was devastating Italy, therefore, it is conjectured, his graphic description must have been derived from hearsay and the reports of eyewit- nesses. In August of the same year it broke out at Dorset, from which county it soon reached Devon and Somerset, and thence rapidly spread throughout England, slaying its thon- sands in its progress. In London alone it has been estimated that the mortality caused by it amounted to a hundred thousand. Hecker assumes that in Europe its victims were twenty-five millions. These however, as well as the following figures, must only be received as approximations to the correct numbers, which, owing to the absence of any contemporary bills of mortality, cannot but be very imperfect : — In Florence there died of tbe black plague . , . 60,000 In Venice . . . . 100,000 In Marseilles, in one month . 10,000 In Sienna . • . 7u,000 In Paris . . 50,000 In St Denis . 14,000 Iii Avignon • . 60,000 In Strasbourg . . 16,000 In Lubeck . . 9,000 In Busle . . 14,000 In Erfurt at least . 16,000 In Weimar . 5,000 In Lemburg . 2,500 In London at least , 100,000 In Norwich . 51,000 To wliich may be added: — Franciscan Friars in Germany. 124,43 !• Minorites in Italy . . . 30,000 From the circumstance — illustrative of the religious and blind bigotry of this period— that the Jews were brutally tortured, massacred, and burnt, on suspicion of having poisoned the welh from which drinking water was drawn, it may be inferred that tbe wells, owing to the entire al)sence of drainage, which led to tlieir contamination by sewage matters, contributed largely to tbe spread of the pes- tilence. Of the potency of the contagion dissemi- nated by the ' Black Death ' Hecker re- cords : — " Every spot which the sick bad touched, their breath, their clothes, spread the conta- gion ; and in all other places tbe attendants and friends, who were either blind to tlieir danger, or heroically despised it, fell a sacri- fice to their .sympathy. " Even tbe eyes of the patient were con- sidered as sources of contagion, which had the power of acting at a distance, either on acconnt of their unwonted lustre, or the dis- 1326 PLAGUE tortion which they always suffer in plague, or in conformity with an ancient notion, accord- ing to wliicli the sight was considered as tlie bearer of a demoniacal excitement. "The pestilential death of the sick, who ex- pectorated blood, caused a terrible contagion far and near, for even the vicinity of those who had fallen ill of plague was certain death, so that parents abandoned tlieir infected children, and all the ties of kindred were dis- solved." There is a striking similarity between the above description, referring to the plague of 1348, and the following, which is extracted from Dr Doppner's official medical report to the Russian government on the plague which manifested itself at Veltiauka in Astrakan as lately as January, 1879. Dr Doppner, writes : — " The necessary remedies were employed to combat the disease. I prescribed especially salicylic acid, muriatic acid, quinine, &o., but everything proved useless. Not a single putient recovered, viz. Dr Koch and six of his assistants died, the priest of the Stanitza, the Cossacks employed in burying the dead; in a word, all those who approached the per- sons attacked with the disease, although fur- nished with the means of preservation used in like circumstances, very few escaped the plague.^ " No case of plague has occurred in England for more than two centuries, altiiough in 1721 it half depopulated Marseilles, and com- mitted ft-arful ravages at Moscow, in 1771. Within the present century it has appeared in Europe at the following places : — At Malta, in 1813 ; at Calabria, in 1816 ; nt Corfu, in 1818; in Silesia, in 1819; and amongst the Russian troops in Bulgaria, in 1824. In Malta between 4000 and 5000 people fell victims to it. It made its last appearance in England in 1665, and was especially fatal in London, where it carried off, as we have already seen, 65,596 peciple. Because of the frightful mor- tality it occasioned, this particular outbreak of the disease has been named by historians "The Great Plague of London." Rapidly spreading from Westminster, where it first manifested itself, to the more closely built city, its progress increased with the warm weather, until during the sultry months of August and September it reached its height. "Thus," writes Pepys in his diary, August 31st, 1 665 " this month ends with great sadness upon the public through the greatness of the plague everywhere through the kingdom almost. Every day sadder and sadder news of its increase. In the city died this week 7496, and of them 6102 of the plngne. But it is feared the true number of the dead this week is near 10,000 ; partly from the poor that cannot be taken notice of through the great- ness of the number, and partly through the * Laucet.' Quakers and others that will not have the bell ring for them." The general aspect of the pestilence stricken city is thus described by Pepys, " To the Exchange, where I have not been a great while. But, Lord ! how sad a sight it is to see the streets empty of people and very few upon the 'Change. Jealous of every door that one sees shut up, lest it should be plague ; and about us two shops in three, if not generally more, shut up." The doors of a house infected with the plague were marked with a red cross, and on them was written the words, " The Lord have mercy upon us." Pepys tells of the fright he experienced when he came upon two houses of this description, in Drury-lane, for the first time ; and as he adds that he was compelled to buy some roll tobacco to smell and to chew, it may be concluded that this substance was at that time regarded as somewhat of a safe- guard against the disease. Large carts called nightly at the infected habitations and collecting the bodies of any dead conveyed them to pits, into which they were flung, covered with quicklime. This rude kind of burial became a necessity as the disease gained ground, because the ordinary grave-yards were full to overflowing. " This is the first time," writes Pepys, " since I have been in the church since I left London for the plague, and it frightened me indeed to go through the church more than I thought it could have done, to see so many graves lie so high upon the churchyards where people have been buried of the plague." Such was the fury of the pestilence, and frequently so sudden were its attacks, that wayfarers were often assailed with it in the streets, and staggering like drunken men fell down into the road or pathways ins 'nsible or dead. Merchants in their counting-houses, clergymen in the act of reading the burial service, buyers and sellei's in the market-place, were similarly assailed by the malignant malady, and it was no uncommon occurrence for the mourner at the grave of a relative or friend one day, to be himself borne to his own tomb the next. It is not improbable the infection may have been conveyed by the rapidly decaying and putrid corpse to large numbers of people, owing to the custom that prevailed of crowds of mourners attending the obsequies. Pepys records how he saw in broad daylight two or three burials, one at the very heels of another, each followed by forty or fifty people. Furthertuore, he states that one day on his way to Greenwich, during the month of August in 1665, ho passed a coffin, " with a dead body therein, dead of the plague, lying in an open close belonging to Coombe Farm." If this exposure of plague-stricken corpses were at all general, it will readily he perceived how greatly it must have aided the propaga- tion of the pestilence. Another important agent in the diffation of PLAICE— PLASTER 1327 the pl»gu(> iini»t have been the infected cloth- ing, whi th r of tlie dead or of tliose who had been in ne r or close contigaity to them. Ou this pnrt of our suhjcct Ur Guy, remarks : — " Nor will this surprise us if we imagine the frantic and successful efforts that must have been made by the non-infected to escape, and the temptation to servants and nurses to appro- priate aiul remove the property of the dying and the dead. Indeed, Dr Hodges accuses the nurses of strangling tlieir patients, and si'cictly conveying the pestilential taint from sores of tlie infected to those who were well ; and he justiHes his accusations 'of these abandoned miscreants' — the Gamps and Prigs of the seventeenth century — by two instances ; the one, of a nurse who, 'oa she was leaving the house of a family, oil dead, loaded with lier robberies, fell down dead under her burden in the streets ;' the other, of a worthy citizen who, being considered dying by his nurse, wus beforehand stripped by her, but recovering iigiiin, he came a second time into the wurld n^iked." Lastly, in endeavouring to account for the fjreat prevalence and excessively fatal charac- ter of this pestilence, we must not leave out of consideration one important factor — viz. fear. We cnn easily conceive how powerfully the appalling incidents by which tlie pliigue was a<^comp>inied must have affected the imagina- tiotts of those who were in its midst, and tliu^ have stimulated tlie fear, which, acting liy its depressing mental effect, would predispose and prepare men and women for the reception uf the contagion. In ' Pepy's Diary' wo find a circumstance recorded corroborative of this. A eirtuin alderman, stumbling at night over a dead body in the sti*eet, when he reaches home tells his wile of his adventure, and she is forthwith seized with the plngue and dies of it. Fur- thermore, the belief derived from knowledge of the dciidly character of the disease, operat- ing upon the minds of those who were attacked by it, would greatly diminish the chances ol their recovery, since they would most likely regard seizure and death as synonymous. There is an old Eastern fable which tells of a traveller journeying from an infected city, and ovcrtiiliing the plague, who had not long lelt it. The traveller accosts the plague and reproaches him for having slain thirty thou- sand people in the city. " You are in error there," replied the plngue, " I slew only ten thousiind, fear slew the rest." Tropical climates are never visited by plague. In those countries which suffer firom its ravages it prevails most during the hot months of the year, and its virulence and spread appeiir to becommensurate with increase of tempiritiire. In northern climates it diminishes with the approach of cold weiither. In Europe it has always been most fatal dur- ing the sumuier and autumn, and in the great plague of London the greatest mortality pre- vailed during the months of August aud Sep- temlier. PLAICE. The Plateita vulgarii, a well- known Hat fish, common to both the English and Dutch coasts. Its flesh is good, and easy of digestion, but more watery than that of the flounder. PLANTAIN. The plantain, which belongs to the nat. ord. Musacese, and is a native of the East Indies, is cultivated in all tropical and subtropical regions of the world, in many * of which it constitutes the principal food of the inhabitants. There are a grent many varieties of the plantain, in some of which the stem is 16 or 20 feet high, whilst in others it does not exceed 6 feet. It is one of the largest of the herbaceous plants. The fruit is sometimes eaten raw, but is more generally boiled or roasted. It contains both starch aud sugar. Boiled and beaten in a mortar, it forms the common food of the negroes in the West Indies. It also consti- tutes the chief food of the Indians of North and South America. Humboldt has calculated that the food pro- duce of the plantain is 44 times greater than that of the potato and 133 times that of wheat. The banana is a species of plantain. See Banani. PLASMA. The liquor sanguinis. A tena- cious plastic liquid, forming the cciagulatiug portion of the blood, and that in which the cor|iU8z. ; laid, l^oz. ; melt, add of turpen- tine, IJ oz., nnd afterwards of red lend, 4 oz. ; dip pieces of linen into the melted mixture, pass these between rollers, and, when cold, polish them, as before, and cut them into squares. The insuo plaster (issue paper; charta ud fontieulos) of the Ph. Suecica is a nearly similar compound, with the addition of about l-48th part of verdigris, in very fine powder, and being spread upon paper. Plaster, Kennedy's. See Plastebs, Cobn. Plaster, Kirkland's. See Plasieb, Am- MONIAOAL. Plaster of Lab'dannm. See Plabteb, C'i;i'UALio. Plaster of Lead. Syn. Lead plaster, Li- TnAHOK p., (Common p., Diachylon, Simple DIACHYLON, White d.j Emplasteum plumbi (B. 1'., Ph. L.), E. LYTUAKGYBI (Ph. E. & D.), 10, COMMnNE, UlAOUYLON BIMPLEX, L. Prep. 1. (Ph. L.) Oxide of lead (lithiirge), in very fine powder, 6 lbs.; olive oil, 1 gall.; water, 1 quart ; boil them over u slow fire, constantly stirring to the consistence of a plaster, adding a little boiling water, if nearly the whole ,of that used in tho beginning should be con- sumed before the end of the process. 2. (Ph. E.) Litharge, 5 oz. ; olive oil, 12 fl. oz. ; water, 8 11. oz. ; as the last. 3. (Ph. D.) Litharge, 5 lbs.; olive oil, 1 gall. ; water, 1 quart. ■t. (Otto Kohnke.) For each lb. of litharge employed, iidd \ pint of colourless vinegar (each fl. oz. of which is oipable of saturating i dr. of carbonate of potassa) ; add the oil, boil until all moisture is evaporated, and until only a few striaj of litharge rise to the surface, then remove the vessel from the heat, add trraduaily J tn i as much vinegar as before, and boil the mixture to a proper consistence. 5. (Wholesale.) From Genoa oil, 7 galls, (or 65 lbs.) ; lithar^'e (perlectly free from copper), 2S lbs. J water, 2t galls.; boil to a plaster, as before. 6. (B. P.) Oxide of lead, in very fine pow- der, 1 ; olive oil, 2J ; water, 1 j boil all the in- gredients together gently by the heat of a steam bath, and keep thein simmering for 4 or u h'lurs, stirring constantly until the product acquires tlio proper consistem-e for plaster, adding more water during the process, if necessary. Obe. The London College orders too little oil. The second, fourth, and fifth formula: produce beautiful plasters, that keep well ; those of the others, although very white, get hard and brittle much more rapidly. The proper proportion of oil is fully 2i times the weight of the litharge, — 2J times appears the be^t quantity; and without this is used, the plaster speedily gets hard and non-adhesive. The process consists in putting the water and the litharge into a perfectly clean and well- polished tinned copper or copper-pan, mixint; them well together with a spatula, adding the oil, and boiling, with constant stirring, until the plaster is sufficiently hard, when thoroughly cold. This process usually occupies from 4 to 6 hours, but by adopting the fourth formula an excellent plaster may be made in from 20 to 30 minutes. Ibis plaster is generally cooled by immersion in cold water; nnd to render it very white, a quality highly prized in the trade, it is usual to submit it to laborious ' pulling,' in the manner already noticed. Use. As a simple defensive plaster or strap- ping; but principally as > basis for other plasters. Plaster, Listen's. See Plaster, Coubt. Plaster, Mahy's. St/n. £.mfla3tbum PLUMBI CABBONATia, E. P. 0. COMPOSITITH, L. I'rep. (Ph. U.S.) CarhonntPOtlead(pure white lead), 1 lb. ; olive oil, 32 fl. oz. ; water, q. s. ; boil them together, constantly stirrin); until perfectly incorporated ; then add, of yellow wax, 4 oz. ; lead plaster, 1 i lb. ; and when these are melted, and the mass somewh.>t cooled, stir in of powdered orris root, 9 oz. A favourite application in the United States of America to inflamed and excoriated surfaces, bed sores, burns, &c. Plaster of Mel'ilot. Si/n. Emplastbum meli- LOTi, E. ii MELILOTO, L. I'rep. 1. (Ph. E. 1744.) Fresh melilot, chopped small, 6 lbs. ; suet, 3 lbs.; boil until crisp, strain with pres- sure, nnd add, of yellow resin, 8 lbs. ; bees- wax, 4 lbs., and boil to a plaster, stimulant. Used to dress blisters, &c. The greater portion of this plaster in the shops is made without the herb, and is coloured with verdigris. (Sie the next formula.) 2. (Wholesale.) Take of yellow resin, 18 lbs. ; green ointment, 4 j lbs. ; yellow wax, 3 lbs.; finely powdered verdigris, q. n. to give a deep-green colour. Plaster, Mercu"rial. Sj/n. Emplastbdm MEKCUKIALE, E. HYDEABGYEI (B. P., Ph. L., E., & D.), L. Prep. 1. (Ph. L.) Add, gradually, of sulphur, 8 gr., to heated olive oil, 1 fl. dr., and stir the mixture constantly with a spatula until they unite; next add of mercury, 3 oz., and triturate until globules are no longer visible; lastly, gradually add of lead plaster (melted over a slow fire), 1 lb., and mix them all well together. (About 1 fl. dr. of balsam of sulphur maybe substituted for the oil and sul pimr ordered above.) These propor- tions are the same as those of the B. P. 133i PLASTER 2. (Ph. E.) Resin, 1 oz. ; olive oil, 9 fl. dr. ; mix by heat, cool, add of mercury, 3 oz., and triturate until its globules disappear; then add of litharge plaster, 6 oz. (previously liquefied), and mix the whole thoroughly. 3. (Ph.D.) Oilof turpentine, 1 fl.oz. ; resin, 2 oz. ; dissolve, with the aid of heat ; add of mercury, 6 oz. ; triturate until the globules disappear, and the mixture assumes a dark grey colour, then add of litharge plaster (pre- viously melted), 12 oz., and stir the whole until it sti^ens on cooling. 4. (Wholesale.) Take of mercury, 7 lbs.; prepared serum, i lb. ; triturate until the glo- bules disappear, and add the mixture to lead plaster (melted by a gentle heat), 36 lbs. ; stir them well together, and until they concrete. Very fine bluish-slate or lead colour. Obs. Mercurial plaster is used as a dis- cutient in glandular enlargements, and other swellings; and is also applied over the hepatic regions in liver complaints. Plaster, Mercurial, with Belladon'na. St/a. EmPLASTEUM HYDEAEOTKI CDM BELliDONNA, L. JPrep. Prom mercurial plaster, 6 dr. ; ex- tract of belladonna, 2 dr.; olive oil, 1 dr.; mixed by a gentle heat. One of our most useful anodyne and discutient applications, in painful scirrhous, scrofulous, and syphilitic tumours. The Medico-Chirurgical Phiirm. orders J fl. dr. of hydrocyanic acid to be added to every 2 oz. of the above. Plaster of Mezereon and Cantharides. (Ph. G.) /Sy». Emplastkum mezeeei oanthaei- DATUM. Prep. Cantharides in coarse powder, 3 oz., mezereon cut and dried, 1 oz. acetic ether, 10 oz. by weight. Macerate for 8 days, filter, and dissolve in' the filtered liquid 175 gr. of sandarac, 87 gr. of eleme, 87 gr. of resin, which, spread on silk previously covered with the following solution ; isinglass, 2 oz. ; distilled water, 20 oz. ; rectified spirit, 5 oz. by weight. Plaster of Miu'inm. Si/n. Emplastbum: MINII, E. E MINIO, E. PITJMBI OXTDI KUEEI, L. Prep. (Ph. L. 1746.) Olive oil, 4 lbs. ; minium (red lead), in fine powder, 2i lbs. ; water, q. s. ; proceed as for lead plaster (which it closely resembles). Obs. To ensure a good colour and the quality of keeping well, the quantity of oil should be increased about l-3rd. When discoloured by heat it forms the 'brown minium plaster' (emp. & minio fuscum) of old pharmacy. Lead plaster, either alone or with the addition of a little red lead, is usually sold for it. Plaster of Minium (Compound). St/n. Ntr- BEMBEEQ' PLASTEE ; EMPLASTEUM: MINII OOM- POSITUM, L. ; EmplAtke DE NnBEMBEK&, Pr. Prep. (Soubeiran.) Red lead, 12 parts; olive oil, 8 parts; grind them together on a por- phyry slab, and add the mixture to lead plas- ter, 50 parts, beeswax, 24 parts, melted together; lastly, when nearly cold, stir in of camphor, 1 part. Plaster, Morrison's Adhesive. S^n. Mob- eibon's adhesive paste. From wheaten flour, 2 oz. ; mild ale, i pint; stir them together, and heat the mixture to the boiling point; when cold, add of powdered resin, 3 oz. ; and, constantly stirring, again heat them to boiling. Used as a depilatory in ringworm, &c. Plaster of Mu'cilagea. Syn. Diachylon COMPOaiTUM, EmPLABTBTTM E MUOILACmriBUS, L. Prep. (Ph. L. 1746.) Beeswax, 20 oz.; oil of mucilages, 4 oz. ; melt, and add them to strained ammoniacum, 3 oz. ; common turpen- tine, 1 oz., previously melted together. Stimu- lant and emollient. Plaster of Mns'tard. Syn. EMPiASTEtm siNAPis, L. This is always an extempora- neous preparation. Flour of mustard is made iuto a stiff paste with lukewarm water, or with vinegar, and is then spread on a piece of calico or linen (folded two or three times) ; over the surface of the mustard is placed a piece of gauze or thin muslin, and the plaster is then applied to the part of the body it is intended to medicate. Its action is tbat of a powerful rubefacient and counter-irritant; but its ap- plication should not be continued long, unless in extreme cases. Its effects are often ap- parently wonderful. We have seen very severe cases of facial neuralgia, sore throat, painful joints, rheumatic pains, &c., relieved in a few minutes by means of a mustard plaster or ' poultice.' Plaster, Nuremberg. See Plastee, Minitjh (Compound). Plaster of Oak-mistletoe. (Hardy.) Si/n. Emplasteum tisci (JUEEcini. Prep. To 2 parts of melted beeswax add gradually 1 part of juice of true oak mistletoe, and form a plaster. In neuralgic pains. Plaster of Cpinm. St/n. Emplasteum ANODTNUM, E. OPII (B. P., Ph. L. E. & D.), L. Prep. 1. (Ph. L.) Lead plaster, 8 oz.; melt, and add of frankincense (thns), 2 oz. ; next, add of extract of opium, 1 oz., previously dissolved in boiling water, 1 fl. oz. ; and, con- stantly stirring, evaporate the mixture over a slow fire to a proper consistence. This plaster is much stronger than that of the Ph. L. 1836 and of the other British Colleges. 2. (Ph. L. 1836.) Lead plaster, 1 lb. ; melt, add of powdered thus, 3 oz. ; mix, and further add, of powdered opium, i oz., water, 8 fl. oz , and boil to a proper consistence. 3. (Ph. E.) Litharge plaster, 12 oz.; Bur- gundy pitch, 3 oz. ; liquefy by heat, then add, by degrees, of powdered opium, i oz., and mix them thoroughly. This and the pre- ceding contains only l-3rd part of the opium ordered in the present Ph. L. & D. 4. (Ph. D.) Resin plaster, 9 oz. ; opium, in fine powder, 1 oz. ; as the last. Same as B. P. 5. (Ph. B.). Powdered opium, 1 oz ; resin plaster, 9 oz. ; melt the plaster and add the opium. Obs. The above plaster is reputed aundyne, and useful in various local pains ; but its vir- PLASTER 1335 tiie« in this way have been greatly exnggerated. Tlif formula "f the Ph. L. 1836, from bHing lens costly, is etill often employed in place of tliBt of the I'h. L. 1851. The following is eoMiuionly used : — Lend plaster, 14 lbs.; yellow resin, '^ lb". ; powdered opium, i lb. Plaster of Opium and Camphor. ( Dr Paris. ) Si/n. Emplabtbum opii et camphoeje. Prep. 0|iium and camphor, of each i dr. Lend plaster q. ■. Mix. Plaster of Ox'ide of I'ron. Syn. Iron PLASTKR, FbANKINCKNSE P., StBENGTHENINO p.; Emplastbuu bobobanb, E. pkbki (B. p., I'll. L. E. & D.), K. THUEia, E. pebei OXTDi ECDEi, L. Prep. 1. (Ph. L.) Lead plaster, 8 oz. ; f rankincenite (thus), 2 oz. ; melt them together over a slow fire, sprinkle into the mixture sesquioxide of iron, 1 oz., and mix the whole well together. 2. (Ph. E.) Litharge plaster, 3 oz. ; yellow resin, 6 dr. ; beeswax, 3 dr. ; melt them together, then add of red oxide of iron, 1 oz., previoii"ly triturated with olive oil,3i fl. dr. 3. (I'h. D.) Litharge plaster, 8 oz. ; Bur- gundy pitch, 2 oz. ; peroxide of iron, in fine powder, 1 oz. ; as No. 1. Same as B. P. 4. (Wholesiilc.) From lend iilusier (quite dry), 84 lbs. j powdered yellow resin, 14 lbs.; • crocus martis' (lively coloured), 14 lbs. ; olive oil, 3 pints ; as No. 2, 5. (B. P.) Add hydrnted peroxide of iron in fine powder, 1 oz., to Burgundy pitch, 2 oz , and litharge plaster, 8 oz., previously melted together, und stir the mixture eori^tiintly till it stiffens on cooling. Obs. Iron plaster is reputed strengthening and stimulant. It is employed as a mechan- ical support in muscular relaxation, weak- ness of the joints, &c., especially by public dancers. Us tonic action is probably wholly imaginary. No. 4 is the ' emplasthilm bo- BOBANB ' of the shops at the present time. Plaster, Oxycro'ceam. Sga. Ksiplastbttm OXYOBOCEITM, L. Prep. 1. (Ph. E. 174 i.) Beeswax, 1 lb. ; black pitch and strained gal- lianum, of each J lb.; melt, and add of Venice turpentine, powdered myrrh, and olibanum, of each 3 oz. ; powdered saffron, 2 oz. :.'. (Wholesale.) From blaik pitch, 9 lbs. ; black resin, 11 lbs. ; beeswax and lard, of each liilbs. ; melted together. Warm ; diseutient. Still popular with the lower orders. The saffron of the original formula never finds its way into the oxycroceum plaster of the druggists. Plaster, Palm. S^n. Emplabtbum diapal- MUM, L. ; Diapalme, Empiatke diapaimb, Fr. Prep. (P. Cod.) Lead plaster, 32 parts ; yellow wax, 2 parts ; melt them together, add of sulphate of zinc, 1 part, dissolve iu a little water, and continue the heat, with constant agitation, until all the water is evaporated. 04*. This plaster originally contained palm oil. and this ingredient is still ordered in the formula) of PIcnck and Reuss. Soubeiran directs white wax to be employed. Plaster, Paracelsus's. Si/n. EMPLAsiarM Pabacklsi, E. STYpnciTM," L. Prep. From lead plaster, 28 lbs. ; galbannin plaster, 2 lbs. ; powdered white canella and gum thus, of each li lb.; melted together. The original formula, as well as that of the Ph. L. 17:il were similar, although much more compli- cated. Plaster of Pitch. Syn. PooE man's plabtkb. Gout p., AKTI-BHErMATIC p. ; PyMPLASTErM PAUPEEIS, E. ANTIEHEl'MATICUM, E. AXTAB- THEITICUM, E. PICIS COMMTTNE, L. This has been already noticed under the bead of Rksin Papeb. It is also, but less frequentl.v , spread on cloth and leather. Plaster, Prestat's Adhe'sive. Prep. From lead plaster,2J lbs.; yellow resin, 5 oz. ; Venice turpentine, 4 oz.; gum aunnouiacuiu and mas- tic, of each li oz.j made into a plaster, and spread on linen or calico. Plaster of Eed lead. See Piastee of MlNIBM. Plaster of Bes'in. Si/n. Adhebivs plastee, liESINOCB p.; EmPIASTEUM AIiIIESIVDM, K. BESINJi (B. p., Ph. L. & D.), E. BESIKOSIM (Ph. E.), E. LVTHAEOIEI CUM BESINA, L. Prep. 1. (Ph. L.) I'o lend plaster, 3 lbs., melted by a gentle heat, add of resin, i lb., also liquefied by heat, and mix. Tlie formula (if the Ph. V. S. is similar. 2. (Ph. E.) Litharge plaster, 5 oz. ; resin, 1 oz.; mix with a moderate heat. 3. (Ph. D.) To litharge plaster, 2 lbs., melted liy a frciitle heat, add, of powdered resin, 4 oz., Casiile soap, in powder, 2 oz., and mix them intimiitily. 4. (\\'li"le9ale.) Pale lead plaster (from a previous hatch, and quite dry), 72 Ihs. ; olive oil (Genua). 3 lbs.; melt them together in a bright and perfectly clean copper pan, and silt iu of pale vellow resin (in powder), 12 lbs., stirring all the while. The mixture is to be cooled, aud ' pulled' or ' worked,' after the uiauner of lead plaster. 5. (B. P.) Resin (in powderX 2 ; litharge plaster, 16 ; bard soap, 1 ; melt the plaster wiih a gentle heat, add the resin aud soap, first liquefied, and mix. Obs. Resin pl.ister, spread upon calico, forms the well-kuown ' STRAPPING* or ' ADHESIVE PLASTKB* so extensively used to protect raw surfaces, support parts, and for dressing ulcers, retiining the lips of recent cuts and wounds in contact, &c. It is gently stimulant, and is thought to assist the healing process. It is also employed as a basis for other plasters, rile 'HOSPITAL plastee' of certain houses is of this kind. See Plasteb oe Soap, Com- pound. Plaster, Eesol'vent. Si/n. Emplastbum be- SOLVENS, E. ex MIXTI3 QXJATUOB, L. Prep. (P. Cod.) Galbanum, hemlock, mercurial, and soap plasters, equal paits, melted together. Plaster, Roper's Koyal Bath. Prep. (Cooley.) Strained black pitch, 16 oz.; Burgundy pitch, 10 oz.; tar and beeswax, of each 1 oz.; melt. 1336 PLASTER and, when considerably cooled, add of expressed oil of mace, 2 dr. ; croton oil, 1 dr. j and spread the mixture upon heart-shaped pieces of white sheep-skin, without remelting it. Stimulant and counter-irritant; recommended by its proprietor as a cure for all human ailments. The ' Bath-piasteb Pills,' also prepared by Mr Roper, resemble several of the aperient pills already noticed. (See 'Anat. of Quackery.') Plaster, Scott's. Prey. From lead plaster, 14 oz. ; olive oil and white resin, of each 1 oz. ; melted together, and spread on calico. Plaster, Sharp's Black, trej). From olive oil, 5 parts ; carbonate of lead, 4 parts ; bees- WHX, 1 part ; boiled to a plaster. Plaster, Simple. See Plaster, Wax. Plaster of Soap. %». Emplasteum e SAPONE, E. SAPONIS (Ph. L. E. & D.), L. Prep. 1. (Ph. L.) To lead plaster, 3 lbs., melted by a slow heat, add of Castile soap, sliced, 4 lb., re»in, 1 oz., both (also) liquefied by heat, and, constantly stirring, evaporate to a proper consistence. 2. (Ph. E.) To litharge plaster, 4 oz., gum piaster, 2 oz., melted together, add of Castile soap, in shavings, 1 oz., and boil a little. 3. (Ph. D.) To litharge plaster, 2i lbs., melted over a gentle fire, add of Castile soap in powder, 4 oz., and heat them together (constantly stirring) until they combine. 4. (B. P.) Hard soap (in powder), 6; lead piaster, 36; resin (in powder), 1; to the lead plaster, previously melted, add the soap and the resin, first liquefied, then, constantly stirring, evaporate to a proper consistence. OS*. Care must be taken to evaporate all the moisture from the above compounds, as, if any is left in the plaster, it turns out crumbly, and does not keep well. Much heat discolours it. (SeeieioOT.) Soap plaster is emollient and resolvent, and is used in abrasions and excoriations, and as a dressing to soft corns, lymphatic tumours, &c. Plaster of Soap (Camphora,ted). (P. Cod.) Syn. Emplabtkum saponis camphouatum. Soap planter, 10 oz.; camphor, 48 gr. Plaster of Soap (Compoimd). Syn. Emplas- teum SAPONIS COMPOSITUM, E. ADHJEKENS, L. Peep. (Ph. D. 1826.) Besin plaster, 3 oz. ; soap plaster, 2 oz. ; melted together. Ohs. Less emollient, but more stimulant, than the simple plaster. The ' emplasteum E MiNio CUM saponb' — Ph. E. 1744 was made by melting 1 part of soap with 5 parts of minium plaster. Neither of the above must be put into water. See Plasteb oe Eesin, Ph. D. Plaster of Soap-ce'rate. Syn. Emplasteum CBEATi saponis (,B. P.). Pre]). 1. From soap cerate, heated by means of a water bath until all the moisture is evaporated. Sometimes 2 or 3 dr. each of powdered mastic and gum ammoniacum are added for each pound of cerate. The product is generally spread whilst still warm. Said to be suppurative, resol- vent, cooling, and desiccative. See Ceeatb (soap). 2. (B. P.) Hard soap, 10; beeswax, 12i; oxide of lead (in powder), 15 ; olive oil, 20 ; vinegar, 160 ; boil the vinegar with the oxide over a slow fire, or by a steam bath, constantly stirring them until they unite ; then add the soap and boil again in a similar manner until all the moisture is evaporated; lastly, mix with the wax previously dissolved in the oil, and continue the process till the product takes the consistence of a plaster. Plaster of Squill, Componnd. Syn. Em- plasteum SCILL^ COMPOSITUM. Prep. Gal- banum, J oz. ; soap, i oz. ; litharge plaster, 2 oz. ; melt together, and add opium, 1 dr. ; ammoniacum, J oz.; vinegar of squills, 3 oz., mixed together; keep them over the fire con- stantly stirred till they are incorporated. Plaster, St Andrew's. Prep, Prom yellow resin, 8 oz. ; gum elemi, 2 oz. ; Bordeaux tur- pentine and oil of the bay-laurel, of each 1 oz. ; melted together by a gentle heat. A stimu- lant, resolvent, and adhesive plaster, once sup- posed to possess extraordinary virtues. Plaster, Stick'ing. See Plasteb, Couht, Plabtee op Resin, &c. Plaster, Stoni'ach. See Plasteb, Aeomatio, &c. Plaster, Strength'ening. See Plastees or Feaneinoense and Oxide op Ieon. Plaster, Styp'tic. See Plastee op Oxide op Ieon, Paeacelsus's p., &c. Plaster of Snl'phate of Qninine'. Syrt. Em- plasteum QUINI^, E. Q. DISULPHATIS, L. Prep. 1. Sulphate of quinine, 1 dr.; resin plaster, 1 oz. Applied to the abdomen in intermittents. 2. Sulphate of quinine, 1 dr. ; mercurial plaster, 2 oz. In affections of the liver or spleen, following intermittents, applied over the regions of those viscera. 3. Resin plaster, 9 dr. ; sulphate of quinine, 1 dr.; camphor and oil of cajeput, of each \ At. Applied over the epigastrium as ~ pro- piiylactic of cholera. Plaster of Thus. See Plasteb op Fkank- INCENSE. Plaster of Ver'digris. Syn. Emplasteum aiEUGINIS, E. OUPEI SUBACETATIS, L. Prep. (P. Cod.) Beeswax, 4 parts; Burgundy pitch, 2 parts ; melt, add of Venice turpentine and prepared verdigris (in powder), of each 1 part, and stir until the mass is nearly cold. For other formuliE, see Plastee, Coen, &c. Plaster, Ver'mifuge. Syn. Emplasteum termipuqum, E. anthelminticum, L. Prep. From powdered aloes, 1 dr. ; oil of chamomile, 10 drops ; croton oil, 2 drops ; oil of turpentine, q. s. Plaster, Vigo's. Syn. Emplasteum tiqokis, L. Prep. (P. Cod.) Lead plaster, 40 oz. ; mercury, 12 oz. ; liquid styrax, 6 oz. ; bees- wax, turpeuiine, and resin, of each 2 oz. ; am- PLATE-PLATINUM 1337 tnonincum, bdellinni, myrrh, and olibanam, of each 5 dr. ; HnfFron, S dr. ; oil of lavender, 2 dr. ; niHcie into a pUetor 8. a. Plaster, Warm. See Calkpaoiknt plabteb, BUBOONUT PITCH P., &C. Flatter of Wax. St)n. Simple plaster ; F.MPLASTnlrM ATTBAHENS, E, SIMPLEX (Ph. E.), B. CEU.E, L. Prep. 1. (Ph. E.) Bi-es- wux, 3 oz. ; 8uet and yellow resin, of each 2 oz. ; melt them together, und stir the mixture briskly until it concretes by cooling. 2. (Ph. L. 1836.) Yellow wax and suet, of each 3 lbs. ; yellow resin, 1 lb. ; as the last. Intended to be employed as a simple dressing, especially to blistered surfaces. It is now seldom used. Plaster, White SiacVyloa. See Plastbe OF Lrad. Plaster, Tellow Diachylon. See Plaster OF Oaldanum. Plaster, Zinoo-lead. St/n. Ehplastbum ZINOOPLOMBICUM, E. DIAPOMPHOLYOOS, L. J'rep. (Pi). Suec.) Beeswax, 1 lb ; olive oil and graphite (black lead), of each 6 oz. ; carbonnteof lead, 4oz. ; oxide of zinc ^impure), 8 oz. ; olibanum, 1^ oz.; boil to a plaster. Astringent and desiccant. Otiier forma sub- stitute an equal weight of litharge for the graphite. PLATE. The name is commonly given to gold anil silver wrought into instruments or utensils for domestic use. The cleaning of plate is an important opera- tion in a large estHblishment, as its durability, and much of its bi^iiuty, depend on this beiii^' properly done. The common practice of using mercurial plate powder is destructive to both of these, as mercury not only rapidly eriides the surface of silver, but renders it soft, and, in extreme cases, even brittle. The only powder that may be safely used for silver is prepared chalk, of the best quality. For gold, the form of red oxide of iron, known as Jeweller'i Rouge, is the most useful and appi'upriate. in his 'Workshop Receipts' Mr Spon re- commends tlie following : — " Take an ounce ciuh of cream of tartar, common salt, and alum, and boil in a gallon or more of water. After the plate is taken out and rubbed dry it puts on a beautiful silvery whiteness. Pow- dered magnesia may be used dry for articles slightly tarnished, but if very dirty it must be used tirst wet and then dry." Chamois leather, a plate brush, or very soft woollen rags, should alone be used to apply them ; and their application should be gentle and long continued, rather than the reverse. Dirty plate, after being cleaned with boiling water, may be restored by boiling it in water, each quiirt of which contains a few grains of carbonate of soda, and about an ounce of prepared chalk, calcined hartshorn, or cultle-fiah bone, in very fine powder. The ebul- lition sets up a gentle friction, which effects iU purpose adiuirably. The boiled plate, after being dried, is best ' finished off' with a piece of soft leather or woollen cloth which has been dipped into the cold mixture of chalk and water, and then dried. The same method answers admirably with German silver, brass, pewter, and all the softer metals. See Powdee (Plate), &c. PLATINA. See Platimjm. PLA"TING. The art of covering copper and other metals with either silver or gold. Plating is performed in various ways. S'>metimes the silver is fiuxed on to the sur- face of the copper by means of a solution of borax, and subsequent Exposure in the 'plating furnace,' and the compound ingot is tlien rolled to the requisite thinness between cylin- ders of polished steel. The common thickness of the silver plate before rolling is equal to about the l-40th of that of the compound ingot. Sometimes the nobler metal is pre- cipitated from its solutions upon the copper by i\ie action of chemical affinity, or, more frequently, by the agency of electro-chemical decomposition (electro-plating). The metal employed lor plating is a mixture of copper and brass, annealed or hardened, as the case may require. For electro-plated goods, ' nickel silver ' is now almost invariably employed. See ELEOTBOiypK, Gildikg, Pla- tinising, Silvebing, &c. PLAT'INISING. Metals may be coated with platinum by nearly similar processes to those already referred to under Plating. In the 'moist way ' vessels of brass, copper, and silver are conveniently platinised in the following manner : — Solid bichloride of platinum, 1 part, is dissolved in water, 100 parts, and to this solution is added of common salt, 8 parts ; or, still better, 1 part oC ammonio-cliloride of platinum and 8 parts of chloride of ammonium are placed in a suitable porcelain vessel, with about 40 parts of water, and the whole heated to ebullition ; the vessels or utensils, pre- viously made perfectly bright, are then im- mersed in the boiling liquid. In n few seconds they generally acquire a brilliant and firmly adhering layer of platinum. Silver plates for voltaic batteries are com- monly platinised by immersing them for a tew seconds in a mixture of saturated solution of bichloride of platinum, 1 part ; dilute sul- phuric acid, 3 parts ; water, 4 to 6 parts. Platinum battery plates are covered with a pulverulent deposit of platinum by means of the electrotype. Platinised asbestos is prepared by dipping asbestos into a solution of bichloride of plati- num, or one of the double chlorides of that metal, and then gradually heating it to red- ness. It is used as a substitute for spongy platinum. See Electbottpe, Voltaic elec- TRICITT. PIAT'INUM. Pt. Sj/n. Platina, White GOLD ; Platinum, L. A heavy, greyish- white metal, occurring chiefly in certain of the alluvial districts of Mexico and Brazil, in the 1338 PLATINUM Ural mountains of Eussia, in Ceylon, and in a few other places. It occurs in nature under the form of grains and small rolled masses, associated with palladium, rhodium, osmium, ruthenium, iridium, and a little iron. It has only been known in Europe since 1748. Prep. The native alloy of this metal (crude platinum) is acted upon, as far as possible, by nitro-hydrochloric acid containing an excess of hydrochloric acid, and slightly diluted with water, in order to dissolve as small a quantity of iridium as possible ; to the deep \ ellowish-red and high acid solution thus produced ammonium fchloride is added, by which nearly the whole of the platinum is thrown down in the state of ammonio-chloride. This substance, after being washed with a little cold water, is dried and heated to red- ness; the product is spongy metallic platinum. This is made into a thin uniform paste with water, introduced into a slightly conical myuld of brass, and subjected to a graduated pressure, by which the water is squeezed out, and the mass rendered at length sufficiently solid to bear handling. It is next dried, very care- fully heated to whiteness, and hammered, or subjected to powerful pressure by suitable means, whilst in the heated state. It will now bear forging into a bar, and may after- wards be rolled into plates, or drawn into wire, at pleasure. Prop., Sfc. Platinum is one of the heaviest substances known, its sp. gr. being 21'5. It is whiter than iron, harder than silver, infusible in the strongest heat of our furnaces, and melts only when exposed to the highest tem- perature obtained by Deville's oxyhydrogeu gas furnace. It is unaffected by air, water, and all the ordinary acids, and even its polish is uninjured by the strongest heat of a smith's forge; aqua regia, however, dissolves it, though with much more difBculty than gold ; it is also superficially oxidised by fused hydrate of potassium. Spongy platinum, powdered pla- tinum, and even perfectly clean platinum foil, possess the remarkable property of causing the union of oxyi,'en and hydrogen gases, with more or less elevation of temperature. Platinum is precipitated from its solutions bv deoxidising substances under the form of a black powder (platinum black), which has the power of absorbing oxygen, and again imparting it to combustible substances, and thus causing their oxidation. In this way alcohol and pyroxylic spirit may be converted into acetic and formic acids, &c. Platinum black is simply platinum in a fine state of division, and is readily obtained as follows: — 1. A solution of platinic chloride, to which an excess of carbonate of sodium and a quantity of sugar have been added, is boiled uniil the precipitate which forms after a little time becomes perfectly black, and the super- natant liquid colourless ; the black powder is then collected on a filter, washed, and diied by gentle heat. 2. Platinie-amraonium chloride, reduced to very fine powder, is moistened with strong sulphuric acid, and a small piece of zinc is thrust into the mixture ; after the whole is reduced to a black powder it is washed, first with hydrochloric acid, and then with pure water, and is, lastly, dried. 8. (Zdrawkowitch.) Platinum black, in a highly active condition, can be obtained, ac- cording to the author, by adding 3 to 5 c.c. of solution of perchloride of platinum, drop by drop, to a boiling mixture of 15 c.c. of glycerin and 10 c.c. of solution of caustic potash of 108 sp. gr. 4. (Ph. B.) Boil down rapidly, solution of potash, 2 pints, in a silver or clean iron vessel, until there remains a fluid of oily consistence, a drop of which removed on a warm glass rod solidifies on cooling. Pour this into proper moulds, and when solidified and while still warm put it into stoppered bottles. Platinum, in the state of platinum black, possesses the property of condensing gases, more especially oxygen, into its pores, and afterwards giving it out to various oxidisable substances. When placed in contact with a solution of formic acid it converts it, with copious effervescence, into carbonic acid ; alco- hol, dropped upon it, becomes changed by oxidation into acetic acid, the rise of tem- perature being often sufficient to cause inflammation ; exposed to a red heat, it shrinks in volume, assumes the appearance of spongy platinum, and, for the most part, loses these peculiarities. That prepared with zinc explodes, when heated, like gunpowder. The spongy platinum is obtained by igniting the ammonium platinic chloride at a red heat. The salts of platinum are recognised as follows : — Sulphuretted hydrogen throws down from neutral and acid solutions of the platinic salts a blackish-brown precipitate, which is only formed after a time in the cold, but immediately on heating the liquid. Ammonium sulphide also gives a blackish-brown preci- pitate, which completely redissolves in a large excess of the precipitant, provided the latter contains an excess of sulphur. Chloride of ammonium and chloride of po- tassium give yellow crystalline precipitates, insolnble in acids, but soluble in excess of the precipitate, upon the application of heat, and decomposable by heat, with production of spongy platinum. Ammonia and potassium hydrate also give similar precipitates in solu- tions previously acidulated with hydrochloric acid. ISstim. This may be effected by throwing down the metal in the form of chloride of ammonium and platinum, which, after being washed on a filter with a little weak spirit to which a little of the precipitate has been added, and afterwards with the spirit alone, may be carefully dried at 212° Pahr., and weighed. Or, the precipitate may be ignited in a platinum crucible, and weighed in the PLATINUM 1339 ■tate of a iponf^y platinum. 193-23 gr. of the platinic and ainmoiiiuin chloridea arc equi- valent to 08'7& gr. of metallic platinum. t jc.t. Platiuum ia valuable for the forma- tion of cruciblca, capsules, and other utensils or InHtrumentB inti--iidcd to he exposed to a strouK heiit, or to the action of acids. Platinic cliloride and the platinic and sodium chloride are much used in chemical analysis. Uuth of these are also used in medicines with the same intentions, and in the same doses, as the cor- responding salts of gold. These compounds are poisonoux. The antidotes and treatment are siniiliir to those described under Gold. Concladinff Memarks. — Daville and Debray have introiluced a metliod of refining pla- tinum, wliich has already done much to ex- tend the useful applications of the metal. The pruce'is consists in submitting the crude metal to the action of an intensely high temperature, obtained by the combustion of hydrogen (or coal-gas) with oxygen, in a crucible of lime, liy tliis means large qunntities of platinum (5U lbs. or more) can be kept fused until the sulphur, phiisphorus, arsenic, and osmium, generally occurring in crude platinum, are oxidised and volatilised, and the iron and copper are oxidised and absorbed by the lime forming the crucible. At the International Exhibition of 1862 an ingot. of pure platinum, weighing over 2 cwt.,wa8 exhibited hy Me>ara Johnson & Miithey, as an illustration of the priietiial results of this process. Platinic Chloride. PtCI^. £yn. Bichloride OF platinum:, Chlouide op platinum, PKBOHLdUlDK OP p. J PlAIINI BICnLOBIDUM (Pll. L.), L. PlATINI TETHACnLOUIDUM. Prep, liy dissolving platinum in nitro-hy- drocliloric acid, and evaporating the solution to dryness at a gentle heat. Prop., Sfo, lieddish-brown, deliquescent, and very soluble in both water and alcohol, yielding orange- coloured solutions. It combines with a va- ri'ty of metallic chlorides to form 'double salts." Used as a test in chemical analysis, and as an alterative in secondary syphilis, &c. — Dose, tV '0 i gr , dissolved in distilled water, or made into a pill with syrup and liquorice powder. Some per&oiis prescribe much larger doses, but unsafely. Hoefer recommends an ointment made with it as an application to indolent ulcers. In doses of 5 gr. and up- wards it acts as a violent caustic poison. This last salt is the ' chloride of platinum ' of the shops, and the one used in the arts and medi- cine. It forms one of the tests included in the .\ppendix to the Ph. L. Flatinic-Ammoniom Chloride. Pt(NHj)jCl5, or PtCI^ 2NH4CI. Sj/n. Ammonio chlokide OP platinum, Platino-chloride op ammo- nium. Prep. A solution of chlnride of ammo- nium is added to a strong solution of platinic chloride, and the precipitate washed with dilute .ilcohol. Prop. Minute, transparent, yellow octa- hedral crystals very feebly soluble in waUr, j leas 80 in dilute alcohol, and insoluble in acids ; heat converts it into spongy platinum. Platinic- Fotassium Chloride. PtK^Cle, or PtClj2KCl. Sy». Platino-chlobide'of po- tassium, Potabsio-Chlobidk op platinum. Prep. A bright yellow, crystalline precipitate, formed whenever solutions of the chlorides of platinum and of potassium are mixed ; or a salt of potassium, acidulated with a little hy- drochloric acid, is added to platinic chloride. In appearance, solubility, &c., it closely resem- bles ammonio-chloride of platinum. Platinic - Sodium Chloride. PtNiijCl,, or PtCl42NaC]. Syn. Chloride op platixcm and sodium, Sodio-chloeidb op platinum, Platino-biohlobide op sodium ; Platini et SODII CHLOBIDDM, PlATINI SODIO-CHLOEI- DIUM, kc, h. Prep. (Redwood.) Platinic chloride, 17 parts ; chloride of sodium, 6 parts ; dissolve tlie two salts separately in water, q. s., mix the solutions, and evaporate, that crystals may form. The crystals are large, transparent, and of a yellow-red colour. — Dose, -jl^ to i gr.; in the same cases as the bichloride. Platinic Oxide. I'tO,. iSyn. Binozids op PLATiNiM. Prep. 1. By exactly decom- posing the platinic sulphate with nitrate of barium, and adding pure hydrate of sodium to the filtered solution, so as to precipitate only half the oxide. (Berzelins.) — 2. By boiling platinic chloride with hydrate of sodium, in con- siderable excess, and then adding acetic acid. Prop., ice. As the hydrate (Pt(HC) 1,), it is a bulky brownish powder; this, when gently heated, becomes black and anhydrous. It forms salts with the acids, and combines with some of the bases. The salts have a red or yellow colour, and a remarkable tendency to form double salts with the alkaline salts. Obs. Both the oxides of platinum are re- duced to the metallic state on ignition. Platinons Oxide. PtO. Syn. Oxide op PLATINUM. Prep. By heating to below red- ness the platinic chloride and digesting with hydrate of potassium the residue. Prop., Sec. A black powder, soluble in excess of alkali, and freely so in the acids, forming brown solutions of the platinons salts. These are distinguished from solutions of the platinic salts by not being precipitated by chloride of ammonium. Platinons oxalate, in fine copper-coloured needles, may be obtained by heating platinic oxide in a solution of oxalic acid. Platinum Gas. Syn. Gazplatine ; Gil- lard's GAS. In Paris this gas is employed by gold- and silversmiths and electro-platers because it gives rise to no sulphur product and burns without giving ofE soot or smoke. It is free frum smell. Steam is decomposed by being made to pass through a retort filled with red-hot charcoal. The hydrogen being freed from the carbonic acid which is associated with it, by means of crystalli-ed carbonate of soda, is burnt from an Argand burner provided with numerous small holes. The flame, which 1340 PLEURISY— PLUM is not luminous in itself, is surrounded by a network of moderately fine platinam wire, which on becoming white-hot becomes lumi- nous. It burns quite steadily, and its illumi- nating power is said to exceed slightly that of coal gas. Platinam, Spongy. Frep. 1. By boating ammoaio-chloride of platinum to redness. 2. Crude bichloride of platinum and chlo- ride of ammonium are separately dissolved in proof spirit, and tbe one solution added to the other as long as a precipitate forms ; this is collected, and, whilst still moist, formed into little balls or pieces, which are then dried, and gradually heated to redness. Prop., S(c. Tliese have been noticed above. Small balls of spongy platinum are used for the hydrogen instantaneous-light lamp (Dobe- reiner's lamp) ; but they are apt to absorb moisture from the atmosphere, and then lose their power of inflaming hydrogen, until they are re-dried and heated. PLEURISY. Inflammation of the pleura, or membrane covering the lungs. The sym- ptoms of pleurisy are a sharp pain in the side, which is rendered more acute when a deep breath is taken \ quick, short, difficult inspira- tion ; a quick pulse ; and fever. Much pain is also experienced if the attempt be made to lie on the affected side. Pleurisy sometimes accompanies pneumonia or inflammation of the substance of the lungs. If allowed to run on, the disease produces effusion ot serum or of lymph into the cavity of the chest, in either case giving rise to adhesions, which cause embarrassment of breathing. On the contrary, it may terminate by resolution or complete recovery. Pleurisy generally arises from exposure to the cold. A blow or a wound will also cause it, and a not uncommon origin is the splintered end of a broken rib. In every case the advice of the medical practitioner should be souglit upon the first indications of the disease. The following treatment is suggested for adoption only by emigrants, or others unable to procure the services of the medical man in cases of urgency : — • Under these circumstances the patient, sit- ting in an upright posture, should be hied until lie is able to breathe without feeling pain. If after bleeding the pain should return, leeches, if obtainable, should be applied to the painful part, and a large blister should be placed near the afiected spot. After being bled the patient should have n hot bath. Should the pain not subside, leeching must be had free recourse to, or bloud be drawn by cupping. A brisk purgative should be given at the commencement of the disease, and after this has ceased acting the patient should take two grains of calomel and a quarter of a grain of opium every four hours, but this treatment must not be continued longer than is neces- sary. The patient should remain in bed in a room which has a uniform temperature of 60° P., and adopt a low diet. In Hobses. — Symptoma. Fever, indicated by shivering, indisposition to move or turn, quick pulse, painful cough, and hurried re- spiration. " Place the animal without delay in a cool, airy, loose box, and bleed to the extent of seven or eight quarts, or until the pulse falters. Bleeding is never justifiable after the third day, when the pulse reaches 70. Three or four drachms of aloes in solution will suffice for the horse, and clysters must also be given. Until the physic operates sedatives must be used with great caution. Twenty minims of Plemming's tincture of aconite should be given every three hours. " Towards the close of the second day the aconite may be discontinued, and a scruple of calomel and a drachm of opium given in a bolus, and repeated every four hours until four or five doses have been given. Apply liniment of ammonia or mustard to tbe sides. If the animal be thirsty give water in which nitre has been dissolved. Keep the animal perfectly quiet, and let it have soft laxative food." (Finlay Dun.) PLUG'GIITG. The introduction of a mass of lint, sponge, or other suitable material, into a wound or cavity, with the intention of arrest- ing bajniorrhage. It is now seldom adopted, except in cases of bleeding from tbe nose, and that only after more approved methods have failed. PLUM. A name applied to several varieties of the Prunus domesticus (Linn.), or wild plum. Among the cultivated varieties, the damson, greengage, French plum, magnum bonum or Mogul p., mirabelle p., Orleans p., and prune, are those best known. Grocers' * plums' are raisins, or dried grapes. In the following table will be found the composition of the principal varieties of plum. PLUMBAGO— PNEUMONIA 1341 MirabHle, conimon yelluw. Grccn^'ige. Blark- blue, niitidlo sized Plums. Dark black-red Flumi, [ Miuiel Plums. Yellow- green, luiddle size. Large green, very Bweet. ' Conimon. Italian, T,ry s«eet. Soluble mailer — Sugar .... Free ncid, reduced to equiraleiit in malic acid Albuminous Bubstanees Pectous substances, &c. Ash ... . lutoluhle matter — Hieds Slcins, &c. . IVctose [^Aihfrom insoluble mat- ter included on weight) given'] .... Water. 3-584 0-582 0197 5-772 0-570 5-780 0179 1-080 [0-082] 82-256 2-960 0-960 0-477 10-475 0-318 3-250 0-680 0-010 [0-039] 80-841 3-405 0-870 0-401 11-074 0-398 2-852 1-035 0-215 [0-037] 79-720 1-996 1-270 0-400 2-313 0496 4-190 1 0-509 [0-041] 88-751 2-252 1-331 0- 126 5-851 0553 3-329 1-020 [0-063] 85-238 5-793 n-9o2 0-785 3-616 0-734 3 540 r 1-990 1 0-030 [0094] 81-930 6-730 0-.S41 o,s:t2 4-105 0-590 3-124 0-!l72 ! 1-534 [0-066] 81-272 100-00 99-971 100-00 99-925 100-00 100-00 10000 FLUMBA'GO. 8g». Gbaphite, Blaok-lead. One of the nntive forms of cnrbon. It contains from 95 to lOO^j of pure carbon ; has a metallic lustre, and conducts electricity nearly ns well as the metals. It was formerly regarded as a carbide of iron, but the iron generally found is now known to be merely in a state of mix- ture. There are two distinct varieties of grnphite — crystiiUised or foliated graphite, ob- tained chiefly from Ceylon; and amorphous graphite (the ordinary plumbago or black- lead), largely imported to this country from Germany. The Borrowdale mine in Cumber- land, from which the finest black-lead was formerly derived, is now nearly exhausted. The foliated graphite of Ceylon and other parts is the principal material employed for making plumbngo crucibles and other lire-re- sisting goods. The amorphous graphite is used for milking black-lead pencils, polishing pow- der for stoves and grates (' lustre,' ' serviiiits' friend,' &<'.), and to diminish friction in heavy machinirv (anti-friction powder). Its powder is also used to give conducting surfaces to articles on which it is desired to deposit cop- per by the electrotype. In medicine plum- bago has been used with apparent advantage in lierpes and several chronic skin diseases — externally, as an ointment made with four times its weight of lard; and internally, made into pills. Purification. For medical and chemical use graphite may be treated as follows : — 1. (Dumas and Stas.) Heat it to redness with caustic potiissa, in a covered crucible, then v/ash it well with water, boil it in nitric acid and in aqua regia, again wa^ll it with water, dry it, and expose it at a white heat to a stream of . dry chlorine gas ; lastly, wash it with water, and again heat it to dull redness. In analysis. 2. (Ph. Bor.) Pure native plumbago, 1 lb., is boiled in water for 1 hour, then drained, and digested for 24 hours in a mixture of water, 8 oz.i nitric acid and hydrochloric acid, of each 2 oz. ; it is, lastly, well washed with water, and dried. 3. (Brodie's patent.) This process is only applicable to the hard varieties of graphite, as that of Ceylon. It consists in introducing coarsely powdered graphite, previously mixed with j)jth of its weight of chlorate of potas^a, into 2 parts of concentrated sulphuric acid, which is heated in a water bath uutil the evo- lution of acid fumes ceases. The acid is then removed by water, and the graphite diied. Thus prepared, this substance, when heated to a temperature approaching a red heat, swells up to a voluminous mass of finely divided grnphite. This powder, which is quite free from grit, may be afterwards consolidated by pressure, and used for making pencils or other purposes. PLUM'BIC ACID. Binoxide of lead occa- sionally receives this name on account of its combining with some of the bases to form compounds which have been called plum- bates. PLUM'BUM COR'KEUM. See Lead, Chlo- ride OF. PIUM'OSE AL'UM. The old name of the silky amianthine crystals of the double sul- phate of aluminum and iron occasionally found on alum slate. Asbestos has also been so PLUNKETS CANCEE REMEDY. See CArsTic, Plunket's. PNEUMONIA. Inflammation of the sub- 1342 PNEUMONIA stance of the lungs. Wlien the inflammation extends to the pleura, or covering of the lungs, the disease is distinguished as Pletteo-pneu- MONIA. By most pathologists pneumonia is described under the three general heads of — (1) Croupous pneumonia, (2) catarrhal pneu- monia, (3) chronic pneumonia, each of which have, by some medical writers, been subdivided into other forms and varieties. 1. Acute okoupous pneumonia. This first description of pneumonia is most common amongst persons of from twenty to thirty yuiirs of age, although no age escapes it, and it is generally very severe in character when it attacks the very young or old. It prevails more amongst men than women, since the former, from their more frequent exposure to the weather and to changes of temperature, run greater risk of being overtaken by a very fertile cause of croupal pneumonia, viz. a sudden chill when the body is unusually heated. It frequently seizes those suffering from chronic or acute disorders, as well as those who are intemperate and drunken. It olten assails patients suffering from contagious and acute maladies, such as measles, smallpox, pyai-mia, puerperal fever, typhus, and as ap- pears from the accounts of the recent out- break of AstraUan plague in that disease also. It likewise frequently prevails amongst the poor and badly fed living in the overcrowded quarters of large towns and cities. The following are the principal symptoms of acute croupous pneumonia, given by Dr Roberts :' — " In some cases there are premonitory signs of general indisposition for a short time. In primary, or nnmixed pneumonia, the attack sets in usually very suddenly, the invasion being attended with a single^ severe^ more or less prolonged rigor. There may be great prostration witli fever; vomiting or nervous symptoms, viz. headache, delirium, restless stupor, or, in children, convulsions. The special symptoms are local and general. " Local symptoms. — Pain in the side is usually present, commonly stabbing or piercing, in- creased by a deep breath. Difficulty of breath- ing. Cough also commences speedily ; it does not coviie on in violent paroxysms, but is short and backing and difficult to repress. Soon expectoration occurs, the expectorated matter presenting peculiar characters. It is scarcely at all trothy but extremely viscid and adhe- sive, and the vessel which contains it may often be overturned without its escaping. The expectorated matter has a rusty colour or pre- sents vaiious tints of red, from admixture of blood, and as the case progresses, changes of colour are observed through shades of yellow, until filially they become merely like the ex- pectoration of bronchitis. In some cases of croupdl pneumonia pain and other symptoms 1 • Handlionk of the Tlieory alitl Practice of Medicine,' by r. J. llulierts, M.D., &c. Lewis, 1873. are sometimes very slight or absent, and the expectoration may be merely like that in bronchitis, absent, or in low cases present the appearance of a dark, offensive, thin fluid, resembling liquorice or prune juice. " General symptoms. — These may he summed up generally as severe fever with great de- pression and prostration. The skin is hot, dry, and burning. The temperature rises with great rapidity to 102°, 103°, 105°, or sometimes higher. It has been known to reach 107° in cases which recovered, and in fatal cases it has attained to 109'4°. In a large number of instances it does not exceed 104°. There is usually considerable flushing of the cheeks. The pulse ranges generally from 90 to 120, or may be much above this." In the majority of cases this variety of pneumonia has a favorable termination, but however slight the form in which it shows itself, or the mildness of its attack, the pro- perly qualified practitioner should be called in to combat it. We have described the nature and cause of the disease and given the course to be followed in treating it, for the benefit only of the emigrant and others similarly situated. The above comments are meant to apply to the other descriptions of pneumonia, which will be adverted to in the course of the present article. Treatment to he followed in croupous pneu- monia. — Bleeding was formerly had recourse to, but this treatment has either been aban- doned of late years, or very rarely practised, the only case in which its moderate employ- ment is recommended being that in which the patient is threatened with death from partial privation or suspension of breath. Leeches may be applied to the spot in pain, and a large blister near it, but it is preferable to first try the effect of hot fomentations and poultices containing laudanum ; or turpentine sprinkled on a warm damp flannel may be tried. A third of a grain of tartarised anti- mony, with a few drops of laudanum, or a third of a grain of hydrochlorate of morphia may be given every four hours. " In all low forms of the disease the only chance is in free stimulation. At the same times full doses of carbonate of ammonia, with bark, spirits of chloroform, ether, cam- phor, and such remedies, must be administered. In some cases quinine with iron is use- ful."2 The best diet consists of milk and beef tea. The patient, it is needless to say, should he kept in bed, and the temperature of his chamber should be maintained at about 60° F. It is also most essential that the room should be thoroughly ventilated, and all the expec- torated matter, stools, &c., thoroughly disin- fected before removal. 2. Cataebhal PNEtJMONiA. The acute va- riety of this form of pneumonia is that which principally attacks infants and children, and ' Br Roberts. PNEUMONIA 1313 frequently complicates diphtheria, hooping- ''ough, lueasles, luid influenza ; although it may ui'CHHionally occur when not associated wilh these diseases. In the othervariety— chronic catarrhal pneu- monia — the greater number of cases arise from bronciiitis. Many authorities look upon tlie liiat variety of pneumonia as tlie cause of a grrat proportion of the cases of pulmonary phthisis. Syinptomt. — These differ, in the great majo- rity of cases, from croapal pneumonia, in not being preceiled by rigors. There is always fever and a rise of bodily temperature from 103° to 195°. There is often copious perspira- tion and increased pulse. As the disease pro- gresses the breathing becomes more difficult and rapid, the cough changes its character, and " becomes short, harsh, hacking, and pain- ful, tlie child endeavouring to repress it, and having an expression of pain or crying and diminished expectoration."' The treatment of this form of pneumonia couHists in keeping up the strength of the patient by means of good nourishing food, and stimulants judiciously administered. Ammonia and seup);a should be given if the sufferer is very weak. In ordinary cases ipecacuanha wine will be found useful. Poultices of lin- seed or mustard to the chest are also pre- scribed. During convalescence the patient requires canful watching; his diet should be generous, and should include wine; cod-liver oil, quinine, and iron, or other tonics are ad- diuonally necessary. 3. CimoNio PNEUMONIA. This disease, in which the substance of the lung is in a more or less abnoimal or altered condition, is mostly the result of some previous pulmonary all'ec- ti(m. It frequently follows successive attacks of the catarrhal variety of pneumonia and the l>roncljial irritation arising from the inhala- ticm of small particles of dust given off by substances employed in certain occupations or mauufaetnres, such as coal, steel, granite, &c. The symptoms are pains in the side, cough, sometimes occurring in severe paroxysms, shortness of breathing, the patient meantime gradually becoming Lhinner and weaker. .Simetimes nifjht sweats occur, but generally there is liUle or no fever. The be-t treatment is nourishing diet, com- bined with tonics and cod-liver oil. Of late years the doctrine of the contagious nature of some forms of acute pneumonia (whether complicated with pleurisy or not) seems to have been gaining ground amongst medical practitioners. The well-known fact that the pleuro- pneumonia of cattle is propa- gated by contagion, if it does not prove thi- contention, ia at any rate "worthy," as Dr Parkes remarks, "of all attention." The following cases, selected from amongst many others equally striking, would appear to lend considerable support to this view : ' Dr Kobtrls. 1. The 'Lancet' for January 9th, 1862, contains a communication from Dr Bryson, describing an epidemic of pleuro-pneumonia which occurred in 1860 amongst the Mediter- ranean fleet. The infectious character of the disease is stated to have been very marked ; besides which there were several points of resemblance between it and the pleuro-pneu- monia which attacks cattle. 2. Professor Bock of Christiana has re- corded an outbreak of pneumonia which took place in the Akerhas prison of that city in 1866. Out of 360 prisoners 62 of them were attacked with pneumonia in six months. The prison, like the cattle sheds, ravaged by pleuro-pneumonio, was badly ventilated and overcrowded. The following illustrations are extracted from Dr Wynter BIyth's valuable ' Dictionary of Hygiene and Public Health." 1. "Mr Alfred Mayo, Mildenhall, Suffolk, in a private letter to the author, gives a series of cases in which the infectious character of the malady was well marked. The first ca~e was that of a bricklayer, about thirty-tive years of age, who was taken ill with pleuro- pneumonia. His mother, who nursed him, very shortly afterwards took the ►ame disea-c and died. A neighbour, a heidthy young woman over thirty, who came in to nurse the last patient, was also taken similarly ill, and died with all the physical and other signs and symptoms well developed; and lastly, her child contracted the disease, but eveutually recivered. There were other cases in the neighbourhood at the same time, and all ot tliem were remarkable for their fatality." 2. " Dr Richard Budd, of Barnstaple, has communicated to the author the following remarkable cases: — 1. A clergyman, after attending a public meeting, became affected with acute pneumonia. 2. The nurse in attendance became ill of the same disease about a week afterwards. 3. The clergyman's sister, taking the place of the nurse, was iu her turn also seized with pneumonia. 4. A brother of the clergyman, who now undertook the duty of nurse, was in a very short time laid up with the same malady. Tire nurse and sister died, the two brothers recovered. Dr Budd concludes his commuiiications as fol- lows : ' Since tliat time I have witnessed in- numerable instances of the occurrence of this disorder iu several members of the same family in succession, and I am thoroughly convinced that it spreads by infection, as the facts I have observed admit of no other explanation.' " The following table, from the Registrar- General's Report for 1875, gives the yearly number of deaths from pneumonia in England from 1818 to 1875:— 1818 . . 21,868 1852 . . 21,l-21 IS 19 . . 21,194, l,s.->3 . . 2 1X198 1S50 . . 20,303 ls.j I. . . 23,523 1851 . . 22,001 lSo5 . . 2(!,052 134:4, POACHING— POISON 1856 . . 22,653 1866 . . 25,155 1857 . . 23,452 1867 . . 21,118 1858 . . 26,486 1868 . . 19.908 1859 . . 24,514 1869 . . 25,246 1860 . . 25,264 1870 . . 23,729 1861 . . 22,914 1871 . . 22,768 1862 . . 23.713 1872 . . 20,282 1863 . . 24,181 1873 . . 22,904 1864 . . 24,470 1874 . . 25,927 1865 . . 22,489 1875 . . 27,161 As a commentary upon the high death-rate from pneumonia for 1875, we may quote the Report for 1877 of the Registrar-General to the President of the Local Government Board. He writes, " The winter of 1875 was unusually severe ; extremes of temperature, with a long continuance of east winds, were fatal to in- fants and to elderly people, and no less than 162,156 deaths were registered in England for the first quarter of the year ; the mortality was at the annual rate of 27*5 per 1000, or 2'6 per 1000 above the average of the thirty- eight years— 1838-75." In animals. For pneumonia and ordinary pleuro-pneumonia, the treatment prescribed fur pleurisy may be followed. Epidemic PLEnEO -pneumonia of cattle. It is now universally admitted that this dis- ease is very often traceable to contagion, and hence that its propagation has been largely due to the practice of purchasing infected animals in open market, and afterwards allowing them to herd with healthy ones. When a cow is attacked with this epizootic disease, the fli'st noticeable symptoms are generally tenderness and flabbiness of the udder, and a frothy condition of the milk. These symptoms are accompanied with a dry cough and irregularity of appetite; at the same time the mouth, horns, and legs become hot, the pulse becomes more rapid, and the breathing also. When on its feet the animal arches its back, and when lying down rests itself upon its breast bone. Generally, how- ever, when in the recumbent posture, it lies on that side where the affected lung is. The treatment, omitting the bleeding, is very similar to that recommended for pleurisv, except that it should be supplemented by the application to the sides of fomentations of hot water, followed by the rubbing in of mustard or of some vesicant. "If no improvement occur after the third or fourth day, give three times daily an ounce each of ginger and gentian, with four drachms of sulphate of iron. Where there is debility, arrested secre- tion, and cold extremities, give several times a day a quart of warm ale, with an ounce each of ginger, cardamoms, fenugreek, or other aromatics."' POACH'ING. Amongst cooks, a peculiar method of cooking small articles by a slight boiling or stewing process. Poached eg&s are prepared by breaking ^ Finlay Dun. | them into a small saucepan or stewpan con- taining about i a pint of boiling water, to which a teaspoonful of common salt, and, oc- casionally, a little vinegar, is added, and gently simmering them for 3 or 4 minutes, or until sufficiently firm to bear removal with a spoon or ' slice.' Another method is to employ melted butter instead of water, and to dress them either with or without stirring. Poached eggs are commonly served on toast, or with fried ham or bacon, with spice or vege- table seasoning at will. They form an excel- lent breakfast, or ' make-shift dinner.' PODOPH'YILIN. Si/». Resin op podo- PHTILTIM ; Resina podophylh (B. P.). Ob- tained from the root of the Podophyllum pelta- tum (Linn.), or may-apple, a substance officinal in the Ph. U. S. Prep. 1. The alcoholic extract of may-apple is digested in cold ether to remove fatty matter, and is then dissolved in rectified spirit; the solution is decoloured with a little animal char- coal, and filtered ; it is, lastly, allowed to eva- porate spontaneously. 2. (B. P.) Podophyllum, in coarse powder, 1; rectified spirit, 3|, or a sufficiency; dis- tilled water and hydrochloric acid, of each a suflRciency ; exhaust .the podophyllum by per- colation with the spirit; distil over the spirit; slowly pour the liquid remaining after the dis- tillation of the tincture into three times its volume of water acidulated with -^fh part of its weight of hydrochloric acid, constantly stirring; let it stand 24 hours; collect the re.sin which falls, wash on a filter with distilled water, and dry in a stove. Cholagogue purga- tive ; used as a substitute for calomel. — Dose, ^ to J gr., or even 2 gr. It is best to begin with ^ gr. (Squire.) Prop., ^c. An amorphous, greyish-white mass, soluble in alcohol, and slightly soluble in water. It is a safe and certain cathartic, supe- rior in activity to resin of jalap. — Dose, ^ to 3 gr. See Extract op May-'Appie. PODOPHYLLUM SCOT. Syn. Podophtlli RADIX (B. P.) The dried rhizome of the Podo- pkyUum peltatitm ; imported from North Ame- rica. Active and certain cathartic. — Dose, 10 to 20 gr. POIS'GN. Syn. ToxicuM, Venenum, L. Any substance which, when swallowed or ap- plied in any particular way to the living body, disturbs, suspends, or destroys one or more of the vital functions. In sufficient quantity, or in small doses long continued, the com- mon result of the administration of dele- terious substances is either impaired vitality or death. Poisons are classified by Orfila under four heads : — 1. Iehitant poisons, or such as inflame or corrode the parts with which they come in contact. Their chief effects are upon the ali- mentary canal, with, sometimes, ulceration of the tongue, fauces, and oesophagus. Nausea, vomiting, stomachic and intestinal pains, ex- rOLAUISATlON— POLYCHRESr 1345 troiue «nxiety mid nnguish, quick and feeble pulse, cold and clammy skin, iind mucous, bilious or Moody diarrlicea, are nmon'ESS. Polish, Leather. See Blacking. POL'LARD. See Floue. POL'YCHREST. Si/n. Poltchsestus, L. A term formerly applied to several medicines on account of the numerous virtues they were 85 1346 POLYCHROITE— POMMADE supposed to possess. Sal polyerestus is the old iiHme for sulphate of potassa. POL'YCHKOITE. The name formerly given to the colouring matter of saffron, from the variety of colours which it exhibits with dif- ferent reagents. Its alcoholic and aqueous solutions are of a golden yellow ; nitric acid turns it green ; sulphuric acid, first blue, and then lilac. POM'ACE. See Cidee. POMA'TUM. Syn. Pommade, Fr. This term was originally applied to a fragrant oint- ment prepared with lard and apples ; but is now wholly restricted, in this country, to solid greasy substances used in dressing the hair. The pomatums of French pharmacy (POMMADES, aEAISSES M^DIOAMENTEtTBES — P. Cod. ; IIPAEOLES — Guibourt ; LIPAEOIES and IIPAEOID^S— Beral; steaeoles — Che- reau) are soft ointments, having a basis oflurd or fat, without resinous matter. See Oint- ment and Pommade. POMEGEAN'ATE. The Tunica granatum (Linn.), a small tree indigenous in Persia and the East. Fruit (pomeqeanjite; geanata, MALA pitnica) is cooling and astringent; fruit-rind (POMEGEANATE PEEL; MATACO- EIUM, COEI-EX GEANATI ; GEANATUM — Ph. L.) and root-bark (geanati eadix — B. P., Ph. L., E., & D.) are powerfully astringent, detersive, and anthelmintic ; the last more par- ticularly so. The double flowers of the wild tree (balaustines ; BALAUSTias, as well as those of the cultivated one (cttini), are tonic and aiitringent. — Dose, 15 to 20 gr. of the root-bark, repeated every 30 or 46 minutes, until four doses have been taken, followed by castor oil ; in tapeworm. As an astringent, all the parts described are commonly given under the form of decoction. POMMADE. [Fr.] The term applied by Continental perfumers to any soft fragrant ointment (pomatum). In the preparation of pommades one of the first objects of consideration is to obtain their fatty basis in as fresh and pure a state as pos- sible. Lard, beef, and mutton suet, beef mar- row, veal fat, and bear's fat, are the substances commonly employed for this purpose, either singly or in mixtures of two or more of them. The fat, carefully selected from a young and healthy animal, after being separated from extraneous skin and fibre, is pounded in a marble mortar, in the cold, until all the mem- branes are completely torn asunder. It is next placed in a covered porcelain or polished metal pan, and submitted to the heat of a water bath, which is continued until its fatty portion has liquefied, and the albuminous arid aqueous matter, and other foreign substances, have completely separated and subsided. The liquid fat is then carefully skimmed, and at once passed through a clean flannel filter. In this state it may be aromatised or perfumed at will ; after which, when it is intended tliat thepoumiade should he opaque and white, it is assiduously stirred or beaten with «. glass or wooden knife, or spatula, until it concretes; but when it is desired that it should appear transparent or crystalline, it is allowed to cool very slowly, and without being disturbed. To prevent the accession of rancidity, a little benzoic acid, gum benzoin, or nitric ether may be added to the fat, whilst in the liquid state, as noticed under Fat and Ointment. Some- times a small portion of white wax or bees- wax (according to the intended colour of the product) is melted with the fat to increase its solidity. Some parties employ a few grains of powdered citric acid per ounce, in a like manner, with the intention of increasing the whiteness of the compound ; but the practice is not to be commended, as pommades so prepared prove injurious to the hair. The French perl'umers, who are celebrated for the variety and excellence of their pom- mades, divide them into four classes : — 1. Pommades by infusion. These are made by gently melting in a clean pan, over a water bath, 2 parts of hog's lard, and 1 part of beef suet (both of the finest quality, and carefully ' rendered '), and adding thereto one part of the given flowers, previously carefully picked and separated from foreign matter ; or, if the odorous substance is a solid, then coarsely bruised, but not reduced to fine powder. The mixture is next digested at a very gentle heat for from 12 to 24 hours, with occasional stir- ring, the vessel being kept covered as much as possible during the whole time. The next day the mixture is reheated, and again well stirred for » short time, after which it is poured into canvas bags, and these, being securely tied, are submitted to powerful pres- sure, gradually increased, in a screw or barrel press. This operation is repeated with the same fat and fresh flowers, several times, until the pommade is sufticiently perfumed. A good pommade requires thrice to six times its weight in flowers to be thus consumed; or gf the aromatic barks and seeds a corresponding proportion. The pommades of cassia, orange flowers, and several others kept by the French perfumers, are prepared in this manner. 2. Pommades by contact (enfleueaoe). These are made by spreading, with a palette knife, simple pommade (made with lard and suet as above) on panes of glass or pewter plates, to the thickness of a finger, and stick- ing the surface all over with the sweet-scented flowers. These last are renewed daily for one, two, or three months, or until the pommade has become sufficiently perfumed. On the large scale, the panes are placed in small shallow frames, made of four pieces of wood nicely fitted together, and are then closely piled one upon another. On the small scale, pewter plates are generally used, and they are inverted one over the other. In some of the perfumeries of France many thousands of frames are employed at once. The pommades of jasmin, jonquil, orange flowers, narcissus. POMMADE 1347 tuberose, violet, and r>f gome other delicate flowers, are prepared in tliis mauner. 3. PoMMADES BT ADDITION. These are prepared by simply adding the fragrant essences or esnential oils, in tliu required quan- tity, to the simple pominiide of lar^l and suet t) produce the proper odour. In tliis way the jinnimades of bi-rgainotte, c^drat, cinnamon, lemons, lemon thyme, lavender, limettes, mar- joram, Portu?«l roses, rosemary, thyme, ver- bena, and about 40 others kept by the Parisian perfumers, are made. 4. Mixed foumadeb. Of these a great variety exists, prepared by the addition of judiciiiu'i combinations of the more esteemed perl'uiues to simple pomraade ; or, by the ad- mixture of the different perfumed pommades, whilst in the semi-liquid state. (See below.) The coloueed pommades derive their re- spective tints from tinctorial matter added to the melted fat before peifuming it. Geeen is given by gum guaiacum (in powder), or by the green leaves or tops of hpinach, parsley, liivendt'r, or walnut;— bed, by alkanet root and carmine; — yellow and oeanoe, by an- natto or palm oil ; white fommades are miide with mutton suet, instoid of beef suet. The BEOWN and black hard pomatums, vended under the name (Vf ' OOSMBTKJWB,' arc noticed at pajje 513. A few compound pommades are used as skin cosmetics. Pommade. Syn. Pomatum. Prep. 1. (Plain pomatum, Simple p.)— a. From lard, 2 lbs. ; beef suet, 1 II). ; carefully rendered as above. The ordinary consistence for temperate climates. J, Liird and suet, equal parts. For warm climates. Both may be scented at will. 2. (Scented pomatum.)— o. Plain pomatum, 1 lb. ; UK'lt it by the least possible degree of heat, add of essence of lemon or essence of lierpiMHit, 3 dr. ; and stir the mixture until it concretes. Tliis forms the ordinary ' pomatum' of tlie shnps. 4. Pla n pomatum, 1 J lb. ; essence of berga- mot, li dr.; essence of lemon, 1 dr. ; oils of rosemary and cassia, of each i dr. ; oil of cloves, 20 drops. More fragrant than the last. Pommade, Castor Oil. Prep. 1. From castor oil. 1 lb.; white wax, 4oz. ; melt them together ; then add, when nearly cold, of essence of bergamot, 3 dr. ; oil of lavendi r (English), i dr. ; essence of ambergris, 10 drops. Supposed to render the hairy glossy. 2. (Crystallised.) From castor oil, 1 lb ; spermaiiti, 3 oz. ; melt them togntlier by a gentle heat, add, of essence of bergamot. 3 dr. ; oil of virlieiia, lavender, and rosemary, of each i dr. ; pour it into wide-mouthed glass bottlfs, and allow it to cool very slowly and undistnrl'ed. Pommade, Castor Oil and Glycerine. (Ameri- can receipt.) White wax, IJoz. ; glycirin, 2 02. ; insior oil, 12 oz. ; essence of lemon, 5 dr. J essence of bergamot, 2 dr.; oil of laven- der, 1 dr. ; oil of cloves, 10 drops ; annatto, 10 gT. ; rectified spirit and distilled water, of eacb a sufficient quantity. By a moderate heat dissolve the wax in a small portion of the castor oil (one fourth), and triturate it with the remainder of the oil and glycerin till quite cool; then add volatile oils. Lastly, rub the annatto with a drachm of water till smoothly suspended ; add a drachm of alcohol, and stir the colouring into the pomade until it is thoroughly mixed. Avoid much heat. Pommade, Cazeuave's. Prep. From pre- pared beef marrow, 4 oz. ; tincture of can- tharides (P. Cod.), 3 to 4 dr. ; powdered cin- namon, J oz. ; melt them together, stir until the spirit has, for the most part, evaporated, then decant the clear portion, and again stir it until it concretes. Recommended as a remedy for baldness and weak hair. It is to be used night and morning ; the head being washed with soap-and-water, and afterwards with salt-and-water, before applying it. Dr Cattell scents it with the oils of origanum and bergamot instead of cinnamon. Pommade, CoUante. Prep. 1. Oil of almonds, 3 oz. ; white wax, J oz. ; melt them together, and add, of tincture of mastic (strong), 1 oz. ; essence of bergamot, i dr. Used to stiffen the hair, and keep it in form. 2. Burgundy pitch (true), 3 oz. ; white wax, 2 oz. ; lard, 1 oz. ; melt, and, when consi- derably cooled, stir in, of tincture of benzoin, 1 oz. ; essenie of bergamot, J dr. Used to fasten false curls. Pommade, Cowslip. Prep. From plain pommade, 2 lbs. ; essence ol bergamot, 3 dr. ; essence of lemon and essence of orange peel, of each 1 dr.; huile an jasmin and essence de petit grain, of each i dr. ; essrnce of amber- gris, 6 drops. Pommade, Crystallised. Prep. From nlive oil and spermaceti, as crystallised castor oil pommade, with scent at v\iU Pommade of Cucnmbera. Syn. Pommade db CorcoMBUES. Unguentum cucfmis. Prep. Lard, 10 oz. ; veal suet, 6 oz. ; balsam of tolu, 9gr.; rose water, 44 minims; cucumber juice, 12 oz., by weight. Melt the lard and the suet over a water bath, and add tlie tolu, previously dissolved in a little alcohol, and then the rose- water. When clear, decant it into a tinned basin, then add to a third of the cucumber juice, and stir continually for 4 hours ; pour ofE the juice and add another third, stir as Ijelbre, then pour off, and add the remainder of the juice; separate as much a^ possible the fat from the liquid, melt by a water bath, and after some hours skim, and put into pots. (Beat, when in a semi-liquid state, with a woollen spatula, when it will become much lighter and nearly double in bulk.) Pommade d'Alyon. See Ointment op Niteic acid. Se.' Cups. Pommade de Beauty. Prep. From oil of al- monds, 2 oz. ; spermaceti, 2 dr. j white wax, IJ^ dr. ; glycerin, 1 dr. ; balsam of Peru, i dr. ; 13i8 POMMADE mixed by a gentle heat. Used as a skiu cos- metic as well as for the hair. Pommade de Casse. Prep. From jilain pommade, 1 lb. ; palm oil, i oz. ; melt, ppur ott'the clear, and add oil of uussiaand huile au jasmin, of ench 1 dr. ; neroli, 20 drops j oil of verbena or lemon grass, 15 drops; otto of roses, 5 drops ; and stir until nearly cold. Very fragrant. Pommade d'Hebe. Frep. To white wax, 1 oz., melted by a gentle heat, add, of the juice of lily bulbs and Narbonne lioney, each 2 oz. ; rose water, 2 dr. ; otto of roses, 2 drops. Applied night and morning to remove wrinkles. Pommade de Ninon de I'Enclos. Prep. Take of oil of almonds, 4 oz. j prepared lard, 3 oz. ; juice of houseleek, 3 fl. oz. Used chiefly as a skin cosmetic. Said to be very softening and refreshing. Pommade Divine. Prep. 1. Washed and purified beef marrow, 2 lbs.; liquid styrax, cypress wood, and powdered orris root, of each 2 oz. ; powdered cinnamon, 1 oz. ; cloves and nutmegs, of each (bruised) 4 oz. ; digest the whole together by the beat of a water bath for six hours, and tlien strain through flannel. 2. Plain pommade, 2 lbs.; essence of lemon and bergamot, of each 2 dr. ; oils of lavender and origanum, of each 1 dr. ; oils of verbena, cassia, cloves, and neroli, of each 12 drops; huile au jasmin, 3 dr. ; essence of violets, i oz. Pommade, Dupnytren's. Prep. 1. Take of prepared beef marrow, 12 oz. ; melt, add of baume nerval (see Ointment, Nervine), 4 oz. ; Peruvian balsam and oil of almonds, of each 3 oz. ; and lastly, of alcoholic extract of can- fcharides, 36 gr. ; (dissolve in) rectified epirit, 3 fl. dr. This is the original formula for this celebrated pommade. The following modifi- cations of it are now commonly employed : — 2. (Cap.) Beef marrow, 2 oz. ; alcoholic extract of cantbarides, 8 gr. ; rose oil, 1 dr. ; essence of lemons, 30 drops. 3. (Guibourt.) Beef marrow and ' baume nerval ' (page 1179), of each 1 oz. ; rose oil, 1 dr.; alcoholic (or acetic) extract of can- tbarides, 6 gr. ; (dissolved in) rectified spirit, q. o. These compounds are used to promote the growth of the hair and to prevent bald- ness, for which purpose they are usually co- loured and scented according to the taste of the manufacturer. To be useful, they should be well rubbed on the scalp, at least once daily, for several weeks, and the head should be occasionally washed with soap-and-water. Pommade, East India. Prep. Take of suet, 3 lbs.; lard, 2 lbs.; beeswax (bright), \ lb.; palm oil, 2 oz. ; powdered gum benzoin, 3 oz. ; musk (previously triturated with a little lump sugar), 20 gr. ; digest the whole together in a covered vessel, by the heat of a water bath, for 2 hours, then decant the clear portion, and add, of essence of lemon, \ oz. ; oil of lavender. J oz.; oils of cloves, cassia, and verbena, of each i dr. A favourite pommade In the East Indies. Pommade for Freckles. (' New York Drug- gists' Circular.') Prep. Citrine ointment and oil of almonds, of each 1 dr. ; spermaceti ointment, 6 dr.; oil of roses, 3 drops. Mix well in a wedgewood mortar, using a wooden or bone knife. Pommade, Hard. Syn. Haed pomatum. Roll p. Prep. 1. Take of beef suet, 2 lbs. ; yellow wax, \ lb. ; spermaceti, 1 oz. ; pow- dered benzoin, i oz. ; melt them together, then add, of oil of lavender, 2 dr.; essence of ambergris, \ dr. Before it concretes pour it into moulds of piiper or tin foil. 2. Mutton suet and lard, of each I lb. ; white wax, 6 oz. ; melt, and add, of essence of lemon, 2 dr. ; oil of cassia, i dr. Other per- fumes may be einplnyed at will. Hard pomatums are used to gloSs and set the hair. They act both as 'pommade' and ' fixateur.' See Cosmetiqtje. Pommade, Macassar. Prep. Prom castor oil, 5 oz. ; white wax, 1 oz. ; alkanet root, i dr. ; heat them together until sufiiciently coloured, then strain, and add, oil of origanum and oil of rosemary, of each 1 dr. ; oil of nut- meg, \ dr.; otto of roses, 10 drops. Said to be equal in efficacy to macassab oil. Pommade, Marechal. Plain pommade scented by digesting it with poudre marechale. Pommade, Marrow. Syn. Maekow poma- tum. Prep. Piom prepared beef marrow, i lb. ; beef suet, J lb. ; palm oil, i oz. ; melted together and scented at will. Pommade, Millefleur. Prep. From plain pommade scented with a mixture of essence of lemon and essence of ambergris, each 4 parts ; oil of lavender, 2 parts; oil of cloves and essence de petit grain, of each 1 part; or with other like perfumes so proportioned to each other that no one sliall predominate. Much es- teemed. Pommade, Roll. See Pommade, Haed. Pommade, Eoman. See below. Pommade, Rose. Si/n. Eose pomatum. This is plain pommade or hard lard, which has been well beaten with eau de rose, or, better still, scented with otto of roses. It is sometimes tinged with alkanet root. Pommade, Soft. Plain pomatum scented at will. Pommade, Sonbeiran'a. Prep. From beef marrow, 1^ oz. ; oil of almonds, i oz. ; disul- pliate of quinine, 1 dr. Recommended for strengthening and restoring the hair. Pommade, Transparent. Prep. Spermaceti, 2 oz. ; castor oil, 5 oz. ; alcohol, 5 oz. ; oil of bergamot, -j dr. ; oil of Portugal, i dr. Pommade, Vanilla. Syn. Roman pommade, Pommade a la vanille, Pommade Romain. Froin plain pommade and pommade k la rose, of each 12 lbs. ; powdered vanilla, 1 lb. » heat them together in a water bath, stir constantly for 1 hour, let it settle for another hour POPPT— PORTER 13^9 decant the clear, and add, oil a lu rose, 2^ lbs.; bt'ijrimot, 1 I z. POPPY. Si/n. White poppy ; Papaver' BOHNIFEHOH, L. Tlie c«psul>-» or fruit (" ma- ture" — Ph. L. ; " not quite ripe" — Pli. E.) fnnn tile poppies or jioppy-lieails of the shops (PAPAVEKIS CAPSCL^; PAPAVEB— Pll. L., E., 1^ U.). Tliey are anodyne and narcotic, similar to opium, but in onl.v a very slight degree. The seeds (maw seed), which are Kweet, oleaginous, and nutritious, are used a< a substitute for almonds in confectionery and mixtures, and are pressed for their oil. See ExTBAOT, Opium, and Stbup. Poppy, Ked. Syn. CoBN poppT, Corn eose ; Papaveb bhceab, L. The fresh petals or Howers (rhcbadob petalaj bhceas — Ph. L., K . & D.) are reputed pectoral, but are chiefly employed ou account of their rich colour. Slt SykuP. POP'ULIIf. S(/n. POPULISUM, h. A pe- culiar neutral, crystallisahle suhstnnce, for- merly supposed to be an alkuliiid, found, asso- ciated witli BALIOIN, in the root-bark of the Populus tremula (Linn.), or a«pen. Prep. Concentrate the decoction by a gentle heut, and set it aside in a cool situation to iiysLullisc ; dissolve the cr^Ktals which are -ited in rictiftud spirit, decolour them by tlit;L'-tinn with animal *charconl, filter, aiid again crystallise. To render them still purer they may be redissolved and crystallised a second and a third tira«, if necessary. Prop., S(c. It resembles saliciu in appear- ance and solubility, hut, unlike that substance, has ■• penetrating swict tiiste. Dilute acids couveit it into benzoic acid, grape sugar, and saliretiii ; and with a mixture of sulphuric acid and bichromate of potassa it yields u large quantity of 8;ilicylou3 acid. It appears to be tunic, stomachic, and febrifuge. POR'CELAIIT. See Pottery. PORE. The value of pork as an article of diet Is well known. That from the young and properly fed animal is savoury, easy of diges- tion, and, when only occasionally employed, highly wholesome j but it is apt to disagree with some stomachs, and should, in such cases, he avoided. To render it proper for food, it should be thoroughly but not overcooked. When salted it is less digestible. The fre- quent use of pork is said to favour obesity, and to occasion disorders of the skin, especially in the sedentary. See Meat. POR'PHYEIZED, PORPHORIZA'TION. Words coined by recent pharmaceutical writers, and possessiiis; similar meanings to levigated and LEVIOATION. POEPHY'ROXIN. A neutral crystallisable substance discovered by Merck in opium. It is soluble in both alcohol and ether, insoluble in water, and is characterised by assumins; a purpl'sh-red colour when heated in dilute )iydrochloric acid. PORRI'GO. See Ringworm. FOR'TEK. This well-known bcverap-o. now the common drink of the inhabitants of Lon- don, by whom it is generally termed ' beer,' originated with a brewer named Harwood. in 1722. Previously to this date, 'ale,' 'beer.' and 'twopenny,' constituted the stock in trade of tlie London publican, and were drnuk, either singly or together, under the names "f ' halt-and-half or 'three threads,' for wliicii the vendor was compelled to have recnurse to two or three different ca>ks, as the case might demand. The inconvenience and trouble thus incurr-ed led Mr Harwood to endeavour to produce a beer which should possess the flavour of the mixed liquors. In this he succeeded so well that his new beverage rapidly super- seded the mixtures then in use, and obtained a general preference among the lower classes of the people. At first this liquor was called ' entire' or ' entire butt,' on account of it being drawn from one cask only, but it after- wards acquired, at first in derision, the now familiar name of ' porter,' in consequence of its ^'er.cral consumption among porters and labourers. The word ' entire' is still, however, frequently met with on the signboards of taverns about the metropolis. The characteristics of pure and wholesome porter are its transparency, lively dark brown colour, and its peculiar bitter and slightly burnt taste. Originally, these qualities were derived from the ' high-dried malt,' with which alone it was browed. It is now generally, if not entirol V, miide from ' pale' or * amber malt,' mixed with a sufficient quantity of 'patent' or 'roasted malt' to impart the necessary flavour and colour. Formerly, this liquor was 'vatted' and 'stored' for some time before being sent out to the retailer, but the chant'C in the taste of the public during the last quarter of a century in favour of the mild or new porter has rendered this unnecessary. The best ' draught porter,' at the time of its con- sumption, is now only a few weeks old. In this state only would it be tolerated by the modern beer-drinker. The old and acid beverage that was formerly sold under the name of porter would be rejected at the pre- sent day as ' hard' and unpleasant, even by the most thirsty votaries of malt liquor. The ' beer' or ' porter' of the metropolitan brewers is essentially a weak mild ale, coloured and fiavoured with roasted malt. Its richness in sugar and alcohol, ou which its stimulating and ni'tritive properties depend, is hence less than that of an uncoloured mild ale brewed Irom a like original quantity of malt. For pale malt is assumed to yield 80 to 84 lbs. of saccharine per quarter; whereas the torrefied malt employed by the porter brewers only yields 18 to 24 lbs. per quarter, and much of even this small quantity is altered in its pro- perties, and is incapable of undergoing the vinous fermentation. In the manufacture of porter there is a waste of malt which does not occur in brewing ale ; and the consumer must, 1350 POKTEE therefore, either pay a higher price for it or be content with a, weaker liquor. The hygienic properties of porter, for the most part, resemble those of otiier malt liquors. Some members of the faculty con- ceive that it is better suited to persons with delicate stomachs and weak digestion than either ale or beer. That there may be some reason for this preference, in such cases, we are not prepared to deny, but undoubtedly, when the intention is to stimulate and nourish the system, ale is preferable. Certain it is, however, that the dark colour and strong taste of porter render its adulteration easier than that of ale, whilst such adulteration is more dif&cult of detection than in the paler varieties of malt liquors. " For medical purposes, ' bottled porter' (cbrbvisia laoenaeia) is usually preferred to ' draught porter.' It is useful as a restorative in the latter stages of fever, and to support the powers of the system after surgical operations, severe accidents, &c." (Pereira, ii, 982.) When ' out of condition' or adulterated, porter, more than perhaps any other malt liquor, is totally unfit for use as a beverage, even for the healthy ; and when taken by the invalid, the consequences must necessarily be serious. Dr Ure says that pure porter,' " when drank in moderation, is a fur wholesomer beverage for the people than the thin acidulous wines of France and Germany." The manufacture of porter has been described in our articlj on Beewino, and is also referred to above. It presents no difficulty or pecu- liarity beyond the choice of the proper ma- terials. A mixture of 'brown' and 'black malt' is thought to yield a finer flavour and colour to the pale malt that gives the body to the liquor than when ' black' or ' roasted malt' is employed alone. The proportion of the former to the latter commonly varies from l-6th to l-4th. When * bl»ck malt' is alone used, the proportion varies from the I-lOth to l-15th. 1 lb. of 'roasted malt,' mashed with about 79 lbs. of pale malt, is said to be capable of im- parting to the liquor the flavour and colour of porter. The following formulae were formerly commonly employed in London : — 1. (Deauqht pobtee.) From pale malt, 3i qrs. ; amber malt, 3 qrs. ; browi< malt, Ij q. ; mash at twice with 28 and 24 barrels of water, boil with brown Kent hops, 56 lbs., and set with yeast, 40 lbs. Prod. 28 barrels, or 3i times the malt, besides 20 barrels of table-beer from a third mashing. 2. (BOTTLIHa POETEB; BeOWN STOUT.) From pale malt, 2 qrs. ; amber and brown malt, of each 1^ qr. ; mash at 3 times with 12, 7, and 6 barrels of water, boil with hops, 50 lbs., and set with yeast, 26 lbs. Prod, 17 barrels, or li times the malt. The purity and quality of porter, as well as of other malt liquors, may be inferred in the maimer noticed under Beee; but can only be positively determined by a chemical exami- nation. For tills purpose several distirujt opera- tions are required : — ■ 1. Richness in ALCOHOL. This may be coi - rectly found by the method of M. Gay-Lussac ; or from the boiling point. (See Alcoholome- TET and Ebtiilioscopb.) The method with anhydirous carbonate of potassa will also give results sufiSciently near to the truth for ordinary purposes, when strong or old beer is operated on. The quantity of the liquor tested should be 3600 water- grains measure; and it should be. well agitated, with free exposure to the air, after weighing it, but before testing it for its alcohol. The weight of alcohol found, multiplied by 1'8587, gives its equivalent in sugar. This may be con- verted into ' brewer's pounds' or density per barrel, as below. 2. Richness in baochaeine or exteactite MAITEE. A like quantity of the liquor under examination, after being boiled for some time to dissipate its alcohol, is made up with distilled water, so as to be again exactly equal to 3600 water-grains measure. The sp. gr. of the resulting liquid is then taken, and this is reduced to 'brewers' pounds' per barrel, by multiplying its excess of density above that ot water (or 1000) by 360, and pointing off the three right-hand figures as decimals. 3. AoBTio ACID 0? TINEQAE. This is de- termined by any of the common methods of AOIDIMETEY (which see ; see also Acetime- tbt). Each grain of anhydrous acetic acid so found represents 16765 gr. of sugar. 4. OravUy of oeioin AL woet. This is ob- tained by the addition of the respective quanti- ties of saccharine matter found in Nos. 1, 2, and 3 {above). These results are always slightly under the true original density of the wort, as cane sugar appears to have been taken by the Excise as the basis of their calculations. More eoriectly, 12g of proof spirit is equiva- lent to 19 lbs. of saccharine per barrel. lOJlbs. of saccharine are equiv. to 1 gall, of proof spirit. 5. Detection of NAECOTics. This may be effected either by the method described under Alkaloid, or by one or other of the following processes : — a. Half a gallon of the beer under examination is evaporated to dryness in a water bath ; the resulting extract is boiled for 30 or 40 minutes in a covered vessel with 10 or 12 fl. oz. of alcohol or strong rectified spirit, the mixture being occasionally stirred with a glass rod, to promote the action of the menstruum ; the alcoholic solution is next filtered, treated with a sufficient quantity of solution of diacetate of lead to precipitate colouring matter, and again filtered ; the filtrate is treated with a few drops of dilute sulphuric acid, again filtered, and then evaporated to dryness ; it may then be tested with any of the usual reagents, either in the solid state, or after being dissolved in distilled water. Or the extract, obtained as above, may be boiled as directed with rectified spirit, the PORTER 1351 soliitlou filtered, the spirit distill.il olT, and a «inall quantity of pure liquor of putuwa added to tliu aqueous residue, wliich is then to be shaken up ivitli about 1 fl. oz. of ether ; lastly, the ethereal solution, which separates and floats on the surface, is decanted, evaporated, and the residuum tested, as before. The alkaline liquid, from wliich the ether has been de- canted, is then separated from any precipitate which may have formed, and both of these separately tested for alkaloids. A. From 2 to 3 oz. of purified animal char- coal arf diffused through I gall, ol the beer, and is digested in it, with frequent agitation, for from 8 to 12 hours ; the liquor is next filtered, and the chareonl collected on the filter is boiled with about i pint of rectified spirit; the resulting alcoholic solution is then further fronted as above, and tested. This answers well for the detection of strychnia or nux vomica. 6. PiCElO ACID. This substance, which was formerly employed to impart bitterness to London porter in lieu of hops, may be de- tected as follows : — a. A portion of the liquor agitated with a little solution of diacetate of lead loses its bitter fliivour if it depends on hops, but retains it if it depends on picric acid. b. Pure beer is decoloured and deodorised by anim^il elmrcoal; but beer coi:taining picric aciil, when thus treated, ret lins a lemon-yellow colour and the odour. c. Unbleached sheep's wool, boiled for six or ten minutes, and then washed, takes a canary-yellow colour if picric acid be present. The test is so delicnte that 1 grain of the adulterant in 150,000 gr. of beer is readily detected. d. (Vitiite.') The author ngitates 10 cc. of the suspected beer in a test tube with hiilf its volume of pure amylic alcohol. It the mix- ture is left to settle, the amylic stratum sepa- rates entirely, and is drawn off with a pipette, evaporated to dryness at a convenient tem- jierature in a porcelain capsule, and the residue is filially taken up in a little distilled water with the aid of heat. The aqueous solution is divided into portions, and submitted to the following reii;;ent8. One portion is treated with a solution of ammonio-sulphate of cop- per, which, iu dilute solutions of picric acid, instantly produces a turbidity, due to the formation of very minute crystals of the ammouio-picrate of copper, of a greenish colour. Another portion may be treated with a coneeiitiutod solution of cyanide of potas- ►ium, which produces a blood-red colour, more or less intense, according to the quantity of picric acid present, in consequence of the formation of iso-purpurio acid. A third por- tion may be submitted to the action of sul- pliide of ammonium, rendered still more alka- line by the addition of a few drops of ammonia. Here also a blood-red colour is * * Chemical Ne«i,' vol. xxxv, p. 75. produced, which becomes more intense on the application of heat, and is due to the formation of picramic acid. 7. MiNEEAL MATTEH. — a. A Weighed quan- tity of pure beer evaporated to dryness, and then ineinerated, does not furnish more than from '20^ to -SSg of ash, the quantity varying \yithin these limits with the strength of the liquor anil the character of the water used in brewing it. 4. A solution of this ash, made by decoction with distilled wiuer, should be only renderid slightly turbid by solutions of acetate of lend, biciiloride of platinum, nitrate of baryta, nitrate of silver, oxalate of ammonia, and sulphuretted hydrogen. V. If the beer contained common salt, the above solution will give a cloudy white preci- pitate with a solution of nitrate of silver. Each grain of this precipitate is equivalent to i gr. of common salt (nearly). d. If GREKN COPPERAS (sulphate of iron) is present, ferridcyanide of potassium gives a blue precipitate, and ferrocyanide of potassium a bluish-wliite one, turning dark blue in the air; solution of chloride of barium gives a white precipitate, each grain of which, after being washed, dried, and ignited, represents 1'188 gr. of crystallised protosulphate of iron. e. The ash, digested in water slightly acidu- lated u'ith nitric acid, and then bi>iietassitim and pre- ventiui; its separation from the finely divided carbonaceous matter. Prud. 3{5 to l-S ol tuo weight of tartar acted on; 1 lb. \ieliied 28U gr. Prop., S(c. Pure p itassium is a brilliant white metal, with a hgh lustre; at the com- mon temperature of the air it is soft, .ind may be easily cut with a knife, but at 32" Fahr. it is brittle and crystalline ; it melts completely at 136° Fahr., and in close ve-sela distils nu- altered at a low red heat. ."Sp. gr. •865. Its most remarkable property is its affinity for o\yc:eii, which is so great that it takes it from most other substances containing it. Exposed to the air, its surface is instantly tarnished, and quickly becomes coveted with a crust of oxide or hydrate. It inflames spontaneously when thrown on water, and burns with a beau- tiful purple or purple-red flame, yielding a pure alkaline solution. It can only be pre- served in naphtha, rock oil, or some other fluid hydrocarbon. The salts of potassium are all soluble in water, the tartrate, periodate, and fluosilicate being the least so; they are usually colourless, unless the acid be coloured, crystallise readily, and form numerous double compounds. They can be re<;ognised as follows : — 1354 POTASSIUM Sulpliuretted hydrogen, sulphide of ammo- nium, and carbonate of ammonium, do not affect them. A solution of tartaric acid, added in excess, to moderately strong neutral or al- kaline solutions of potassium salts, gives a quickly subsiding, gritty or crystalline, white precipitate, which is redissolved on heating the liquid, and again separates as it cools; and is also soluble in aqueous solutions con- taining free alkali, or free mineral acids. Platinic chloride produces, in neutral and acid solutions, a yellow crystalline precipitate. Al- kaline solutions require to be first slightly acidulated with hydrochloric acid. The sepa- ration of the precipitate here, as well as that produced by tartaric acid, is promoted by vio- lent agitation and frietion against the sides of the vessel, and the delicacy of both is in- creased by the addition of some alcohol. When converted into carbonate by igniting with excess of carbonate of ammonium and alcohol, and treated with sulphuretted liydro- gen solution and nitro-prusside of sodium, gives a splendid violet colour, turning through red to green on standing. Potassium salts give with sodium periodate and hydro-fluosilicie acid white precipitates soluble in much water. Heated in the inner flame of the blow-pipe on platinum wire, they impart a violet colora- tion, masked, however, by a mere trace of sodium salts. Potassium, Acetate of. KC2H3O2. Syn. Acetate op potash, Potassio acetate; Potass* acetas (B. P., Ph. L., E., D.). Prep. (Ph. L ) Acetic acid, 26 fl. oz. ; distilled water, 12 fl. oz. ; mix, and add, gradually, carbonate of potassium, 1 lb., or q. 3. to saturate the acid ; next, filter the solution, and evaporate it by the heat of a sand bath, gradually applied, until the salt is dried. Prop,, Sfc. Acetate of potassium, prepared as above, occurs in shining white masses, hav- ing a foliated soft texture, a slight but peculiar odour, and a warm sharp taste ; it deliquesces in the air ; dissolves in rather less than its own weight of watfr, and in about twice its weight of alcohiil ; and by exposure to a red heat is converted into pure carbonate of potassium. In trade it is preserved in well-corked and sealed bottles. Pur. It is entirely soluble in water, and in rectified spirit. These solutions neither affect litmus nor turmeric, nor are they dis- turbed by either chloride of barium or nitrate of silver ; but if from a stronger solution any- thing is thi-own down'by nitrate of silver, the sfime is again dissolved on the addition of water or dilute nitric acid. Sulphuric acid being added, the vapour of acetic acid is evolved. 100 gr. of this salt, digested in sul- phuric acid, tlje solution evaporated, and the residuum dried at a high temperature, furnish 88'8 gr. of sulphate of potassium. Uses, Sfc. Acetate of potassium has been found useful in dropsies, febrile aiTections, jaundice, scurvy, calculus, and several chronic skin diseases. During its exhibition the nrine becomes at first neutral, and then alkaline, owing to the salt being converted into carbo- nate of potassium in the system. — Dose. As a diaphoretic and antiscorbutic, 15 to 20 gr. ; as a diuretic, 20 to 60 gr. ; as an aperient, 2 to 3 dr. ; in each case dissolved in some bland liquid, or in the infusion of some mild vege- table bitter. Potassium Antimoniatea. The normal po- tassic antimoniate may be obtained by heating, in an earthen crucible, 1 part of metallic anti- mony with 4 parts of nitrate of potash. The mass so obtained is reduced to powder, and afterwards washed with warm water to remove the excess of potash and potassic nitrite. The residue must be boiled in water for an hour or two; the insoluble anhydrous antimoniate is tlius converted into a soluble bydrated modi- fication (KjSbaOg'SHjO.) The insoluble residue now consists chiefly of acid antimoniate of potassium. The normal salts possess the pro- perty of readily dissolving the acid antimoniate, which is precipitated when such a solution is mixed with any neutral salt of one of the al- kalies. The normal antimoniate does not crystallise, and has an alkaline reaction. Acid antimoniate of potassium (KjSb^On.) may be procured by passing a stream of car- bonic anhydride through a solution of the normal antimoniate. Acid metantimoniate of potash, or hydro- potassic metantimoniate is prepared as fol- lows : — Potassic antimoniate is first formed by deflagrating antimony with nitre, the residue being washed and boiled as described above, so as to bring the whole of the normal antimo- niate into solution ; the resulting liquid is filtered, and evaporated to a syrup consistence in a silver dish, fragments of caustic potash are then added, and the evaporation is con- tinued until a drop of liquid placed upon a cold slip of glass begins to crystallise ; it is then allowed to cool and the alkaline super- natant liquid is poured off the crystals, which are allowed to drain upon a porous tile. This salt is employed as a test for sodium. Potassium, Arseniate of. KH2ASO4. St/n. Abseniate op potassa, Monopotassic abse- uiate, Potassittm DTHTDBIO AHSENIATE; I'OTASSJE BINAESENIAS, L. Prep. Take of iirsenious acid (white arsenic) and nitrate of potassium, of each, in powder, 1 part ; heat the mixture to dull redness in a glass flask, until it fuses and red vapours cease to be evolved ; dissolve the residuum, when cold, in boiling distilled water, 50 parts ; concentrate the solution by evaporation, and set it aside to crystallise. Prop., ^c. This salt forms large crystals, which are permanent in dry air, soluble in about 4i parts of water, and insoluble in al- cohol. It is reputed tonic, alterative, and antiperiodio. — Dose, xs to | gr. dissolved in POTASSIUM 1355 •weeUncd water. It is also used to form a resist-piute ia calico printing, and in the mnniifaeture of cobalt blui". Potassium, Borate of. K4B4O8. Syn. Po- TASSA BOBA8, L. Prep. From dry carbonate of potassium and dry boracic acids, equal parts, reduced to powder, and heated to redness in a covered crucible ; the sublimed mass, when rold, bein^ dissolved in boiling water, and the flltcri d solution concentrated by evaporation, and then xet aside to crystallise; or at once completely evaporated to dryness. — Dose, 1 to 6 gr. ; in calculi, &c. Fotassiam, Borotartrate of. S^n. Potass^ BOBOTAttTEAS, CBKMOE TABTABI SOLCBILIS, L.J CEliMB DB TABTBK SOLUBLE, Fr. Prep. (P. Cod.) Crystallised boracic acid, 1 part ; bitartrate of potassium, 4 parts ; water, 24 parts ; dissolve, by the aid of heat, in a silver basin, and, constantly stirring, evaporate the resulting solution, either to dryness, and then powder it, or merely to a syrupy consistence, when it may be spread upon plates, and dried in scales, by the heat of a stove. It must afterwards be preserved from the ulr. Prop., 1(0. A white, deliquescent powder, freely soluble in water. It has been used as a solvent fill' lithic calculi, and in gout, &c. — Dose, 15 to 30 gr. In doses of 2 to 3 dr. it is laxative, and is very popular as such on the Continent. Potassium, Bromide of. KBr. Syn. Po- TASSii BBOMiDtrM (B. P.). Prep. Exactly as the iodide, which it resembles in its cha- racter, only being somewlint lies soluble in water and more in ahohol. Employed in similar cases and given in similar duses to the iodide. Potassium, Carbonate of. K0CO3. Syn. CaBBONATB op POTA8SA, SUBCABBONATE OP POTASSA, Salt op tabtab ; Potassje cabbo- NAS (B. p., Ph. L., E., D.). Impure or crude carbonate of potassium is chiefly imported from America and Russia, and is obtained by lixivinling wood ashes, and evaporating the solution to dryness. The mass is then trans- ferred into iron pots, and is kept in a state of fusion for several hours, until it becomes quies- eeiit, when the heat is withdrawn, and the wliolc is left to cool. It is next broken up and packed in air-tight barrels, and in this state constitutes the ' potashes ' or ' potash ' of commerce. Another method is to transfer the black salts, or product of the first evaporation, from the kettles to a large oven or furnace, so constructed that the flame is made to play over the alkaline mass, which is kept con- stantly stirred by means of an iron rod. The i;;iiition is continued until the impurities are burned out, and the mass changes from a blackish tint to a dirty or bluish white. The whole is next allowed to cool, and is then brnken into fragments, and packed in casks as before. It now constitutes 'pearlash.' When pe.irlash is dissolved in cold distilled water, the solution depurated, filtered and crys- tallised, or simply evaporated to dryness, it forms ' refined ashes,' or carbonate of potash sufliciently pure for most pbarmacentical and technical purposes. The granulated carbonate of potash, salt of tartar, or prepared kali, of the shops, is simply refined ashes which, during the evaporation, and more especially towards the conclusion of the desiccation, has been assiduously stirred, so that it may form small white granulations, instead of adhering together to form an amorphous solid mass. In this state it constitutes the ordinary or carbo- nate of potassa of the Piiarmacopoeias. Ordi- nary potash or pearlash may be refined as follows: — Raw potash, 10 parts, is dissolved in cold water, 6 parts, and the solution is allowed to remain for 24 hours, in a cool place ; it is then filtered, and somewhat concentrated by evaporation, crystallisation being prevented by continually stirring the mass until the whole is nearly cold j it is next decanted into a strainer, and the mother-liquor allowed to drip off ; the residuum is evaporated to dryness at a gentle heat, and redissolved in an equal quantity of cold distilled water; the new solution, after filtration, is again evaporated to dryness. The product is quite free from potassium sulphite, and is nearly free from both potassium chloride and silicates. Potassium, Pure Carbonate of Carbonatb op potassa (P0TAS8.E CABBONAB PUKCM — Ph. E. & D., and Ph. L., 1836).— (I'h, L., 1836.) From bicarbonate of potassium, in crystals, heated to redness in a crucible. (Ph. E.) As the last. Or, more cheaply, by dissolvincr bitartrate of potassium in thirty parts of boiling water, separ.itins: and washing the crystals which form on cooling, heatiuir them in a loosely covered crucible to redness as long as fumes are riischarged, breaking down the mass, and roasting it in an oven for two hours, with occasional stirring ; lixivint'ng the product with (cold) distilled water, filter- ing the solution thus obtained, evaporating it to dryness, granulating the salt to.i'ards the close by brisk agitation ; and, lastly, heating the granular salt thus obtained nearly to redness. (Ph. D.) Bitartrate of potassium, 2 lbs., is exposed to a red heat in an iron crucible, as before ; the powdered calcined ma-s is boiled for 20 minutes in water, 1 quart, the solution filtered, and the filtiaie waslied with water, 1 pint, to which ammonium sesquicarbonate, \ oz., has been added ; the mixed and filtered liquors are evaporated to dryness, and, a \ovi red heat having been applied, the residuum is rapidly reduced to powder in a warm mortar, and at once enclosed in (dry and) well-stoppered bottles. Prop. These are well known. It exhibits most of the properties of hydrate of potassium, but in a vastly less degree. It is very deli- quescent, effervesces with acids, exhibits a marked alkaline reaction w ith test paper, is in- solulilein alcohol, but dissolves in Uss than its own weight of water, its affinity for the last 1356 POTASSIUM bi'irg so great tliat it takes it from alcoliolic mixtures. Pur., S(e. Carbonate of potassium frequently contains an undue quantity of water, as well as silicic acid, sulphates, and chlorides. The water may be detected by the loss of weight the salt suffers when heated; the silica, by adding to it hydrochloric acid in excess, evapo- rating to dryness, and igniting the residuum, by which tliis contamination is rendered in- soluble; the sulphates and chlorides may be detected by adding nitric acid in excess, and testing the liquid with nitrate of silver and chloride of barium. If the former produces a white precipitate, a chloride is present; and if the latter does the same, the contamination is a sulphate. Carbonate of potassium deliquesces in the air, and is almost entirely dissolved by water; in an open vessel it spontaneously lique- fies. It changes the colour of turmeric brown. Supersaturated with nitric acid, neither carbo- nate of sodium nor chloride of b.arium throws down anything:, and nitrate of silver very little. 100 gr. lose 16 gr. of water by a strong red heat; and the same weight loses 263 gr. of carbonate anhydride when placed in contact with dilute sulphuric acid. Fotassinm, Bicarbonate of. KHCOg. Syn. Potassium htdeogen carbonate, Bioakbo- nate of potassa; potass.e bioaebonas (b.p., Ph. L., E., & D.). Frep. 1. (Ph. L. 1836.) Carbonate of potassium, 6 lbs. ; distilled water, 1 gall. ; dissolve, and pass carbonic anhydride (from chalk and sulphuric acid diluted with water) through the solution to saturation ; apply a gentle heat, so that whatever crystals have been formed may be dissolved, and set aside the solution that crystals may again form ; lastly, the liquid being poured off, dry them. 2. (Ph. D.) Carbonic anhydride, obtained by the action of dilute hydrochloric acid on chalk (the latter contained in a perforated bottle im- mersed in a vessel containing the acid), is passed, by means of glass tubes connected by vulcanised india rubber, to the bottom of a bottle containing a solution of carbonate of potassium, 1 part, in water, 2J parts ; as soon as the air is expelled from the apparatus the corks through which the tubes pass are ren- dered air-tight, and the process left to itself for a week; the crystals thus obtained are then shaken with twice their bulk of cold water, drained, and dried on bibulous paper, by simple exposure to the air. From the mother-liquor, filtered, and concentrated to one half, at a heat not exceeding 110° Fahr., more crystals mav he obtained. The tube immersed in the solution of carbonate of potassium will have to be occasionally cleared of the crystals with which it is liable to become choked, else the process will be suspended. 3. (Ph. B.) The same. 4. (Apothecaries' Hall, London.) Potassium carbonate, 100 lbs. ; distilled water, 17 galls. ; dissolve, and saturate the solution with car- bonic anhydride, as in No. 1, when 35 to af\ 15 gr. \ oz. of lemon juice tartaric acid, and POTASSIUM 1357 Fotutium, Chlorate of. KCIO,. St/n. CllLOUATB OF POTASH ; P0TA8B« CHIX)KA8 (B. P., Ph. L. & n.), L. Prep. 1. Chlorine gaa h conduotud by a wide tabe into a mode- rately fitroDg and warm solution of hydrate or carbonate of potassiuiii, until the absorption of the gaa ceases and tbe alkali is completely neutnilised ; tlic liquid is then kept at the boiling temperature for a few minutes, after which it is gently evaporated (if oecessary) until a pelliclu forms on the surface, and is next set aside, so as to cool very slowly; the crystals, tlius obtained, are drained and care- fully washed on a filter, with ice-cold water, and are purified by re-solution and re-crystal- lisation. The product is chlorate of potassium. The mother-liquor, which contains much chlo- ride of potassium mixed with some chlorate, is either evaporated for more crystals (which are, however, less pure than the first crop) or is preserved f'>r a future operation. Obi. The product of the above process is small, varying from 10 to 45g of the weight of the potassium consumed in it, according to the skill with which it is conducted ; this apparent ISyn. Bichromate of po- TASSA, HeD CHBOMATB OP POTASH, ACID C. op P. J POTASSJE BICHBOMAB, L. Prep. 1. To a concentrated solution of yellow chromate of pota'sinm, sulphuric acid, or, better, acetic acid, is added in quantity equal to one half that required for the entire decomposition of the salt; the liquid is then concentrated by evapora- tion and slowly cooled, so that crystals may form. 2. (Jacqnelain.) Chrome ore, finely ground and sifted, is mixed with chalk ; the mixture is spread on a thin layer on the hearth of a re- verber;itory furnace, and heated to bi'ij^ht red- ness, with re)icated stirring, for 9 or lU hours. The yellowish-green product consists essen- tially of neutral chromate of calcium, mixed with ferric oxide. It is ground and stirred up with hot water, and sulphuric acid is added till a slight acid reaction becomes apparent, a sign that the neutral chromate has beeu converted into bichromate. Chalk is now stirred in to precipitate the ferric sulphate, and after a while the clear solution is run off into another vessel, where it ia treated with carbonate of potassium, which precipitates the lime and leaves bichromate <>f potassium in solntion. Tlie solution is then evaporated to the crystallising point. This process, when carried out on a large scale, is very economical. Prop., S^e. It forms very beantiful square tables, or flat four-sided prismatic crystals ; permanent in the air; soluble in 10 parts of water at 60°, and in le«s than 3 parts at 212° Pahr. J it has a metallic, bitter taste, and is poisonous. It is chiefly used in dyeing and bleaching, and as a source of chromic acid. The tests, &c., are the same as for the yellow chromate. Potassium, Citrate of. KaCjH/);. Syn. PoTAsaa; OITEAs, b. Prep. From a solution of citric acid neutralised with carbonate of potassium, evaporated, and granulated, or crys- tallised; very deliquescent. Or, extempora- neously, in the form of solution, by adding car- bonate or bicarbonate of potassium to lemon juice, as in the comuiou effervescing draught. (Ph. B.) The same. Potassium, Cyanate of. KCyO, or KCNO. Prep. 1. By roa>ting, at a red heat, dry ferro- cyanide of potassium, in fine powder, upon an iron plate, constantly stirring it until it becomes fused into one mass, which most be reduced to fine powder and digested in boiling alcohol, from which crystals of the cyanate will be de- posited as the solution cools. 2. (Liebig.) A mixture of ferrocyanide of potassium, with half its weight of peroxide of manganese, may also be used to produce this salt, as the last; the compound shonld be kindled by a red-hot boily, and allowed to smoulder away, after which it may be treated with alcohol, as before. 3. A mixture of ferrocyanide of potassium and litharge is heated as before, and dissolved out by alcohol, and crystallised. Prop. Crystallisahle colourless or white salt, readily soluble in alcohol and water, but readily decomposed when moist into bicar- bonate of potassium and ammonia, or in soln- tion into the carbonate of potassium and ammonium. This salt is poisonous. The cyanntes of silver, lead, and many other metals may be made by adding a solution of cyanate of potassium to another of a neutral salt of the base. Potassium, Cyanide of. KCN, or KCy. Syn. Ctanidk op potash, Cyancket op POTASSIUM ; POTASSII CTANIDUM, P. CYANU- HETCM, L. Prep. 1. (Medicinal cyanide op potas- sium.) — a. A solution of pure hydrate of po- tassium, 2 parts, in highly rectified spirit, 7 parts, is placed in a receiver furnished with a safety tube, and surrounded with bnii-cd ice ; 1360 POTASSIUM the beak of a tubulated retort, containing f en-ocyanide of potassium, in powder, 4 parts, is then adapted to it in such a manner that any gas or vapour evolved in the retort must traverse the solution in the receiver; the ar- rangement being complete, sulphuric acid, 3 parts, diluted with an equal weight of water, and allowed to cool, is cautiously poured into the retort, and the distillation conducted very slowly, a very gentle heat only being applied, as circumstances may direct ; as soon as the force of ebullition in the retort has subsided, the distillation is complete, and the connec- tion between the retort and receiver is broken; the contents of the receiver, now transformed into a mixture of a crystalline precipitate of cyanide of potassium, and an alcoholic solu- tion of undecomposed hydrate of potassium, is carefully thrown on a filter, and the pre- cipitate, after the mother-liquor has drained off, very cautiously washed with ice-cold and highly rectified spirit, and then drained, pressed, and dried on the same filter. The product is chemically pure, and equal to fully log of the ferrocyanide employed. This is a modification of what is commonly known as * Wiggei*'s process.' i. Expose well-dried and powdered ferro- cyanide of potassium to a moderate red heat, in a close vessel; when cold, powder the fused mass, place it in a funnel, moisten it with a little alcohol, and wash it with cold water; evaporate the solution thus formed to dry- ness, expose it to a dull red heatiu a porcelain disli, cool, powder, and digest it in boiling rectified spirit; as the spirit cools, orvstals of cyanide of potassium, nearly pure, will be de- posited. The alcohol employed in both this and tlie preceding process may be recovered by distillation from calcined sulphate of iron. 2. (CeUDB or COMMEEOIAL CYANIDE — Liebig.) Commercial ferrocyanide of potas- sium, 8 parts, rendered anhydrous by gently heating it on an iron plate, is intimately mixed with dry carbonate of potassium, 3 parts; this mixture is thrown into a red-hot earthen crucible, and kept in a state of fusion, with occasional stirring, until gas ceases to be evolved, and the fluid portion of the mass becomes colourless ; the crucible is then left at rest for a few minutes, to allow its contents to settle, after which the clear portion is poured from the heavy black sediment at the bottom upon a clean marble slab, and the mass, whilst yet warm, broken up, and placed in well- closed bottles. Obs. A cheap and excellent process. The product is said to contain about l-8th part of cyanate of potassium, and, though not sufiiciently pure for employment in medicine as potassium cyanide, is admirably adapted for the various technical applications of this substance, as in electro-plating, electro-gild- ing, photography, &c. It may also be advan- tageously substituted for the ferrocyanide in the preparation of hydrocyanic acid by the distillation of that substance along with dilute sulphuric acid. Prop., ^c. When pure, this salt is colour- less and odourless ; it forms cubic or octahe- dral crystals, which are anhydrous ; it ia freely soluble in water and in boiling alcohol, but most of it separates from the latter as the solution cools ; it is fusible ; and under- goes no change, even at a full red heat, in close vessels; it exhibits an allcaline reaction; when exposed to the atmosphere, it absorbs moisture, and acquires the smell of hydro- cyanic acid. If it effervesces with acids, it contains carbonate of potassium, and if it be yellow it contains iron. It is employed in chemical analysis, and for the preparation of hydrocyanic acid ; cyanide of sodium may be made in the same way. The dose is -Jj to ^ gr., in solution; in the usual cases in which the admiuistration of hydrocyanic acid is iudicated. — Antidotes. The same as for hydro- cyanic acid. Potassium, Ferricyanide of. KjPeCyj, or Kj, FeCgNg. Syn. Fbebidctanide op po- tassium, Fbbkicyantjret op p.. Red peus- SIATE OP potash ; POTASSII PEEKICTANIDUM, P. PEUSsiAS ettbrum:, L. This important and beautiful salt was discovered by L. Gmelin. At first it was merely regarded as a chemical curiosity, but it is now extensively employed in dyeing, calico printing, assaying, &c. Prep. 1. Chlorine gas, prepared in the ordinary manner, is slowly passed into a cold solution of ferrocyanide of potassium, 1 part, in water, 10 parts, with constant agitation, until the liquid appears of a deep reddish- green colour, or of a fine red colour by trans- mitted light, and ceases to give a blue pre- cipitate, or even a blue tinge, to a solution of ferric chloride, an excess of chlorine being carefully avoided; the liquor is next evapo- rated by the heat of steam or boiling water, until a pelli(de forms upon the surface, when it is filtered, and set aside to cool ; the crystals are afterwards purified by re-solution and re-crystallisation. — Another method is simply to evaporate the original solution to dryness, by a steam heat, with agitation, then to re- dissolve the residuum in the least possible quantity of boiling water, and, after defeca- tipn or filtration, to allow the new solution to cool very slowly, that crystals may form. 2. (Extemporaneous.) Add nitric acid, very gradually, to a cold solution of ferrocyanide of potassium, with constant agitation, until a drop of the mixture ceases to impart a blue colour to a solution of ferric chloride, care- fully avoiding excess of acid. It may be at once used in solution, or evaporated, &c., as before. Prop, Sfc. Magnificent regular prismatic or, sometimes, tubular crystals, of a rich ruhy- red tint; permanent in the air ; combustihle; decomposed by a high temperature ; soluble in 4 parts of cold water ; insoluble in alcohol. I'OTASSIUM 1361 Olotira ft^rrir salU a pale brown, gives with ferrous aalts a deep blue, and precipitates bia- muth saUa pile yelluw ; cadmium and mer- curic nalta, yellow ; zinc salts, deep yellow ; mercurous, cupric, molybdenic, silver, und uranic salts, reddish brown ; cobalt salts, dnrk brown ; manganous salts, brown ; cupric salts, greenish ; and nickelous salts, olive brown. Potassium, Ethylate. (CjHjKO.) Ldweg and Weidmann obtained this compound by heating together acetate of ethyl and potas- sium. Dr B. W. Richardson, some few years ago, recommended the employmentof the alka- line ethylates as caustics, and they are now fre- quently used as such in surgery. When first applied to the body the etiiylates produce no aclion, but as they absorb water from the tissues they are decomposed, the potassium or sodium is oxidised, yielding caustic potash or soda in the fresh condition, while alcohol is reformed from the recombination of hydro- gen derived from the water. Dr Kichardson believes the ethylates of potassium and so- dium will be found the most effective and manageable of ail caustics, and that in cases of cancer, when it is important to destroy structure without resorting to the knil'e, and in the removal of noevus and other simple growths, they will be of essential service. The ethylates dissolve in alcohol of dilferent strengths ; tlie solution may either be applied with a glass brush or injected by the needle, and a slow or quick effect can be insured according to the wish of the operator. The ethylate of potiissium is the more powerful agent. Potassium, Perrocyanide of. K^, FeCy,, or K,, PeCjNii. Sy». Pkbbooyaktjret op po- TAS9IUM, PltUSSIATE OP POTASH, YeLLOW P. OF P.; Potass^ peubsia plata (B. P.), Po- TA38II PEKttOOYANIunM (Ph. L., E., & U.), L. This valuable salt, the well-known ' prussiate of potash ' of commerce, was discovered by the illustrious Scheele about the middle of the 18th century. It is now only manufactured on the large scale. Prep. Good ' potash ' or ■ pearlash,' 2 parts, and dried blood, horns, hoofs, woollen rags, or other refuse animal matter, 5 or 6 parts, are reduced to coarse powder, and mixed with some coarse iron borings ; the mixture is then injected into egg-shaped cast-iron pots in a state of moderate ignition ; the mass is fre- quently stirred with an iron spatula, so as to prevent it running together, and the calcina- tion is continued until fetid vapours cease to be evolved, and flame is no longer seen on stirring the mixture, care being taken to ex- clude the air from the vessels as much as possible ; during the latter part of the process the pots are kept constantly covered, and the ignited moss stirred less frequently ; the hot pasty moss is then removed with an iron ladle, and excluded from the air until cold ; it is aeit exhausted by edulcoratiou with boiling VOL. II. water, and the resulting solution, after defe- cation or filtratii)n, is concentrated by evapo- ration, BO that crystals may form as the liquid cools ; these are redissolved in hot water, and the Holntion allowed to cool very slowly, when large and beautiful yellow crystals of ferrocya- nide of potassium are deposited. — Product. 1 ton of dried blood or woollen refu-u, with 3 cwt. of pearlash, yields from 2 to 2 J cwt. of commercial ferrocyanide. The mother-liquor contains sulphate of potassium. Prop. It forms large and very bountiful yellow crystals, which are permanent iu the air, and very tough and difficult to powder; it is soluble in 4 parts of cold and 2 parts of boil- ing water ; has a mild saline taste; at a gentle heat loses water ; at a higher temperature, in closed vessels, it is for the most part con- verted into cyaniile of potassium, and, when exposed to the air, into cyanate of potusi.ium. Precipitates solutions of antimonous, bismuth, mercurous, and zinc salts, white; cadmium salts, of a pale yellow; cuprous salts, white, turning red ; ferrous salts, white, turning blue; leadsalts, white ;manganous salts, white, turned red; mercuric salts, white, turning bluish ; nickelous salts, white, turning green ; silver salts, white ; stannous salts, white ; co- balt salts, green ; cupric salts, chocolate red ; ferric salts, dark blue; palladous salts, green ; stannic salts, yellow ; uranic salts, reddish brown ; and zinc salts, white. Cf»ea, S;c. Ferrocyanide of potassium is chiefly used in dyeing and calico printing, in the manufacture of Prussian blue, in electro- plating, and, in chemistry, as a test, and a source of hydrocyanic acid. As a medicine it is said to be sedative and astringent, and in large doses purgative, but appears to pos- sess little action. — Dose, 10 gr. to \ dr., dissolved in water ; in hooping-couith, chro- nic bronchitis, night-sweata, lencorrhcea, &c. D'Arcet swallowed a solution containing \ oz. of this salt without experiencing any injurious effects. Potassium, Hydrate of. KHO. Syn. Po- TASSA HTDBATB, HYDRATE OP POTASSA, PO- TAS8A, Caustic p., Hydrated oxide op po- tassium; Potass A OAtrsTiCA (B. P.), Potass a (Ph. E.), P. CAUSTIOA (Ph. D.), P. IIYDBAS (Ph. L.), P. PU3A. Prep. 1. (Ph. L.) Liquor of potassa, 1 gall. ; evaporate the water in a clean iron vessel over the fire until the ebulli- tion being finished, the residuum nf potassium hydrate liquefies; pour this into proper moulds. 2. (Ph. E. & D.) As the last, but pouring the fused hydrate upon a bright and clean iron plate (silver or iron dish — Ph. D.) ; as soon as it solidifies, break it quickly (into fragments), and put it into stoppered glass (green-glass — Ph. D.) bottles. 3. (Pure.) The hydrate, obtained as above, is dissolved in alcohol or rectified spirit, and, after repose for a few days in a closely stopped green-glass or silver vessel, the solu- 86 1362 POTASSIUM tion is decanted, and cautiously evaporated in a deep silver basin, out of contact with the air. 4. (Pure.) M. Polacci states that he procures very pure hydrate of potash in a few minutes by the following process. He heats together ill an iron vessel to a red heat a mixture con- sisting of 1 part of nitrate of potash well triturated with 2 or 3 parts of iron filings. The mass becomes red in a few minutes, and, alter cooling, it is treated with water, left to settle, and then decanted. A more or less concentrated solution may thus be obtained, or it may be evaporated to produce the solid potash. Prop., S(c. When perfectly pure it is white, solid, very soluble in water and in alcohol ; very deliquescent; intensely acrid and corro- sive; and exhibiting the usual signs of alka- linity in the highest degree. That of the shops has usually a greyish or bluish colour. Potassium, I'cdate of. KIO3. Syn. Po- TASS« lODAS. L. Prep. Neutralise a hot solution of hydrate of potassium with iodine, evaporate to dryness hy a gentle heat, powder the residuum, and digest it in alcohol, to remove iodide of potassium, dissolve the in- soluble portion in hot water, and crystallise. Obs. lodate of potassium is resolved at a red heat into oxj'gen gas and iodide of potas- sium. It has beeu recommended in bron- chocele. — Dose, 1 to 5 gr. Potassium, Iodide of. KI. Syn. Potassti lODiDCM (B. P., Ph. L., E., and D.). 1. (Ph. L. 1836.) Take of iron filings, 2 oz. ; distilled water, 2 quarts ; iodine, 6 oz. ; mix them, and heat the solution until it turns green, and then add of carbonate of potassium, 4 oz., dissolved in water, 1 quart ; filter, wash the residuum on the filter with water, evapo- rate the mixed filtered liquors and crystallise. — Product, 1 oz. of iodine yields 1 oz. 45 gr. of iodide. The formulae of the Ph. D. and Pn. E. are very similar. 2. Add iodine to a hot solution of pure hydrate of potassium until the alkali is perfectly neutralised, carefully avoiding excess ; eva- porate the liquid to dryness, and expose the dry mass to a gentle red heat in a platinum or iron crucible ; afterwards dissolve out the salt, gently evaporate, and crystallise. An excel- lent process, yielding a large product, but, if the ignition be not carefully managed, it is apt to contain a little undecomposed ibdate. To obviate this, Mr Scanlan proposes the addition of a little powdered charcoal to the mass before ignition — a plan adopted in the Ph. U.S. 3. Iodine is treated with a small proportion of phosphorus in water, and is thus converted into 'hydriodic acid;' hydrate of calcium is then added, and the ' iodide of calcinm' formed is first fused, and then decomposed by sulphate of potissium into ' sulphate of calcium,' which ie precipitated, and 'iodide of potassium,' which remains in solution, and may be crystallised, as in the other processes. This is a modifica- tion of a method devised by Liebig. 4. (Ph. B.) Put solution of potash, 1 gall., into a glass or porcelain vessel, and add iodine 29 oz., or q. s., in small quantities at a time, with constant agitation, until the solution ac- quires a permanent brown tint. Evaporate the whole to dryness in a porcelain dish, pul- verise the residue, and mix this intimately with wood charcoal in fine powder, 8 oz. Throw the mixture, in small quantities at a time, into a red-hot crucible, and when the whole has been brought to a state of fusion, remove the crucible from the fire and pour out its contents. When the fused mass has cooled, dissolve it in 2 pints of boiling distilled water, filter through paper, washing the filter with a little distilled boiling water ; unite the liquids, and evaporate till a film forms on the surface. Set aside to cool and crystallise. Drain crystals and dry quickly with a gentle heat ; more crystals may be obtained by evaporating the mother liquor, and cooling. The salt should be kept in a stoppered bottle. Prop. It crystallises in cubes, which iu the pure salt are extremely white, though fre- quently opaque ; these arc anhydrous ; fuse when heated, without decomposition ; dissolve in less than an equal weight of water, at 60° Pahr., and very freely in alcohol; and do not deliquesce in moderately dry air unless they contain undecomposed hydrate of potassium. Its solution dissolves the iodine freely, and also, less readily, several of the insoluble metaUic iodides and oxides. Pur. It is entirely soluble in both water and alcohol. Its aqueous solution alters the colour of turmeric either not at all or but very slightly, nor does it affect litmus paper, or effervesce with acids. Nitric acid and starch being added together, it becomes blue. It is not coloured by the addition of tartaric acid with starch. No precipitate occurs on adding either a solution of hydrate of calcium or of chloride of barium. 100 gr., dissolved in water, by the addition of nitrate of silver, yield a precipitate of 141 gr. of iodide of silver. Assay. The iodide of commerce frequently contains fully one half its weight of either chloride or carbonate of potassium, or both of them, with variable quantities of iodate of potassium, a much less valuable salt. The presence of these substances is readily de- tected by the above tests. As the first of these is only very slightly soluble in cold alcohol, and the others insoluble in that liquid, a ready method of determining the richness of a sample in pure iodide, sufficiently accurate for ordinary purposes, is as follows : — Reduce 50 gr. of tlie sample to fine powder, introduce this into a test tube with 6 fl. dr. of alcohol, agitate the mixture violently for one minute, and tlirow the whole on a weighed filter set in a covered funnel, observing to wash what remains on the filter with another fl. dr. of POTASSIUM 1363 alcohol. The filtrate, evaporated to dryness, gives the quantity of pure iodide, and the filter, dried by the heat of boiling water, that of the impurities present in the sample ex- amined, provided it contained no hydrate of potassium. The quantity of allcali, whether iiyiirate or carbonate, may be found by the c xumoQ method of ' alkalimetry.' {/»«», ifo. Chiefly in photography, medicine, and pharmacy. — Dose, 1 to 10 gr., twice or thrice daily, made into pills, or, better, in solu- tion, either alone or combined with iodine ; in bronchocele, scrofula, chronic rheumatism, dropsy, syphilis, glandular indurations, and various other glandular diseases. Also exter- nally, made into a lotion or ointment. Potassium, Nitrate of. KNOj. Syn. Niteatb OF POTASH, NiTEE, SaLTPETEE ; PoTASSm KITEAS (B. P., Ph. L.,E.,&D.), NiTEUMt.SAL NiTiiit, Sal PETEJj-f, Kali NiTSATUM-f, L. This salt is produced naturally in the soil by the action of the atmosphere, and crystallises upon its surface, in various parts of the world, especially in the East Indies. On tlie Conti- nent it has Ion); beeu produced artificially, by exposing a mixture of calcareous soil and animal matter to the atmosphere, when c.ilcium nitrate is slowly formed, and is ex- tracted by lixiviation. The liquid is then decomposed by the addition of wood ashes, or carbonate of potassium, by which carbonate of calcium is precipitated, and nitrate of potas- sium remains in solution. The places where these operations are performed are called ' nitriiiries,' or 'nitriftres artilicielles.' The British market is wholly supplied from India. The salt of the first crystallisation, by either process, is called ' crude nitre' or 'rough salt- petre.' This is purified by solution in boiling water, skimming, and, after a short time allowed for defecation, straining (while still hot) into wooden crystallisinij; vessels. The crystals thus obtained are called 'single re- fined nitre ;' and when the process is repeated ' double refined nitre.' 1. (PoTAsaiE NITEAS PtTK0M —Ph. D.) Com- mercial nitre, 4 lbs. ; boiling distilled water, 1 quart ; dissolve, withdraw the heat, and stir the solution constantly as it cools ; the minute crystal*, thus obtained, are to be drained, and washed, in a glass or earthenware percolator, witli coUl distilled water, until that which trickles through ceases to give a precipitate with a solution of nitrate of silver, the contents of the percolator are then to be withdrawn, and dried in an oven. Prop. White, pellucid, six-sided prisms; per- manent in the air; soluble in 7 parts of water at 60° and in 1 part at 212° Fahr.; insoluble in alcohnl ; its taste is cool, saline, and slightly bitter and pungent; at about 560° it fuses to an oily-looking mass, which cnncretes on cooling, foi ining ' sal prunella ;' at a led heat it gives out oxvfron, and, afterwards, nitrous Innics; sp. gr. I'Oiij to 1975. Pur. Coramorciiil riitre generally contains chlorides, sulphates, or calcareous salts. The first may be detected by its solution giving a cloudy white precipitate with nitrate of silver. The second by chlorides of barium or calcium giving a white precipitate, and the third by oxalate of ammonium giving a white pre- cipitate. Assay. Of the numerous methods prescribed for this purpose, few are sufiiciently simple for mere practical men. The proportion of chlorides, sulphates, and calcareous salts may be determined as above ; and the general richness of the sample by the method of Gay- Lussac, modified as follows : — 100 gr. of the sample (fairly chosen) are triturated with 50 gr. of lampblack and 400 gr. of common salt, and the mixture placed in an iron ladle, and ignited or fused therein, due care being taken to prevent loss; the residuum is exhausted with hot water, and the solution thus obtained tested by the usual methods of alkalimetry for carbonate of potassium. The quantity of car- bonate found, multiplied by 2°125 or 2^, gives the per-centage richness of the sample in nitrate. Uses, Sic. Nitre is chiefly employed in the manufacture of gunpowder, fireworks, and nitric acid. It is also used in medicine as a sedative, refrigerant, and diaphoretic, and as a cooling diuretic. It has been recommended in active heemorrhages (especially spitting of blood), in various febrile affections, in scurvy, and in herpetic eruptions ; and it has been highly extolled by Dr Basham as a remedy in acute rheumatism, — Dose, 5 to 15 gr., every 2 hours. A small piece, dissolved slowly in the mouth, frequently stops a sore throat at the commencement. In large doses it is poi- sonous. The best treatment is » powerful emetic, followed by opiates. Potassium, Nitrite of. KNO,. S/in. Ni- TEITE OF POTASSA ; POTASSJE NITBIS, L. Prep. 1. By heating nitre to redness, dissolving the fused mass in a little water, and adding twice the volume of the solution in alcohol ; after a few hours the upper stratum of liquid is decanted, and the lower one, separated from the crystals, evaporated to dryness. 2. (Coreuwinder.) Nitric acid, 10 parts, are poured on starch, 1 part, and the evolved gas passed through a solution of hydrate of potassium of the sp. gr. 1-380, to saturation ; the liquid is then either neutralised with a little hydrate of potassium (if necessary), and kept in the liquid form, or at once evaporated. Fused pinkish mass, or clear colourless soluble crystals, used iu chemistry as a reagent, and deoxydiser. Potassium, Oxalate of. KnC204. Syn. Nett- TRAIi OXALATE OF POTASSA; POTASSJE 0XALA8, L, Prep. Neutralise a solution of oxalic acid, or the acid oxalates, with carbonate of poiassium, evaporate, and crystallise. Transparent colour- less rhombic prisms, soluble in 3 parts of water, and of the formula KjCO,, Aq. Potassium, Hydrogen Oxalate of. KHCJO4. 1364 POTASSIUM Syn. PoTAasiUM: binoxaiate, Salt of 80KBBL, EsSEHTIAL SALT OF LEMONS; PoTASS^ BIKOXALAS, L. Prep. By saturating a solution of oxalic acid, 1 part, with carbonate of potas- sium, adding to the mixture a similar solution of 1 part of oxalic acid, unneutralised, and evaporating for crystals. It may also be obtained from the expressed juice of wood or sheep's sorrel, by clarifying it with eggs or milk, and evaporating, &c., as before. Colour- less rhombic crystals of the formula KHC2O4, Aq, soluble in 40 parts of cold and 6 parts of bqiling water, yielding a very sour solution. Fotassinm, Trihydrogen Oxalate of. KH3 (C2O4), or KHC2O4, H2C2O4. Syn. POTASSIUM QUADEOXALATE, POTASSIUM ACID OXALATE. Prep. By neutralising 1 part of oxalic acid with carbonate of potassium, adding to the solu- tion .■? parts more of oxalic acid, evaporating and cr\stallisin^. Besembles the last; has the formula 1^113(0304)2. 2Aq ; but is less soluble, and more intensely sour, and forms modified octahedral crystals. The salt is occasionally sold under the names of ' sal aeetosellsB,' ' salt of sorrel,' and ' essential salt of lemons.' Both are used to remove ink and iron stains from linen, to bleach the straw used for making bonnets, and, occasionally, in medicine, as a refrigerant. Potassinm, Oxide of. K2O. Prep. Burn pure potassium in a current of oxjgen. White powder, rapidly absorbing water and forming the hydrate. Potaesium, PercUorate of. KCIO4. Syn. I'OTASSA PEECHLOEAS, L. Prepared by pro- jecting well -dried and finely powdered chloiate of potassium in small portions at a time, into i\ arm nitric acid. The salt is separated from the 'nitrate' by crystallisation. Potassium, Fras'siate of. See Potassium FEEEIOYANIDE and FEEEOCTANIDE. Potassium, Salicylite of. Formed by mix- ing salicylous acid (artificial oil of niendow- sweet) with a strong solution of hydrate of po- tassium ;' it separates, on agitation, as a yellow crystalline mass, which, after pressure in bibulous ' paper, is recrystallised from alcohol. Golden-yellow crystals, soluble in both water and alcohol; damp air gradually converts them into acetate of potassium and melanic acid. Potassium, Silicate of. (Ure.) Syn. Vo- TASS^ SITICAS. Prep. Mix 1 part of pow- dered quartz or flint, or of fine siliceous sand, with 2 parts of carbonate of potash, and fuse them in a Hessian crucible. Dissolve the mass in water, filter the solution and evaporate it to dryness. — Dose, 10 gr. to 15 gr., in 6 or 8 oz. of water, twice a day. To dissolve gout concretions. An impure silicate of potash is used as a water-glass. Potassium, Sulphate of. K2SO4. Syn. Po- TASS.E SULPHAS (B.P., Ph. L., E., &D.). Prep. The sulphate of potassium of commerce is a secondary product of several chemical and manufacturing processes. Thus, the residuum of the distillation of nitric acid from nitre is dissolved in water, the solution neutralised with carbonate of potassium, and, after defeca- tion, evaporation until a pellicle forms; it is then strained, or decanted, and set aside to crystallise. Or, the residuum is simply Ignited, to expel excess of acid, and then dissolved and crystallised as before. Prop., S(o. Anhydrous, heavy, quartz-like crystals; permanent in the air; soluble in 12 parts of water at 60° and in 5 parts at 212° Fahr. ; insoluble in alcohol ; extremely nau- seous, and bitter-tasted. It crepitates on the application of heat; fuses at a red heat, but loses nothing in weight. 100 gr. dis- solved in distilled water, on the addition of chloride of barium and hydrochloric acid, fur- nish 132 gr. of sulphate of barium, dried at a red heat. Potassinm, Bisnlphate of. KHSO4. Syn. PoTASSIUM-HTDEOOBir SULPHATE, ACID PO- TASSIUM SULPHATE ; Potass^ bisulpeas. Prep. 1. (Anhydrous.) Neutral sulphate of potassium and oil of vitriol, equal parts; hot water, q. s. (not more) to dissolve ; anhydrous bisulphate crystallises out, in long delicate needles, as the solution cools. If these are left for several days in the mother-liquor they are redissolved, and crystals of the ordinary hydrated bisulphate are deposited. 2. (Hydrated.)— a. (Ph. L. 1836.) Salt left in distilling nitric acid, 2 lbs. ; boiling water, 3 quarts; dissolve; add of sulphuric acid 1 lb.; concentrate by evaporation, and set the liquid aside, so that crystals may form. b. (Ph.D.) Sulphate of potassium (in pow- der), 3 oz. ; sulphuric acid, 1 fl. oz. ; mix them in a porcelain capsule, and expose it to a heat capable of liquefying its contents, until acid vapours cease to be evolved ; powder the residuum, and preserve it in a well-stopped bottle. Prop., c5"c. Sour and slightly bitter-tasted rhombic prisms; soluble in about 2 parts of cold and 1 part of boiling water, the solution exhibiting a strongly acid reaction. It is much employed, in lieu of tartaric acid, for the production of carbonic acid, in ' gazogenes,' &c. ; also to adulterate cream of tartar and tartaric acid. According to Dr Paris, it forms a "grateful adjunct to rhubarb." — Dose, 12 gr. to \\ dr., in solution, combined with rhubarb or bitters, as the neutral sul- phate. Potassium, Sulphide of. Syn. Sulphtteet OF POTASSIUM, LiTEE OF SULPHUEf ; Po- TASBII SULPHUEETCM (Ph. L., E., & U. S.), Hepab sulphueis (Ph. D.), L. Prep. 1. (Ph. E.) Sulpliur, 1 oz. ; carbonate of potas- sium, 4 oz. ; mix, heat them in a covered crucible till they form a uniform fused mass; when cold, break it into fragments, and preserve it in well-closed vessels. The formulas of the Ph. L. 1836 and Ph. U. S. are similar. 2. (Ph.D.) Sublimed sulphur, 4 oz. ; car- POTATO 1365 bonateofpoUasinm (from penrlash, first dried, iind then reduced to powder), 7 oz. ; mix in u warm mortir, heat thura in a Hessian crucible, as before, pour the fused mass into an iron cup, over which immediutely invert a second vessel, to exclude the air, and, when cold, break the muss into fragments, and preserve it in a green-glass stoppered bottle. Prop., S(c. A hard, brittle, liver or greenish- brown coloured solid ; inodorous whilst dry ; soluble in water, forming a highly-fetid solu- tion ; and, in ucids, evolving strong fumes of sulphuretted hydrogen; reaction, alkaline; exposed to the air, it is gradually converted into sulphate of potassa. As a medicine it is reputed diaphoretic, expectorant, and stimu- lant. — Doie, 2 to 6 gr., in solution, or made into pills with soap; in gout, rheumatism, liver affections, and various chronic skiu dis- eases. Externally, made into a lotion and oint- ment. It is highly acrid and corrosive, and in Urge doses poisonous. fotosBinm, Sulphocyauide of. KCNS, or KCyS. Sl/n. StTLPHOOYANUEET OP POTAS BIUM; POTASSII BULPHOOrANIDnM, P. SUL. PHO-OTANDEETUM, h. Prep. 1. Fenocyanicie of potassium (anhydrous, or dried by a gentle heat), 46 parts ; sulphur, 82 parts ; pure carbo- nate of potassium, 17 parts ; reduce them to powder, and very gradually heat the mixture to low redness in a covered iron crucible, which it will less than one half fill ; remove the half- relVigerated and scill soft mass, crush it, ex- haust it with water, and evaporate the aque- ous solution to dryness ; powder the residuum, and exhaust it with hot alcohol or rectified spirit; the alcoholic solutiun will yield beau- tiful white crystals as it cools, and the resi- duum or mother-liquor may be evaporated for the remainder of the salt. 2. Cyanide of potassium, 3 parts; sulphur,! part; water, 6 parts; digest ihera tofretlier for some time, add 3 parts more of water, filter, evaporate, and crystallise. Prop., ^c. Ijong, slender, colourless prisms or plates, which are anhydrous, bitter- tasted, deliquescent, fusible, very soluble in both water and alcohol, and non-poisouous. It is chielly used as a test for ferric oxide, for which purpose it is preferable to all other sub- stances. Potassium, Tartrate of. K-iCjA^Oe. Syn. XEnTBALTABTBATKOP POTASSIUM, TaETEATB OF POTASSA, NeUTEAL TABTAE, SoLUBLS T. ; P0TAS6.E taetbab (B. p.. Ph. L., E., & D.), Kali TAiiTABiZATUMf, L. Prep. (Ph. D.) Carbonate of potassium, 8 oz. ; distilled water, 2 quarts; dissolve, and to the solution, whilst boiling hot, gradually add of hitartrate of po- tassium, in fine powder, 1 lb., or q. s., so that the liquid, after ebullition for a couple of minutis, i-eases to change the colour of either blue or reddened litmus paper; next filter the liquid through calii'o, evaporate it until a pel- licle forms on the surface, and set it aside to erystallise; after 12 hours collect the crystals, dry them on bibnlnus paper, and preserve them from the air. The formula of the Ph. L. 1836 is nearly similar. Prop., S(c. The crystals of this salt, which are obtained with difficulty, ore right rhombic prisms, and are deliquescent. The salt of commerce is usually in the form of a white granular powder, which is obtained by simply evaporating the solution to dryness, with con- stant stirring. In this state it requires about 4 parts of cold water for its solution. Acids convert it into the hitartrate. As a medicine it acts as a gentle diuretie and aperient, and is valued for correcting the gripiug properties of senna and resinous purgatives. It is also antiscorbutic. — Doie, \ dr. to \ oz., in pow- der, or dissolved in water. The solution changes the colour neither of litmus nor tur- meric. The addition of almost any acid throws down crystals of hitartrate of potas- sium, which cenerally adhere to the vessel. The precipitate occasioned by either chloride of barium or acetate of lead is dissolved by dilute nitric acid. Potassium, Bitartrate of. KHC^HjOj. Syn. Acid tabtratk op potassa, Supek-taetkatk OF p., Ckeam op taetab; Ceemob taetabi, Potass* bitaeteas(B. P., Ph. L., E., & D.), Potass* supeb-taetbas, Taetabi ceystalm, L. This well-known salt is deposited during the fermentation of grape juice as a crust on the sides of the casks or vats. In its unpre- pared or crude state it is called white or red tartar or argol, according to the wine from which it has been obtaiued. It is purified by boiling it in water, crystallisation, resolution in water,and treatment with freshly burnt char- coal and aluminous clay, to remove the colour; the clear liquid is then decanted, whilst still hot, and allowed to cool slowly; the resulting crys- tals form the ' cream of tartar" of commerce. Prop., Sfc. Small, translucent, gritty, pris- matic crystals, irregularly grouped together ; permanent in the air; requiring fnlly 100 parts of cold water, and about 15 parts of boiling water, for their perfect solution; the solution has a harsh, sour taste, and, like that of the tartrate, suffers spontaneous decomposi- tion by keeping. Its solution reddens lituius. At a red heat it is converted into carbonate of potassium. Entirely soluble in 40 parts of boiling water; 40 gr., in solution, are neu- tralised by 30 gr. of crystallised carbonate of soda. — Doxe. As an aperient, 1 to 3 dr. ; as a diuretic, J dr. to 1 dr. ; as an antiscorbutic, 10 to 20 gr. frequently. It is much used to make a pleasant cooling drink (' Imperial'), and in tooth-powders. POTA'TO. This well-known and valuable article of food is the tuber of the Solanum tu- berosum or esculentum, a plant which was in- troduced to this country by either Sir Francis Drake or Sir Walter Raleigh, towards the latter part of the 16th century. It is now extensively cultivated in all the temperate climates of the world. It yields a vast quantity 1366 POTATO of food on a small space of ground, but only about l-7th part of the weight of the tuber is nutritious, and this is chiefly farinaceous. Its farina or starch is, however, accompanied by no inconsiderable portion of saline matter, more especially of potassa, which renders it highly antiscorbutic, and a powerful corrective of the grcssncss of animal food. When form- ing part of a mixed diet, perhaps no sub- stance is more wholesome than the potato, and, certainly, no other esculent hitherto dis- covered appears equally adapted for universal use. Boussingault gives the following as the average composition of the tubers of the potato :— Moist Dry. Water . 75-9 . ^ Albunieij 2-3 . . 96 Oily matter 0-2 . . 0-8 Fibre . 0-4 . . 1-7 Starch . 20-2 . . 83-8 Salts . 10 . . 4-1 1000 1000 Manuring experiments on potatoes in 1867- 1869 show that on light soils a mixture of mineral superphosphate, crude potash salts, and ammonium sulphate, produces very bene- flcial results; on stiff soils nitrogenous manures have little effect. Further proof is given that manuring with common salt tends to decrease the yield. Analyses, conducted by A. Stocltardt, of potatoes grown in eight different years, show tbnt those manured with salt invariably con- tain less starch than those nnmanured, the decrease being from 10 to 20 per cent, of starch ; the same effect is produced when the salt is mixed with other manures. Under the microscope the cells are seen to be very sparingly fitted with starch grains. Unmanured potatoes contained '43 per cent, of sodium chloride in the dry substance, and those which had received a small dressing of common salt 1'34 per cent.' No certain rule can be laid down for ' dress- ing ' potatoes. " If boiled, it may be that they require to be put into boiling water, or, may be, into cold, and either boiled quickly or slowly ; but this you must find out. Choose them all about the same size, with a, smooth skin, and when they are boiled and begin to crack, throw off the water immediately, as it only damages the rout. When dressed let them stand near the fire, with a cloth over them, and serve them in their skins. Salt may be put into the water at the beginning. A watery potato will require quick boiling, and, sometimes, to be put into boiling water." (Soyer.) To retain the highest amount of n ourishment in potatoes they should be ' dressed' with their skins on them. The bruised or damaged parts, worm-holes, &c., being removed with a knife, the dirt should be carefully cleaned out of the ' eyes,' and from the rough parts of the skins, by means of a brush and water, after which tbey should be well rinsed in clean water, and drained in a colander. If they are at all dry or shrivelled, they may be advantageously left to soak for 3 or 4 hours in clean cold water before cooking them. Potatoes 'dressed' in the skins have been found to be nearly twice as rich in potassa salts as those which have been first peeled. The skins are easily removed before sending them to table. New potatoes should have their loose outer skin rubbed off with a cloth or stiff brush before being dressed or cooked. Potato starch granules. jMasheb potatoes are prepared by crushing, with the back of a spoon, or with a rolling- pin, the hot 'dressed' tubers, placed in a bowl ^ '(J> Potato stai-ch granules swollen by liquor potassv. or dish, or on a pie-board. A little milk, 1 Voelcker ' Key. Afiric, Society's Journal,' quoted in Journal of Chemical Society," vol. x.tv. I'OT POUREI— POTTERY 1367 battor, and salt may be added to them at will, Bad tli(>v rany be either at once 'served up,' or prpHsed into * lorins,' and first ' browned off* in tlio ovi'ii, Potacoea, if not soft and mealy, and well manticated, frequently escape the Hiilvint action of the stomach, and pass olf uudi^i^sted, often to the serious derangement of tile bexlth. By mashing them this incon- venience is removed. The delicate, the dy- i peptic, and the aged should take them in no other form, Potatoes may be preserved so as to stand the longest voyages unchanged, by thoroughly desiccating them in an oven, or by steam heat. For this purpose the roots, either raw or three parts dressed, are generally first cut into dice ol' above i inch square, to facilitate the operation. Under a patent granted to Mr Uownes Edwards, Aug., 1840, the billed potatoes are mushed and granulated by fiyed, in this country, to produce the be^t kind of earthenware (Stapfokdshibe ware) are the fine white clays of Devonshire and Cornwall, and powdered chert or flint. This is brought to a perfectly homogeneous plastic mass with witer, and in this state is fashioned upon the potter's wheel and lathe, or by moulding, into all the varied nhjects of utility and ornament, which are made in this material. After the newly formed ve-al on the surface. Poultice of Clila"ride of So'da. S,i/n. Cata- PLA8MA SOD« CHLOBINATJE (B. P., Pll. L.), L. Prep. 1. (Ph. L.) Boiling water, 6 11. oz.; lin- seed meal, 41 nz. ; mix gradually, then add of solution of chlorinated soda, 2 fl. oz. Applied to foul ulcers, gangrenous parts, &c. 2. (B. P.) Solution of chlorinated soda, 1 ; linseed raeal, 2; boiling water, i; add the linseed meal gradually to the water, stirring constantly, then mix the solution of chlori- nated soda. Pooltice, Compound Farina. Syn. Cata- FLASMA FABIN* COMP03ITUM. Prep. Kye Hour, 1 lb.; old yeast, 4 oz.; salt, 2 oz.; hot water, q. d. Foaltice, Commin. (L. Ph. 1788.) St/n. Cataflasma CPIIINI. Prep. Cummin seeds, 1 lb.; bay berries, scordlum leaves, serpentaria root, of each 3 oz. ; cloves, 1 oz, ; to be powdered together and mixed with thrice their weight of hunev. I Pooltice, Discotient. Si/n. Cataflasm;! DI80BTIEN8. Prep. Barley meal, 6 OZ. ; fresh hemlock, 2 oz. ; vinegar, q.s. Boll and add sal ammoniac, i oz. (Fr. Hosp.) The same, with 2 dr. of acetate of lead added. Poultice, Effervescing. Syn. Cataflasma bffeevescens. Prep. Fresh wort thickened with oatmeal, and a spoonful of yeast added. Foaltice, Emetic. Si/n. Cataflasma bmb- TICUM. Prep. Bruised groundsel (Senicio vu/garis) applied over the stomach produces vomiting. CataplasmaofFig. Syn. Cataflasma Koi. Prep. A dried fig, roastel or boiled (some- times in milk), is frequently applied to gum- boil, &c. Poultice, Foxglove. (Mr AUand.) Si/n. Cataflasma digitalis. Prep. A stron;,' decoction of foxglove, with bread-crum, or linseed meal, q.s. Poultice, Galbanom. Syn. Cataflasma O-ALBANi. Prep. Lily roots, 4oz. ; fip-, 1 oz. ; boil till soft, and bruise them with li oz. of onions and J oz. of galhnnum, triturated with yolk of egg and a sufficient quantity of linseed meal. Foaltice, Galvanic. (Recamier.) Syn. Ca- taflasma QALVANicnM. It consists of cotton wadding containing a layer of very thin zinc plates, and another layer of copper ones. This pad, conveniently quilted, is enclosed in a bag, one face of which is of quilted calico, the other of impermeable tissue. The natural perspira- tion, confined by the impermeable tissue, ex- cites galvanic action between the metals. Pooltice of Hem'lock. Syn. Cataflasma CONII (B. P., Ph. L.), L. jPrep. 1. (Ph. L.) Boiling water, J pint; linseed meal, 44 oz , or q. s. ; make a poultice, and on this spread of extract of hemlock (Ph. L.), 1 oz., first softened with a little hot water. Anodyne. In irrit- able and painful cancerous, scrofulous, and syphilitic sores, tumours, &c. 2. (B. P.) Hemlock leaf, in powder, 1 oz. ; linseed meal, 3 oz.; boiling water, lu oz. ; mix the ingredients, then add them to the water gradually, constantly stirrir a;. Foaltice, Henbane. Syn. Cataflasma HTOSOTAMI. The same as Poultice of FOFFT. Foaltice, Hop. (Dr Trotter.) Syn. Cata- flasma HUMULI. Hops softened with hot water. To foul ulcers. Foaltice, Iodine. Syn. Cataflasma iodu- betum. To a commou poultice add solutiou or tincture of iodine. Pooltice, Lead. Syn. Cataflasma plumbi. Prep. Goidard water, 1 lb. ; bread crum, q. s. Pooltice, Lily. Syn. Cataflasma lilii. The pulp of the white lily boiled and bruised. Poultice, Lime. Syn. Cataflasma calcis. Prep, Slaked lime, 2 oz. ; oatmeal, 2 oz. ; lard, 4 oz. Formerly used at Bath Hospital. Foaltice of Linseed Meal. Syn. Cataflasma LINI (B. P., Ph. L.), L. Prep. 1. (Ph. L.) To boiling water, 4 pint, add, gradually, constantly 1370 POULTICE stirring, of linseed meal, 4i oz., or q. s. Emol- lient. Used to promote the suppuration or 'ripening' of tumours. A little oil or lard should be added, and some smeared over the surface as well, to prevent its getting hard. For small 'gatherings,' as of the fingers, a little chewed b;"end and butter is an efficient and convenient substitute. 2. (B. P.) Linseed meal, 4; olive oil, i; boiling water, 10; mix the linseed meal with the oil, add the water gradually, constantly stirring. Obs. Linseed meal prepared from the cake, from which the oil has been expressed, is less adapted for poultices than that prepared from the unpressed, whole seed. The latter is or- dered in the Ph. L. Poultice, Malt. (Guy's Hosp.) S^n. Cata- PLASMA BYNES. Prep. Ground malt, with yeast, q. s., to form a poultice; to be applied warm. Poultice, ffiatnrative. (L. 1745.) Syn. Cata- PLABMA MATUBAN3. Prep. Pulp of figs, 4 oz. ; resin ointment, 1 oz. ; strained galbanum, 2 oz. Poultice of Mus'tard. Syn. Catapiasma SINAPIS (Ph. L.), L. Prep. 1. (B. P., Ph. L.) Linseed meal and powdered mustard, of each 2^ oz., or q. s. ; boiling water, \ pint ; mix as before. 2. (Ph. L. 1836.) As the last, but substi- tuting boiling vinegar for water. Used as a powerl'ul counter-irritant, stimulant, and ru- befacient; in low fevers, apoplexy, coma, &c., where there is a determination of blood to the head ; in deep-seated inflaramatory pains, neuralgic pains, &c. It should not be left on long enough to raise a blister. See Plastees. Poultice, Onion. Syn. Cataplasma CEPiE Prep. Onions roasted and mashed. Poultice of Pop'py. Syn. Cataplasma pa- PATEEIS, L. Prep. 1. (P. Cod. 1839.) A strong decoction of poppies, thickened with crum ol bread. Anodyne. Poultice, Potash, Acetate of. Syn. Cata- plasma POTASS.B ACETATIS ; CATAPLASMA KEtfTEALE. Prep. Acetate of potash, 1 oz. ; water, 1 pint ; crum of bread, q. o. To ill- conditioned sores. Poultice of Po'tato. Syn. Cataplasma SOLANI TUBEKOSi, L. Prep. Prom the raw potato, scraped or grated fine. A popular application to fresh bruises, extravasations, burns, scalds, &c. Poultice of Potato Starch. (P. Cod.) Syn. Cataplasma feoul.^. Prep. Potato starch, 2 oz. ; mix with a little cold water, add to it 20 oz. of boiling water, and boil for an instant. Cataplasms of rice and wheat starch are made in the same manner. Poultice, Pradier's. Syn. Peadiee's cata- plasma; CATAPL4SME DE Peadiee, Fr. Prep. Take o\ balsam of Mecca, 6 dr. ; rectified spirit, 16 oz. ; dissolve ; next, separately, take red cin- chona bark, sarsaparilla, and sage, of each 1 oz. ; saffron, 4 oz. ; rectified spirit, 32 oz.; digest for 48 hours, and filter; mix the two liquors ; add to them twice their weight of lime water. In gout; 2 fl. oz. are sprinkled on the surface of a hot linseed-meal poultice sufficiently large to surround the affected part. It is said that the Emperor Napoleon gave je2500 for this receipt. Poultice of Pyroligneous Acid. (Dr Eeece.) Syn. Cataplasma acidi pieoliososi. Prep. Bran, 1 lb.; linseed meal, 1 oz.; impure pyro- ligneous acid, q. s. For scrofulous ulcers; occasionally 30 minims of tincture of perchlo- ride of iron, and 3 dr. of extract or powder of hemlock, are added. Poultice of Eed 'Wine. (Gl. Hosp.) Syn. Cataplasma tini eubei. Prep. Linseed meal, IJ oz. ; boiling water, 5 oz. ; stir it over a slow fire tor a minute, remove, and add 2 oz of red wine. Poultice, Eoasted Apple. Syn. Cataplas- ma MALI. The soft pulp of roasted apple, applied to infiamed eyes. Other ingredients are sometimes added. Poultice, Rose. Syn. Cataplasma 'BOsm. Prep. Powdered alum, 30 gr. ; confection of roses, 4 oz. ; mix. Poultice of Sea-wrack. (Dr Russell.) Syn. Cataplasma pcci. Prep. Fresh bladder fucus (sea-wrack) bruised. Applied to glan- dular tumours, ike. Poultice, Sim'ple. Syn. Cataplasma sim- plex, L. Prep. (Ph. D. 1826.) Powder for a cataplasma and boiling water, of each q. s. to form a poultice, the surface of which is to be smeared over with olive oil. Emollient. Bread poultice and linseed-meal poultice are now generally called by this name. See Powdee (Poultice). Poultice of Slippery Elm. Cataplasma ULMi. The powdered bark of the slippery elm ( Ulmusfulva) mixed with a sufficient quantity of hot water. Poultice of Soap. Syn. Cataplasma ba- PONIS, L. Prep. From white soap (scraped or sliced), 1 oz. ; boiling water, i pint ; dissolve, and add crum of bread, q. ». As an application to scalds and burns. Poultice, Sorrel. Syn. Cataplasma ox- alis. Prep. Bruised sorrel leaves, mixed with oatmeal and beer. Poultice, Stimulating. (Dr Hugh Smith.) Syn. Cataplasma stimulans. Prep. Bye flour, 1 lb. ; old yeast, 4 oz. ; common salt, 2 oz. Poultice, Sulphate of Lime. (Blizard.) Syn. Cataplasma calois sqlphatis. Prep. Paris plaster mixed with water to a soft paste, and applied before it hardens. Formerly applied to ulcers to form an artificial scab ; now occa- sionally used to atford mechanical support in some surgical cases. Ponltice of Sulphate of Soda. (Kirkland.) Syn. Cataplasma sod.b sulphatis. Prep. Sulphate of soda, 1 oz.; boiling water, ^ lb.; crum of bread, a sufficient quantity. POULTRY— POWDER 1371 Ponltice to canse Snppnration. (E. Ph. 1774.) Syn. Cataplasma snpprBANS. To an emollient cataplaim add bruised onions, 1) oz.; bBKilicon oiiitiiient, 1 oz. Poultice of Taanate of Lead. (0. Ph.) 8t/n. Cataplasua ad decumbituu ; Pluubdm TiNNIcnM PDLTIFOHMB. Prep. Boil 2 OZ. of oak bark in auflicient water to yield 10 oz. of strained decoction ; add to this 1 oz. (by weight) of liquid Subacetate of lead, collect the pre- cipitate on a filter, and put it into a bottle with 2 dr. of TectiSed spirit. Ponltice, Tonic. (G. Hosp.) Si/n. Cata- PtASMATONlcuM. Prep. Powdered bark, 1 OZ. ; cburcoul, 1 oz. ; camphor, li dr.; oil of tur- pentine, q. 8. Poultice, Turnip. Syn. Cataplasma bapi. Prep. I'cul turnips, boil them till soft, beat them to a pulp, and apply warm. Ponltice, Turpentine. (Dr Reece.) Si/n. CATAPLABMA TBHEBINTHINiE. Prep. Oil of turpentine, 2 dr. ; olive oil, 1 oz. ; linseed meal, 1 oz. ; Oiitmeal, 4 oz. ; boiling water, q. a. To indolent ulcers, and, with more turpentine, to deep burns, scalds, and chilblains. Poultice of Via'egar. Syn. Cataplasma ACBTi, L. Prep. From crum of bread soaked in vinegar. Applied cold in bruises, extrava- sations, &c., especially black eyes. Verjuice is often employed in the same way. Poultice of Walnut Leaves. (Perfect.) Syn. Cataplasma juolandis. Prep. Tlie fresh IciiVLs of wiilnut bruised and mixed with honey- Applied over the abdomen as a ver- mifuge, Ponltice of Yeast. Si/n. Cataplasma peb- MhNTI (B. P., Ph. L.), C. F. CEBEVISIJE, L. Prep. 1. (Ph. L.) Beer yeast and water at 100° Fahr., of each 5 fl. oz. ; mix, stir in flour, lib., and place it near the fire until it rises. In gangi cnovis or foul ulcers ; to correct the fetor of the discharge, and to hasten the sloughing, 2, (B, P.) Beeryenst, 6j flour, 14; water (at 100° Fahr.), 6 ; mix. Place the mass near the fire till it rises. POUL'TRY. Domestic birds, which are pro- pagated and fed for the table, and for their eggs, feathers, &c. The poultry of this country are the common domestic fowl, the turkey, the duck, and the g"0ed by pattern drawers, for sprinkling over pricked papers, are also called ' pounce.' For liquid pounce,see Mabe- ING INK. POWDER. Syn. Pulvis, L. Powders are divided by pharmaceutical writers into two classes — simple and compound. The first are prepared by simple pulverisation ; the second by the admixture of two or more simple pow- ders. For use the appropriate doses are sepa- rately weighed, and placed in separate pa]>ers. They are usually exhibited in a little honey, sugar, or milk, either taken frim a spoon or made iiito an electuiiry or bolus, and swallowed in the semi-solid form. Metallic and other heavy powders are best taken in the latter st'ite. Very active substances shou'd be, in all cases, mixed with some inert powder, as that of starch, gum, liquorice, or marshmallow, at the time of 'dispensing' them. " This form of preparing medicines is tlie simplest, and perhaps the least objectionable ; but it is not applicable to all the articles of the Materia Medica. Those remedies which are very unpleasant to the tnste; those which deliquesce rapidly when exposed to tlie air, or are very volatile; and those which require to be given in very large doses, or \vhiv h nvo not diffused readily in water, cannot, with pro- priety, be administered in the form of powder. Some substances cannot be reduced to powder unless they be very much dried, and tiic heat 1372 POWDER necessary for that purpose alters their proper- ties." Nor can we " be surprised that a great alteration siiould be effected in a short time by the action of the air on so great an exten- sion of surface as takes place in the operation usually adopted fur reducing drugs to a tine powder." (A. T. Thomson.) In this country compound powders appear to be a favourite form of medicine in the dis- eases of infancy and childhood. " It is necessary that whatever we order to be reduced to powder should be rubbed tlirough a fine sieve, so that the impurities and coarser parts may be separated ; and it is needful that most powders should be recently prepared, and not too long kept." (Ph. L.) ' As nearly all powders suffer by exposure to the air and light, they should be preserved in closely-corked opaque or green-glass bottles, or in tin canisters from which the external air is carefully excluded. See Pulveeisation, (!tc. Powder, Algaroth'e. See Antimony, Oxy- OHLOEIDE. Powder of Al'oes (Compound). Syn. Pulvis ALOES COMPOSITUa (Pll. L.), p. ALOES CUM GUAiACO, L. Prep. (Ph. L.) Socotrine or hepatic aloes (in powdei), 1\ oz. ; guaiacum (in powder), 1 oz. ; compound cinnamon pow- der, \ oz. ; rub them togetlier. A warm, sudo- rific purgative. — Dose, 10 to 20 gr. Powder of Aloes with Canel'la. Syn. Aloetic powdeb. Holy BiTTEEf ; Hieea piOBAf, Pulvis aloe3 cum oanhlla, L. Prep. From powdered Socotrine or hepatic aloes, 4 pnrts; powdered white canella, 1 part. Uses and dose, as the last. Ohs. Once a highly popular remedy. It was originally made into an electuary with honey, and in this form was frequently called ' HIERA LOGADIl.' It is still a favourite in domestic medicine and veterinary practice. The principal objection to both this and the preceding preparation is the nauseous flavour of the aloes, which is ill concealed by the aromatics. The * HIERA PICRA* for Carriers is usually made with the cheapest Cape aloes. Powder of Aloes with Iron. (L. Ph. 1788.) Syn. Pulvis aloetious cum perbo. Prep. Aloes, li oz. ; myrrh, 2 oz. ; sulphate of iron, 1 oz. ; dr'cd extract of gentian, 1 oz. Powder of Al'um (Compound). Syn. Styp- tic powder; Pulvis siyptiods, P.aluminis coMposiTus (Ph. E.), L. Prep. (Ph. E.) Alum, 4 ciz. ; kino, 1 oz. ; mix them, and re- duce them to fine powder. Astringent and styptic. — Dose, 5 to 15 gr. ; in diarrhoea, profuse menstruation, &c. Externally, in hffimorrhages, &c. Powder, Alum, Opiated. (Bouohardat.) Syn. Pulvis ald minis opiatus. Prep. Alum, 1 dr. ; sugar, 1 dr. ; opium, 4 gr. ; mix lor 12 powders. 2 or 3 daily in obstinate diarrhoeas and passive ha3morrhage8. Powder of Alum with Capsicum. (Dr Turn- bull.) Syn. PULTIS aluminis ocm capsico. Prep. Alum, 3 parts ; concentrated tincture of capsicum, 1 part ; mix, dry, and triturate again. Applied to the tonsils. Powder of Alum with Gnm. (Frankel.) Prep. Alum, gum tragacanth, of each equal parts. Applied to sore breasts. Powder of Alum with Starch. (St. Th. Hosp.) Syn. Pulvis aluminis cum amylo. Prep. Alum and starch, equal parts. In insu£3ation of rhinorrhcea. Powder of Ambergris with Knsk. (Bat. Ph.) Syn. Pulvis AMBEROEisEa; MosCHATUs. Prep. Ambergris, 6 dr. ; musk, 1 dr. ; oil of cinnamon, 2 scruples ; refined sugar, llj oz. ; mix. Powder, Ammonlated Aromatic. Syn. Pul- vis AMMONIAXUS AROMATICUS ; LeaYSON'S •AMMONIACAL COLLTEIUM. Prep. Muriate of ammonia, 1 dr.; slaked lime, 1 oz.; char- coal, 15 gr. ; cinnamon, 15 gr. ; cloves, 15 gr. ; bole, i dr. Put them into a buttle and moisten with a little water. Powder of Ancho'vy. Syn. Pulvis clupej; ENCBASICOLI, L. Prep. Pound anchovies to a paste, then rub them through a sieve, and add enough flour to make a dough, which must be rolled out into thin slices and dried by a gentle heat in a stove ; it is, lastly, pow- dered and bottled. Colouring is frequently added. Chiefly used to make sauces. British anchovies are frequently substituted for the genuine fish. Powder, Authrakokali, Compound. Syn. Pulvis anthrakokali, compound. Prep. Authrakokali, 2 gr. ; washed sulphur, 6 gr. ; mix. For 1 dose. Powder, Authrakokali, Simple. (Poy)a.) Syn. Pulvis antheakokali simplex. Prep. Authrakokali, 2 gr. j liquorice powder, 6 gr. ; mix. For 1 dose. Powder, Antiepileptic, Syn. Pulvis anti- epilepticus (E. Ph., 1744.) Prep. White dittany, pseony, valerian, mistletoe of the oak, equal parts. — Dose, 10 to 6 gr. (Behrends.) Prep. Valerian, 4 dr.; magnesia, muriate of ammonia, oil of cajeput, of each 1 scruple. — Dose. A tea spoonful three times a day. Dr Paris says the following was used successfully by a Dutch empiric : — Sulphur, 1 scruple ; sulphate of potash, 10 gr. ; rhubarb, 5 gr. ; nutmeg, 2gr. ; mix. (Germ. Hosp.) Prep. Oxide of zinc, 16 gr. ; carbonate of magnesia, 48 gr. ; oleosaccharum of cajeput, 3 dr. Mix for 8 doses. Poudre de Ragolo. Oxicle of zinc, 10 gr. ; valerian, mistletoe, sugar, orange leaves, of each 4 dr. ; magnesia, 2 scruples ; oil of cajeput, 2 scruples ; a teaspoonful three times a day. Pasquier prescribes — Wall crop, 10 gr. ; gum Arabic, 10 gr. ; 1 to 4 powders daily for eight times. Sommer's specific consists of — Wall crop, 6 to 10 gr. ; oleo-sac- charnm of mint, 8 gr. ; one morning and evening for six times. See Pulvis aetkmisijs SACOHAEATUS. The Poudre de Guttete consists of mistletoe, 2 parts; white dittany, 2; pasony POWDER 1373 root and seeda, S ; prepared coral, 1 ; elk's boof, 2 ; seeda of oriiche, 3. Given in doBes of a few grains in convulaions of infanta, or in larf^er doses for epilepsy. Powder, Antihydrophobic. (Dr Mead.) Si/n. Pbitis ANTILT88U8. Prep. Aah-coloured ground liver-wort (Pettidea canina), i oz. ; black pepper, 2 dr. ; miic, and give a fourth part every morning for 4 times. Powder, Antlmo"nlBl. St/n. Peveb pow- DEE, LiSLE's p., JAMBS'B P. ; PULVIS JACOBI, PULVIS ANT1M0NIALI8 (B. P., Ph. E., & D.), PULVIS ANTIMONII COMPOSITIJS (Ph. li.), L. Prep. 1. (Ph. L.) A mixture of teraulphide of antimony, 1 lb., and hartahorn shavings, 2 lbs., is reduced to powder, thrown into a cru- cible heated to whiteness, and stirred con- stantly until vapour no longer rises ; the cnlcincd mixture is then rubbed to powder, ngain put into the crucible, and the beat gra- dually increased to whiteness, and maintained so for 2 hours; the residuum is, lastly, re- duced to a very fine powder. 2. (Ph. E.) From aulphide of antimony nnd hartshorn shavings, equal weights ; as the last. 8. (Ph. D.) Tiirtariscd antimony, 4 oz., is I dissolved in water, ^ gall., and added to solution of phosphate of soda, 4 oz., in water, 1 quart; a solution of chloride of calcium, 2 ni , in water, 1 quart, and to which solution of ammonia (Ph. D.), 4 fl. oz,, has been added, is next poured in, and the whole boiled for 20 minutes; the precipitate is then collected on a calico filter, and washed with hot distilled water, until the liquid which passes ceases to give a precipitate with a weak solution of ni- trate of silver ; it is, lastly, dried by a steam or water heat, and reduced to a fine powder. 4. (B. P.) Oxide of antimony, 1 ; precipi- tated phosphate of lime, 2 j mix. — Dose, 2 to 6gr. Uses, ^0. Febrifuge and diaphoretic. In- tended as a substitute for the proprietary and more expensive James's powder. — Dose, 3 to 10 or 12 gr., or more, repeated every fourth or filth hour until diaphoresis is set up ; in fevers, rheumatic affections, chronic skin diseases, &,c. It is a very uncertain and va- riable compound, unless it has been carefully prepared. Dr EUiotson exhibited it in doses of 100 gr. without producing any sensible effect. A spurious article, made by triturating 1 oz. of tartar emetic with 18 or 19 oz. of burnt hartahorn, is frequently sold for it in the shops. See Antimonious acid and James's POWDEE. Powder, Antispasmodic. (P. Cod.) Syn. PnLTiB aniispasmodious. Prep. Cyanide of zinc, 3 gr. ; calcined magnesia, 24 gr. ; oiunaraon, 12 gr. ; mix. For 6 doses. Powder, Antispasmodic. (Jourdan.) Si/n. PcLVis AXTI3PA8MOUICCB. Prep. Valerian, 1 oz.; oxide of zinc, 1 scruple; musk, 8 gr. ; mix. Powder, Aromat'ic. See Powdkb, Com- POUSD CINNAMON. Powder, Arsenical. See Powdeb, Escha- BOTIC. Powder of Asarabas'ca (Componnd). Set; Snppp (Cephalic). Powder, Astrin'gent. Syn. PrLVisASTEiw- OBNS, P. 8TTPTICU8, L. Prep. 1. From Aleppo galls and burnt alum, in fine powder, equal parts. Used in piles, soft polypi of the nose, chilblains, &c. Powder, fia"kiDg. Prep. 1. Tartaric acid, ^ lb. ; bicarbonate of soda and potato farina or British arrow-root, of each f lb. (each in powder); separately dry thtm perfectly liy a very gentle heat, then mix them in a dry room, pass the mixture through a sieve, nnd at once put it into packets, observing to press it bard, and to cover it with tinfoil or close-made paper, to preserve it as much as possible from the air and moisture. 2. (Delforte's.) Powdered tartaric acid, J lb. ; powdered alum, \ lb. ; bicarbonate of soda, J lb.; farina, 1 lb.; dry separately, na before, mix, and further add of sesquicarbonate of ammonia (in powder), 3 oz.; lastly, closely pack it in tinfoil. 3. (Green's.) Tartaric acid, 35 lbs. ; ses- quicarbonate of soda, 56 lbs. ; potato flour, 1 cwt. ; mix as before. Uses, cf'o. Baking powder is chiefly employed as a substitute for yeast. 1 or 2 tcaspoonfuls are mixed with the dry flour and other ingre- dients, which are then made into a dough, as quickly as possible, with cold water, and at once baked or boiled as the case may be. By the addition of about \ dr. of turmeric pow- der to each pound of the mixture it is con- verted into egg powder. When intended to be kept for any length of time it should be preserved in bottles or tins, so as to prevent the ' absorption of moisture. We have dis- covered traces of arsenic in some of the baking powders of the shops, which we refer to com- mon washerwoman's soda being used in their composition, instead of the pure carbonate or sesquicarbonate. Powder, Basil'ic. Syn. Royal powbeb, COENiCHINl'S p. ; Pl'LVIS BASIMCCS, P. CoE- NACHINI, L. Prep. From scammony, calo- mel, cream of tartar, and diaphoretic antimony, equal parts. This is the formula generally adopted for this compound, which has now long been omitted from the Pharmacopoeias. It is still a favourite with many practitioners, as an alterative purgative, and vermifuge for children. — Dose. For a child, 2 to 8 gr. ; for an adult, 5 to 20 gr. Compound powder of scammony is now generally sold for it. Powder, Belladonna, Saccharated. (Wertz- ler.) Syn. Puivis belladonnje sacchabatus. Prep. Belladonna root, 15 gr.; pure sugar, Idr. ; mix. For 72 powders. One twice a day, or oftener, according to the age. In hooping- cough. X374 POWDER Powder, Blaine's Distem'per. The basis of this preparation is tlie ' aurum musivum,' or bisulphuret of tin. (Dr Paris.) Powder, Blancmauge'. Fr^, From sago meal, 1 lb. ; essence of lemon, 15 drops ; mace, 12 gr. ; mix. Powder, Bleach 'ing. Chlorldeor hypochlorite of lime. Powder, Blue. See Smalts. Powder, Bronze. See Siannic sulphide, Ubonzikg, &c. Powder of Burnt Hartshorn. Syn. Pultis coENir OEBVIKI USTI, L. Prep. From pieces of hartshorn calcined to whiteness, and pow- dered. It consists principally of phosphate of lime. — Dose, 10 to 30 gr. ; in rickets, &c. Powder of Burnt Hartshorn with O'pium. Syn. PuLTis 0PIATU3, Pulvis corhu tisti CUM OPIO, L. Prep. From powdered calcined hartshorn, 1 oz. ; powdered opium and cochi- neal, of each 1 dr. — Dose, 5 to 20 gr. Powder of Camphor. Camphor may be readily pulverised by triturating it with the addition of a tew drops of rectiiied spirit or ethfr. Powder, Camphorated Nitre. (SwediHur.) Syn. Pdlvis kitko camphoeatds. J?renipound prepared by different houses vary so greatly from each other in the proportions of the ingredients, that it is uifiicult to regard any one as a stand- ard. The following are therefore merely given as examples : — Prep. 1. Corianders, 1 lb. ; tnrmeric, J lb.; black pepper, i lb.; scorched mustard, i lb. ; ginger, 2 oz. ; cnmin seed, 1 oz. ; cap- sicums, f oz. ; mace, \ oz. (all in powder); mi.K well. 2. Coriander seeds and black pepper, of each 8 lbs. ; turmeric and cumin seeds, ot each ilbs., allspice, J lb. ; mace, 1 oz. (all in powder) ; mix. This receipt is employed by an eminent wholesale house that does very largely in curry powder. 137S POWDER 3. (See page 524.) Used as a condiment and flavouring ingre- dient. The addition of a few heads of garlic gives it an increased zest for Indian veterans. Powder, Cust'ard. Frep. From sago meal, 2 lbs.; powdered turmeric, i 02. J bitter-almond powder, cassia, and mace, of each \ dr. Powder, Cyprus. Prom Cladonia rangiferina, or reindeer moss. It has a very agreeable smell, and, being extremely retentive of odours, is much used as a basis for scent-powders, f^achets, &c. The lichen known as the ragged hoary evevnia also possesses nearly similar properties, and is often substituted for it. See Powders (Scented). Powder, Diapente. (Ed. Ph. 174.4.) Si/n. PULTJS DIAPENTE. Prep. Aristolocbia root, gentian, bay berries, myrrh, ivory dust, of each 2 oz. ; mix. Powder, Disinfect'ing. Syn. PuLVis disin- PECTAN3, L. Prep. (Keist.) Bisulphate of potassa, 41 parts ; sugar of lead, 7 partfe ; binoxide of manganese, 3 parts, reduce them separately to a fine powder, and, when wanted for use, mix a proper quantity in any suitable vessel. For other formulae, see DiaiirPEOTiNa COMPOUNDS. The name is generally applied to hypochlorite of lime. Powder, Diuretic. (P. Cod.) Syn. Pultis DiURETicns. Prep. Gum Arabic, 6 oz. ; sugar of milk, 6 oz. ; nitrate of potash, 1 oz. ; marshmallow root, 1 oz. ; liquorice root, 2 oz. ; mix. Powder, Dover's. Syn. Pctltis Doveei, L. Prep. (Original formula.) Nitre and sulphate of potassa, of each 4 oz. ; melt tliem together in a red-hot crucible, reduce the cold fused matter to powder, and add powdered ipeca- cuanha, liquorice, and opium, of each 1 oz. This is the formula adopted in the Paris Codex. Compound ipecacuanha powdeb is now sold under this name. (See telom.) Powder, Duke of Portland's. Syn. Pultis ANTiAETHElTicus. Prep. Round birthwort, gentian, tops of lesser centuary, tops of ground pine, and germander, of each equal parts. — Dose, 1 dr. Powder, Egg. See Powder, Bakin&. Powder of Elaterium, Compound. (B. Ph.) Puvis elatebii oompositus. Prep. Elate- rium, 10 gr. ; sugar of milk, 90 gr. Rub them together to fine powder. — Dose, ^ gr. to 5 gr. Powder, Emmen'agogue. Syn. Pulvis em- MENAG-OaUS, P. aaiMATINUS, P. CONTRA AMB- HOBEHiBAM, L. Prep. 1. Saccharine car- bonate of iron, 3 parts ; powdered myrrh, ginger, and nutmeg, of each 1 part; divide into i-dr. papers. One for a dose, twice or thrice daily. 2. (Augustin.) Myrrh, 12 gr. ; saffron, 3 gr. ; oil of cloves, 1 drop. For a dose, as the last. 3. (Klein.) Calomel, 4 gr. ; extract of yew, 10 gr.; powdered savine, 1 dr.; Quevenne's iron, i dr. ; loaf sugar, 2 dr. For 6 powders ; as before. Powder, Emulsive, of GInten. (Taddel.) Syn. Pultis aiUTENis emulsivus. Prep. Fresh vegetable gluten, 10 oz. ; soap, 2 oz. ; water, 1 pint. Dissolve, evaporate the solution, dry it on plates, and reduce to powder. As an anti- dote to coiTosive sublimate. Powder, Escharot'ic (Arsenical). Syn. Pul- tis eschaeoticus AESENICALIB, L. ; POUDBE DU Feeees Cosmb, Fr. Prep, 1. (Original formula.) From white arsenic, 12 gr. ; burnt hartshorn, \ dr. ; cinnabar, 1 dr. 2. (P. Cod.) Red sulphuret of mercury and powdered dragon's blood, of each 2 parts; levigated arsenious acid, 1 part ; carefully mixed together. See Caustic, Aesekioal. Powder of Extract of Col'ocynth (Compound). Syn. Pultis extbaoti colooynthidis com- PosiTi, L. Prep. From compound extract of colocynth (Ph. L. 1836), dried by a gentle heat, and powdered. Obs. This, like many other articles em- ployed I)y lazy dispensers, does not represent the preparation for which it is used as a sub- stitute ; whilst, from its peculiar character, it is very open to sophistication — a practice, we regret to say, very general with certain drug- gists. Indeed, some of these pai-ties make this article by simply throwing the ingredients of the extract into a pan along with a little water, and, when they have become soft, stirring them together with a spatula, after which they are desiccated and powdered. This is then la- belled by certain houses, " Pulv. Ext. Coloc. CO. — P. L.," and sold to their unfortunate customers as such, although no such an ex- tract has been in the Ph. L. since that of 1836. Powder, Faynard's. The charcoal of beech- wood, finely powdered. (Paris.) Used in piles, and as a styptic. Powder, Fe'ver. See Powdee, Antimonial {above ). Powder of Flint. Syn. Silex conteitus (Ph. L.), L. Prep. As powdered glass. (Sec page 805.) It is ordered in the Ph. L. to be employed, instead of magnesia, for the purpose of mechanically dividing the essential oils used in the preparation of distilled water. It is also used as an escharotic. Powder, Fly. Prep. From white arsenic, 5 oz. ; white sugar, 6 lbs. ; rose pink, 2 oz. ; mix, and put 6 dr. in each paper. Used to kill flies. It is poisonous, and should be employed with great caution, particularly where there are children. Powder, Fu"mlgating. Syn. Pultis pu- malis, L. Prep. (Ph. Buss.) Amber, mastic, and oHbanum, of each 3 parts; storax, 2 parts ; benzoin and labdanum, of each 1 part; reduce them to coarse powder, and mix them well. See FuMiaATioN. Powder, Galls of (Componnd), Syn. Pultis Och-isLM coMPOSiTUs, L. See Powbbb, As- TEINOENT. POWDER 1377 Powder, Oascoign's. 5y». PtiLVis EcnKLis COMPOSITES. Prep. Prepiired crab sliellB, 1 lb. ; prepared chalk, 3 oz. ; prepared corul, 3 oz. ; mix. Powder, Goelia'a Aiitihec'tic. Prep. From burnt hartshorn, powdered nutmeg, black pepper, iind roastid lunrel beriies, ot each 1 part; lujnoiice puwder, 3 parts. — Dose, \ to 1 dr. ; in the hectic fever of Bcrufulous subject!). Powder, Gold. Syn. Pulvis auei. Tri- turate gold leaf with 10 or 12 times its weight of sulphate of potash till bright particles are no longer visible; pass it through a sieve, mix with boiling water, wash what remains on the filter, and dry in a stove.' Powder, Gold Compound. Syn. Pultis auei COMPOSITDS. Prep. Auro-chloride of sodium, 1 gr. ; lycopodium, starch, or washed orris powder, 1 scruple J mix. A-i'jthpart, gradually increased to ith part, of this powder to be rubbed on the gums. Powder of Gold and Iron. (Buckler.) Syn. PuLTis AUKi ET FEUBI. Prep. Pulverised foMt'i scrujiles; clean levigated iron Klings, 'Z scru|iles ; gum Arabic in powder, 30 gr. ; mix. Fi)r one dose, to be given in water acidu- lated with a few drops of sulphuric acid, as an antidote lor corrosive sublimate. Powder, Goulard. EtHoresced sugar of lead. Poisonous. Powder, Grey. Mercurial powder. Powder, Gregory's. See Powdeb op ItH0- BAllB (Compound). Powder of Guarana, Compound. (Dr Gav- rcUe). Kyii. PULVIS PACLLINiaS OOMPOSIIUS. Prep. Ouarana, 1 dr. ; compound ciiiuaiuon powder, 4 dr. Mix. Powder, Gum. (G. Ph.) Syn. PnLVia onMsiDfUS. Prep. Gum Arabic, 3 oz. ; liquorice, 2 oz. ; refined sugar, 1 oz. Mix. Powder, HBBmostat'io. Syn. Pulvis um- MOSTAllcus, L. Prep. 1. (Guibourt.) Char- c"al and gum Arable, of each, in powder, 1 part ; jiciwdered resin, 4 parts, 2. (.Mialhe.) From powdered alum, gum trogneanth, and tannin, equal parts. Used to check local bleeding. 3. (P. Cod.) Prep. Resin, 4 dr.; gum Arabic, 1 dr.; powdered catechu, 1 di'. Mix. Powder, Hair. Syn. Pulvi3 peo oeine, L. Starch reiliieid to a very fiue powder, and then scented according to the fancy of the artist; it is, lastly, passed through a gauze sieve. In its simple form, without any addi- tion, it constitutes 'plain hair powder.' In other cases it is distinguished by the name of the substance added to perfume it. Thus, we liavc 'rose hair powder, 'violet h. p.,' &c. Potato farina, well triturated, is now com- monly used for hair powder. Amongst the lower classesi, the contents of the 'flour dredger' ol the kitchen are frequently misap- pro]piiate(l to this purpose. See I'OWDEKS, Si INTED {below.) Powder, Hand. Prep. From almond powder, VOL. II. 1 lb. ; powdered cuttle-fish bone and white soap, ot each 4 oz.; orris powder, 1 oz. ; mix. Used to clean the hands, and to render them soft and white. See Potvdeb, Cosmetic. Powder, Helvetius's. Syn. Pulvis Helte- Tii, L. A mixture of powdered alum and dragon's blood. (Dr Paris.) Powder, Herrenscwand's Specific. See Pa- tent Medicines. Powder, Hiera Picra. Powder of aloos with caiiella (see above). Powder, Hnfeland's. Syn. HcPELiXD'a QUINQUINA PACTICE, PuLVls (INCnONi: PAC- TiTiDa, p. 8ALICISC0MP0SITUS, L. Prep. From bennet(the herb), calamus arorauticus, chestnut bark, gentian root, and willow bark, equal parts ; reduced to powder. Powder, Hunter's. See Powdeb, Wabt {below). Powder, Hunt's. See Powdeb, Hkeak- PABT. Powder of Ipecacuan'ha (Compound). Syn. Doveb's powdeb. Compound powdeb of IPECACUANHA WITH OPIUM ; PiaVlsi DoVEKI, Pulvis iPECACUANUiE cojiposiri's (U. P., Ph. L., E., & D.), L. ; PouDBE d'ipeoacuanha ET d'opium, Fr. Prep. 1. (B. P., Ph. L.) Ipccaeuanha and opium, of each, in fine pow- der, 1 dr.; sulphate of putassa, in fine powder, 1 oz. ; mix them (thoroughly). The Edin. and Dublin FurmuliB are similar. 2. (P. Cod.) Nitre and sulphate of potaasa, of each 4 oz. ; ipecacuanha, liquorice root, and hard extract of opium, of each 1 oz. This clo-ely resembles the original formula. 3. (Wholesale.) From powdered ipecacuanha and opium, of each 1 lb.; powdered sulphate of potassa, 8 lbs. Vaes, J(c. ' Dover's powder, is a powerful and valuable sudorific. — Dose, 5 to ] 5 or 20 gr., followed by warm diluents; in infiammatory ufleetions, rheumatisms, colds, &c. Powder, Itch. Syn. Pulvis antipsoeicus, L. Prep. 1. Sulphur and potato farina, of each J lb. ; essence of bergamot, i oz. ; mix. 2. (Poudre de Pihorel.) A mixture of finely pulverised sulphuret of calcium and farina, in nearly equal quantities. Used either as a dusting powder or mixed with a little oil or fat, and rubbed into the affected part. 3. (Fr. Hosp.) Flowers of sulphur, 1 oz. ; acetate of lead, 1 oz. Mix. 4. Equal parts of sulphur and charcoal. Powder of Jal'ap (Compound). Syn. Pul- vis jALAPi: C0MP0SITU3 (B. P., Ph, L., E., i D,), L. Prep. 1. (Ph. L.) Jalap, 3 oz. ; bitartrate of potassa, 6 oz. ; ginger, 2 dr. ; rub them separately into fine powder, then mix them. 2. (Ph. E.) As the last, omitting the ginger. 3. (Ph. D.) Jalap, 2 oz. ; bitartrate of potassa, 3.i oz. ; giUL'er, J oz. (all in fine pow- der) ; mix by careful trituration. — Dose, 20 to B7 1378 POWDER 60 gr. ; as a purgative in habitual costiveness, dropsies, &c. j also in worms, the tumid bellies of cliildren, &c. 4. (B. P.) Jalap, in powder, 5 ; acid tar- trate of potash, 9; ginger, in powder, 1 ; mix. —Dose, 20 to 60 gr. 5. (PnLVis LENiTivrrsj Sucee okanoe PtmoATiv.) From refined sugar, f lb. ; jalap and cream of tartar, of each 2 oz. ; oil of orange peel, i oz. A popular purgative on the Continent. — Dose, 1 to 3 dr. Powder, James's. Syn. Pultis Jacobi, P. PEBEiEUGUs Jacobi, L. The antimonial pow- der, or compound powder of antimony, of the Pharmacopoeias (see above) is the preparation which usually passes nuder this name; but the true James's powder is a nostrum the pretended secret of tlie preparation of which is claimed to be possessed by only two parties in the kingdom. The patent specification of the once celebrated Dr James runs as follows : — "Talfe of antimony, calcine it with a con- tinued protracted heat, in a tlat, unglazed earthen vessel, adding to it, from time to time, a sufficient quantity of any animal oil and salt, welldephlegmated ; then boil it in melted nitre for a oonsliterable time, and separate tlie pow- der from the iiiire by dissolving it in water." On this it bus been remarked that it yields a product totally different from that which Dr James and his successors have sold under the name, and he has hence been charged with con- cealing the real formula for his powder, and publishing a f.ilse one in its stead. According to Dr Robinson, the original formula for this nostrum, and that still adopted by the vendors of the proprietary article at tlie present day, is — Tartarised anti- mony, 1 pait; prepared burnt hartshorn and calx of antimony, of each 5 parts; carefully mixed together, and divided into 21- gr. pow- ders. (' Phil. Journ. Pliarm.,' vi, 282.) From analyses recently made of three speci- mens of James's powder ('Newberry's,' ' But- ler's,' and a sample of 60 years old obtained by Mr Si[uire), it appears that antimonious acid was pi'eseut in dilFerent proportions, from about 452 to SSj, the amount being greatest in the old specimen ; teroxide of antimony was also present to the extent of from 9{j to less than Ig, tlie greatest quantity being again in the old preparation ; the remainder in each specimen consisted chiefly of phosphate of lime; ni) trace of tartaric acid was discoverable in any of the samples. Perhaps no nobtrum ever received such ex- tensive patronage from the faculty as James's powder. Dr James himself was remarkably successful in its use ; but whether his success depended upon his powder or the mercurials and bark which he commonly employed at the same time is still undetermined. Powder of Kermes with Camphor. (Germ. Hosp.) Sun. Pultis keemetis cum cam- PHOai. JPie/p. Kermes mineral, 3 gr.; cam- phor, 6 gr. ; white sugar, 2 dr. ; mix. For 12 doses. Powder of Eermes with Ipecacuanha. (Fr. Hosp.) Sinn.), pulped through a sieve, made into --^ paste with wheateu flour and a little salt, and then rolled out into thin piecfs, and dried ; these are reduced to powder, sifted, and packed in well-corked bottles. Used to make sauce ; about 1 oz., to water, 1 pint. Other ehell-lish are treated in the siime way. Powder of Oxide of Zinc with Starch. (Caztnavo.) Syn. PcLVis ZINCI o-tTDi cum AUYLO, Prep. Starch, 1 oz. ; oxiile of zinc, 1 dr. ; camphor, io powder, 1 dr. For exco- riations iind bed-sores. Powder. Parturifacient. (E. Ph. 1741). Syn. PCLVIS AD PAUTUM. Prep. Borax, 4 dr.; castor, 1\ dr.; satlVon, IJ dr.; oil of cinniimon, 8 drops; oil of amber, 6 diop-*. Jlix.— Do*?, 20 to 30 gr. (This name, and aUo til it 01 PULVis PAETL'EIFACIENS, has been giiiMi to powdered ergot.) Powder, Pea. Syn. Pea flofe; Faeina PisoBU.\t, L. Prep. From peas, in the usual niiiiiner. Used to make extemporaneous pea- son p. Powder, Pearl. Prep. Prom pure pearl white uiul Flinch chalk (scraped fine by Dutch riislii's), ei|n;il parts ; triturated togetht-r, Some inak.rs add more Ficiirh chalk. U-od ai a skin cosmetii-. This mixture is pnfur- iihle Io |ii-arl wliite alone, Irom being more mihesive. Powder, Pease. Prep. From dried mint and sage, of each 4 oz. ; celery seed and white pepper, of each i oz.; turmeric powder, i oz. ; reduced to fine powder. Used as a condiment and kitchen spice. Powder, Peo'toral. See Powdee of Liquoe- ICE, &c. Powder of Phosphate of Lime, Saccharated. Syn. PULTIS CALCI8 PHOSPHATIS, BACCHA- EATU8. Prep. Precipitated phosphate of lime, 15 gr., white sugar, 85 gr. ; triturate and divide into 20 packets. Two or more pow- ders daily, according to age of child. In rickets. Powder, Piles. Syn. Pulvib antih.I'mob- EHOIDALIS, p. H«MOEEHOIDALIS, L. Prep. 1. (Fr. Hosp.) Precipitated sulphur, 3 oz. ; cream of tartar and black pepper, of each 1 oz. ; oil of cubebs, J dr. — Dose. A teaspoouf ul, in milk or honey, thrice a day. 2. (External.) — a. From Aleppo galls, in very fine powder, 2 oz. ; opium, in fine powder, 1 dr. A pinch to be applied occasionally. b. From sesquioxideof iron, 1 oz. ; powdered acetate (>f lead, \ dr. As the last. Powder of Pitch, Compound. .Syn. Pulvis PICIB COMFOSIIOS; DiSINEECTIKG POWDEE OP COENE AND Demaitx. 100 parts of plaster of Paris ai"e triturated thoroughly with 1 to 5 parts of coal tar. Used as an absorbent and disinfectant to fetid ulcers and wounds. Powder, Plate. Syn. Pdlvis peo aeoento, L. Prep. 1. Jeweller's rouge, J lb.; pre- pared chalk or levigated burnt hartshorn, J lb.; mix. 2. Levisinted putty powder, J lb.; burnt hartshorn, ^ ib. ; prepared chalk, 1 lb. ; rose pink, 1 oz. 3. (Meiictteial.) From quicksilver with chalk, 1 oz. ; prepared chalk, 11 oz. ; mix. Used to clean and polish plate. 8i-e Plate. Powder, Plate Boiling. Prep. From cream of tartar, common salt, and alum, equal parts. A little (if this jtowdcr, added to the water in which plate is boiled, gives to it a silvery whiti^iii s-^. Powder, Plummer's Al'terative. See Anti- mony, Etuiops of. Powder, Poultice. Syn. PuLVis peo cata- PLASMAIE (Ph. D. 1826), L. Prep. From linseed meal, 1 part; oatmeal, 2 parts; mixed togt'tber. Powder, Purgative and Anthelmintic. (Boerhaave). Hyi'. PULVis PUKGANS AN- THELMINTIOUS. Prep. Jala|i, 12 gr. (or agaiie, 8 gi.), Etliiups mineral, 12 gr.;.lbr one (lose. Powder of ftninine. Aerated, (Or Meireu). Syn. Pdlvis quixle aekatus. Prep. Tar- taric iicid, 15 gr. ; disulphate of qoiiiia, li gr. Jli.x, and add bicarbonate of soda, 18 gr. ; leliiied suirar. 30 gr. Mix for oue dose, between the fits of intermittent fever. Powder of Quinine and Tobacco. (Hug.) S(in. Put.VIS QUl.M.E SULPHATIS ET TABACI. Pr,p. DMilpliate of quinine, 12 gr. ; snuff, 1380 POWDER 1 oz. To be used as a snuff for nervous head- acheji. Powder, Rat. See Rats. Powder of Ehu'barb (Compound). Syn. Gkeooet's mixtcee, Ghegoby's powbek ; PiTLVia EHBi coMPOsiTDS (B. P., Ph. E. and D.) L. Prep. 1. (Pii. E.) Calcined mag- nesia, 1 lb. ; rhubarb, 4 oz. ; ginger, 2 oz. (all in fine powder) ; mix, and preserve it Irom the air. 2. (B. P., Ph. D.) Calcined magnesia, 6 oz. ; rhubiirb, 2 oz. ; ginger, 1 oz. 3. Calcined magnesia, 8 oz. ; rhubarb, 3 oz. ; chamomile, 2 oz. ; ginger, 1 oz. Obs. An excellent stomachic, antacid, and laxative. — Dose, 20 gr. to \ dr. Some drug- gists substitute tlie heavy carbonate for tlie uff8 (Medi- cutfd). Powder, Stahl's Sesolvent. S^n. Pultis BsaoiiVENS STAHLii. I'rep. Aiitimonial powder, nitre, prepared crabs' eyes, in equal part<. Powder of Starch with Soda. Si/n. Pultis AHVLI KT BODJS; DfcVEECHJi'e ALKALINK POW- DKB. Preji. .Mix 1 part of carboiinte of soda in fine powder with 10 of white starch. For cxtornal use in some skin diseases. Powder, Styp'tic. See Powdeb, Astbin- QENT, PaYNAKD'b P., &C. Powder, Tonquln. Si/n. Pultis antityssus TU.viituNENBis ; Sir (i. Cobd's tonquin POWDBE. Prep. Musk, II! gr. ; einiiabir, 48 gr. ; to be mixed or washed down with arrack or other spirit. Three doses to be givi'n on three alternate dii\ s, and three more on the thrcr next changes of the moon. Powder of Trag'acanth (Compound). Si/n. Pl'LVta TEAOACANTII.F. COMPOSITUS (U. P., Ph. L. & E), L. Prop. 1. (Ph. L.) Gum tragacanth, gum aciuia, and starch, of each, in line powiUi-, IJ oz. ; powdered white suifar, 3 uz. The Edinburi;h formula is similar. Demulcent.— i)ose, i dr. to 2 dr., in w.iter or any simple liquid; in hoarseness and ca- t.irrhs, comliined with squills and henb me, to allay irritation; in dysentery, combined with ipeciicuahna ; in gonorrhoea, strangury, ic, combined with scetale of potassa or nitre. 2. (U. P.) Tragacaiith, in powder, 1 ; gum Arabic, in powder, 1 ; starch, in powder, 1 ; refined sugar, in powder, 3 ; rub well together. — Cove, 10 to GO gr. Powder of Vanilla, with Sugar. (P. Cod.) ■V/». Pdltis tanilljj cnii saoohaeo; PotJDEK BE VANiLLE sucb£b. Vanilla is re- duced to piiwiltr by cutting it in pieces, and triturating it with 9 times its weight of refined sugar. Powder of Verdigris with Calomel. Si/n. PULVIS -KBrOIMS COM OALOMELANK. Prep. Prepared verdigris, 1 dr. ; ciilomel, 1 dr. ; mix. For extenuil use. Powder, Violet. St/n. Nuhseey powdee. Skin p. This is simply starch, reduced to a very fine pnwder. and scented with orris pow- der or esseuic of violets. The best kinds are also perfumed with a little musk or ambergris, and are now generally made with potato farina. The commoner sort is only scented with a little essence of bergamit or essence of lemon. ' Plain violet powder ' is, of course, unscented. Prep. 1. Powdered starch, 28 lbs. ; pow- dered orris root, 1 lb. ; essence of ambergris and essence of bergamot, of each i oz. ; oil of rhodium, i dr.; mix, and pass the powder through a sieve. 2. Powdered stanh, 14 lbs. ; essence of ber- gnmot, i oz. ; oil of cloves, i oz. ; as last. U-t. n.-d with strong vinegar. Useful for soft corns and warts. 2. (Hunter's.) From savins and verdigri-, eqinil psrts. See CoBN solvent. Powder, Warwick's (Earl of). Sr/n. Pultis CoMiTis Wauwicenois, L. Piep. From scamniony, pvep.ucd witli the fumes of sul- phur, 2 oz. ; diaphoretic antimony, 1 oz. ; cream of tartar, J oz. — Dofe, l.'j to HO gr. Obs. Tliis is a inodifieutiun of Cdunacbini's POWDEB. It is representc'l in tlie present I'liarmacopoeias by roMi'OUND sca.mmony FOVTDER. *' Cornachini wrote a whole book about his powder, the proportions of the in- gredients of whieli he varied according to circuiustsiiict"^." (* .Med. Lex.') Powder, Wash'ing. The numerous com- pounds vcntied under this name hnvc for their basis the soda-ash of coinmetce, blended with common Scotch soda in variable proportions. The best of them consist either wholly or chiefly of the first of these substances. The alkaline matter is reduced to coarse powder, antl stirred up with liquid size, or with a de- coction of lin-eeil, Iri>h moss, or British gum, and is then dried, and again crushed or pow- dered, and at once put into the packages, in which it is rannned tight, and covered up im- mediately. The object aimed at by the manu- facturer is to keep his commodity from the air as much as possible, because exposure renders it less cuustic, and consequently less detergent. Powder of Yellow Bladder-wrack. (Ph. D.) Syn. PuLvis QUEUcCs MAEIN^. Prep. Yellow bladder-wrack, in flower, is dried, cleansed, and heated in a crncible with a per- forated lid till vapours cease to be given oH', and the carbonaceous residue reduced to powder. — Dose, 10 gr. to 2 dr. POWDEES. The foUoning preparations have been placed under this head instead of under ' PowDEB,' because some are invariably spoken of in the plural number, and the others may be conveniently noticed in classes or groups. Powders, Aerated Sherbet (in one bottlb). 1382 POWDERS Double refined sugar, 144 "z-; P'wdert-d orange pee), 12 gr. j bicarbonate of soda, 3| oz. ; essence of cedrat, 12 drops ; oil of orange, peel, 60 drops; tartaric acid, 4 oz. The pow- ders must be carefully dried, mixed quickly, and afterwards kept dry, in a bottle securely corked. A measure holding nearly 3 dr. of the powder should accompany each bottle. Powders, Efferves'cing. Prep. 1. (Pui- VEKES EFFEBTBSCENTES — Ph. E.) Take of tartaric acid, 1 oz. ; bicarbonate of soda, 1 oz. 54 gr. (534 gr.), or bicarbonate of potassa, 1 oz. 2 dr. 40 gr. (640 gr.) ; reduce tiie acid and either bicarbonate separately to fine pow- der, divide each of these into 16 powders, and jireserve the acid and alkaline powders in separate pa pers of different colours. 2. (PtTLTEEES EEFEBVBSCENTES CITEATI — Ph. D.) Take of citric acid (crystallised), 9 dr.; bicarbonate of soda, 11 dr., or bicar- bonate of potassa, 13 dr., proceed as last, dividing each into 18 parts. 3. (PULVEEES EFFEKTESCENTES TAETAEI- ZATI — Ph. D.) Take of tartaric acid (in crys- tals), 10 dr. ; bicarbonate of soda, 11 dr., or bicarbonate of potassa, 13 dr. ; reduce them to powder, and divide them into 18 parts, as before. (See helow.) Powders, Effervescing, with Iron. (P. Cod.) Sl/n. PULTEEES EFFEttVESCENTES OtfM FEEEO. Prep. Tartaric acid, 2j oz. ; bicarbonate ol yndii, 2 oz. ; powdered sugar, 9 oz. ; dried sul- phate of iron, 46 gr. Mix the acid and the sulphate of iron (previously reduced to coar-se powder), add the sugar, and lastly the soda, not in very fine powder. All the ingredients must be very dry. Half an ounce of this powder is to be quickly added to 2 pints of pure water (without air) contained in a bottle, which is to be immediately corked. Powders for Gazogene. For 2 pints : — Pow- dered tartaric acid, 14 scruples; bicarbonate of soda, 17 scruples. For 3 pints : — Powdered tartaric acid, 17 scruples ; bicarbonate of soda, 21 scruples. For 5 pints: — One each change of 2 and 3 pints. Powders, Gin'ger Beer. Si/n,. Pulteeeb EFFEEVESCENTES CUM ZINGIBEEE, L. iVep. 1. Powdered white sugar, 1 to 2 dr.; bicar- bonate o£ soda, 26 gr. ; finest powdered Jamaica ginger, 6 gr. ; essence of lemon, 1 drop ; mix, and wrap it in blue paper. In the white paper put of powiered tartaric acid, 35 gr., or of powdered citric acid, 30 gr. 2. Finest Jamaica ginger, 1 dr. ; bicarbonate of soda, 5 dr. ; white sugar, 16 dr. ; essence of lemon, 6 Or 8 drops; mix, and divide it be- tween 12 papers (blue). For the white papers, divide tartaric acid, 6 dr., in the same way. By taking the drachms as ounces, the quantity will be sufficient for 8 dozen. For use dissolve one of each colour separately in somewhat less than half » glass of water, mix the two, and drink the mixture whilst effervescing. 3. (In one bottle.) — a. The sugar and the saline ingredients are separately dried by a very gentle heat, then mixed in a dry room with the ginger and essence of lemon, and at once put into bottles. b. By adding to the ' acidulated kali,' noticed at page 929, about l-16th of its weight of the finest powdered Jamaica ginger (i. e. \ dr. to each oz. ; 1 oz. to each lb.) at the time of mixing the ingredients together. A dessert- spoonful, thrown into a tumbler two thirds filled with cold water, produces an excellent glass of ginger beer. Powders, Ink. The article usually sold under this name is noticed under Ink. Another formula, which we have adopted with con- siderable success, is as follows : — Good black ink, 3 pints, lump sugar, li oz., and gum Arabic, \ oz., are put into a cleau iron pan, and evaporated by the heat of boiling water, with occasional stirring, to dryness; the dried mass is reduced to powder, and divided into 12 parts, which are enveloped in either tin- foil or glazed paper, and kept dry. One of these papers dissolved in \ pint of hot water forms that quantity of excellent black ink, without sediment, and which answers well with the copying press. Powders, Lem'onade. Syn. Lemon shee- BET ; LiMONADnM SICCTTM, PtJLVIS PEO LIMINADO, L. Prep. 1. Powdered citric or tartaric acid, 12 gr. ; powdered white sugar, J oz. ; essence of lemun, 1 drop (or a little of the yelli>w peel of a lemon rubbed off on a piece of sugar) ; mix. For one glass. 2. White sugar, 4 lbs. ; citric or tartaric acid, li oz. ; essence of lemon, i oz. ; mix well, and preserve it in a bottle for use. 1 to 2 dessert-spoonfuls make a glass of lemonade. It is also put up in papers containing about 2i dr. each. 3. (Effeevescing.) — a. For the blue papers, take of powdered white sugar, 1 lb. ; bicarbonate of soda, ^ lb. ; essence of lemon, la dr.; mix, and divide it between 6 dozen papers. Next divide tartaric or citric acid, 5 oz., between 6 dozen white papers. Or the two may be kept in bulk, iu separate bottles. I. (In one bottle.) As ' aciduiated kali." Some makers slightly increase the quanti- ties of acid and essence of lemon there ordered. Powders, Orangeade. Syn. Aeeatedshee- BET. Prep. Powdered sugar, 14^ oz. ; pow- dered orange peel, 12 gr. ; oil of orange peel, 60 drops ; essence of cedrat, 12 drops ; bicar- bonate of soda, 3i oz. ; mix, and put 145 gr. in each blue paper. In the white paper put 32 gr. of tartaric acid (or 30 gr. of citric acid). Or the alkaline and acid powders may be put into separate bottles, with a measure holding the proper proportions of each. The orange peel may be omitted, if necessary. Powders, Pol'ishing. Frep. 1. (For brass and copper.) — a." From rotten stoue, 8 oz. ; powdered soap, 1 oz. POWDERS 1383 i. From rotten stone, 7 oz. ; powdered oxalic iicid, 1 oz. Until are used with a little water. See Bbass FA8TB. 2. (For pfilil.) Jeweller's rouge. See Ses- QtTIOXIDE OP I 111 IN. 8. (For ivory.) Pumice stone and putty powder. 4. (For plate.) See Plate and Powdeb, 1'latb. 6. (For silver.) As the last. Powders, Scented. Prep. 1. Cosmetic rowDEBS. — a. (PoCDEEDK CHIPBE.) .Macerate oiilt moss in running water for 2 or 3 days, then dry and powder it. Used as a basis for other powders, on account of its being higlily retentive of odours. Reindeer moss and ragged hoary evernia are also used for the same pur- pose. See Cypbus powdeb (above). b. (POUDKB DE OHIPEE DE MONTPEMF.tt.) From poudre de chipre 2 lbs.; musk, 30 gr. ; civet, 20 nr. (the last two powdered by means of a little sugar) ; cloves, i oz. e. (POUDEK DE FLEUR3 D'OEAHaES.) From starch or Cyprus powder, 25 lbs. ; orange flowers, 1 lb. ; mixed in a covered chest, and stirred twice or tlirice daily; the process being repented, witii fresh flowers, a second and a third time. Or, the plain powder is Bi'ented by the addition of » little neroli or essence of petit 1,'riiin. d. (PouDBE DE PEANOIPANNI.) From pou- dre (If fleurs d'urunges and poudre de chipre, of each 6 Ib-s. ; essence of ambergris, 1 oz. ; civpt (powdered with sugar), i dr. Ash-grey colour. s, and calamus aromaticus, of each 4 oz. ; la- vender flowers, 8 oz. ; rhodium wood, 1 dr. ; musk, 20 gr. c. From corianders, nrri", calamus aromati- cus, and red roses (dried), of eai-h 1 oz. ; lavender flowers, 2 oz. ; mace and cloves, of each 1 dr. ; essential oil of almonds, 10 drops. d. As last, but substituting inu^k, 5 gr., for the oil I if almonds. e. From patchouli, 8 oz. ; lavender flowers, (lightly dried), 3 oz. ; orris root, 2 oz. ; cloves, 1 oz. ; essence of berfraraot, 1 dr. ; essences of ambergris and musk, of each ) dr. The.se are used, along with cotton wool, to fill scent bags, cassolettes, &c. ; and as scent pow- der for boxes, drawers, and the like. The scent is added to the dry ingredients, separately reduced to powder, and the whole is then passed through a fine sieve, to ensure perfect admixture. 3. Paefum poue lbs autees poudbbs. From poudre d'amlirette, 12 lbs.; civeitc, IJ oz.; musk, 1 dr. ; reduce the last two to powder by grinding them with some dry lump sugar, then mix the whole together, and pass it through a sieve. Used to perfume hair powder, sachet.s, &c. Powders, Seidlitz. Syn. Pui.veees effee- tescentes apeeientks, L. Prep. 1. Potas- sio-tartrate of soda (Rochelle salt), 2 dr ; bi- carbonate of soda, 40 gr. ; mix, and put it in a blue paper; tartaric acid, 35 gr. ; to be put in a white paper. For about i pint of water. Laxative. 2. (In one bottle.) From potassio-tartrate of soda, 12 oz. ; bicarbonate of do., 4 oz. ; tar- taric acid, 3J oz. ; white sugar, 1 lb. (all in fine powder) ; dry each separately by a gentle heat, add of essence of lemon, \ dr. ; mix well, pass the mixture through a sieve, and put it at once into clean dry bottles. — Dose. A des- sertspoonful, or more, to a tumblerful of water. Obs. The above mixtures, though now nni- versally sold as Seidlitz powder, do not, when dissolved, exactly resemble the natural water, which contains carbonates, sulphates, and. chlorides of calcium and magnesium. How- ever, the factitious article is equally effective,^ and much more agreeable. Powders, Sher'bet. These are made of the same materials as lemonade powders, the fla- vouring ingredient being varied to suit the particular case. Powders, So'ii a- water. Syn. Effeevescino 1384 POWDERS POWDEEB, E. SALINE P., SODAIO P., AbBATED BOSA P.; PDIiVEKES EFIfEETESCBNTES, L. Prep. 1. From bicarbonate of eod«, 30 gr. in each blue paper ; tartaric acid, 25 gr. (or citric acid, 24 gr.), in each white paper. One of each is dissolved separately in about half a glassful of water, and the two solutions mixed, and drank immediately. A cooling, wholesome summer bevernge, but it should not be indulged in to excess. 2. (Chalybeated.) By adding 1 gr. of dried, protosulphate of iron to each paper of acid. Tonic. 3. (Midgeley's.) Made by adding ^ gr. of tartarised aiitimony to each paper of acid. Refrigerant and diaphoretic. J?or the Ph. formulae see Powdebs, Effervescing (above). Powders, Soup. See Powdee, Cueey, I'ow- DEE, Pea, Spioe, &c. Powders, Spruce Beer. Si/n. Pdlveees ef- FEKVESCENTES CUM ABIETE, L. I'rep. As ginger-beer powders, but substituting essence of spruce, 3 to 6 drops, for the powdered ginger. Powders, Tooth. Si/n. Pultis deniifeicii, L. The general principles which sliould be kept in view in the selection of the materials, and in the preparation of dentifrices, have been already fully noticed undi-r Dentifeices, and need not, therefore, be repeated here. Care must be taken that all the dry ingredients be finely pulverised, and that, the harder and gritty ones be reduced to tiie state of an im- palpable powder, either by levigation or elu- triation. The mixtui'e of the ingredients must also be complete. This is the most readily effected by stirring tliem well together until they form an apparently homogeneous powder, and then passing this powder through a very fine sieve. Those which contain volatile sub- stances should be preserved in closely toiked wide-mouth bottles, and those which contain acidulous or gritty matter should not be frequently employed. The selection of the tooth brush likewise deserves attention. It should be sufiiciently stiff to eff'ect its purpose completely ; but, at the same time, it should be so formed as not to cause irritation or injury to the gums during its use. Frep. 1. Cuttle-fish bone and prepared chalk, of each 2 oz. ; oil of cloves, 20 drops. This may be perfumed at will, and medicated by any of the substances referred to under Den- tifrices. 2. To the last add of powdered Castile soap, 2 oz. 3. Prepared chalk, 12 oz. ; cuttle-fish bone, 8 oz. ; orris root, 4 oz. ; dragon's blood, 1^ oz. j oils of cloves and cassia, of each i dr. 4. Prepared chalk, 1 lb. ; pumice-stone, in impalpable powder, i lb. ; orris root, 2 oz. ; pure rouge, J oz. ; neroli, i dr. 5. Yellow cinchona bark and myrrh, of each i oz. ; recently burnt charcoal, 3 oz. ; cloves, 1 dr. 6. Pumice-stone, red coral, and powdered rhatany root, of each, 2 oz. ; orris root, J oz. ; essence of vanilla, i dr. 7. (Aeomatic tooth powder.) From cut- tle-fish bone, 4 oz. ; calamus aromaticus, 2 oz. ; powdered Castile soap, 1 oz. ; oil of cloves, idr. 8. (Asiatic dentifeioe.) From prepared red coral. Si lbs. ; Venetian red, f lb. ; pre- pared challi and pumice-stone, of each li lb.; China mask, 30 gr. 9. (Cadet's.) From lump sugar and charcoal, of each 1 oz. ; Peruvian bark, ^oz. ; cream of tartar, i oz. ; cinnamon, ^ dr. 10. ^Camphorated.) See Camphoeated CHALK. 11. (Chaeooal DENTIFEICB.) From char- coal, prelerably that from the willow or the areka nut, either alone or combined with twice its weight of prepared chalk. Scent or medi- cinals injure it. (See 9, 19, and 26.) 12. (CoEAL DENTIFEICB.) See 16, 23, and 25 [heloio), 13. (Deschamp's alkaline dentifeioe.) From powdered tale, 4 oz.; bicarbonate of soda, 1 oz. ; carmine, 6 gr. ; oil of mint, 12 or 15 drops. 14. (Ploeentine dentifeioe.) Fi-om pre- pared shells, 4 oz. ; orris root, li oz. ; bitar- trate of potassa, f oz. ; Florentine lake, q. s. to colour. 15. (Galvanic dentifrice.) From gold, 3 leaves ; silver, 4 leaves ; triturate them with alum and sulphate of potassa, of each \\ dr. ; then add, of dry common salt, pellitory of Spain, and Peruvian bark, of each 1 dr.; prepared hartshorn, 1 oz.; mi.t, and either colour it blue with smalts or red with lake. A useless com- pound. 16. (Grosvenor's.) Prom red coral, 3 lbs.; prepared oyster-shells, 2^ lbs. ; orris powder, i lb. ; oil of rhodium, 25 drops. Rose-pink is now commonly substituted for the coral. 17. (Hemet's.) From cuttle-fish bone, 6 oz.; cream of tartar, 1 oz. ; orris root, i oz. 18. (' Lancet.') Red bark and Armenian bole, of each 1 oz. ; powdered cinnamon and bicarbonate of soda, of each \ oz. ; oil of cinnamon, 2 or 3 drops. 19. (Lardner's.) From charcoal, in very fine powder, 1 oz. ; prepared chalk, 3 oz. ; mix. 20. (Mialhe's eational dentifeicb.) From sugar of u.ilk, 3 oz. ; pure tannin, 3 dr.; red lake, 1 dr. ; oils of mint and aniseed, of each 7 or 8 drops ; neroli, 4 or 5 drops. 21. (Mtkeii dentifrice.) From cuttle-fish bone, 6 oz. ; myrrh and orris root, of each 2 oz. 22. Peael dentifeioe.) From heavy car- bonate of magnesia or precipitated chalk, 1 lb.; finest smalts, 3 dr.; essence de petit grain, i dr. 23. (Pelletier's quinine dentifeioe.) I'rom prepared red coral, 3 oz. ; myrrh, 1 dr. ; disul- phate of quinine, 12 to 15 gr. 24. (Ph.Russ.) Cinchona b irk, 4 oz. ; orris root, 2oz. ; catechu and myrrh, of each 1^ oz.; sal ammoniac, 1 oz. j oil of cloves, 20 drops. 25. (PonDEE DENTIFEICB — P. Cod.) Red POX 1385 rorni, red bole, nud cuttle-flah bone, of each 3 ni. ; dragon's blood, 1^ 07„ ; cinnnmon, } oz. ; coi-liineal, 3 dr. ; cloves, 1 dr. ; bitiirtrate of potassa, 4i oz. ; reduce them Beparntely to very tine powder U'lore mixing tboin. This is the ' coral dentifrice ' of the French. 26. (Uifinini's.) From charcoal, 1 oz. ; yel- low baric, i oz. 27. (Rose UENTiFKiCE.) From precipitated chalk, Goz.; cuttle-K>h bone, 3 oz. ; bicarbo- nate of soda, li uz. ; red lake, i oz. ; otto of rosHii, 2<) drops. 'M. (Uuspini's.) From cuttle-fish bone, 8 oz.; Roinim aliiiij and orris root, of each 1 oz. ; cream ot till t.ir, :i oz. ; oil of rhodium, 6 or 8 drops. 211. (Violet tooth powdeb.) From orris root, 3 oz. ; cuttle-fish bone and rose pink, of eiich 6 oz. ; precipitated chalk, 12 oz. ; pure indigo, q. s. to give it a pale violet tinge. 30. (Zieter's.) From finely powdered cal- cined hartshorn and cuttle-fish bone, of each 6oz. ; calaniusaromaticus, cassia, and pellitory of Spain, of each 1 oz. ; essence of vanilla, 1 dr. ; essence of ambergris, 10 or 12 drops. 31. Chalk, carbonate of magnesia, and pale bark, of each 1 oz. ; oil of peppermint, 5 drops. 32. Creiira of tartar, sugar of milk, of ciicli 2 oz. ; carmine, 88 gr. (all in very subtle pow- der) ; oil of peppcnuint, 4 drops. Powders, Worm. Si/n. Pdlveres anthkl- MiNTlci,RvBKMiFnGi,L. Prep. 1. (Bouchar- dat.) Powdered Cursican moss and worm-seed, of each 5dr. J calomel, 40 pr.; rub tliem together. 2. (Collier.) From powdered jalap and seammoiiy, of each 1 dr. ; creain of tartar, 2 dr. ; Ethiops minenil, 3 dr. 3. ((luibuurt.) Sulphate of iron, 1 dr. ; tansy, 2 dr. j worm-seed, 3 dr. 4. (!'. Cod.) Cinsicaii moss and worm seed, of eadt 2 oz. ; rhubarb, 1 oz. ; rubbed to a hue powder, and innlidly mixed. POX. A corruption of a Saxon word, ori- ginally applied to pustules or eruptions of auy kind, but now restricted to varicella, variola, vaccinia, and, in its unqualified form, to syphilis. {Sec below.) Pox, Chick'en. Sm. Water- pox ; Vam- CELLA, L. All eruptive disease, consisting of smooth, semi-transparent vesicles, of varous sizes, which aftiTHiirds become white and stiaw-coloured, and about the fourth da\ break and scale off, without leaviiig any per- manent mark behind them. In hot weather the discharge sometimes becomes purulent, and iit others the eruption is attended wiih con- siderable fever. Sometimes the vesicles assume a pointed form, and the fluid remains clear throughout the disease; it is then frequently called the "swine-pox." When the vesicles lire l:irrr<. and globular, and their contents, at first "hoy-coloured, alterwards turn yellow, it is popularly known iis ' hives.' The treatment of chiekeu-pox consists in the adoption of a light, vegetable diet, and in the adniinirtration of mild saline aperients and cooling drinks. The chicken-pox, except in children of a very bad habit of body, is an extremely mild dis- ease. Like the smallpox, it rarely attacks the same person more than once during life. Pox, Cow. Syn. Vaccinia, Vaeiola vac- cina, L. This disease was proposed as a substitute and a preventive of smallpox by Dr Jenner in 1798, and its artificial produc- tion (vaccination) has rendered smallpox a comparatively rare disease in Britain. There appears no reason to doubt that the preten- sions of the advocates of vaccination have heeu fully justified by the experience of more than half a century ; or that this disea-e, when actively developed, evinced by the complete- ness and maturation of the pustules, acts as a prophylactic of smallpox. The process of vaccination is similar to that of inoculation for smallpox. Tne point of a lance is wetted with the matter taken from one of the pustules, aud is then gently inserted under the cuticle, and the scratcn afterwards rubbed over with the same. Ha- morrhage should be avoided, as the blood is upt to wash away the virus, or to form a cake which shields the living tissue from its action. Pox, Small. Syn. Vaeiola, L. This dis- ease comes on with the usmil symptoms of in- flammatory fever. About the third day red spots, resembling flea-bites, make their np- pearance on the face aud head, and gradually extend over the whole body. About the fifth day small circular vesicles, depie>sed in tlio centre, surrounded by an areola, and contain- ing a colourless fluid, begin to form, when the feverish symptoms abate ; about the sixth day the throat becomes sore ; about the eighth day the face is swollen ; and about the eleventh day the pustules acquire the size of a pea, and cease to eidarge, the matter which they con- tiiin becomes opaque and yellow, a d:iik eelitml spot forms on each, the swelling of the faeo subsides, and secondary symptoms of fever come on ; the pustules become rough, break, and scab over, and a dark spot remains for some days, often followed by permanent inden- tations, popularly known a-. ' pock-marks.' At the end of the sixteenth or eighteenth day the symptoms usually disappear. In the con- fluent smallpox, a severer form of the di». ease, the pustules coalesce, the eruption Is irre- gular in its progress, and the Inflaiumati-'ry symptoms are more severe. The treatment of ordinary cases of smallpox resembles, for the most part, that mentioned above for chicken-pox. As soon as the fe- brile symptoms become marked the patient should not be suffered to lie in a hot bed, but on a mattress, in a cool and well-ventilated apartment, and antiseptic cooling drinks should be freely administered. When convuWons occur, or great irritability exists, small doses of morphine, opium, or camphor may be ad- ministered, and obstinate vomitiiiL' arrested by effervescing saline draughts. When the skin is pale and cold, the pulse weak, and the erup- 1386 PRECIPITATE— PRESCRIBING tiou lauguidly developed, the warm or tepid bath is often serviceable. An infusion of the rootof Sarraeenia pupurea, an American plant, has been strongly recommended as a preven- tive and cuie of smallpox, but many of our most eminent physicians regard it as valueless. The application on the third day of a mask formed of thin muslin, covered with mercurial ointment, and having holes cut in it for the nostrils, eyes, and moutli, will effectually pre- vent ' pitting.' (Dr. Stewardson.) With the same intention some persons recommend the puncture of the pustules as soon as they are raature. A solution of india rubber in chloro- form is now olten painted over the face when the eruption has become fully develojied. The chloroform quickly evaporates, leaving an elas- tic film of india rubber, which almost entirely removes the itchiness of the pustules and prevents ' pitting.' To remove the pock- marks, whether recent or old, nothing appears to be better than warm sea-bathing, or the use of tepid iodiiretted lotions. The smallpox is eminently contagious, but only attacks the same person once during life. Formerly, a milder form of the disease was propagated by inoculation, a practice intro- duced into England from Turkey by Lady Mary Wortley Montague, about the year 1721. At the present day, in England, inoculation, as well as the exposure of a patient labouring under smallpox, is penal, the punishment being either by tine or imprisonment. See Pox, Cow {above). " The absolute necessity for enforcing this measure after smallpox is conclusively shown by the following cases which occurred during the late severe outbreak of the disease at Ipswich. In the first instance a young man brought a bundle of infected linen with him irom London and had it washed at Ipswich. Twelve days after, the servant who washed it showed symptoms of smallpox. In another case, a woman who had been at Highgate Hos- pital brought with her a shawl which she had worn during convalescence, but had not been disinfected ; and in fourteen days her sister, who washed the shawl, was attacked with smallpox." — Sanitary Record, PRECIPITATE. Any substance which has separated from its solution in a solid and, usually, a pulverulent or flocculentform. The substance by which such a change is produced is called the * precipitant; ' and the act or operation by which it is effected is called ' precipitation.' The old chemists gave this name to several compounds. Red precipitate, or precipitate per se, is the red oxide of mer- cury prepared by heat. White precipitate is the Ammoniated merctjey of the B. P. PEECIPITA'TION. The formation or sub- sidence of a precipitate. (See above.) When the precipitate is the chief object of the pro- cess, it is necessary to wash it, after it is sepa- rated, by filtration. This operation requires little attention when the substance thrown C^-^ down is insoluble in water; but when it is in some degree soluble in that liquid, great attention is required to prevent the loss which might result from the use of too much water. Precipi- issisSi ^ tales soluble in water, ^^P' W but insoluble in al- ?» Q ^ cohol, are frequently, on the small scale, washed with spirit more or less concentrated. The best precipitating vessel is a very tall glass jar, furnished with a lip and spout, and narrower at the bottom than at the month, so that the precipitate may readily collect by subsidence, and the supernatant liquor be decanted off with more ease. PEEGITAHCT. For the preservation of the health, and the prevention of the numerous discomforts and dangers which so frequently attend this condition, nothing is so effective as exercise. It is this that is so favorable to the humble peasant, and it is its absence that inflicts such calamities on the wealthier classes. Exercise, moderate and unfatiguing, when assisted by regular habits, and a diet nutri- tious, but not too liberal, is, indeed, capable of not only affording pleasure and increasing the comforts of existence, but is also generally sufficient to greatly lessen the severity of the sufferings, and to ward off the not unf requently fatal results which terminate this interesting condition. The sickness of pregnancy may be greatly ameliorated, if not removed, by the occasional use of a saline aperient, and by effervescing draughts formed with the bicarbonate of po- tassa and citric acid. The oxalate of cerium is strongly recommended by Professor Simpson, of Edinburgh, as a remedy for obstinate vomit- ing in pregnancy. — Dose, 1 gr. to 2 gr. three times a day in pills. PEESCEI"BING (Art of). Besides a know- ledge of diseases and their treatment, much of the success of the physician depends on cir- cumstances connected with the form in which the remedies are exhibited. In writing a pre- scription it is necessary to consider the age, sex, temperament, habits and idiosyncracy of the patient, as well as the conditions of climate and season, before the selection of tlic leading medicament and the apportioning of the dose. The most convenient form of exhibiting it, whether it should be given alone or in some simple form, or combined with other ingre- dients, the compatibility nf the latter, and how far these are likely to assist, impede, or modify its operation, must also receive the con>ideration of the practitioner. Without a careful attention to all these circumstances the most valuable remedies may be rendered worthless, and the highest medical skill and the best intentions frustrated. A prescription generally contains several PRESCRIPTIONS— PRESSURE 1387 mcdicinnl substances, Hliich arc diatinguislied bv medical writers by names indicative of the otBce wliieh each of them performs. These lire — 1. The DA8ia, which is the principal or nicist sctive ingredient; — 2. The adjuvant, or that which is intended t5 promote the anion of the base; — 3. The oonnECTiVE, in- tended to correct, modify, or control its action, or to cover its odour or taste, as when we add carininiitives or diaphoretics to cathartics, or aromatics or liquorice to nauseous substancei; ; — 4. The EXCIPIBNT, or that which gives the whole a commodious or agreeable form, and which, consc(|uently, gives the prescription its peculiar character, as that of draught, mix- ture, pills, &c. To these, certain Continental writers add a 5th, the INTBEMEDim, which is the sabstance employed to unite remedies which are not, by themselves, miscilile witli each other, or with the exoipient. Of this character are the yolk of egg and muuilage, employed in the preparation of emulsions. The medicinal substances, with the quan- titie< to bo taken, generally arranged as above, are said to form the ' inscription,' — the di- rections as to their combination or dispensing, which usiiiilly comes next, the ' subscription,' and — the orders for the exhibition of the com- pound medicine, which follow these, the ' in- structions.' These distinctions are, however, in many cases more technical than useful. In clioosing tlie form of a prescription it should be recollected that solutions and emul- sions generally act with more certuiuty and rapidity than powders diffused through water; iind these, again, than the semi-solid and solid ~ firms of medicine, represented by electuaries, boluses, and pills. On these matters, how- ever, the taste and wishes of the patient should not bo disregarded. Foi* this purpose the taste of .nauseous medicines should bo dis- guised as much as possible by tlie judicious seketion of an appropriate corrective or ex- cipient. Thus, the disagreeable Havnur of Epsom salt may be in a great measure covered by dissolving it in peppermint water ; that of aloes by liquorice; that of castor oil and copaiba by orange peel ; and that of powdered bark by mixing it with milk immediately before ttking it; whilst the bitterness of all bitter substMueesis concealed by strong cott'ee. In order that a prescription may be well made it is not necessary to unite all the ele- ments above referred to. The basis and the excipicnt are the only two which are abso- lutely necessary, since there are many medi- cines which have no need of an adjuvant. The agreeable flavour and odour of some, and the mild and harmless nature of others, often render the intervention of a corrigent unne- cessary when they are employed. A single substance may also " be capable of answering two or more purposes. Thus, the adjuvant may also act as a corrigent, as when the addi- tion of soap to aloes, or to extract of jiilap, lessens their griping properties, and ut the same time promotes their action. In the same way neutral salts correct the colic which follows the use of resinous purgatives, and acce- lerate their action." According to Gaubins, the number of ingredients in a prescription should scarcely ever exceed three or lour. See Dose, Medicises. Incompatiblks, Pills, &c. PEESCRIP'TIONS. Recipes or formula; for the preparation and exhibition of mcdieines intended, generally, for immediate use. See Prescribino (above). PSESEBVES'. A general term, under which are included the various fruits and vegetables which are seasoned and kept in sugar or syrup, more especially those which are so preserved whole or in slices. See Candtiho, Jam. Makmalade, &c. PRESS (Correcting for the). See Pboopb. PRESSURE, BAROMETRIC, on the Phe- nomena of Life. M. Bert has contributed to the 'Comptes Rendns '' (Ixxiii, 213, 503 ; Ixxiv, fil7; Ixxv, 29, t>s) an account of the following experimental researches on the in- fluence of changes in the Barouietric I'ressnre on the Phenomena of Life : — He finds that at pressures under 18 centi- metres of mercury animals die from want of oxygen ; at a pressure of one to two atmo- spheres, from want of oxygen and presence of carbonic acid ; at 2 — G atmospheres, from the presence of caibonic acid alone; at 6 — 15 atmospheres, from the presence of carbonic acid and of excess of oxygen; and at l.> — 23 atmospheres, from the poisonous action of o.xygen alone. Animals die from want of oxygen when the amount contained in their arterial blood is not suflicient to balance a pressure of 3 5 per cent, of oxygen in the atmosphere. They die from poisoning by carbonic anhydride when the amount contained in their venous blood is sufficient to balance a pressure of 26 to 28 per cent, of carbonic anhydride in the atmospliero in the case of fparrows, of 2H to 30 Iit mam- mals, and of 15 or 16 for reptiles. As the pressure of oxygen in the .-nrround- ing air depends on two factors, the percentiige proportion and the barometric pressure, the barometric pressure may be reduced to 6 cen- timetres for sparrows, if the proportion of oxygen in the air is increased ; and it may be raised to 23 atmospheres without causing death, if the proportion of oxygen is reduced by mixing the air with nitrogen. Aeronauts niiglit, therefore, ascend higher than it has hitiierto been possible to do by taking with them a bag of oxygen to inhale ; and the danger tliat threatens divers of being poisoned by the oxygen in the compressed air might be averted by using a mixture of air and nitrogen. From an examination of the gases in the blood of animals confined in rarefied air the author finds that both the oxygen and the car- bonic anhydride in the, blood diminish. The dyspucca which is felt in ascending mountains 1 'JoumHl Cliemual ^uclcty,' vol. xxv. 1388 PRINCE'S METAL— PRINTING is therefore dae to v/ant of oxygen in tlie blood. The dimiuutiou in oxygen becomes diminished at 20 centimetres pressure, yet this is the pressure under which the inhabi- tants of tlie elevated Mexican plateau of Anahuiic live. The oxygen diminishes more quickly and more regularly than the carbonic anhydride. Although there are but very small quantities of gases simply dissolved in the blood, the chemical combinations in which they take part are dissociated very easily and in a progressive manner under the influence of diminished pressure, and this dissociation takes place more easily in the organisms than in experiments in vacuo. PRmCE'S METAL. One of the names for Dutch giild. (See Gold, UniOH.) PRINT'mCr (Anastatic). A method of zincography, patented in 1815, having for its object the reproduction of drawings, engrav- ings, and letter-press, from copies howe^'er old. To describe briefly the preparation of a plate or cylinder, let us suppose a newspaper about to be reprinted by this means. The sheet is first moistened with dilute acid and placed between sheets of blotting paper, in order that the superfluous moisture may be absorbed. The ink resists the acid, which attacks the blanks only. In all cases where the letter-press is of recent date, or not per- liaps older than half a year, a few minutes suf- fice for this purpose. The paper is then care- fully placed upon tlie plate with which the letter-press to be transferred is in immediate contact, and the whole passed under a press, un removal from which, and on carefully dis- engaging the paper, the letters are found in reverse on the plate. A preparation of gum is then applied to the plate by means of a roller, after which the letters receive an addi- tion of ink, which is immedialely incorporated with that by which they are already tormed. These operations are effected in a few minutes. The surface of the plate round tlie letters is next bitten in a very slight degree by dilute acid, and on the fresh application of the ink it is rejected by the ziuc, and received only by the letters, which are charged with the ink by the common roller used in hand-pririting. Each letter conies from the press as clear as if it had been imprinted by type n;etal; and the copies are fac-similes, which cannot easily be distinguished from the original sheet. When pen-and-ink drawings are to be repro- duced, tbey are made on any paper free from hairs or filaments, and well-sized. The ink used is a preparation made for the purpose, closely resembling lithographic ink, and may be mixed to any degree of thickness in pure distilled water. It should be used fresh, and slightly warm when a fine effect is to be given. In making or copying a design a pencil may be used; but the marks must be left on the paper, and by no means rubbed with India rubber or bread. It is necessary to add that the paper should be kept quite clean and free from friction, and should not be touched by the fingers, inasmuch as it will retain marks of very slight touches. Before closing this notice of anastatic print- ing it may be proper to remark, that the great pretensions originally set up by the patentees have not been fulfilled by its extensive adop- tion in trade. PKINXING (LetterpreBs).' Syn. Ttpo- OKAPHY. The art of collecting together and arranging movable types for the purpose of printing, in one or more colours, by pressure applied from a flat surface or by means of a cylinder biting the paper to be printed, and which is inserted between itself and the type. In illustration of this sectiop, some specimen types are appended, the greater portion being from the well-known foundry of Messrs V. & J. Figgins, and should now be carefully read down to render the further remarks Intelligible. The key is contained in itself by reading the column as one continuous paragraph with the helpof the foot-notes. Some idea may thus be formed of the vast number of distinct kinds of type necessary to carry out the requirements of the present system of printing. Mention there has been made that the name of the body is determined by its number ot lines to a foot; but this must be qualified. The Imperial foot, or inch, or yard, is an arbitrary measure of length in reality as well as in name. When one foundry was sufficient to supply all the types that were required for use in the early ages of printing, then a nai e and its dimensions could be taken as absolute. But with the increase of printing, type-found- ers also increased; and this has produced the variations of bodies which are so annoying tn the typographer, for one single letter or space taken from a' body larger than its own, yet of the same name, will be enough to throw the column of type out of a straight line all the way through. Still, when we look to the fact that, according to the ancient masters, the large-sized type called Pica (No. 3 and Nos. 18, 19, 20 & 21) requires 72J lines to the foot, and that Nonpareil, half its size (No. 9, and Nos. 26, 27, 28 & 29), requires 145 lines to the foot, and recollecting that the slightest varia- tion multiplied 145 times must produce a very sensible deviation, the wonder is that each of the founders should approach each other so closely as they do. An attempt was made some years ago to introduce a certain fixity of stand:ird for each body throughout the trade, based on the French system ; the difficulties of altering the standards and matrices of each foundry were seen to be so great that the effort was unavailing. . Daring the latter half of the present century there has been a growing disposition to return to the cut of the letters as used by the early printers. To meet this desire, nearly all the type-founders have introduced Old-stjie faces, I The Editor is mucli indebted to Mr J. E. Adlard for this interesting article. PRINTING 1389 The ordinary printing^ types are technically known" as Book Founts — those more' especially adapted for newspapers* are styled Nrw.s Founts. Each fount* is divided into two distinct portions — the" roiiiuti or upright letters forming one part,' and the italic, or sloping, the other. There is,' moreover, an addition of shall capitals to the roman' Bootion of the typo-founders' bill for a complete fount ofi" a parttcnlar weight. Tlie lieifflit of a typo is ratlier more n than T'» at ku Inch, thua givlog deptli at tbo aicfef for luckiag-uf the U l^^onsi^^rufion tfpea. Tbe Kmal1e*t fount cut t* /& tke. J^ai7LencLc±iLtLe.- 14 Ki ^PtinttnQ;C|)ptsare lctj)iucal(]j nanub accorliing to/^ first, the BODY, that is,^^ how many lines, when'' order, will make, by Measurement, the length of a^^ FOOT. HAVING NOW DETERMINED^^ THE NAME OF THE BODY, -^ The SPECIAL. CUT, or" 1F/S\(glj D§ A©©!© TTG^lK^lTOj " thus completing ttae ITAIWi: by wbicb 26 Type-Fouaders and lypographers recognise " EACH DISTmCTIVE SIZE AHD «» STYLE OF THE MANV-VARIED TVPES USED IN THE Frodufltion of that luxury which has now beoome an ^ APPARENT NECESSITY OF THE AGE— PRINTING. RcfcrencCB to the above types — by rCHcIing HCross. BODT. BOOKWORK FACE. DISPLAY FACE. 1 Great Primer — llDUum ^* Gt. Primer Manuscript 15 „ JUxt. Onmniented 18 „ Black * English— Komnn 17 „ Condensed Black > Pica- Kuniuu 18 Pica Antique 18 „ Clarendoa 20 „ Rustic * Small Pica— Rnmau *i „ Narrow Gauge * \m\% Primer- - Rom 11 n ** Long Primer rCondensed LSanastril' • Bourgeois— Huniiin ? Brevier- Aomtin ^3 Brevier Grotesque « „ Extended ■ Minion— Rom & Italic " „ Open Sansaerif " Nonpareil Egyptian • iNonpiireil — Roman "7 „ Hair line -« „ Oriiamentrd '-^ „ Coudenaed Gro- w Rubv— R'tninn tesque " P.»rl- Human 30 Pearl Clarendon '* Diamond — Horn. in 81 Diiimoud Grotesque " Small Pica 2-line I. Nc. 4 doubled) German Text bnt yet modernised iis to their pecaliarities. Considering that this article would not be complete without bome sucli notice thereof, as well as to show the contrast, the following is here introduced to the reader. Thele Old-faced Types CUT BY THE CELEBRATED William Caslon, in or about the years 1716-30, are even now viewed with great satisfaction, and held in high efteem, by judges of the typographic art as mafter-pieces of fhape and finiih. To the list of types presented, and which give a sufficient general vitw, may be added Emerald — between Minion and tlonparril — for book-work, and also for borders and flowers to be used in neat and artistic work ; Gem and Semi- Nonpareil for music j utui Minikin, for inusii; and Oriental work. The larger sizes of typo are, with very few exceptions, simple mult plis of the Pica; for instance, Q-line Roman tuenns a roman letter of the depth of six lines of Pica; 20-line Antique, an antique of the depth of twenty lines; and so on. Very little more need be fnid on the names applied to the different faces. Letters used in Title-pages are especially cut for and styled Titling — Square, Condensed, and if very much condensed in width, Compressed or Narrow- Qauge. On tbe other hand, when the letters seem pulled out right and left, they are styled Extended. If the reader will notice the type in which this volume is composed, he will observi' that the bottoms of the tail letters are very clo-e down upon the top-j of the tall letters, and all but touch : this is termed solid. When a page or book is required to look light and less wearisome to the visinn, the lines of type are removed from each other, and i\ spnce-line in- serted between them — the piigc is now termed leaded. These space-lines u^ed to be cut, by the compositor, from milled lead, first in strips of the necessary width, then of the required length ; hence the term leads, by which name tlicy are commonly known. However, they were but poor appliances at the best. Moulds are now used for casting the metal to the specified thickness in strips of about 9 inches long, then cut by h machine to a set gauge; by these means the thickness of the space- lines, or leads, is not only more uniformly se- ciire.l, bnt lav greater regularity obtained in tbe leu^ths cut. Here, as in the large type, as above mentioned. Pica is the standard which regnhites the lead ; in other « ords, leads are cast as 3 to a pica, that is, 3 Iciids form the solid measurement of the Pica boily ; 4rto-pica requires 4 leads, and the body of the lead con- tinues to decrease according to the prefixed figure, which simply denotes into how many parts the pica is to be divided. Leads are 1390 PRINTING INK cast so delicately fine that 16 form the pica, but they are seldom used. In many of the News offices brass space-lines have superseded those cast from type-metal. The method of manufacturing type is — The face having been determined upon — light or heavy, round or narrow, as well as the thickness of the downstroke — a piece of prepared soft iron is taken, and upon the tip- end thereof the proposed letter is cut in re- lief; when this cutting is finished it is case- haidened, and afterwards styled the punch. The strike is the next operation. The punch (the letter cut upon which, by-tlie-bye, is backward) is now punched, or struck, into an oblong piece of copper, about 3 inches long and ^rd of an inch thick, the breadth such as the size of the letter may require : this is the matrix. A most particular part has now to be performed, called justifying ; which means that the matrices shall, when placed in the mould, deliver the letters perfectly upright, and all to be true on a line as fine as a razor's edge. When the process of justifying is ac- complished, the matrix is fixed at the bottom of a mould, of the shape of a parallelogram, of the size of the body one way, of the width of "the letter the other, and the depth the standard height of the type ; the molten metal is forced down this tube, either by hand or by a pump worked by hand or steam, the metal filling the matrix (the sunk letter upon which is now forward) receives the shape of the lettei*, which is once more reversed, or in a backw^ard position, like as the original punch was cut. The castings are released from the mould by a very ingenious method of opening from the two diagonal corners. The types as cast are forwarded on to the dressers to remove burrs and other superfluities; then are placed in long lines in a frame for finishing ; next turned face downwards, and a grooving plane driven across the feet to insure correctness in height; finally looked over for blemishes, when all faulty letters are thrown out ; the process is completed by ranging into lines of handy length, and tied up — ready for delivery to the typographer. PEINX'ING INK. Frep.—a. TheTAENlSH. Linseed or nut oil, 10 or 20 galls., is set over the fire in an iron pot capable of containing fully as much more ; when it boils, it is kept stirred with an ir(m ladle, and, if it does not take fire of itself soon after the smoke begins to rise, it is kindled by means of a piece of burning paper, stuck in the cleft end of a long stick ; the pot is shortly afterwards removed from the fire, and the oil is suffered to burn for about hulf an hour, or until a sample of the varnish cooled upon a palette knife may be drawn into strings of about i inch long, between the fingers ; the flame is now extin- guished by the application of a closely fitting tin cover, and, as soon as the froth of the ebul- lition has subsided, black resin is added, in the proportion of | lb. to 1 lb. for every quart of oil thus treated ; the mixture is next sth-red until the resin is dissolved, when dry brown soap, cut into slices, 1| lbs., is further added (cautiously), and the ingredients are again stirred with the spatula until the whole is united, the pot being once more placed over the fire to promote the combination ; when this is effected, the varnish is removed from the heat, and, after a good stirring, is covered over and set aside. b. The INK. Indigo and Prussian blue, of each, in fine powder, 2\ oz. ; mineral lamp- black (finest), 4 lbs. ; vegetable lampblack, 3J lbs. ; stir them gradually into the warm var- nish (a), and submit the mixture to careful grinding, either in a mill or by means of a slab and muller. On the large scale, steam power is now generally employed for this purpose. An extemporaneous superfine black ink may be made by the following formula: — Take of balsam of copaiba (pure), 9 oz. ; lampblack, 3 oz. ; indigo and Prussian blue, of each | oz. ; Indian red, | oz. ; yellow soap (dry), 3 oz. ; grind the mixture to an impalpable smooth- ness by means of a stone and muller. Canada balsam may be substituted for balsam of copaiba where the smell of the latter is ob- jectionable, but the ink then dries very quickly. COLOUEED PKiNTiNa INKS are made in a similar way from the following pigments : — Carmine, lakes, vermilion, chrome yellow, red lead, orange red, Indian red, Venetian red, for red ; orange chrome, chrome yellow, burnt terra di sienna, gall-stone, Roman ochre, yel- low ochre, for orange and yellow ; verdigris, Scheele's green, Schweinfurt green, blues, and yellows mixed, for greens ; indigo, Prus- sian blue, Antwerp b., cobalt b., charcoal b., for blue ; lustre, bronze powders, &c., for metallic colours ; and umbia, sepia, &c., for brown. Obs, It is necessary to prepare two kinds of varnish, varying in consistence, from more or less boiling, to be occasionally mixed to- gether as circumstances may require; that which answers well in hot weather being too thick in cold, and vice versd. Large charac- ters also require a thinner ink than small ones. Old linseed oil is preferable to new. Yellow resin soap is preferied for black and dark-coloured inks, and white curd soap for light ones. A good varnish may be drawn into threads like glue, and is very thick and tenacious. The oil loses from 10§ to 14g by the boiling. Mr Savage obtained the large medal of the Society of Arts for his black ink made as above. A PBINTEH'S INK EASILY BEMOVED FKOM WASTE PAPEB. The following process for the preparation of a printer's ink that can be far more readily removed from waste paper than ordinary printer's ink has been patented by Kirscher and Ebner. Iron is dissolved in some PRINTS— PRUNES 1391 acid — Bulpliuric, hydroo'nlorlc, acotic, Ac. will Hnswer, and hull of the solution is oxidised witli nitric acid and added to the other half anil the oxide precipitated from the mixture by means of soda or potash. The precipitate it thoroughly washed, and treated with equal parts of solutions of tiiunic and gallic acids, »nd the bluish black, or pure black pigment formed, is thoroughly washed and dried, und mixed with linseed-oil varnish, and can then be immediately used for printing from type, copper, wood, steel, or stone. Waste paper printed with it can be bleached by digesting it for li'l hours in a lukewarm bath of pure water, :ind 10 per cent, of caustic potash or soda, and then grinding it well in the rag engine, and throwing the pulp upon cloth and allowing it to drain. It is then to be waslied with pure water, containing 10 per cent, of hydrochloric, acetic, or oxalic acids, or of bin- oxalate of pota-s:i, and allowed to digest for 24 hours, and may then be worked up iuto paper, or it can be dried and used as a substitute in the manufacture of finer paper. PEINTS (Ackerman's Liquor for). Frep. Take of the tinest pale glue and wliito curd sonp, of each 4 oz. ; boiling water, 3 pints ; dissolve, then add of powdered alum, 2 oz. Used to siie prints and pictures before colour- ing them. PEINTS, To Bleach. Simple Immersion of the prints in a solution of hypochlorous acid (tbe article remaining in the solution for a lciuj;or or shorter space, according to the strength of the solution) is generally uU that is required to whiten it. FEIVI£S. See Watebclosbts. PROOF. See Acbtimetby, Alooholomk- TET, &C. PROOFS (Correcting). The specimen on tbe next piige, with the notes, will, if carefully perused, put the reader into possession of all the secrets nf tliis useful art. PROPYLA'MINE. Syn. TErrYiAJiiNB. CaHjN, or C3H, , This compound or sub H In. hJ stitutcd ammonia, in which one of the three atoms of hydrogen is displaced by the radicle propyl or trityl (C3H;), is isomorphous with trimethyliimine, which has been often mistaken for it. Piopo-ied as a remedy for acute and chronic rheumatism. Heijce it is that the commercial substance known under the name of 'propylamine,' which has been proposed and employed as a remedy for rheumatism, has been shown to be not propylamine, but its isomer, triniethyla- aiiue, or a mixture of this latter, in varying proportions, with ammonia. Mendius gives the following process for the preparation of propylamine : — 36 grams of cyanide of etliyl, 600 grams nf common alcohol, 2U0 grains of water, and 50 Rrams of i;o per cent, hydrochloric :icid, are allowed to act on excess of granulated zinc, and then distilled. The distillate is put back once, and 400 grams of hydrochloric acid are added. The product is distilled to get rid of the alcohol, then excels of alkali added to the residue, and the distillation continued, where- upon propylamine and water come over. Men- dius says 36 grums of the cyanide of ethyl yield 9 grinn< of pure propylamine. The propylamine is dried by distillation from solid potash. Propylamine is a bright, colourless, highly refracting, very mobile liquid, possessing a peculiar, strongly ammouiacal odour. It mixes with water, heat beinj^ generated by the mixture. It boils at M' C, and has a sp. gr. of -7134 at 21° C. Propylamine combines with acids, and forms crystallised salts. The chloride is a very deliquescent salt. The sulphate occurs in crystals, and is also deliquescent. See Tbi- METHTLAMINB. PROPYL'IC ALCOHOL. CjHjO. Syn. Ht- DBATED OXIDE OF PBOPTL, ThITVL ALCOHOL. A liquid boiling at 201-8' l''uhr., obtained by repeiitedly rectifying the first products of the distillation of tbe fusel oil of marc brandy. It stands to ethylic alcohol (ordinary alcohol) in the same relation in which the latter stands to methylic alcohol (pyroxylic spirit). PRO'TEIN. The name given by .Mulder to a substance which he regiirded a-^ the original matter from which animal albumen, casein, and fibrin, were derived; but which is now considered as a product of the decomposition of those important principles by moderately strong caustic alkali. Frep. (Liebig.) Albumen, casein, or fibrin is dissolved in moderately strong potoss:i, the solution heated for some time to 120° Fahr., and acetic iicid added ; a gelatinou'i precipitate subsides, which, after being washed and dried, is protein. Ohs. The names binoxiilo and teroxide of protein have been given by Jl alder to pro- ducts of the long-continued action of boiling water upon fibrin in contact with the air. PEO'TIDE. A soluble, straw-yellow sub- stance, formed, along with other products, by tbe action of strong solution of potassa on albumen, fibrin, or casein. See Ebythbo- PHOTIDB. PR0T0-. See Nomexclatuee. PEOVr'SlONS ( Preservation of ). See Putrefaction. PRUNES. [Fr.] Tbe frnit of cultivated varieties of Pntnus domesiica (Linn.). The dried fruit (French pehnes or plums ; pku- NUU— B. P., Ph. L., PEUSA— Ph. E. & D.) is cooling and gently laxa'.ive, and, as such, is uselul in habitual eostiveness and fevers. Prunes, Pulp of. S, As the vine^ which has long fiom. twined its graceful foliage about the oaky and been lifted by it into sunshine, will, when the hardy plant is rift^^ ed by the thunderCZ^bolt, cling rounds it with its caressing tendrils, and bind Alts shattered boughs up^, ^ so is it {^ordered \ beautif ullyy T'LfiiM by Providence, that woman an/ who is the mere depend^t {,'ui/ and ornament of man in tlie -^v/ happier hours, should ^ his 'Ian on/ stay and solace "^ / fWhen smitten by sudden calamity / winding herself ™ into the rugged recesses of his ifature, ten- derly supporting the droop- ing -tfrad-j and binding up me/iur the broken heart. [It also .^^ is /interesting to /notice how ^^g some MINDS seem almost to ^.(y/' create themselves, springing up un'^r, and working their /^solitary, ( but irresistible way,A r through cles J/ a thousand obsta- Nature seems^ &c. [The same corrected.^ As the vine, which has long twined its graceful foliage about the oak, and been lifted by it into suushine, will, when. the hardy plant is rifted by the thunderbolt, cling round it with its caress- in°; tendrils, and bind up its shattered boughs BO is it beautifully ordered ))y Providence, that WOMAN, who is the mere dependant and orna- ment of man in his happier hours, should be his stay and solace when smitten by sudden calamity ; winding heraelf into the rugged reresses of his nature, tenderly supporting the drooping head, and binding up the broken heart. It also is interesting to notice how someminils seem almost to create themselths, springing up under every disadvantage, and working their *• solitary, but irresistible way," through a thou- sand obstacles. Nature seems, &r. mVING. ^Explanation of the marTcs : 1. "When a letter or word is to he in italics. 3. "When a letter is turned upside down. 8. The substitution of a comma for another point or letter. 4. Tlie insertion of a hyphen ; also marked (-). 5. 'When letters should be close together. 6. When a letter or word is to be omitted. 7. When a word is to be changed to ronian. 8, 9. Two methods of marking a transposition: when there arc leveral words to be transposed, and they are much intermixed, it is a common plan to number them, and to put the usual mark in the margin. 30. Substitution of a capital for a small letter. 11. "When a M'ord is to be changed from small letters to capitals. 13. The transposition of letters in a word. 13. The substitution of one word for another. 11. When a word or letter is to be inserted. 15. When a paragrnph occurs improperly. 16. The insertion of a semicolon. 17. When a space or quadrat stands up, and is seen along with the type. 18. When letters of a wrong fount are used. 19. When words crossed iff are to remain. 20. The mark lor a paragraph, when its com- mencement has been neglected. Sometimes the sign [, or % or the word ' hreak,^ is used instead of the syllables 'New Par* 21. Tor the ijiaertion of a space when omitted or insufhcient. 22. To change capitals to small letters. 23. To cliangc small letters to small capitals. 24. "When lines or words are not straight. 25,36. The insertion of inverted commas. The apostrophe is similarly marked. 27. The insertion of a period when omitted, or in place of another point or letter. 28. Substitution of one letter for another. 29. The method of marking an omission or insertion when too long for the side margin. PKUNING- PRUSSIAN BLUE 1393 lo cover tliem, nnd tlien pressed, first through n fine cano sieve, and afcerwnrds through a fine hair sieve ; the pulp ia, lastly, evaporated by the hent of a water bath to the consistence of a confection. A better plan is to use as little water as possible, by which the necessity of subsequent evaporation is avoided. Used in the prennrntion of coufnction of senna. FBU'KINQ varies according to the kind of plant or tree operated on and the particular object in view, and its skilful performance must, therefore, greatly depend on the expe- rience and knowledge of the gardener. " In the operation of pruning, the shoots are cut off close to the buds, or at a distance not greater than the diameter of the branch to be cut off; because without the near proximity of a bud the wounds will not heal over. In shoots which produce their buds alternately the cut is made at the back of the bud slop- ing from it, 80 that it may be readily covered by the bark in the same or in the following year; but in the case of branches where the buds are produced opposite each other, either one bud must be sacrificed or the branch must be cut off ut right angles to its line of direc- tion, which is most conveniently done with the pruning shears." (Loudon.) PRUS'SIAK AI'KALI. Ferrocyan'ide of potassium. FEUS'SIAN BLUE. Syn. Beblin blub PaBIS B., FEBBOOYiNIDK OF lEON, PbUSSIATE OP I., CiANBEBT OF I. TIlis is the well- known blue pigment of the shops. Prep, 1. The crude but clear solution of ferrocyanide of potassium (blood lye) is precipitated by a mixed solution of alum, 2 parts, and greeu sulphate of iron, 1 part ; the dingy greenish precipitate that falls gradually becomes blue by absorption of atmospheric oxygen, which is promoted by exposure and ngitation of the liquor; as soon us it has ac- ((uired its full colour, the sediment is re- peotedly washed with water, and is then drained, and dried, at first in a stove, but afterwards on chalk stones. Product large, but infirior in quality. 2. Repeatedly digest and wash the preci- pitate obtained by the above process in very dilate hydrochloric acid, and then iu pure water; drain and dry it, as before. Superior. 3. (Paris blue.) — a. Neutralise the solution of ferrocyanide of potassium (blood lye) with dilute sulphuric acid, precipitate the liquid with a solution of any persalt or sesquisalt of iron(as the persulphate, nitrate,Besquichloride, or peracetate) ; well wash the precipitate with water, and dry it, as before. A very rich and intense colour. 4. (Hochstatter.) Crystallised ferrocyanide of potassiuraandgroensulphateof iron, of each 6 parts, are each separately dissolved in water, 13 parts; after the admixture of the solutions, and frequent agitation, oil of vitriol, 1 part, and fuming hydrochloric acid, 24 parts, are stirred in; after some hours have elapsed a VOt. II. strained solution of chloride of lime, 1 parti dissolved in water, 80 parts, is gradually added, the addition beins; stopped as soon as an effer- vescence from tlic escape of chlorine is per- ceived; the whole is now left for 5 or 6 hours, when the precipitate is thoroughly washed in pure soft water, drained, and dried. Or, instead of the above, the precipitate is at once washed iu dilute nitric acid until its colour ceases to be improved by the process. The product is of the finest quality. Prop. Insoluble in water and in dilute acids, except the oxalic, in solutions of which it dissolves freely when pure; oil of vitriol dissolves it to a white pasty mass, which is again precipitated of the usual blue colour by water; alkalies instantly decompose it, and so do red oxide of mercury and some other oxides when boiled with it ; it burns in the air like tinder, leaving an ash of oxide of iron. It is not poisonous. Pur., Sfo. The quality of Prussian blue may be estimated by the richness of its colour, and by the quantity of potassa or soda required to destroy this. If it effervesces with acids, it contains chalk ; and if it forms a paste with boiling water, it is adulterated with starch. It is pure if, " after being boiled with dilute hydrochloric acid, ammonia throws down nothing from the filtered liquid." (Ph. L. 1836.) It is distinguished from indigo by exhibiting u coppery tint when broken, but which is removed by rubbing with tlie nail. Concluding Remarks. The commercial Prus- sian blue is not purt ferrocyanide of iron, but a mixture of this salt with varying pro- portions of the ferricyanide of iron and potas- sium, which also has a fine deep blue colour. The oliject in employing alum is to prevent or lessen the precipitation of oxide of iron by the free alkali in the blood lye, but a portion of alumina is in consequence thrown down with the blue, and tends to render it paler and increase the product. The quantity of alum employed may be varied according to the shades of the intended blue. Samples con- taining this contamination mnst not be em- ployed medicinally. (iSee page 324.) Finssian Blue, Sol'uble. Prep. 1. (Basic Prussian blue.) By adding a solution of protosulpliate of irou to a solution of ferro- cyanide of potassium ; a bluish-white precipi- tate, turning dark blue by free exposure, is formed, which, after it has acquired this colour, is washed until it begins to dissolve in the watei", and colour it blue ; it is then either collected and dried, or is at once dissolved in pure water. This variety is not precipitated from its solution by alcohol. 2. (Feeeoctanidk op potassium and ieon.) By precipitating a solutiou of a ses- quisalt or persalt of irou (as the persulphate, pernitrate, peracetate, or sesquichloride) with a stronger solution of ferrocyanide of potassium, so that the latter may be in considerable exce.ss. A bine precipitate is formed, which is treated 1394 PRUSSIC ACID— PULVERISATION as before. Tliis variety is precipitated by al- cohol. Both are freely soluble in pure water, but not in water wliich has the slightest saline contamination. Hence it is that lengthened exposure to the atmosphere and the use of the common steel pen causes the gradual precipi- tation of this substance from its solution when used .as ink. See Wbitin& fluids. PRU"SSIC ACID. See Hydeocyanic acid. PSEU'DO-MOK'PHIA. A substance of little importance, occasionally found in opium. It differs from morphine chieily in not decom- posing iodic acid. It is said to contain ni- trogen. PTIS'AN. Syn. Ptisanj, L. A decoction made of pearl barley, liquorice, raisins, and otber like vegetable matters, either alone or so slightly medicated as to be taken as a com- mon drink in fevers, catarrhs, &c. Those re- tained in English pharmacy have been alreiidj noticed. The French physicians often employ this form of medicine. The 'tisanes' of the P. Cod. are numerous. Ste Decoction, In- pirsioif, JuiEP, Tisane, &c. PTY'ALIN. A peculiar animal matter, analo- gous to diastase, obtained from the saliva. It is soluble in water, but insoluble in al- cohol. Mialhe named ptya'iu " animal diastase," and regarded it as the principal agent in etl'ecting the digestion of starchy foods, by converting them into soluble glucose. One part of ptjalin, according to Mialhe, was capable of transforming 800 parts of in- soluble starch into sugar. It has been com- pute4 that the average daily secretion of ptyalin by an adult amounts to 116 grains. It very quickly decomposes, and in properties somewhat resembles sodic albuminate. PUCHA PAT. Syn. Patchouli. Pucha pat is the dried foliaceous tops of Pogostemon Patchouli, an Indian species oi Lahiatce. It is much used in perfumery, particularly for making sachets ; but its odour, although very durable, is not so agreeable as that of many other substances, unless it is combined with lavender, hergaitiot, ambergris, musk, or some other like perfume. PUD'DINGS. The instructions given under Cakes, Pies, &c., will be found, with some slight modifications, also to apply to puddings, and, therefore, need not be repeated here. Soyer tells us that every sort of pudding, if sweet or savory, is preferably dressed in a basin instead of in a cloth. If boiled in a basin the paste receives all the nutriment of the materials, which, if boiled in a cloth, are dissolved out by the water, when by neglect it ceases boiling. To cause them to turn well out, the inside of the basin should be tho- roughly ' larded ' or rubbed with butter. In the preparation of meat puddings the " first and most important point is never to use any meat that is tainted; for in pudding, above all otber dishes, it is least possible to disguise it by the confined progress which the ingredients undergo. The gradual heating of the meat, which alone would accelerate de- composition, will cause the smallest piece of tainted meat to contaminate all the rest. Be particular, also, that the suet and fat are not rancid, ever remembering the grand principle that everything which gratifies the palate nourishes." " A pudding cloth, however coarse, ought never to be washed with soap ; it should be simply dried as quickly as possible, and kept dry and free from dust, and in a drawer or cupboard free from smell." (Soyer.) PUD'DLING. See Ieon. PULMONI'TIS. Inflammation of the lungs. PULP. Syn. Pulpa, L. The softer parts of plants, more particularly of fruits, sepa- rated from the fibrous and harder portions. " Pulpy fruits, if they be unripe, or ripe and dried, are to be placed in a damp situation until they become soft; then the pulp is to be pressed out through a hair sieve ; afterwards it is to be boiled with a gentle heat, frequently stirring; and finally, the (excess of) water is to be evaporated in a water bath, until the pulp acquire proper consistence. " Press the pulpy fruits which are ripe and fresh through a hair sieve, without boiling them." (Ph. L. 1836.) PULVEEISA'TION. The reduction of any substance to dust or powder. On the small scale, pulverisation is usually performed by means of a pestle and mortar; on the large scale, by stamping, grinding or cutting the substance in a mill. A few soft substances, as carbonate of magnesia, carbonate of lead, &c., may be pulverised by simply rub- bing them through a fine sieve, placed over a sheet of paper ; whilst many hard, gritty sub- stances can only he reduced to fine powder by porphyrisation or levigation. Elutriation, or ' washing over,' is adopted for several sub- stances, as chalk, antimony, &c., which are required to be reduced to fine powder on the large scale. For some articles which are very tough, fibrous, or resisting, a rasp or file is employed. Whichever of these methods is adopted, the body to be powdered must be very dry, and where spontaneous drying is insuffi- cient, artificial desiccation in a stove or oven, gently heated, is employed. To facilitate this, the substance should be first cut into pieces or crushed small. On the other hand, a few sub- stances, as rice, sago, nux vomica, and St Ignatius's bean, are often soaked in water, or steamed, before being further opeiated on. Whenever a substance cannot be dried com- pletely, without an alteration of its properties, an intermedium is had recourse to, by which the moisture may be absorbed, or its state of aggregation modified. Thus, sugar is employed in pulverising civet, musk, nutmeg, atid vanilla. When camphor is to be pulverised, the addition of a very small quantity of alcohol renders the operation easy. In other cases the interme- dium is of so hard a nature as to assist in break- PUMICE STONE-PUNCH 1395 iag down the substance to be powdered ; thus, gold lent is reduced to powder by rubbing it with sulphate of potassa, and afterwards re- moving this lust by meau!i of water. Fusible luotals, us zinc and tin, are powdered by pour- ing thfin into a mortar, and stirring them rHpidly whilst cooling; or, by briskly agitating them, in the melted state, in a wooden box covered with chalk or whiting. Phosphorus is powdered by melting it in urine or lime water, and thtn shaking the bottle uutil its contents have become quite cold. Qlass, quartz, and silicated stones, require to be heated red hot, and in this state to be thrown into cold water, by which they become sufficiently friable to admit of pulverisation. Many salts which are reduced to fine powder with very great diffi- culty, arid do not dissolve in spirit of wine, are easily obtained in a pulverulent form, bv agitating their concentrated aqueous solution with a considerable quantity of rectified spirit; the disengaged fine crystallised powder may then be dried, nml further divided by tritura- tion. Potivssio tartrate of antimony may be advantageously thus treated. A large number of salts, including nitre, sal aminoniiic, and carbonate of potash, may also be reduced to powder by keeping their solutions in a state ot constant and violent agitutiuu during their rapid evaporation. The following rules should be observed in the preparation of powders : — 1. If possible, perfectly dry articles should alone be operated on, and only in dry weather. 2. The nature of the mortar, and the mode of operating, should be adapted to the nature of the substance. Thus, woods and barks should he pulverised in an iron mortar ; suj;ar, alum, and nitre, in oue of marble or wedg- wooil-warc ; and corrosive sublimate, only in Dne of glass. 3. Ihe mortar should be provided with a cover, to prevent loss and annoyance to the operator. It' much powder escapes, or if it is dangerous or disagreeable when breathed, or it' the substance is rare or costly, the mortar should be covered with a skin of leather, to Vrhich the pestle is attached, so that the latter may be freely moved without causing the slightest opening for the escape of the dust occasioned by the process. When aloes or gamboge is powdered, a few drops of olive oil are commonly added with the same inten- tion. 4. The pulverised portions should he sepa- rated from time to time by aid of a sieve, the coarser paitieles being returned to the mortar to be again beaten and triturated ; and this alternate pulverisation :ind sifting is to be repestc'l until the process is complete. PUM'ICE STONE. Sy». 1'umex, Lapis PITHiCKDs, L. FCMicis, L. Found in the neighlwnrhood of volcanoes. Used, in the ■olid form, to pnli^h wood, paint, &c. ; also, when pulveri-ed, ik a polishing powder for gla'S, bone, ivory, marble, metals, &c. PUMP FOE USE IN CHEMICAL, PAPEE, and other Works. The Perreaux Pump Valve is made of vulcanised india rubber, and is of the form of the valves in the human body. It is of the greatest, and perhaps the really only valuable improvement in valves applicable, equally, to the common hand or jack pump, and the most elaborate mechanical combinations for raising water. The valve may be taken as the key of the pump; a perfect valve renders an indilferent pump avaiuable and effective macliine, whereas an imperfect valve, in an otherwise excellently constructed pump, renders it practically use- less. The pump which Simon the tanner, of Joppi, used for pumping his pits, nearly two thousand years ago, may be taken as the type of the comiyoii hand pump in use to this day. Various mechanical improvements have been made in its form and construction, but, prac- tically, and effectively, the only real and valu- able improvement is the Perreaux valve, now under oonsideiation. Constructed of a flexible material, and made in form, as nearly as may be, to the valves of the human body, they may be said to be auto- matic in their action, or self acting; upon the pump being actuated, tlio least motion of the pump ensuring a corresponding action of tiie valve, and the most rapid action of the pump, beiiij; equally responded to by the pul- sation of tlie valves. Although the most perfect valves for pump- ing clear water, because, what is mechanically termed the duty of the pump is complete, in other words, the quantity displaced is dis- charged, absolutely without loss, yet their most valU'ible feature is that they pump semifluids equally well as clear water. For the pulps and stuffs in paper mills, for bleaches, dye.-*, and corrosive liquors, for liquid manures and other such semi-tluids, tliey stand alone, they are absolutely uncbok- able. Used in conjunction with cylinders or barrels made of toughened glass, they form the most perfect pump where the fluid to be raised is of a caustic or corrosive nature, and where the fluid would be destructive to or destroyed by its action upon metals, such fur example as the caustic bleach used in the maiiuiacture of p iper, &c. See Valves. PUNCH. An acidulous, intoxicating; beve- rage, conipostd of water sweetened with sugar, with a mixture of lemon juice and spirit, to wliich some aromatic, as nutmeg, mace, or cin- namon, is occasionally added. Wine is some- times substituted for spirit. It is much less drunk than formerly. Rum punch is themost popular amongst sailors, who are now the principal consumers of ihis beverage. Frtp. I. Juice of 3 or 4 lemons; yellow peel of 1 lemon ; lump sugiir, J lb ; boiling wat<'r, 3t pints; infuse \ an hour, strair, and add, of bitter ale, J pint ; rum and brandy, of 1396 PURGATIVES— PURPLE each f to 1 pint (or rum alone, li to 2 pints). More hot water and sugar may be added if the punch is desired either weaker or sweeter. 2. Cold punch.) From arrack, port wine, and water, of each 1 pint ; juice of 4 lemons; white sugar, 1 lb. 3. (Gin punch.) From the yellow peel of i a lemon ; juice of 1 lemon ; strongest gin, -J pint ; water, If pint ; sherry, 1 glassful. 4. (Iced punch.) From champagne or Rhenish wine, 1 quart ; arrack, 1 pint ; juice of 6 lemons ; yellow peel of 3 lemons ; white sugar, 1 lb. ; soda water, 1 or 2 bottles ; to be iced as cream. 5. (Milk punch; Vbedee.) Steep the yellow rinds of 18 lemons and 6 oranges, for 2 days, in rum or brandy, 2 quarts ; then add 3 quarts more of either spirit ; hot water, 3 quarts ; lemon juice, 1 quart ; loaf sugar, 4 lbs. ; 2 nutmegs, grated ; and boiling milk, 2 quarts; mix well, and in 2 hom's strain the liquor through a jelly-bag. 6. (NoKPOLK PUNCH.) Take of Trench brandy, 20 quarts ; yellow peels of 18 oranges and 30 lemons ; infuse for 12 hours ; add, of cold water, 30 quarts ; lump sugar, 20 lbs. ; and the juice of the oranges and lemons; mix well, strain through a hair sieve, add of new milk 2 quarts, and in 6 weeks bottle in. Keeps well. 7. (ORANftE PUNCH.) As No. 1, Using oranges, and adding some orange wine, if at hand. A little curacoa, noyau, or maroschino improves it. 8. (Raspbekrt PUNCH.) As the last, but using raspberry juice, or raspberry vinegar, for the oranges or lemons. 9. (Reoekt's PUNCH.) From strong hot green tea, h-mon juice, and capillaire, of each li pint ; rum, bi'andy, arrack, and curacoa, of each 1 pint ; cliampague, 1 bottle ; mix and slice a pineapple into it. 10. (Tea punch.) From strong hot tea, 1 quart; arrack, J bottle; white sugar, 6 oz. ; juice of 8 lemons ; and the yellow rinds of 4 lemons; mixed together. 11. (Wine punch.) From white sugar, 1 lb.; yellow peel of 3 lemons; juiceof 9 lemons; arrack, 1 pint; port or sherry (hot), 1 gall. ; cinnamon, i oz.; nutmeg, 1 dr. ; mix. 12. (Yankee punch.) Macerate sliced pineapple, 3 oz. ; vanilla, 6 gr. ; and amber- gris (rubbed with a little sugar), 1 gr., in the strongest pale brandy, 1 pint, for a few hours, with frequent agitation ; then strain with ex- pression ; add, of lemon juice, 1 pint ; lemon syrup, and either claret or port wine, of each 1 bottle; with sugar, ^ lb., dissolved in boiling water, 3 i pint. See Shkub. PURG'ATIVES. %n. Dejectoeia, Pue- GANTIA, PuHSATiVA, L. These have been divided into five orders or classes, according to their particular actions. The following are the principal of each class : — 1. (Laxatives, lenitives, or mild cathae TICS.) Manna, cassia pulp, tamarinds, prunes. honey, phosphate of soda ; castor, almond, and olive oils ; ripe fruit. 2. (Saline or cooiiiro laxatives.) Epsom salt, Glauber's salt, phosphate of soda (tasteless salt), seidlitz powders, &c. 3. (Active cathaeticb, occasionally acrid, frequently tonic and stomachic.) Rhubarb, senna, aloes, &c. 4. (Deastic or violent cathaetics.) Jalap, Ecammony, gamboge, croton oil, colocynth, elaterium, &c. 5. (Meecueial puegatives.) Calomel, blue- pill, quicksilver with chalk, &c. In prescribing purgatives regard should be had to the particular portion of the alimeutary canal on which we desire more immediately to act, as well as to the manner in which the medicine effects its purpose. Tlius, Epsom salt, sulphate of potassa, and rhubarb, act chiefly on the duodenum ; aloes on the rectum; blue pill, calomel, and jalap on the larger in- testines generally ; and tartrate and bitartrate of potassa, and sulphur on the whole length of the intestinal canal. Again, others are stimu- lant, as aloes, croton oil, jalap, scammony, &c. ; others are refrigerant, as most of the saline aperients ; magnesia and its carbonate are both aperient and antacid; whilst another class, including rhubarb, damask roses, &c., are astringent. Further, some produce only serous or watery deject'ons, without greatly increasing the peristaltic action of the bowels ; whilst a few occasion a copious discharge of the fseces in an apparently natural form. See Deaught, Mixtuee, Pills, Peesceibino, &c. PUEI. Frep. To ale or beer, i pint, gently warmed, add of bitters, 1 wine-glassful, or q. s. Some add a little spirit. A favourite beverage with hard drinkers early in the morning. PUE'PLE. A rich compound colour, pro- duced by the admixture of pure blue and pure red. This colour has always been the distin- guishing badgeof royalty and distinction. The celebrated Tyrian purple was produced from a shell- fish called murex. Purple An'iline. Si/n. Peekin'S pueple. Mauve. This valuable dye-stuff is prepared under W. H. Perkin's patent, by mixing solu- tions of sulphate of aniline and bichromate of potassa iu equivalent proportions, and, after some hours, washing the black precipitate with water, drying it, digesting it repeatedly in coal-tar naphtha, and, finally, dissolving it in boiling alcohol. It may be further purilied by evaporating the alcoholic solution to dryness, dissolving the residue in a large quantity of boiling water, reprecipitating by caustic soda, washing with water, dissolving 'in alcohol, filtering, and evaporating to dryness. Thus pui'ifiert, mauve forms a brittle substance, having a bronze-coloured surface. It imparts a deep purple colour to cold water, though dissolving sparingly in that liquid ; it is more soluble in hot water, and very soluble in PUKPLE DYE— I'UTREl'ACTION 1397 alcohol. See Pdbflb dve (below), and Tab COLOCBS. Purple of Cassins. Sgn. Pcrfle rRECiFi- TATE OP OASSIUa, GOLD FDBPLE, GOLD FBE- FABED WITH TIN ; ACBtTM STANNO PABATUM, PDKPDBA MIKKEAL18 CaSII, L. Trep. 1. CryatuH'mcd protuchloride of tin, 1 pait; crys- tallised peroliloride of tin, 2 parts ; dissolve each separately, mix the solutions, and add of crystallised tercliloride of gold (in solution), 1 part ; carefully wash, and dry the precipitate. Very fine. 2. (Frick.) Dissolve pure grain tin in cold dilute aqua rcgia until the fluid becomes faintly opalescent, then take the metal out and weigh it; next, dilute the solution largely with water, and add, simultaneously, a dilute solution of gold and dilute sulphuric acid in SMch prnportion that the tin in the one shall be to the gold in the other in the ratio of 10 to 36. 8. (P. Cod.) Turchloi ide of gold, 1 part, is dissolved in distilled wuter, 200 parts; another Bolutioa is made by dissolving in the cold, pare tin, 1 part, in a mixture of nitric acid, 1 part, and hydrochloric acid, 2 parts ; this last solution is diluted with distilled water, 100 parts, and is then added to the solution of tercliloride of gold until precipitation ceases to take place; the powder is, lastly, washed by decantation, and dried by a very gentle heat. 4. Silver, 150 parts ; gold, 20 parts ; pure grain tin, 35 parts; fuse them together under charcoal and borax, cool, laminate, and dissolve out the silver with nitric acid. Obs. Purple of Cassias is generally supposed to be a combination of oxide of gold and ses- quioxidc of tin, in which the latter acts as an acid. Heat resolves it into a mixture of metallic gold and binoxide of tin. It is used as a purple in porcelain painting, and to com- municate a ruby-red colour to glass, when melted In open vessels. PUKPLE DTE. The purples now in vogue are the numerous shades of ' mauve ' and 'magenta' obtained by the * aniline colours.' (See above, also RsD.) For silk and woollen goods no mordant is required. The proper proportion of the clear alcoholic solution is mixed with water slightly warm, any scum that may form is cleared otf, and the goods are entered and worked until the required shade is obtained ; a small quantity of acetic or tar- taric aeid is recommended to be added in some cases. For dyeing on cotton with the aniline colours, the cloth or yarn is steeped in sumac or tannic acid, dyed in the colour, and then fixed by tin ; or it may be steeped in sumac and mordanted with tin, and then dyed. Pur- ples were formerly, and are still occasionally, produced by first dyeing a blue in the ' indigo vat,' and then dyeing a cocliiueal or lac scarlet upon the top. See Vioiet dye. PDK'PUaATE OF AMMO'NIA. See Mw- KBXISK. PORPU'KIC AWD. See MuREXAN. PUEPUHIN. CjHjOj. Si/n. Maddbe FUH- FLE. The name given by Kiliiijuet and Colin to a beautiful colouring principle obtained from madder, Pre-p. Coarsely powdered madder is allowed to ferment with water, after which it is boiled in a strong solution of alum ; the decoition is next mixed with sulphuric acid, and the re- sulting red precipitate is purified by one or more crystallisations from alcohol. JProp.,Sfc. Crystalline red needle.*, insoluble in cold water, but soluble in hot water, and in alcohol, ether, and solutions of alum and the alkalies. It ditfersfrom alizarin or madder red in containing 2 atoms less of carbon. PUR'EEE. Syn. Indian yellow. A yellow substance, of duulitl'ul origin, imported from China and India, and now extensively used in both oil and water-colour painting. According to the researches of Stenhouse and Erdmaiin it consists of purreic acid, a ^trllngly tinc- torial vegetable substance, united to mag- nesia. PUEEE'IC ACID. Syn. Euxanthio acid. This substance is obtained frt)m purree. It crystallises in nearly colourlc-s needles, which are only sparingly soluble in cold water, and forms rich yellow- coloured compounds with the alkalies and earths. Heat converts it into a neutral, crystallisable substance, called pur- renone. PUS. The cream-like, white or yellowish liquid secreted by wounded surfaces, abscesre-, sore*, &e. PUTREFACTION. Syn. Putbefactio, L. The spontaneous decomposition of animal and nitrogeni^ed vegetable substances, under the joint influence of warmth, air, and moisture. The solid and fluid matters are resolved into gaseous compounds and vapours, which escape, and into earthy matters, which remain. The most striking characteristic of this species of decomposition is the ammoniacal nr fetid ex- halations that constantly accompany it. The nature of putrefaction, and the conditions essential to its occurrence, have been briefly alluded to under fermentation, to which we must refer the reader. It may here, however, be useful to reiterate that this change can only be prevented by the abstraction or exclusion of the conditions essential to its occurrence. This may be affected by — reduction of tempe- rature, — exclusion of atmospheric air, or — the abstraction of moisture. The antiseptic pro- cesses in common use are efiective in precisely the same degree as these preventive means are carried out. Frozen meat may be preserved for an unlimited period, while the same sub- stance will scarcely keep for more than a few days at the ordinary heat of summer. Animal 3ub^tances will also remain uninjured for a long period if kept in vessels from which the air is entirely excluded, as in the process now so extensively adopted for the preservation of fresh meat for the use of our armyaud marine. 1398 PUTREFACTION. The third condition is falSUed when nitro- genised matter is preserved in alcohol, brine, or any similar fluid, and when it is dried. In either case water is abstracted from the sur- face, which then loses its propensity to putrefy, and forms an impervious layer, which ex- cludes atmospheric oxygen from the interior and softer portion of the substance. Creasote, and most of the antiseptic salts, also act in this way. Among special antiseptic processes are the following : Application op cold. The accession of putrefaction is prevented, and its progress arrested, by a temperature below that at which water freezes. In the colder climates of the world, butchers* meat, poultry, and even vege- tables, are preserved from one season to the other in the frozen state. In North America millions are thus supplied with animal food, which, we can state, from personal experience, is often superior in flavour, tenderness, and apparent freshness, to tliat from the recently killed animal. In temperate climates, and in cold ones daring their short summer, ice- houses and ice-safes afford a temperature suffi- ciently low for keeping meat fresh and sweet for an indefinite period. Substances preserved in this manner should be allowed to gradually assume their natural condition before cooking ihem ; and on no account should they be plunged into hot water, or put before the fire, whilst in the frozen state. BucANiNO. A rude kind of drying and smoking meat, cut into thin slices, practised by hunters in the prairies and forests. Desiccation or detino. In this way every article of food, both animal and vegetable, may be preserved without the application of salt or other foreign matter. The proper method is to expose the substances, cut into slices or small fragments, in the sun, or in a current of warm dry air, the temperature of which should be under 140° Pahr. Articles so treated, when immersed for a short time in cold water, to allow the albumen and organic fibres to swell, and then boiled in the same water, are nearly as nutritious as fresh meat cooked in the same manner. If a higher degree of heat than 140° be employed for animal substances, they become hard and insipid. Owing to the practical difficulties in the way of applying the above process to fresh meats, it is "usually employed in conjunction with either salting or smoking, and, frequently, with both of them. EXCLTTSION OP ATMO3PHEEI0 AIE. This is effected by the method of preserving in sugar, potting in oil, and, more particularly, by some of the patented methods noticed below. Fresh meat may be preserved for some months in that state, by keeping it in water perfectly deprived of air. In practice some iron filings and sulphur may be placed at the bottom of the vessel, over which must be set the meat ; over the whole is gently poured recently boiled water, and the vessel is at once closed, so aa to exclude the external air. Immbesion in antiseptic hquids. One of the commonest and most effective liquids employed for this purpose is alcohol of 60 to 70^, to which a little camphor, ammonia, sal ammoniac, or common salt, is occasionally added, A cheaper and equally efficient plan is to employ a weak spirit holding a little creasote in solution. A weak solution of sul- phurous acid may be substituted for alcohol. Weak solutions of alum, or carbolic acid, with or without the addition of a few grains of cor- rosive sublimate, or of arsenious acid, are also highly antiseptic. These are chiefly employed for anatomical specimens, &c. A solution con- taining only ^Joth part of nitrate of silver is likewise very effective; but, from this salt being poisonous, it cannot be employed for preserving articles of food. Butchers' meat is occasionally pickled in vinegar. By immers- ing it for 1 hour in water holding ^J^jth part of creasote in solution, it may be preserved unchanged for some time even during summer. Injection op antiseptic liquids into the veins or arteries of the recently killed animal. It is found that the sooner this is done after the slaughter of the animal the more effective it becomes, as the absorbent power of the vessels rapidly decrease by age. See Gannal's PEOCESS {below). Jeekino is a method of preserving flesh sometimes adopted in hot climates. It con- sists in cutting the lean parts of the meat into thin slices, and exposing these to the sunshine until quite dry and brittle, when they are bruised in a mortar, and pressed into pots. Pickling in vinegae. In this method the substances, lendered as dry as possible by ex- posure to the air, are placed in glass or stone- ware jars (not salt-glazed), o^ wooden vessels, when strong vinegar, either cold or boiling hot, is poured over them, and the vessel at once closely corked or otherwise covered up, and preserved in a cool situation. Meat is occa- sionally thus treated; vegetables frequently so. See Pickle. Pottino in oil. In this case salad or olive oil is substituted for vinegar (see dbove)j andi^ always used cold. Salting acts chiefly by abstracting water from the albuminous portions of the ment, by which its disposition to change is lessened. Smoking. This process, which, as well as the last, is referred to further on, acts both by the abstraction of moisture and the antiseptic properties of certain substances (creasote, &c.) contained in wood smoke. Fresh meat and fish are occasionally smoked ; but, in general, substances intended to be thus treated are first salted. In Donkin and Gamble's patent process the substances, previously parboiled, are placed in small tin cylinders, which are then filled up with rich soup ; the lids are next soldered on PUTTY 1399 quite air-ti|;ht, and a smnll hole ia afterwards made in the centre ; tlie cylinders are then placed in a bath of strong brine, or a strong solution of chloride nf calcium, which is at once heated to the boiling point, to nearly comiileto the cooking process; alter which the small hole in the lid is hermetically sealed by covering it with solder while the vessel still remains boiling hot ; the tins are, lastly, again submitted to heat in the he»ted bath, the duration of which is proportioned to the quan- tity and character of their contents, the ' dress- ing ' of which is to be perfected by this opera- tion. Ihe ends of the tins, on cooling, assume a conc:ive form, from the pressure of the atmosphere, without which they cannot be air- tight, and the prucess has been unsuccessful. To determine this, the patentees expose the canisters, prepared as before, for at least a month in an apartment heated to about 100° t'ahr. J when, if the process has failed, putre- faction commences, and the ends of the cases, instead of remaining concave, bulge or become convex. This is called the ' test.' By this process, which was invented by M. Appert in France about the year 1808, fish, flesh, poultry, and vegetables may be preserved for years in any climate. Ooldner's process differs somewhat from the preceding, in the employment of a higher degree of heat, more hastily applied, and not prolonged or repeated after the tins are sol- dered up. Gnnnal's process, hnving for its object the preservotion of butchers' meat in the fresh state, depends on the peculiarly absorbent pro- perty of the flesh of recently killed animals, above referred to. This process consists in in- jecting a solution of sulphate of alumina, or, letter, of chloride of aluminium, of the sp. gr. 1 070 to 1-085 (10° to 12° Bmm6), into the cnrotid artery, by means of a syphon, as soon as the blood ceases to flow from the slnugh- tered nnimal ; both extremities of the jugular vein being previously tied. 9 to 12 quarts of the solution are sufficient for an ox, and a pro- portionate quantity for smaller animals. A less quantity is also required in winter than summer. When the animal "has been well bled, and the injection skilfully performed, it is I'carcely pereeptilile that the animal has un- dergone any preparation. The injected animal is cut up in I he usual way ; and when intended to be eaten within 2 or 3 weeks merely requires to be hung up in a dry, airy situation free from flies ; but if it is to be kept for a longer period, it is directed to be washed with a mixed solution of common salt and chloride of aluminium at 1U° Baum^ and then simply dried and packed in clean air-tight barrels, and kept in a cool, dry place. If the air cannot be perfectly excluded, it should be packed in dry salt, not for the purpose of pre- serving it, hut to prevent the vegetation of bi8.sus, as, witlimit this precaution, the meat becomes musty from exposure and the action of moisture. Jfeat preserved by this process may be kept for several years, aud merely requires soaking for 24 hours in water, for the purpose of swelling its pores, to ^:ive it the appearance and taste of fresh meat, fit for either roasting or boiling. For hot climaii s a somewhat stronger solution, or a larger quan- tity of the usual one, may be injected. The use of the strong solutions ordered in some recent works, however, deprives the flesh of a portion of its apparent freshness, and makes it more nearly approach in flavour to that which has been slightly salted in the ordinary manner. In addition to the above it may be added that both flesh and fish may be preserved by dipping them into, or l.riishin;,' them over with, pyroligneous acid, and then dr\ ing them. This gives them a smoky flavour; but if pure acetic acid (Ph. L.) be nsed, no taste will be imparted. These fluids may be applied by means of a clean painter's brush, or even .i stiff feather. A taLilc-spoonful is suffieieiit to brush over a large surface. Fish and flesh so prepared will bear a voyage to the East Indies and back, uninjured. Fish may also be preserved in a dry state, and perfectly fresh, by means of ^ugar alone. Fresh fish may be thus kept for some days, so as to be as good when boiled as il just caught. If dried and kept free from mouldjness, there seems no limit to their preservation ; and they are much more nutritious in this way than when saUed. This process is particularly valu- able in making what is called ' kippered sal- mon;' and the fi~h preserved in this manner are far superior in quality and flavour to those which are salted or smoked, A few table- spoonfuls of brown sugar are sufficient for a salmon of five or six pounds' weight; and if salt be desired, u teaspoonful or two may be added. Saltpetre may be used instrad of salt, if it be wished to make the kipper hard. The well-kno"ivn property possessed by ether, alcohol, pyroxylic spirit, chlorolorni, and cer- tain other hydrocarbons, of averting putrefac- tion, has been thus applied by JI. Kobin : — He encloses the meat or other substances to be pre- served in a glass case, along with a sponge or a capsule containing the preservative liquid, which latter is continnally evolved in a vapor- ous condition, and exercises the preservative agency. In this way the vapours of hydro- cyanic acid are found to be very efficacious. Camphor is thus employed in the mummt cases in the British Museum. It has been asserted by Mr George Hamilton that in an atmosphere of binoxide of nitrogen, in the dark, flesh preserves its natural colour and freshness for about five months ; and eats well provided it be boiled in open ves.-els, to expel nitrous fumes. See Candtixo, Egg, Fish, Fbuit, Milk, Pickles, Pottiko, Pbe- SESVES, Salting, Smoking, Stuffing, Vb. OETABLK SDB3TANCES, &C. PUT'TY. This name is given to the follow- 1400 PUZZOLANA— PYROMETER ing preparations (when used alone, ' Glazier's putty' is generally indicated) : — Putty, Glazier's. From whitingraadeintoa stiff paste with drying oil. It is used to fix panes of glass in sashes, to fill holes and cracks in wood before painting it, &c. Putty, Plasterer's. A fine cement used by plasterers, made of lime only. It differs from ' PINE stupe' in the absence of hair. Putty, Polisher's. Sgn. Pbttt powdeb. Calcine; Cineebs stanni, Stanni oxtdum CBUDUM, L. A crude peroxide of tin, obtained by exposing metallic tin in a reverberatory furnace, and raking off the dross as it forms ; this is afterwards calcined until it i)ecoines whitish, and is then reduced to powder. Another method is to melt tiu with rather more than an equal weight of lead, and then to rapidly raise the heat so as to render the mixed metal red hot, when the tin will be immediately fiung out in the state of * putty' or ' peroxide.' The products of both these processes are very hard, and are used for polishing glass and japau work, and to colour opaque white enamel. See Tin. Putty, To Soften. Take 1 lb. of American pearlash and 3 Ihs. of quick-lime. After slaking the lime in water add the pearlash, and let the mixture be made of a. consistence about the same as that of paint. When required for use apply it to both sides of the glass, and let it remain in contact with the putty for twelve hours ; after which the putty will have become so softened that the glass may be removed from the frame without any difficulty. PUZZOLA'ITA, PuozzOLANA, or, more cor- rectly, PuzzuoLANA, is a volcanic ash found at Puzzuoli, near Naples. When mixed with lime it forms an excellent hydraulic cement. A good FACTITIOUS PUZZOLANA may be made by heating a mixtur-e uf 3 bushels of clay and 1 bushel of fresh-slaked lime for some hours to redness. (M. Bruyere.) See Cement and MOETAE. PYEI'TES. A term applied to several native metallic sulphides. IBON pybites is the best known of these. P Y'RO-. The term is applied to several acids that are obtained by the action of heat on other substances ; as, PYEOQALLIO ACID, PYEO- LIQNEOCS A., &C. PYROACE'TIC SPIRIT. See Spieit (Pyro- acetic). PYKOGAI'LIC ACID. HCsH^Oj. St/n. AciDUM PTEOQALLIOUM, L. Frep. 1. From either gallic or tannic acid, heated in a retort by means of an oil bath, and steadily maintained at a temperature of about 420° Pahr. as long as crystals are formed in the neck of the retort, or in the receiver, both of which should be kept well cooled. Pure. If a much higher heat is employed, the product consists chiefly of meta- gallic acid. 2. From Aleppo galls, in very coarse pow- der, heated in a dish covered with thin filter- ing paper pasted to its edge, and connected with a well-cooled receiver. Dr Ure says that the so-called Chinese g.tlls furnish, by dry distillation, a " very concentrated solu- tion of pyrog.iUio acid, which, evaporated on the water bath, yields of brown crystalline pyrogiiUic acid nearly lo^ of the weight of the galls." 3. (Dr Stenhouse.) By sublimation from the dry aqueous extract of nut-galls, in aMobr's apparatus, in the same way that benzoic acid is obtained from benzoin resin, observing the precautions referred to in No. 1 (above). Nearly pure. The product is fully lOg of the weight of extract operated on. Prop. Light crystals, which, when perfectly pure, are quite white; freely soluble in water, but the solution canitot be evaporated without turning black and suffering decomposition; it strikes a rich blackish-blue colour with the protosalts of iron, and reduces those of the sesquioxide to the state of protoxide; when heated to 480° Fahr., it is converted into METAOALLIC ACID and water. UseSt Sfc. Pure pyrogallic acid is now very extensively employed in photography. A solu- tion of the crude acid mixed with a little spirit is used to dye the hair, to which it imparts a fine brown colour, but has the disadvantage of also staining the skin when applied to it. PY'EOBEN ACIDS. Those generated by heat. PYRO'LA. See Wintbe geeen. PYROLIG'HEOUS ACID. Sy». Vineoae op WOODt, SpIEIT of -W.t, SmOKINQ LIQUOEt, Essence op SMOKEf; Acidfm pteomono- SUM, L. Impure acetic acid, obtained by the destructive distillation of wood in close vessels. It comes over aloug with tar creasote, and other liquid and gaseous matters. In this state it contains much empyreumatic matter in solution ; but by separation from the tar, saturation with slaked lime or chalk, defeca- tion, and evaporation, an impure acetate of pyrulignate of lime is obtained, which, after being gently heated, to destroy part of its em- pyreumatic matter, without injuring its acetic acid, is again dissolved and defecated, and then precipitated by a solution of sulphate of soda, when a solution of acetate of soda and a pre- cipitate of sulphate of lime are formed by double decomposition. The solution is next evaporated to dryness, the dry mass (pyrolig- nite of soda) dissolved in water, and the new solution filtered and recrystalli-ed. The crys- tals of acetate of soda, obtained by the last process, yield nearly pure acetic acid by dis- tillation along with sulphuric acid. See Acetic acid and Vineoae. PYROLIG'MEOUS SPIRIT. See Spieit (Pyroxilic). PYROM'ETER. An instrnment to measure high degrees of heat. Wedgwood's pyeo- METEE, the one best known, depends on the property which clay possesses of contracting when strongly heated. Peop. Daniel's py- PVROPHORUS-PYROTECHNY liOl ROMBTER cotnistn, csdpntinlly, of n small rod or bstr of pintitium, which acts in a precisely oppa' muimcr to the preceding, viz., by its expMHsion. PYROPH'ORUS. Si/n. LriT-ZtnrDBB, Ger. Any substance that inflames spontaneously when exposed to the air. Prep. 1. Neutral cliromate of lead, 6 parts ; sulphur, 1 part; triturate them with water, q. s. to form a paste, and make this into pel- let* ; dry these perfectly by a gentle heat, then beat them in a closed tube until the sulphur is all driven off ; lastly, transfer them to a stoppered phial. 2. (HoMBKBo'sprEOPHOB08.) From alum and brown xugar, equal parts ; stir the mixture in an iron ladle over the fire until dry, then put it Into an earthen or coated glass phiul, and keep it at a red heat so long ae the flarae is emitti^d ; it must then be carefully stopped up and cooled. 3. (Dr Hiire.) Lampbliick, 3 parts; burnt alum, 4 parts ; carbonate of potassa, 8 parts ; as the last. 4. (Gay Lussac.) From sulphnte of po- tnsSB, 9 pirts; calcined lampblack, 5 parts; as No. 2. 5. Alum, 3 parts ; wheat flour, 1 part ; as No. 2. 6. (Lead PYBOPnoutrs — Giibel.) Heat tar- trate of lead to redness in a glass tnbe, and then hermetically seal it. See Tabtuatk of Lkad. Oba. When the above are properly pre- pared, a little of the powder rnpidly becomes very hot, and inflani(;s on exposure to the air. The accession of the combustion is promoted by nloisture, as a dump atmosphere or the breath. With the exception of the first and sixth, "they owe their combustibility to the presence of sulphide of potassium." (Gay Lussnc.) PYROPHOSPHOR'IC ACID. See Dibasic PltosPHOBio ACID (Phosphorus). PYRO'SIS. Si/n. Black wateb, Watee BKASH, VVatkb qualm. An aflvction of the stomach, attended by a sensation of heat and the eructation of a thin, sour liquid, often in considerable quantity, especially in tlie morning. The following pill will be foimd of service in this aSection : — Powdered opium, Jth gr. ; subnitrate of bismuth, 5 gr. ; extract of gen- tian, sufficient to make into 2 pills. To be taken two or three times a day, before meals. The solution of bismuth and citrate of ammonia (I/>>|uar Bismuthi et Ammoniac Citratis, B. P.), in doses of i dr. to 1 dr., taken as above, is another medicine which may be had recourse to, should the above fail to give relief. PYROTARTAR'IC ACID. HjCsHeO^. Ob- tuined by the destructive distillation of tartaric acid. See Tabtaeic acid. PYROTECH'HY. The art of making fire. works. The three principal materials em- ployed in this art are charcoal, nitre, and sul- phur, along with filings of iron, 8t«el, copper, or zinc, orwii^h resin, camphor, lycopodiuui,or other subntiinces, to impart colour, or to modify the effect or the duration of the com- bustion, (iimpowder is used "either in grain, half crushed, or finely ground, for different ptiruoses. The longer the iron filings are, the brighter red and white spots they give ; those beinj; preferred which are made with a coarse fiJe, and quite free from rust. Steel filings and cast-iron borings contain carbon, aiid afford a more brilliant fire, with wavy radin- tions. Copper filings give a greenish tint to flame; those of zinc, a fine blue colonr; the sulpbiilc of antimony gives a less greenish blue than zinc, but with much smoke; amber aflbrds a yellow fire, as well as colophony (resin) and common salt; but the last must be very dry. Lampblack produces a very red colour with gunpowder, and a pink one with niti e in ex- cess; it serves for making golden showers," U'licn this substance is lightly mixed with gunpowder and put into cases, it throws out small stars resemhling the rowel of a spur; this composition has liencc been called ' spur fire.' "The yellow sand, or glistening mica, communicates to fire-works golden radiations. Verdigris imparts a pale green ; sulphate of copper and sal ammoniac gives a palm-tree green. Camphor yields a very white flame and aromatic fumes, which masks the bad smell of other substances. Benzoin and storax are also used, on account of their agreeable odour. Lycopodium burns with a rose colour and a magnificent flame; but it is principally em- ployed in theatres to represent lightning, or to charge the torch of a Fury." (Ure.) See FiiiEs (Coloured), Flame Coloues, Gcnpow- DKB, Stabs, Rockets, &c. The following substances are in requisition by the Pyrotechnist : — Zinc. This metal is employed in the form of fine powder, which is obtained as follows : — The metal, scarcely melted, is poured into a hot mortar, where it is ndnced to powder, being kept dui-ing the operation at a tempe- rature of 401° F. It is then sifted to remove any particles which may have escaped contact with the pestle. CoPPEE. This metal may be obtained in a state of minute division by precipitating it from a solution of sulphate of copper by means of iron, the precaution being taken of using a large quantity of iron. The precipi- tate, after being well washed, is dried between folds of blotting paper, and kept in well stoppered bottles. Ibon-sand. a quantity of sulphur is melted in a crucible over a slow fire, and when it is quite fluid, iron filings are thrown in while the whole is being stirred. The crucible is removed from the fire, and the contents are rapidly stirred until cold. The material is then rolled on a board till it is broken up as 1402 PYEOTECHNY fine as corned powder, after which the sulphur ia sifted out. Soda Powdee. This powder is prepared with the same precaution as ordinary gun- powder, the proportions which answer hest being : Nitrate of soda . . . 630 parts. Sulphur 125 „ Charcoal 125 „ 880 parts. As the nitrate of soda is hygrometric, this powder must be preserved in close vessels from the moisture of the air. Lbad Powdek. This mixture is also pre- pared like gunpowder, and the constituents are used in the following proportions : Nitrate of lead ... 12 parts. Nitrate of potash ... 2 „ Charcoal 3 „ 17 parts. In the mnnufacture of this mixture on a large scale considerable care is necessary, since the mixture of nitrate of lead and charcoal is very liable to ignite by friction. Peepaeed Blood. 450 to 500 grammes of zinc is dissolved in 1340 grammes of hydro- chloric acid 22° B., largely diluted with water, and filtered. This solution is again diluted with its own volume of water, and mixed with fresh blood. The whole is well stirred from time to time for 48 hours, and the clear liquor is siphoned off from the precipitate. The pre- cipitate is well washed with water, dried, and reduced to powder, in which state it may be kept for any length of time. Touch Papeb. This paper is prepared by immersing purple or blue paper in a solution of nitrate of potash in spirits of wine or vin- egar, and carefully drying it. When the touch paper is used with small articles, a piece is tied round the orifice with thread, leaving sufficient paper to form a small tube at the end. This tube is filled with gun- powder, and the paper twisted over it, when all is ready for firing. Touch paper for cupping every description of fireworks, such as squibs, crackers, Roman candles, &c., is prepared in the following manner : — Dissolve 2 oz. of the best saltpetre in 1 quart of warm water, and take care that the water is very clean. After the irtixture has stood for half an hour, pour off li pint into a white basin, then cut your sheets of dark blue double-crown paper in half. The weight of the paper should be 12 or 14 lbs. per ream. Place the paper on a sliib sufficiently large to give you room to use a small piece of sponge, with which you use the liquor to wet your paper. Cover each half sheet with the liquor as quickly as possible, on one side only, and immediately this is done place it on aline. the wet side on outwards, and when nearly dry, if you have a great number of sheets, place them together as evenly as possible under a press for one hour, then lay them out to dry, after which they will be quite smooth and ready for use. In pasting this paper on the work, take care that the paste does not touch that part which is to burn. To use this paper correctly, cut it in strips sufficiently long to go twice round the mouth of the case, or even more if requisite. When you paste on the strips, leave a little above the mouth of the case not pasted ; in small cases a little meal powder is put into the mouth, and then the paper is twisted to a point. In larger cases damp priming is used, and when dry, the capping process is proceeded with. Cbackees. The following mixtures are used for ordinary crackers : — Meal powder . parts 5 15 6 8 16 Fine charcoal 1 4 - 2 17 Coarse charcoal - - 6 - - Sulphur . . „ - - 2 - 1 Saltpetre . . . „ - - 16 1 7 Composition for crackers with Chinese fire- Meal powder parts . . 9 6 16 Saltpetre „ . . . 6 8 - Sulphur ,,...123 Charcoal „ . . . li U 2 Fine iron „ ... 5 - 7 Sand . . „ . . . - 5 - Composition for crackers with brilliant fire — Meal powder . parts 8 8 36 18 32 Sulphur . . „ 1 U 1 1 3 Iron filings . . „ 2 2i - - Litharge . . „ _ _ _ 2 - Steel filings . . „ - - 8 3 12 The paper generally used for cartridge is that known as ' elephant ' or cartridge, the latter being the more frequently employed. Cartridge paper is employed in the prepa- ration of crackers, which vary from 12 to 15 inches, and 3J inches diameter. One edge of the paper is folded down about |-inch in breadth, then the double edge is turned down about i-inch, and the single edge is bent back over the double fold so as to form a channel 4-inch wide. This is filled with meal powder, which is then to be covered by the folds on each side, when the whole is to be pressed very smooth and close, by passing it over the edge of a flat ruler. The part containing the powder is to be gradually folded into the remainder of the paper, each fold being care- fully pressed down. The cracker is then doubled backwards and forwards into as many folds of about 2^ inches as the paper will allow. The whole is pressed together by means of a wooden vice, a piece of twine is passed twice round the middle across the folds, and the joinings are secured by causing the twine to PYEOTECHNY 1403 take a turn round the middle nt every turn. One of the ends of the folds may be doubled short under, which will produce an extra report, but the other must project a little bi'jorul tlie rest, for the priming and capping with the touch paper. When these crackers are fired they give a report at every turn of the paper. The crackers may also be made of two single cards, rolled over each other and covered with paper coated with paste. The crackers are partially filled with the composition by means of a tin funnel. Ordinary powder is then iutroduceil, nnd the remaining space is filled with a little sawdust. Kkvolvino Cbackebs. These crackers are charged at each end with clay to a depth of two lines, and filled with a composition with- out gunpowder. The clay prevents the fire streaming out at the ends, and it escapes through two holes placed opposite each other. The two holes arc united at the same time by connecting them by means of a quick-match, and a rotxtory motion is thus communicated to the cylinder. English Pin Wheels. Pin, or Catherine wheels are of very simple construction. A long wire about i\th of an inch in diameter is the former ; on this wire are formed the pipes, which being filled with composition, are afterwards wound round a small circle of wood so as to form a helix or spiral line. The cases are generally made of double-crown paper (yellow wove), and cut into strips to give the greatest length, and of width sufficient to roll aliout four times round the wire, and pasted at the edge so as to hite firmly at the end of the last turn. When a number of pipes are made and perfectly dry, they are filled with compo- sition. These cases are not driven for filling, hut are filled by means of a tin funnel with a tube } of an inch long, made to pass easily into the mouth of the case, which is gradually filled by lilting a wire up and down in this tube, the diameter of the charging wire being half that of the tube. The dry composition being placed in the funnel, the moment an action of the wire takes place the composition begins to fall into the case, which the charging wire compresses by continuous motion until you have filled the pipe to within | of an inch of the top. The pipe is then removed, and the mouth neatly twisted, which will be the point for lighting. When a number of pipes are ready, place them on a diunp floor, or in any damp situa- tion, until they become very pliant, but by no means wet; then commence winding them round a circle uf wood whose substance must be equal to the thickness of the diameter of the pipe; and when wound, secnre the end with sealing-wax, to prevent its springing open ; after winding the required quantity let them dry. Now cut some strips of crimson or purple paper -,Sjth of an inch wide, and in length twice the diameter of the wheel ; then paste all over thoroughly. Take a strip and paste it across the wheel diametrically, rnb it down, then turn the wheel over, and place the ends down to correspond with the opposite side ; when dry, the wheel will be ready for firing. They may be fired on a large pin or held in tlie hand, but it is preferable to drive the pin into the end of a stick, which will prevent any acciilent. shonld a section of the wheel burst. Squibs. These are either filled with grained powder, or with a mixture consisting of: — (ianpowder, 8 parts ; charcoal, 1 part ; sul- phur, 1 part. The cases, which are about 6 inches long, are made by rolling strips of stout cartridge paper three times round a roller, and pasting the last fold. They are then firmly tied down near the bottom, and the end is either dipped into hot pitch or covered with sealing-wax. The cases are filled by putting a thimble full of the powder in, and ramming it tightly down with a roller, this operation being cnntinued until the case is filled. It is then capped with touch paper. Serpents (Makboon Squibs). A suitable cise being ready, it is filled two thirds up with a powder consisting of : — Saltpetre, 16 parts ; sulphur, 8 parts ; fine gunpowder, 4 parts ; antimony, 1 part. This, after being rammed down into the case tolerably tightly, the remainder of the space is filled with grained or corned powder. Spaeks. These fireworks differs from stars in size, being very small and made without cases. The English method of preparing them is as follows : — A mixture of Fine gunpowder . . 1 part Powdered saltpetre . 3 parts Powdered camphor. . 4 „ is placed in a mortar, and some weak gum- water in which a little gum tragacanth has been dissolved, is poured over it, and the whole worked up into a thin paste. Some lint, pre- pared by boiling it in vinegar or saltpetre, and afterwards dried and unravelled, is placed in the composition so as to absorb the whole. This is then poured into balls about the size of a pea, dried and sprinkled with fine gun- powder. In Germany the following compositions are used: 1404 PYROTECHNY Chlorate of potash , parts Chlorate of potash and copper . „ Chlorate of barjta . „ Nitrate of potash . „ Nitrate of lead . . „ Nitrate of bary ta . „ Calomel . . „ Sulphide of copper . . „ Sulphate of strontia . „ Oxaliite of soda . . „ Chalk . . „ Powdered zinc . . „ Powd ered charcoal . „ Sulphur . „ Gum lac . „ Soap . . . „ Starch . . „ Sugar . . „ Piue soot . „ 1 24 24 12 1 2 40 16 8 3 3 12 10 1 1 4 20 40 13 13 1 5 18 7 3 6 12 14 5 7 26 28 11 8 40 28 28 3 10 9 21 23 12 3 4 10 21 23 12 12 3 4 31 14 4 6 5 6 12 20 8 4 20 3 2 13 96 18 72 18 1 14 40 37 8 The above mixtures are Intended to give coloured sparks, according to the numbers. No. 1 gives a bluish-white colour. 2 and 3 give yellow. 4 gives green. 5 gives green. 6, 7, 8, 9 and 10 give blue. 11 and 12 give violet. 13 gives red. 14 gives purple. The materials are mixed with a small quan- tity of" a solution of starcb, so as to form a thick paste, which is forced through a per- forated plate, the holes in which are twice as large as it is intended the sparks should be on drying. The small pieces fall on a paste- board, to which the workman gives a rupid horizontal motion to round the grains. They are then dried, and those which are perfectly round are selected and separated by sieves of different meshes to collect those of the same size together. Chinese Piee. Sed Chinese or Oerbe Fire. Calibre of the case. 12 to 16 lbs. 16 to 22 „ 22 to 36 „ Saltpetre lib. 1 ,. 1 ,. Sulphur. 3 oz. 3 „ 4 „ White Chinese Fire. Charcoal. 4 OZ. 5 „ 6.. Iron Sand. Ist order. 7 OZ. 7 „ 8 drms 8 „ Calibre. 12 to 16 lbs. 16 to 22 „ 22 to 36 „ Saltpetre. lib. 1 ., 1 ., Bruised Powder. 12 OZ. 11 ,. 11 ,. 7 8 8 Charcoal, OZ. 8 drms. ", 8 „ Iron Sand. 3rd order, 11 OZ. 11 „ 8 drms. 12 „ The iron sand is moistened with n little spirits of wine, and then mixed with the char- coal and saltpetie, which have been previously incorporated in another mortar. Simple Stabs ob Fieeballs. These are generally used in combination with other arrangements, &c., and the composition of which they are made, consists of — saltpetre. PYEOXYLIC SPIRIT— PYROXYLIN. 1405 16 pnrta i Bulplitir, 8 purts ; fine gunpowder, 3 purU. Tlu" Vol. 1, pan 4, No. 1. Ballifere & Co. Saltpetre iSul|)hur Fine small coals Fine gunpowder Coarse cast iron parts Cninpositiou for inimeUmte use. 4 2 1 8 4 plosive compound, discovered by SchOnbein. It is obtained by the action of nitric acid on cotton (cellulin, CjHjqOj), in the presence of sulphuric acid. By varying the strength of the nitric acid three kinds of gun-cotton may be obtained, called respectively mononitro-cellulin [CjH^ (N0j)05], dinitro-cellulin rC'eHsliNO.loO,], and triuitro-cellulin [t'6H;(NO2)305j. 'flie first is but slightly explosive ; the second is not suffi- ciently explosive to be used us a substitute for gunpowder, but is best adapted for the pre- paration of collodion ; the third is highly ex- plosive, and is the variety employed in mining and military operations, Slc. Prep. 1. (B. P., DlNlTBO-CELLtTLIN.) Cot- ton-wool, 1 ; sulphuric acid, 5 ; nitric acid, 5 ; mix the acids, immerse the cotton, ;ind stir with a glass rod for three minutes, or until it is thoroughly wetted, then remove it, and thoroughly wash out the acid, so that the wash- ings cease to produce a precipitate with chlo- ride of barium. Drain on filtering paper, and dry in a water bath. Used in the prcparatiou of Collodion. 2. Concentrated nitric acid (sp. gr. I'BOO) and concentrated sulphuric acid (sp. gr. 1845) are mixed together in about equal measures; when the mixture has become cold it is poured into a glass or wedgwood-ware mortar or basin, and clean, dry caTded cotton, in as loose a state as practicable, is immersed in it for 4 or 5 minutes, the action of the liquid being promoted by incessant stirring with a glass rod ; the acid is next poured off, and the cotton, after being squeezed as dry as possible, by means of the glass stirrer, or between two plates of glass, is thrown into a brge quantity of clean soft water, and again squeezed to free it from superfluous moisture ; it is then washed in a stream of pure water until it becomes perfectly free from acid, and is, lastly, carefully dried by the heat of hot water or steam, at a temperature not higher than about 180° Fahr. 1406 QUACK MEDICINES— QUARANTINE 3. (Sehonbein.) Nitric acid (1-45 to 1-50), 1 part; sulphuric acid (1'85), 3 parts (both by volume) ; proceed as above, but, after the cotton has been squeezed from the acid, allow it to remain in a covered vessel for an hour before washing it, and after washing it, dip it into a solution of carbonate of potassa, 1 oz., in pure water, 1 gall., then squeeze, and par- tially dry it ; next dip it into a weak solution of nitre, and dry it in a room heated by hot air or steam to about 150° Fahr. (See Patent Specif.) 4. (Von Lenk.) The cotton, having been thoroughly cleansed and dried, is steeped, as above, in a mixture of nitrieand sulphuric acids (thestrongest obtainable in coiiiinerce),8queezed as dry as possible, and immersed in a fresh mixture of strong acids, being allowed to re- main in this second mixture 48 hours. It is then washed in a stream of water for several weeks, and finally treated with a solution of silicate of potassa (soluble glass). This is the celebrated Austrian gun-cotton which was reported on so favorably by a committee of the British Association in 1863. The treat- ment with silicate of potassa is adopted merely for the purpose of retHrding the combustion. 5. (' Bulletin de St Petersbourg.')— a. Take of powdered nitre, 20 parts; sulphuric acid (1"830 to 1'835), 31 parts ; dissolve in a glass vessel, and, whilst the solution is still warm (122° Fahr.), add of dry carded cotton 1 part, and employ agitation until this last is well saturated ; then cover over the vessel with a plate of glass, and let it stand, for 24 hours, at a temperature of about 86° Fahr. ; next well wash the cotton, as above, first with cold and afterwards with boiling water, and dry it care- fully at a very low temperature. b. From sulphuric acid (containing 3 equiv. of water), 13 parts ; nitric acid (monohjdrated), 12 parts ; carded cotton, 1 part ; the immer- sion being limited to one hour at a temperature of from 104° to 122° Fahr. (See 'Pharm. Journ.,' vol. xiii. No. 2.) Prop., Sec. Pyroxylin explodes, with a very sudden flash, and the development of very little heat, without either smoke or residue, at a temperature of about 300° Fahr. (No. 3 at 277° Fahr.). Several modifications of pyroxy- lin are known, varying considerably in compo- sition, though they all contain the elements of hyponitric acid, and are all explosive. Some are insoluble in a mixture of ether and alcohol, whilst others are readily dissolved, forming the glutinous solution which is used in surgery under the name of ' collodion,' and which is also extensively used in photography. The best gun-cotton (Von Lenk's) is of no use whatever for making collodion. The pyroxylin prepared by the formula 5, a (above), is soluble in a mixture of 7 parts of ether aud 1 part of alcohol; whilst the product of 5, b, if pre- pared by 2 hours' digestion instead of 1, is said to be even soluble in absolute alcohol. Ois. General von Lenk has overcome all the difficulties which have hitherto prevented gun-cotton being used in place of gunpowder. By spinning the gun-cotton into thread or yarn, and weaving this into webs, he has suc- ceeded in making cartridges which will pro- duce the exact amount of force required. The time needed for the complete ignition of tlie cartridge can be diminished or increased at pleasure by varying the mechanical arrange- ment of the spun threads. Each gun and each kind of projectile requires a certain density of cartridge. In general, it is found that the proportion of 11 lbs. of gun-cotton occupying 1 cubic foot of space produces a greater force than gunpowder of which from 50 to 60 lbs. occupies the same space, and a force of the nature required for ordinary artillery. See Collodion and Xtloidin ; consult also Abel's researches in the ' Transactions of the Royal Society.* aUACK MED'ICINES. See Patent medi- cines. Ointment, Pills, &c. QUAIL. The Coturnix vulgaris, a gallina- ceous bird, allied to the partridge, but of smaller size. Its flesh is highly esteemed by epicure'. It is imported from Turkey, pre- served in oil ; and from Italy, potted with clarified butter. aUARANTINE. The old laws of Quaran- tine, as the French derivation of the word indicates, compelled a vessel coming from the shores of a country liable to, or ravaged by, an infectious disease, such as plague, to those of a region free from contagion, to undergo forty days' isolation before it was unladen, or its passengers were allowed to land at the healthy port. In Europe these ancient enactments against the importation of infection are still more or less vexatiously enforced in Spain, Portugal, Greece and Turkey; and in amodifit-d format Malta and some of the French and Italian ports. In the Mediterranean ports, ships coming from countries which lie in the southern or eastern shores of that sea are usually subjected to a quarantine of from six to fifteen days, during which period the pas- seuL'ers are confined in a sort of barrack called a ' lazaretto,' the merchandise, letters, &c., of the vessel being in the meantime fre- quenily fumigated, or otherwise disinfected. The inconveniences to commerce and the neces.'ary intercourse between nations attend- ing the too rigorous carrying out of quaran- tine have, within the last twelve years, led to a series of sanitary international conferences between the European Government.s with the object of divising some methods which, with- out weakening the safeguards to the public liealih, should as much as possible reduce tlie inoonveniences attending tlie enforcement of quarantine to a minimum. At tlie last o' tbese conferences, which was held at Vienna in 1873, the members were almost uiianiinous in advis- QCAKTAN— QUASSU 1407 iiig thu ahiilition of quarantine on European rivers. Until within the last twenty years tlie old quarantino lawa were pretty strictly enforced in this cimiitry. Since this time, however, they have been considerably relaxed, or, we should rather 8l, as the case may be. See Assaying. QUARTZ. Pure native silica. It is an es- sential constituent of granit3 and many other rocks. Its crystalline, transparent varieties, are known as rock crystal. See Glass, Pow- D£B, &c. QUAS8. St/n. PoscA tenalis. L. Prep. Mix rye-flour and warm water together, and keep the mixture by the fireside until it has turned sour. Used as vinegar in Russia. aUAS'SIA. St/n. Quassia (Ph. L., E., & D. ; Quassia lignum. Quassia wood, B. P). The " wood of Picrcena (Piorasma) excelsa, Liiidl." (B. P., Ph. L.), or Jamaica quassia; and also of the " Quassia amara, Linn." (Ph. E.), or Surinam quassia. The latter is the original quassia, but it is no longer imported. Quassia is characterised by its intense bitter- ness. It is reputed tonic and stomachic, assistini; digestion, and giving tone and vigour to the system. Its name was given to it by Linnajus, in honour of a negro slave who had long employed it as a remeily for the malig- nant endemic fevers of Surinam. When sliced. 140S QUASSIN— QUILLS it forms the ' quassia chips' of the shops. It is generally taken in the form of infusion. This last, sweetened with sugar, forms a safe and effective poison for flies. — Dose (in pow- der), 10 to 20 gr. Roasted quassia, reduced to powder, is largely employed, instead of hops, to embitter porter; and the unroasted powder is used foi' the same purpose in the adulteration of the bitter varieties of ale. ' ftUAS'Sm. Syn. Qttassitb, Qitassina. A peculiar bitter principle, obtained by precipi- tating decoction of quassia with milk of lime, evaporating the (iltrate, dissolving the residue in alcohol, treating with animal charcoal, again evaporatino:, dissolving in water, and crystallising. 8 lbs. of quassia chips yield 1 drachm. QUEEN'S BLUE. Thumb blue. See Blue. QUEEN'S MET'AL. A species of pewter used for teapots, &c., made by fusing under charcoal a mixture of tin, 9 parts, and anti- mony, bismuth, and lead, of each 1 part ; or, tin, 100 parts ; antimony, 8 parts; copper, 4 parts ; bismuth, 1 part. See Beitannia Metal and Pewteb. QUEEN'S YEL'IOW. Subsulphate of mer- cury. QUEECITEIN. The bark of the Quercus tincioria yields a neutral substance, to which the above name has been given. Quercitrin may be prepared as follows by the process of Kochleder: — The bark is boiled with water, the decoction is left to cool, and tiie impure quercitrin which separates is collected, then rubbed to a pulp with alcohol of 35° B., heated over the water bath, collected on linen, and pressed, whereby the principal impurities are removed. The residue is dissolved in a larger quantity of boiling alcohol, the solution is fil- tered hot, and wacer is added to it until it becomes turbid, so that the greater part of the quercitrin separates before the liquid is cold. It is then collected, pressed, and purified by a repetition of the same treatment. Another process, by Zwenger and Dronke, is this: — The bark, in small pieces, is ex- it lUsted with boiling alcohol, the alcohol is distilled off, and the residue, while still warm, is mixed with a little acetic acid, and then with neutral acetate of lead ; the filtrate, freed from lead by sulphuric acid, is evaporated, and the quercitrin which crystallises is purified by repeated crystallisation from alcohol. " Hydrated quercitrin forms microscopic, rectangular, partly rhombic tablets, having their obtuse lateral edges truncated ; pale yellow when pulverised. It is neutral, inodo- rous, tasteless in the solid state, bitter in solu- tion, permanent iu the air."^ QUEE'CITRON. The bark of Quercus nigra or tinctoria, a species of oak indigenous in North America. With alum mordants it yields a very permanent yellow dve. QUEE'CITRON. A yellow dye stuff, com- > Watts. posed of the shavings and powder of the bark of Quercus tinctoria, or Q. nigra, or Q. ci- trina, a kind of oak, a native of North America. It abounds more particularly in Pennsylvania, Carolina, and Georgia. In America quercitron is used for tanning, and in Europe for dyeing only. When em- ployed for the latter purpose it is used in the form of an aqueous decoction, mordanted with alum or chloride of tin. Leesching states that a dye possessing greater colorific powder may be procured by boiling the bark with dilute sulphuric or hydrochloric acid. QUICK'SILVEE. See Mebcuet. QUILLAI BA£K. Syn. Quillat baek. Soap babe. The Qnillaya saponaria, from which yields this bark, is an evergreen tree, growing in the mountainous parts of Chili, in South America. It is believed to take its name from the native word quillay, which signifies to wash. The inner bark only is employed. When bruised and agitated in water it imparts a lather to the water, in the same way that soap does. This quality has been found to be due to the existence in the bark of saponin — the same principle which confers a similar pro- perty on Saponaria officinalis. The bark is free from any bitter principle, as well as from tannic acid. It is very generally used amongst the inhabitants residing on the western sideof South America, where it is employed for re- moving grease from silk, and also in the form of a wash for cleansing and preserving the hair. When had recourse to for cleansing silks, quillai bark is said not to change the colour of the fabric. It is sometimes given as a febri- fuge, and as u remedy for cold in the head. For this latter purpose the powder is snuffed up the nostrils, when it occasions sneezing and profuse discharge from the nose. QUILLS. Prep. 1. The quills or wing- feathers of the goose (goose quills) are se- parately plunged, for a few seconds, into liot ashes, cinders, or sand, of a temperature about equal to that of boiling water, after which they are scraped with a blunt knife, strongly rubbed with a piece of flannel or woollen cloth, and gently ' stoved ;' they are, lastly, tied up in bundles by women or children. A yellow tinge is often given to them by dipping them for a short time into dilute hydrochloric or nitric acid, or into an infusion of turmeric. 2. Suspend the quills in a copper over water sufficiently high to nearly touch the nibs ; then close it steam tight, and apply three or four hours' hard boiling ; next, withdraw the quills, and dry them, and in 24 hours cut the nibs and draw out the pith ; lastly, rub them with a piece of cloth, and expose them to a moderate heat in an oven or stove. Quills prepared in this way are as hard as bone, with- out being brittle, and nearly as transparent as glass. Crow quills and swan quills may be cured in the same manniT. QUINA-QUINIDINE 1409 QOITTA. See QtriNiKB. NjOj. Tliis alkaloid was discovered by Hesse, in 1872, in the b«rk of Cinchona tuccirubra, cultivated at Oarjiliiig, in British Sikbiin. Dr de Viij gives the following process for the prepiiration of qiilnamine: — The mixed alkaliiiils obtniued from tlie red b;irk are converted into nintral sulphates, and tue solu- tion treated with Rochelle salt, whereby the tartrates of quinine and of cinchonidine are separated. After collecting these upon a filter the filtered liquid is shaken with caustic soda and ether. By this process tlie amorphous alkaloid and the quinaoiino are dissolved by the ether, with slisfht traces of cinchonine, whilst the bulk of this last alkaloid remains undissolved. After distilling the ethereal solution the residue is transformed into neu- tral acetate, and the solution of this mixed with n solution of sulphocyanate of potas- sium. By this reaction the sulphocyanate of the ninorphous alkaloid is precipitated in the i'h:ipe of a yellow, soft, resinous substance, whilst the sulphocyanate of quinamine re- mains dissolved. After subsiding and filter- ing, the solution is clear and quite colourless, and by addition of caustic soda the quinamine is precipitated. It is then collected upon a lilter, washed, and dried. It can now easily bo obtained crystallised by dissolving it in boiling spirit, from which it crystallises in cooling. By this process the author obtained 0'38 per cent, of pure quinamine from sam- ples of red cinchona quill bark, which be liad received, through the Secretary of State for India, from the plantations in British Sikhim. QUINCE. Syn. Ctdonia, L. The fruit of Cydonia vulgaris, or common quince tree. Its fliivour in the raw state is austere, but it forms an excellent marmalade (quince marma- lade), and its juice yields an agreeable and wholesome wine. The seed or pips (cydonia seminee; cydoninm — Ph. L.) abound in gummy matter, which forms a mucilage with water, and possesses the advantage of not being af- fected by the salts of iron or alcohol. See Dkcoction, Fixatubb, and Jellt. QUINETUn. The alkaloids contained in the East Indian red bark (Cinchona sued- rubra) consist of a large percentage of cin- chonidine, cinchonine, quinine, and amorphous alkali>id, besides a trace of quinidine, tlie pre- ponderating alkaloid being cinchonidine. Dr de Vrij, of the Hague, has devised a process by which these can be extracted in their entirety, and to the mixed alkaloids so obtained the name 'quinetum' has been given. It is affirmed of qninetum that it possesses a remedial value as a tonic and antiperiodic that renders it, in niony cases, superior to quinine, ague being one of these ; also that it may be advantigenusly employed in affections VOL. II. in which quinine wonld be inadmissible. A medical correspondent informs us that he has used it with signal success in *hay asthma. Another advantage it has over quinine is, it is much lower in price. Quinetum, according to Dr de Vrij's process, as well as a sulphate and hydrochlorate, are prepared by Mr Whiflen, of Battersea. aUINICINE. An altaloid obtained in 1853 by Pasteur, by exposing quinine or quinidine, under lavorable circumstances, to a tempera- ture varying from 248° to 266° Fahr., for several hours. It is very probable that this alkaloid is either identical, or in very close connection, with the amorphous alkaloid solu- ble in ether which occurs in all barks, and particularly in the young barks of the planta- tions in India. aUINIDINE. C.j„Hj<0jN„.2Aq. %». Qui- NIDIA, CONCHIKINB, &c. An alkal.iid con- tained in many species of cinchona, together with quinine and cinchonine, and therefore often found in the mother liquors of quinine manufactures. It is identical with the /3 quinine of Van Heyningen, and was dis- covered, in 1833, by Henry and Delondre. As the cinchonidine discovered by Winckler, in 1818, has been unhappily denominated quinidine by this chemist, there is still a con- fusion about these alkaloids, and, therefore, the quinidine of commerce was very often a mixture of both, till Pasteur made, in 1853, u classical investigation of this matter. He main- tained the name of quinidine for the alkaloid discovered by Heurv and Delondre, because it is isomeric with quinine, and gives the same green colour when treated with chlorine fol- lowed by ammonia, and gave the name of cinchonidine to the alkaloid discovered by Winckler, because it is isomeric with cin- chonine. He determined also the action of the solutions of these alkaloids on the plane of polarisation, and found that the quinidine turned this plane to the right, its molecular rotation in' alcoholic solution being [o] = 250-75° ^ S-, whilst he found that the cinchonidine turned this plane to the left, its molecular rotation in alcoholic solution being [«] = 144-61°^ ^. Prop. ifc. Many of the salts of quinidine are 'very similar to those of quinine, but the normal salt with bydriodic acid is not only very different from that of quinine, but also from those of all the other cinchona-alkaloids. The normal hydriodate of quinidine is so very sparingly soluble in water that 1 part requires, at 60° Fahr., not less than 1200 parts of water to be dissolved. Therefore the presence of sulphate of quinidine in the sulphate of quinine, which often occurs, either from that article being carelessly made or from wilful adulteration, can be easily detected by adding a few minims of solution of iodide of potassium to the saturated solution of sulphate of quinine in water of 60° Fahr., whereby, if quinidine is present, its hydriodate will be separated either 89 14,10 QUININE in the shape of a sandy precipitate or, if only traces are present, in the shape of striajon the sides of the glass where this has been rubbed by a glass rod. For an account of its medicinal properties, the reader should consult the recent report from India upon the experiments made there by order of Government with all the four cinchona-alkaloids, which experiments are very favorable to the therapeutical action of quini- dine compared with that of quinine. QTIININE. CioHijON. Si/n. Qttina, Qtjinia. Till recently it was found in the greatest quantity in good Calisaya bark, parti- cularly in that from Bolivia, but since it has been found in great quantity in some other harks, especially in the bark of Cinchona offici- nalis, for instance, in the bark of that species grown in Ceylon. Red bark contains not only quinine and cinchonine, but also ciuchoni-. dine. Prep. 1. By precipitatini» a solution of sulphate of quinine with a slight exc&ssoi am- monia, potassa, or soda, and washing and dry- ing the precipitate. By solution in alcohol, sp. gr, 'SIS, and spontaneous evaporation, it may be procured in crystals. Crystals may also be obtained from " its solution in hot water with a little ammonia." (Liebig.) 2. (Direct.) By adding hydrate of lime, in slight excess, to a strong decoction of the (frouud bark made with water acidulated with sulphuric acid, washing the precipitate which ensues, and boiling it in alcohol ; the solution, filtered while hot, deposits the alkaloid on cooling. Prop., Sfc. Quinine, when prepared by pre- cipitation, is an amorphous white powder, but when this precipitate is left in the liquor it assumes, after some time, the appearance of aggregated crystalline needles ; when slowly crystallised from its solution, these needles are remarkably fine, and of a pearly or silky lustre. It is freely soluble in rectified spirit and in ether, and of all the cinchona-all^aloids it is the most soluble iu ammonia. It is upon this f actthat Kerner's method for testing the purity of sulphate of quinine is founded. Its normal salts, if dissolved iu water, have a slightly alkaline reaction upon red litmus paper. It is only sparingly soluble in water, even when boiling ; both the fixed and volatile oils dis- solve it with the aid of heat, more especially when it has been rendered anhydrous, or is presented to them under the form of an ethe- real solution. It fuses by a gentle heat, with- out decomposition ; forms erystallisable salts, which are only slightly soluble in water, unless it be acidulated, and, like the pure alkaloid, are extremely bitter, and possess much of the characteristic flavour of cinchona bark. It is precipitated by the alkalies and their carbo- nates, by tannic acid, and by most astringent substances. Pur. See Quinine, Sulphates or, and QuiNOMBTEr {below). Testa. Quinine is recognised by — 1. Its appearance under the microscope. — 2. Its solu- bility in ether, and in pure ammonia water. — 3. Its solubility in concentrated nitric acid, forming a colourless liquid, which does not become yellowish until it is heated.^4. The solubility of itself and salts, when pure, iu concentrated sulphuric acid, forming colourless fluids, " which do not acquire any coloration upon being heated to the point of incipient evaporation of the sulphuric acid, but which afterwards become yellow, and finally brown." (Fresenius.) — 5. Its solubility in concentrated sulphuric acid- to which some nitric acid has been added, forming a colourless, or, at the most, only a faintly yellowish liquid. — 6. It is wholly destroyed by heat. A solution of quinine in acidulated water, and solutions of its salts, exhibit the following reactions : — 1. Ammonia, potassa, and the al- kaline carbonates, give white, pulverulent pre- cipitates, becoming crystalline after some time (see above), and which are soluble iu ammonia in excess, and which, when ether is added after the ammonia, and the whole is agitated, redis- solve in the ether, whilst the clear liquid, on repose, presents two distinct layers. — 2. Bi- carbonate of soda (avoiding excess) gives a similar precipitate, both in acid and neutral solutions of quinine, either at once or after a short time. The precipitate is soluble in ex- cess of the precipitant, and is again precipi- tated from the new solution upon protracted ebullition. " Vigorous stirring of the liquid promotes the separation of this precipitate." (Fresenius.) — 3. If recently prepared chlorine be added to it, and then ammonia, a beautiful emerald-green colour is developed. (Ph. L.) — 4. A concentrated solution of ferrocyanide of potassium being added, in excess, after the chlorine, instead of the ammonia, a dark red colour is instantly produced, which after some time passes into green, especially when freely exposed to the light. This reaction is not cha- racteristic of quinine, for with quinidine one gets the same reaction. — 5. If caustic potassa be used instead of ammonia (see above), the solution acquires a sulphur-yellow colour. " These reactions are restricted to this alka- loid." (Dr Garrod.) Fliiekiger' says : — " The most characteristic test for ascertaining the presence of quinine is the formation of the splendid green com- pound called thalleiochine, which is produced if solutions of the alkaloid or its salts are mixed with chlorine water, and then a drop of ammonia added." If one part of quinine is dissolved in 4000 parts of acidulated water, and then about jL; of the volume of the liquid, of chlorine water, and a drop of ammonia added, a green zone will be readily formed if the liquids are cau- tiously placed in a flask without shaking. If the solution of quinine contain no more > In ■ Jahrb. f. Pliarm.,' A.prU, 1872, 136 (' Ph. Journal,' Srd series, li, 901). QUININE liU than rrfs-H' ^^° green of one mny still be obtained, but in more diluted golotioas the succe!}8 becomes more and more uucertaia. From a prncticHl point oTview we may state that u'sti of the alkaloid is the smallest quan- tity whose preseiue can thus be discovered with certainty; Kerner (1870) has succeeded *'"' soio!!' ''"* ^ """8 "o' "ble to corroborate this statement. The author was also induced to try the action of bromine in place of chlorine. The thalieiockine is then, indeed, produced in solution which contain only i^rJrni °^ quinine. Yet the behaviour of bromine displays some striking differences. Chlorine alone, as already stated, causes no immediate alteration of somewhat diluted solutions of quinine, whereas they became turbid on addition of bromine as long as there is about TtVn °^ more of quinine present. Now, the precipitate which is pro- duced by bromine in solution of quinine does not turn green if u little ammonia is subse- quently added, or, at least, the thalloiochine tlius obtained is rather gre.yish. But in more dilute solutions of quinine bromine acts more readily than chlorine. An excess of bromine-is to be carefully avoided. This is easily performed if the vapour of bromine, not the liquid bromine itself, is allowed to fall down on the surface of the solutions of quinine ; their superficial layer only must be saturated with bromine by gently moving the liquid. Then a drop of ammonia will produce the green or somewhat bluish zone, which is much more persisteut than that due to chlorine. Consequently, for demonstration of the test under notice, chlorine is to be used in com- paratively concentrated solutions. In solu- tions contnining so little quinine (less than T^^ that it is no longer precipitated by the vapour of bromine, the thalleiochine test suc- ceeds much better with bromine, and goes much further, as shown above. The author also shows that morphine gives n dark, dingy brown colour with chlorine and aiumouia, which is capable of more or less uiaiking the reaction of quinine. Another test for quinine is the formation of its iodosulphate, the so-called herapathite. Kor this purpose the quinine is dissolved in 10 parts of proof spirit, acidulated with ^jjth part of sulphuric acid, and to this solution an alcubolic solution of iodine is carefully added, and the liquid in the meanwhile stirred with a glass rod. There appears either imme- diately or after some minutes a black precipi- fctte of iodosulphate of quinine, which if redis- solved in boiling proof spirit, forms in cooling the beautiful crystals of herapathite. 100 parts of this herapatliite, if dried on a water bath, repnseut 56'5 parts of pure quinine. Dr de Vrij prefers the employment of the iodosulphate of chiniodineasa reagent for the detection and estimation of quinine. In a comiouuioation to the ' Pharmaceutical Jour- nal ' he writes :' — " In estimating quinine in a "iixture of cinchona-alkaloids by means of an alcoholic solution of iodine the reagent re- quires to be added in slight excess, in order to ensure complete precipitation. An undue excess of the reagent, however, causes the for- mation of a compound richer in iodine and much more soluble in alcohol than herapathite, and thus renders the determination inaccu- rate." For this reason the author suggests the application of an alcoholic solution of iodosulphate of ehiniodine (so-called sulphate of nmorphons quinine) in place of free iodine. The reagent is made as following: — Two parts of sulphate of ehiniodine are dissolved in eight parts of water containing 5 per cent, of sulphuric acid. To this cl«ar solution, contained in a large capsule, a solu- tion of one part of iodine and two parts of iodide of potassium, in 100 parts of water, is slowly added with continuous stirring, so that no part of the solution of ehiniodine comes into contact with excess of iodine. By this addition an orange - cobmred flucculent precipitate is formed of iodosulphate of chin- iodine, which either spontaneously, or by a slight elevation of temperature, collapses into a dark brown, red-coloured, resinous sub- stance, whilst the supernatant liquor becomes clear and slightly yellow coloured. This liquor is poured otf, and the resinous substance is washed by heating it on a water bath with distilled water. After washing, the resinous substance is heated on the water bath till all the water has been evaporated. It is then !-oft and tenacious at the temperature of boiling water, but becomes hard and brittle after cooling. One part of this substance is now treated with 6 parts of alcohol of 92 or 94 per cent, until it is completely dissolved,, and the solu.tion allowed to cool. In cooling a part of the dissolved substiince is separated. The clear dark-coloured solution is evaporated on a water bath, and the residue dis^olveJ in & parts of cold alcohol. This second solution leaves a small part of iu>oluble substance. The clear dark-coloured solutiou obtained by the separation of this insoluble matter, either by decantation or filtration, constitutes the reagent which the author has used for some time under the name of iodosulphate of chin- iodine, both for the qualitaliie and quantita- tive determination of crystalluable quinine. To determine a quantity of quinine contained in the mixed alkaloids obtained from a sample cif cinchona bark, 1 part of the alkaloid is dis- solved in 20 parts of alcohol, of 90 or 92 per cent., containing 16 per cent, of snlphuric acid, to obtain an alcoholic solution of the acid sulphates of tbe alkaloids. From this solution the quinine is separated by adding carefully, by means of a pipette, the above-mentioned solution of tbe iodosul- phate of ehiniodine, as long as a dark brown- red precipitate of iodosulphate of quinine- ^ 3rd series, vi, 461. 1412 QUININE lierapathite is formedi As soon as all the quinine has been precipitated, and a slight excess of the reagent has been added, the liquor acquires an intense yellow colour. The beaker containing the liquor with the pre- cipitate is now covered by a watch-glass, and heated on a water bath till the liquid begins to boil. After cooling, the beaker is weighed, to ascertain the amount of liquid which is necessary in order to be able to apply later the above-mentioned correction. For although quinine-herapathite is very little soluble In alcohol, it is not insoluble, and therefore a correction must be applied for the quantity which has been dissolved both by the alcohol used for the solution of the alkaloids and the alcohol contained in the reagents. The liquor is now filtered to collect the iodosulpbate of quinine on a small filter, where it is washed with a saturated solution of herapathite in alcohol. After the washing has been completed, the weight of the funnel with the moist filter is taken, and the filter allowed to dry in the funnel. As soon as it is dry the weight is taken again, to ascertain the amount of solution of herapathite which remained in the filter, and which left the dissolved herapathite on the filter after the evaporation of the alcohol. This amount is subtracted from the total amount of liquid, and for the remaining the correction is calculated with reference to the temperature of the laboratory during the time of the analysis. The dry iodosulpbate of quinine is taken from tlie filter and dried on a water bath, in one of a couple of large watch-glasses closing tightly upon each other, so that the weight of the substance contained in the glass may be taken without the access of air. When, after repeatedly ascertaining the weight, it remains constant, this weight is noted down, and to it is added the product of the calculated correction. The sum of this addition is 'the total amount of iodosulphate of quinine obtained from the mix6d alkaloids subjected to the operation, and from this weight the amount of crystallisable quinine can be calculated by the use of Hauer's for- mula, 2C4„H24N2043 (HO1SO3), 31 (old nota- tion), ^hich the author has found to be correct. According to this formula, 1 part of iodosulphate of quinine, dried at 100° C, represents 0'5509 per cent, of anhydrous quinine, or 0'7345 per cent, of disulphate of quinine. The accuracy of this determination may be seen from the following examples : 0*24 gram of anhydrous crystallised quinine gave 0'541 gram of herapathite dried at 100° C.=0'298 gram of quinine. According to Hauer's formula, 0'5336 gram of herapathite = 0'294 gram of quinine, which ought to have been obtained. 1'048 gram of bitartrate of quinine gave 1-224 gram of herapathite =0674 gram of quinine. According to the formula of the bitartrate, Ca,H34N202iC4H(iO, + Aq. = 442 ; 1048 of bitar- trate represents 0'69 of quinine, so that 1'255 gram of herapathite should have been obtniued. Notwithstanding the different circumstances in which the reagent was applied, the results are satisfactory. The two following experiments were made with pure quinine, dried at 100° C, at which temperature it still retains water, under iden- tical circumstances : — 10664 gram of hydrated quinine gave 17266 gram of herapathite = 164'5 per cent. 1"055 grams of the same hydrated quinine gave 1'7343 gram of herapathite =164'3 per cent. The author further states that the iodosul- phate of quinine and of quinidine prepared by means of his new reagent have an analo- gous composition, and are identical with the compound described by Herapath, whilst the iodosulphates of cinchonine and cinchonidine have a different composition from the'former, and both require more iodine to be converted into the optical iodosulphates described by Herapath. Of all these iodosulphates that of quinine is by far the most insoluble in alcohol, and is precipitated first and free from the others by a j udicious application of the iodo- sulphate of chinioidine. Quinine is distinguished from both cincho- nine and quinidine by its comparatively free solubility in ether ; the last of these being very sparingly soluble, and the other wholly insoluble, in that menstruum. The presence of cinchonine may also be positively determined by reference to the behaviour of that alka- loid. Quinidine is also distinguished from qui- nine by the different crystallisation, greater specific gravity, and freer solubility of its salts in cold water.' Estim. See Quinometet. Uses, ^c. Pure quinine is but rarely used in medicine, but several of its salts are em- ployed as remedies, on account of theit great stimulant, tonic, and febrifuge powers. As a tonic in dyspeptic affections, and for restor- ing strength and vigour to morbidly weakened habits, and as an antiperiodic or agent to counteract febrile action, it appears to be supe- rior to all other remedies, provided no abnor- mal irritability of the mucous membranes, or of the circulatory organs, exists. The dose of the salts of quinine, as a tonic, is ^ to 1 gr., twice or thrice daily ; as an antiperiodic, 2 to 5 gr., or even more, every second or third hour, during the intervals of the paroxysms of ague, and of other intermittent or periodic ' An extremely elegant and highly sensitive method of testing for quinine and quinidine by means of the micro- scope, &c., is desoriljed at considerable length, by Dr Herapath, in tlie 'Pharm. Journ.* for November, 1853. QUININE 1413 iffectiona; also in acute rheumatUm. The eiilphute (disulpliate) is the suit gi-norally u^ed ; thin mid other salts are most effective when taken in solution. The nature of the influence exerted upon blood hy quinine was, In 1872, made the sub- ject of a fresh investigation by Schnlte.' Its extraordlniiry power of stopping fermentation and putrefaction, by destroying low organisms, such us bacteria and fungi, lias been before pniuted out. It is supposed to diminish the formation of pus in inflammation by arresting the motions and preventing the exit from the blood-vessels of the white blood-corpuscles, tbeaccuinulHtion of which, according to Cohn- heira, constitutes pus. By depriving the red blood-corpuscles of the power to produce ozone, it diminishes the chsnge of tissue in the body, and thereby lessens the production of heut. Kanke and Keriier have shown the waste of tissue is re- duced wlien large doses of quinine arc ad- ministered, as indicated in the sm.all propor- tion of uric acid and urea excreted. With the object of nsoertaining whether this effect is referable to the direct influence of quinine on oxidation in the blood, or to its indirect influence through the nervous system, Schulte employed a method, bapcd upon the chaiigfs occurring in the alkalinity of the blood, observed by Zuntz, who had noticed that a consideriible formation of acid takes place in freshly-drawn blood, and continues in a less decree till putrefaction commences. The amount of acid formed was estimated from the diminished alkalinity of the blood, as companitively shown by the quantity of dilute phosphoric acid required for exact saturation. k sutticient quantity of chloride of sodium Has sdded to the phosphoric add to prevent tlie blood-corpuscles from being dissolved, and intirferiiig with the reaction hy their colouring matter. The point of saturation » as fixed at the point of transient reddening of carefully pre- pared test paper by the carbonic acid. Schulte has thus been enabled to confirm the experi- ments of Zuntz and Scharrcnbroicb, showing that quinine and berberine lessen the produc- tion of acid, and that quinine can stop it both before and after coagulation ; that sodium nitropicrate has an action similar to, and nearly as powerful as, quinine; while the actiiin of ciiichonine is much less energetic. Harley has shown chat whilst quinine lessens oxidation in blood, some substances, such as snake poisons increase it. BInz found that when putrid fluids were injected into the circulation of an animal, the temperature rose ; but that this increase of temperature could be more or less prevented by the addition of quinine to the putrid liquid, or the simul- taneous inj< olion ol the qninine. With respect to the influences of quinine on ' 'N. Eop. PUarm,' xx. 539 ('Pliarm. Joam.,' 3rd senis. ii, 629). the change of tissne, Schnlte gives the result of some careful experiments made by Zuntz, who found that after taking three 0-6 gram doses of hydrochlorate of qninine for two days, the amount of urine he excreted was Increased by one third, and then deer, ased a* much, the specific gravity falling from 1018 to 1012 ; the urea also showed a marked de- crease. The salts of qninine maybe made by simply saturating the dilute acids with the base, so that part of the latter remains undissolved, and gently evaporating the solutions lor crys- tals, or to dryness. Prince Lucien Bonaparte recommends all these salts to be prepared by the addition of a strong alcoholic solution of quinine to a cold solution of the acid. We have tried this method with success. duinine, Ac'etate of. Sga. Qvmxi acetas, L. frep. 1. (P. Cod.) Mix quinine, 2 parts, with water, 3 parts ; heat the mixture, and add of acetic acid, q. s. to dissolve the alkaloid, and to render the solution slightly acid ; lastly, decanter filter the solution whilst boiling hot, and set it aside to crystallise. The mother water, on evaporation, will yield a second crop of the acetate. 2, Effloresced sulphate of quinine, 17 parts, is dissolved in boiling water, and mixed with crystallised acetate of soda, 6 parts. The metate oC quinine crystallises. Prop., S^c. Satiny, acicular crystals, which are rather more soluble in water than those of the sulphate. — Dose, i to 5 grains. Quinine, Ar8e"niate of. Syn. Quin£ aii- SENIAS, L. Prep, (Bouriferes.) Arsenic acid, li dr.; quinine, 5 dr.; distilled water, 6 fl. oz. ; boil them together in a covered glass vessel until the alkaloid is dissolved, then set the solution a-ide to crystallise. Uses, S(c. liecommended by Dr Neligan, and others, as being more powerfully antipe- riodic than the other preparations of quinine. — Dose,-^ to i gr., made into pills; in agues, neuralgia, &c. ; also in cancer. Quinine, Ar'senlte of. Syn. Qvivm aesenis, L. Prep. Sulphate of quinine, 100 parts, is dissolved in alcohol, 600 parts, and boiled with arsenious acid, 14 parts. The liquid is then filtered. The poisonous salt is deposited in the crystalline form as the liquid cools. Uses, 4"c. As the last. Quinine, Clilo"ride of. Hydrochlorate of quinine (see betoto). Qninine, Ci'trate of. Si/n. Quin.s; citeas, L. Prep. 1. By mixing a hot solution of sulphate of quinine with a like solution of citrate of soda. 2. From quinine and citric acid, as the acetate. Needle-shaped prisms. — jDo*e, ^c. As the sulphate or disulphate. Qninine, Disulphate of. Sulphate of quinine (see below), Qninine, Ferrocy'anide of. Sgn. Ctanide OP lEON AND QUININE ; QuUfa; HTDHOFEREO- CYAHAS, QniN.E FEBEO-PEUSSIAS, L. Prep. 1414 QUININE (P. Cod.) Sulphate of quinine, 100 parts ; ferrocyanide of potassium, 31 parts; distilled water, 2500 parts; boil for a few minutes, and, when cold, separate the impure salt which floats as an oily mass on the surface, wash it with a little cold water, and dissolve it in boiling alcohol j the solution will deposit crys- tals as it cools. Ohs. This compound is by some said to be the most ef&cacious of all the salts of quinia. Pelouze asserts that it is simply quinine mixed with some Prussian blue. — Ilose, 1 to 6gr. Quinine, FerrosnI'phate of. See Quinine AND Iron, Suiphatb oe (below). Qninine, Hydri'odate of. Syn. Iodide ov QiriNINE ; QUIN^ HTDKI0DA8, Q. lODIDTTM, L. Prep. 1. By adding, drop by drop, a concen- trated solnbion of iodide of potassium to a like solution of acid sulphate of quinine, and dry- ing the precipitate in the shade ; or heat the liqnid nearly to the boiling point, and allow it to crystallise. 2. (Pairish.) Effloresced sul[hat6 of quinine, 5 parts, dissolved in alcohol, and decomposed by an alcoholic solution of 3 parts ot iodide of potassium, precipitates sulphate of potassa, and yields, on cooling and evaporating, hydriodate of quinine in fine crystalline needles.' 3. (loDTiEETTBD — Bouchardat.) From an acid solution of quinia and a solution of iodide of iron containing a slight excess of iron, as No. 1. Oba. The above are reputed alterative, tonic, and antipeiiodic. — Dose, 1 to 4 gr. ; in obstinate intermittents, and in the scrofulous affections of debilitated subjects. Quinine, Hydrochlo"rate of. Syn. Chioeide OF QUININE, MdEIATE OE QUININEf ; QuiN^ HTDEOCHLOEAS, QUIN^ MUEIAS, L. Prep. 1. By neutralising dilute hydrochloric acid with the base, as above. 2. (Ph. Bor.) Chloride of barium, 5 dr. ; boiling water, 1 lb. ; dissolve, add, gradually, of sulphate of quinine, 2 oz. ; boil gently for a few minutes, filter the solution whilst hot, and set it aside that crystals may form. 3. (QuiNiE MUEIAS— Ph. D.) Dissolve chloride of barium, 123 gr., in distilled water, 2 fl. oz. ; add of sulphate of quinine, 1 oz., dis- solved in boiling water, IJ pint ; mix, evaporate the solution to one half, filter, and again eva- porate until spiculae begin to appear ; next allow the liquid to cool, collect the crystals, and dry them on bibulous paper. The mother liquor, by further concentration and cooling, will yield an additional product. Obs. Hydrochlorate of quinine occurs in snow-white groups of feathery crystals, of a mother-of-pearl lustre, which are more freely soluble than those of the disulphate. Quinine and Iodide of Iron. Syn. Quin.se: 1 *' 1 and 2 are not identical ; 1 is an acid salt which readily crystnilises, but 3 is a normal salt which I never saw crystttlhse, hut always like a fluid resin, quite amor- phous." — De Vrij. ET FEEEi lODiDTJM. (Bouchardat.) Prep. Pour a strong solution of acid sulphate of quinine into a fresh solution of iodide of iron ; collect the precipitate, dry it quickly by pressing it between blotting paper, and keep it from the air. Quinine, Ki'uate of. Syn. QuiNX KiNAa, L, Prep. By saturating a solution of kinlc acid with quinine, and purifying by crystallisation out of alcohol. The kinate of quinine is obtained in crystalline warts, soluble in 4 parts of water and 8 parts of alcohol. Quinine, Lac'tate of. Syn. QuiN.s; lacias, L. Prep. As the acetate or citeate. By spontaneous evaporation fine crystals may he obtained. Said to agree better with dyspeptic patients than the other salts of quinine. Quinine, Mn"riate of. Hydrochlorate of quinine (see above'). Quinine, ITeutral Hydiobromate of. Syn. QuiNiE HTDEOBEOMAS. (M. Boille.) This salt is prepared by double decomposition of bromide of barium and neutral sulphate of quinia, and is thus easily obtained pure and free from chloride, the great solubility of bromide of barium in alcohol facilitating the removal of any chloride which is insoluble. The two salts are dissolved separately in alcohol and the solutions filtered. The neutral sulphate of quinia solution is gradually added, in slight excess, to the bromide of barium solu- tion until a precipitate ceases to form. Thesolutions, diluted with water,are distilled to recover the alcohol, afterwards filtered to separate the sulphate of quinia which has been precipitated by tlie water, and then con- centrated sufficiently to induce rapid crystal- lisation. 'Ihe addition of water is indispen- sable for the concentration and crystallisation; the hydrobromate, being soluble in alcohol of all proportions, redissolves as the alcoholic liquor is concentrated. M. Boille claims for his neutral hydrobromate of quinine its much readier solubility over the ofiBcinal sulphate, as well as its superior richness in quinine. Quinine, Ni'trate of. Syn. Quin^ nitbas, L. Prep. As the htdeochlokate, substi- tuting ailute nitric acid, or nitrate of baryta (P. Cod.), for hydrochloric acid or chloride of barium. Quinine, Phos'phate of. Syn. QuiNa: phob- EDAS, li. As the acetate. Silky, needle- shaped crystals, with a pearly lustre. It has been highly recommended in intermittents, &c., associated with rickets and stomach affections. Quinine, Salicylate of. Syn. Quisa: saii- CYLAS. This may be made by mixing an alco- holic solution of quinine with an alcoholic solution of salicylic acid to complete satura- tion, and afterwards allowing the alcohol slowly to evaporate. Quinine, Sulphates of. The salt often called * disulphate of quinine' is now generally re- garded as the normal sulphate, while the solu- ble salt, often called the 'neutral sulphate' QUININE 1415 li congidcrcd to bo nn acid salt. This change in nomenclature resulta from doubling the atomic weight of the alkaloid quinine : — 1. Qolnine Acid, Sulphate of. {C^P^'Sfi^. HjS(\.7Aq.) Si/n. HOIPHATB OP QtllNINEt, NkPTEAL BCLPnATB OP QTIININEt, SOLUBLE 8. OP Q. ! QtnN.« BULPHAB S0LCDILI8, L. Prep. From sulphate of quinine, 1 oz., dissolved, by the aid of heat, in water, i pint, previously aiidulotcd with dilute sulphuric acid, 5 fl. dr. ; the solution affords crystals on cooling, and more on evaporation, 04*. This salt possesses tlie advantaerc of being soluble in about 10 parts of water at 60° Fahr; but it is seldom used in the crys- talline form; still, as the officinal sulphate (' disulphate') is generally prescribed along with a small quantity of dilute sulphuric acid to render it soluble, this acid sulphate is, in fact, the compound which is commonly given. It is the ' bisulphate,' 'supersulphate,' or 'acid sulphate of quina' of Soubeiran and other Continental chemists. 2. Quinine, Sulphate of. (C2oH24N20.j)j. 2H2S04.7Aq.) Si/n. NoEMAL bulphate OF QUININE, DlStTLPHATE OP Q., QUININE; QUIN^ DISULPnAB (Ph. L.), QUINZE SULPHAS (Ph. E., U., & U. S., ci; P. Cod.), QuiNiE sul- phas (B. P.), L. ; Sulphate bb quinine, Pr. Frep. 1. (Ph. L. 1836.) Take of yellow cin- chona biu'k, bruised, 7 lbs. ; snlphuric acid, 4i oz. ; (diluted with) water, 6 galls. ; boil them for 1 hour, and strain ; repeat this a second time for 1 hoxir, with a like quantity of acid and water, and again strain ; next boil the bark for 3 hours, in water, 8 galls., and strain ; wash the residue with fresh quantities of boiling dis- tilled water; to the mixed decoctions and wash, ings, add moist hydrated oxide of lead to saturation, decant the supcrnntant lluid, and wash the sediment with distilled water ; boil down the liquor for 15 minutes, and strain, then precipitate the quina with liqnor of am- monia and wash the precipitate (with very cold water) until nothing alkaline is percep- tible; saturate what remains with sulphuric acid, i oz., diluted with water, q. s., digest with animal charcoal, 2 oz., and strain ; lastly, the charcoal being well washed, evaporate the mixed liquors, that crystals may form. 2. (Ph. E.) This process varies from the last one, in the bark (1 lb.) being first boiled in water (4 pints) along with carbonate of soda (4oz.); the residuum, being pressed, is moist- ened with water, and again pressed, and this operation is repeated a second and a third time, the object being to remove, as much as possible, the acids, coluuring matter, gum, and extractive, before proceeding to extract the alkaloid. Carbonate of soda is also used as the precipitant, instead of ammonia, and the pre- cipitate is formed into a sulphate (disulphate) by being stirred with boiling water, 1 pint, to which sulphuric acid, 1 fl. scruple, or q. s., is subsequently added. The crystals, after di- gestion with prepared animal charcoal, 2 di-., are ordered to be dried at a beat not higher than 140° Fahr. 3. (Ph. D.) Yellow bark, 1 lb., is macerated for 24 hours in water, 2 quarts, acidulated with oil of vitriol, 2 fl. dr., and then boiled for half an hour, after which the fluid is de- canted ; this is repeated a second and a third time with water, 2 quarts, and oil of vitriol, 1 fl. dr.; the decanted (or strained) liquors are evaporated to a quart, and filtered, and slaked lime, 1 oz., or q. s., added to the solutiim until it exhibits a decidedly alkaline reaction ; the precipitate is next collected on a calico filter, and, after having been washed with cold water, partially dried on porous bricks, and -ubjected to powerful inta^ure enveloped in blotting paper, is boiled for 20 minutes in rectified spirit, 1 pint, and the liquid, after subsidence, decanted ; this is repeated a second and a third time with a fresh pint of spirit, and the resi- duum being well pressed, the mixed liquors are filtered, and the spirit removed by di.-tillation ; the brown viscid residaum is dissolved in boiling water, IG fl. oz., boiled, and dilute sul- phuric acid, i fl. oz , or q. s., added to render the solution neutral or only sliL'htly acid ; animal charcoal, i oz., is next stirred in, the mixture boiled (or about 5 minutes, filtered, and set aside to crystallise ; the cry.-tals are dried on blotting paper by mere exposure to a dry atmosphere. 4. (B. P.) Yellow cinchona bark, in coarse powder, 16; hydrochloric acid, 3; distilled water, a sufficiency; solution (^ drops of officinal sulphuric ether, with 20 drops of liquor of ammonia, must be added, and the whole well shaken while the top is closed by the thumb. The tube is then to be closely stopped, and shaken gently from time to time, so that the bubbles of nir may readily enter the layer of ether. If the salt be free from cinchonine and quinidine, or contain the latter in no greater proportion than Id", it will be completely dissolved; while on the surface, where contact of the two layers of clear fluid takes place, the mechanical impurities only will be separated. After some time the layer of ether becomes hard and gelatinous, and no further observation is possible." " From the above statement respecting the solubility of quinidine in ether, it appears that the 10 gr. of the salt examined may contain 1 gr. of quinidine, and still a complete solution with ether and ammonia may follow ; but in this case the quinidine will shortly begin to crystallise in a layer of ether. The least trace of quinidine may be yet more delinitely de- tected by employing, instead of the ordinary ether, s ine ether previously saturated with quinidine, by which means all of the quinidine contained in thequinine examined must remain undissolved. It is particularly requisite, in performing this last experiment, to observe, (immediately) after the shaking, »hether all has dissolved ; for. owing to the great ten- dency of quinidine to crystallisation, it may become again separated in a crystalline form, and be a source of error." " If more than 1-lOth of quinidine or (any) cinchonine be present, there will be lound an insoluble precipitate at the limits of the t\yo layers of fluid. If this be quinidine, it will be dissolved on the addition of proportionately more ether, while cinchonine wdl remain un- afl'ected." ^'ute. To Dr Ure's test Dr de Vrij prefers, for several reasons, Dr Kerner's test, ' Zeit- 1420 QUINOVIC ACID— RABBIT sohrift fiir Analytische Cheinie,' von Pre- senius, 1st Jahrg, 1862 ; ' Ueber Die Pruf ung des Kiiufliclien Schwefelsauren Chinins auf freinde Alkaloides,' von Dr G. Kerner. QUINOVIC ACID. CjsHasO,. This is in- soluble in water, also in chloroform, and diffi- cultly soluble in alcohol. It can be obtained from the boiling alcoholic solution, by coolingr, in small crystals. In the leaves, bark, and wood of the cinchona tree this acid is contiiined, to- gether with quinovin, and it is this mixture which hasbeeii recently applied in therapeutics, as a powerful tonic in cases of dysentery, &c. The mixture can easily be obtained from the leaves, bark, or wood of cinchona, and even from bark which has been exhausted by ebul- lition with water or diluted acids, by cold maceration with weak milk of lime, by which it is dissolved, as it combines easily with bases. It is only the quinovate of lime which has till now been used in medicine. — Dose, 2 to 8 gr. every two hours. ftUIKOVIN. CajH^gOg. Syn. Cikchovin, QUINOVIA. QUINOVIIT. A very bitter amorphous glu- coside contained in the genus Cinchona, Naus- lea, and probably in many other allied genera. It is insoluble in water, very soluble in recti- fied spirit and in chloroform, with which last liquid it forms, in concentrated solutions, a jelly. If a current of hydrochloric gas is passed into its alcoholic solution the liquid be- comes hot and the qiiinovin is split up into a peculiar klml of sujiar. aUIN'aUINA. Dr de Vrij states that the substance known under this name is a mixture of hydroehlorate of ciuchonidine and of cin- chonine. See Cinohoka. QUIN'SY. See Theoat AFFECTIONS. ftlTINTES'SElTCE. Syn. Quinta essentia, L. A term invented by the alchemists to represent a concentrated alcoholic solution of the active principles of organic bodies. It is still occasionally employed in perfumery and the culinary art. See EsBBNCE, Tinctuee, &c. QUIITOS. It generally shows itself at the top or coronet of the hoof of the horse, in the form of a fistulous opening (whence quittor is also called ' the pipes '), iilled with a purulent discharge. Quittor invariably points to the presence of an internal ulcer, abscess, or some other irritat- ing cause, the discharge from which, accumu- lating under the hard hoof, slowly works its way to the surface. The origin of quittor is generally some injury to the hoof, such as a corn, a prick, or an inequality of tread. The first thing to be done is to remove the animal's shoe, to cut away any dead or dis- coloured horn, so as to reach the seat of the suppuration, and to allow it to escape by a more direct outlet. Hot-water fomentations and poultices should afterwards be applied for a lew days. Should the sores show an in- disposition to heal, the parts should be washed with a tolerably strong solution of sulphate of zinc, or of bichloride of mercury — 25 grams of the latter to an ounce of water. The appli- cation of strong caustics is to be particularly deprecated. QTJOTID'IAK. Occurring or returning daily. See Ague. £AB'£IT. The Lepus cuniculvs (Linn.) of the Cuvian order Rodentia. The domestic rabbit, when young, is a light and wholesome article of food, approaching in delicacy to the common barn-door fowl; but lias less flavour than the wild animal. The fat is among the 'simples' of the Ph. L. 1618. Its hair and skin are made into cheap furs, gloves, hats, &C. Composition of Rabbit's Flesh (Baetlett).' 1 Ril)bit No. 1. Grains. Rabbit Nil. 2. Grams. Riibliit Nu. 3. Grains. Averajie Grains. Per- cent!! y;e, Griiiiis. Water Fibrin and Syntonin . . . Gelatin Pat Albumen ..... Alcoholic extract, including salts . Watery extract .... Calcium phosphates 5,982 1,143 302 240 276 106 102 16 6,623 1,247 335 272 305 119 108 19 7,315 1,393 350 345 340 135 125 25 6,640 1,261 329 286 307 120 112 20 73-17 13-90 3-63 315 3-38 132 1-23 0-22 Edible portion , Additional gelatin from stewing bones . Bones, &c., dissected out and stewed Shank bones, fur and eyes, thrown away 8,167 215 1,501 313 9,028 232 1,674 352 10,029 251 1,854 382 9,075 233 1 2,027 100-00 2-06 r 17-88 \ waste. 10,201 11,286 12,516 11,335 •Lancet,' March 29tli, 1873. RACAHOUT— RADICLE 1421 Rabbit Pie. Cut ap tn-o young rabbits, eeaion with white pepper, snlt, a little niuce, and nutmeg:, all in fine powder; add also a little Cayenne. Pack the rabbit with slices of ham, forcemeat balls, and hard egg', by turns in luyers. If it is to be baked iu a dish add a little wiiter, but omit the w»t>'r if it is to be raised in a crust. By the time it is taken out of the oven have ready a gravy of knuckle of veal, or a bit of the scrng, with some shank bones ol mutton, seasoned with herbs, onions, mace, and white pepper. If the pie is to be eaten hot, truffles, morels or mushrooms miiy be added, but nob if intended to be eaten cold. If it be made in a dish put as much gravy as will till the dish, but in raised crusts the gravy mu|t be carefully strained, and then put iu cold as jelly. Babbit Fndding. Cut a rabbit into sixteen pieces, and slice a quarter of a pound of bacon ; season with chopped sai^e, pepper, and salt ; then add potatoes and onions according to the size of the family, and hiilf a pint of water Boil for two hours. The meat and vegC' tables must be well mixed. Rice mny be substituted for potatoes if preferred. Sabbit, Ragout of. " Wash and clean a good-sized Ostend rabbit; boil the liver and heart, chop them, and mix with veal stuffing; till the rabbit, sew it up, and tie it into shape Put a piece of fat beef and 1 lb. of bacon, cut in slices, into n saucepan, with 1 oz. of dripping j put in the rabbit to brown, turning it over to brown both sides ; pour o(f the drip- ping, and put in 1 quart of water ; let it sim- mer gently an hour and a half. A quarter of an hour before serving skim o& all the fat, and thicken the gravy with a little corn flour; season with pepper and salt, and, if liked stew a bunch of herbs and half an onion with it. Lay the rabbit on a dish with the hncon round it, and pour the gravy over.' (Tfgctmeier.) RACAHOUT. Si/n. Racahout DKS Arabes This is said to be farina prepared from the acorns of Querms Sallota, or Barbary oak; disguised with a little flavouring. The fol- lowing is recommended as an imitation :— Roasted cacao or chocolate nuts, 4 oz. ; ta pioca, and potato farina, of each fi oz. ; white sugar, slightly flavoured with vanilla, i lb. Very nutritious. Used as arrow-root. RACE'UIC ACID. 5y». Paeatabtabic ACID. This compound was discovered by Eeatner in 1820, replacing tartaric acid in grape juice of the Dep«rtment of the Vosges. Racemic acid and tartaric acid have exactly the same composition, and yield, when exposed to heat, the same products ; the racemates also correspond in the closest manner with the tar- trates. Racemic acid is rather less soluble than tartaric, and separates first from a solu- tion contiiining the two acids. A solution of racemic acid precipitates a neutral salt of cal- cium, which is not the case with tartaric acid. A solntion of racemic acid does not affect a ray of polarised light, while a solution of tar- taric acid rotates the ray to the right. " Dessargnes and Jnngfleisch found by ex- periment that nnder the influence of heat ordinary tartaric acid is readily transformed into inactive tartaric acid and racemic acid, and the latter chemist tlionght to find in this fact an explanation of the production of racemic acid. " But observations continued throngh many years upon mother liquors from various tartaric acid factories showed that although more or less inactive tartaric acid was present in all of them, racemic acid was not, even when they had been subjected to prolonged treat- ment, and its occurence iu appreciable quan- tity was confined to a small number of speci- mens. In fact, some samples of mother liquor from factories where evaporation was carried on in a partial vacuum contained more racemic acid than others from factories where evapo- ration was carried on over a pure lire. Re- cently Jungfleisch noticed tliat the liquors richest in inactive tartaric acid were also rich in alumina, and the suspicion that alumina favoured the conversion was confirmed by direct experiment ; also that the neutral alumi- num sulphate has but little action. Jnngfleiscli has come to the conclusion that wlien there is an accumulation of alumina on the mother liquor, the conditions are favorable tor the production of a large proportion of inactive tartaric acid, and a small proportion of racemic acid, although when the latter is present in considerable quantity, it becomes the most manifest through its comparative insolubility. Examination of liquors from which racemic acid has been deposited has always shown them to contain much inactive tartaric acid. This theory does not exclude the probability that certain vines under particular conditions pro- duce racemic acid."' RACK'INO. See CiDKE and Wines. RAD'lCIiE. Syn. Radical. According to the binary theory of the constitution of saline compounds, every salt is composed, like chlo- ride of sodium (NaCl), of two sides or parts, which are termed its radicals. Tliat part of a salt which consists of a metal, or of a body exercising the chemical functions of one, is called the metallic, basic, or basylous radical ; while the other part, which, like chlorine, by combining with hydrogen would produce an acid, is designated the chlorous or acidulous radical. Every salt, therefore, consists of a basic and of an acid radical. Sometimes ra- dicals are elementary in their nature, when they are called simple; and sometimes they are made up of a group of elements, when they are termed compound. Some radicals, both simple and compound, have been isolated, while many have but a hypothetical existence. In the following tormulffi the vertical line separates the basic from the acid radicals, the * ' PliHrmuceuticiil Journal.' 1422 RADISH— RAIN-GAUGE former being on the left, the latter on the right : — H P Hydroflaorio acid {Fluoride of hydrogen). Na CI Chloride of sodium. K CN Cyanide of potassium. Ca OO3 Carbonate of calcium. NHj CI Chloride of ammonium C2H5 NO2 Nitrite of ethyl. BAD'ISE. The common garden radish (kaphanus, L.) is the root of Eaphanus sa- tivus (Linn.), one of the Cruciferce. There are several varieties. They are all slightly diuretic and laxative, and possess considerable power in exciting the appetite. The seed is pressed for oil. The horseradish (aemoeacia, li.) belongs to a distinct genus. KAIN-GATT6E. Syn. Ombometkc, Pm- yiAMETEB, Udometer. An instrument for determining the quantity of water, which falls as rain, at any given place. A simple and convenient rain-gauge for agricultural pur- poses is formed of a wide mouthed funnel, or open receiver, connected with a glass tube furnished with a stop-cock. The diameter of the tulie may be exactly 1-lOOth that of the receiver, and if tlie tube be graduated into inches and tenths, the quantity of rain that falls may be easily read off to the 1-lOOOth of an inch. The instrument should be set in some perfectly open situation; and, for agri- cultural purposes, with its edge as nearly level with the ground as possible. Another form of gauge is furnished with a float, the height of which marks the amount of liquid. The dia- meter of the gauge should not range between 4 and 8 inches. The quantity of water should be duly measured and registered at 9 a.m. daily. Mr Symonds, F.R.B.S., has drawn the fol- lowing code of instructions for the guidance of those registering the amount of rainfall at any locality : — 1. Site. A rain-gauge should not be set on ii slope or terrace, but on a level piece of ground, at a distance from shrubs, trees, walls, and buildings — at the very least as many feet from their base as they are in height. Tall growing flower.s, vegetables, and bushes must bo kept away from the gauges. If a thoroughly clear site cannot be obtained, shelter is most endurable from north-west, north, and east ; less so from south, south- east, and west; and not at all from south-west or north-east. 2. OW Gauges. Old-established gauges should not be moved, nor their registration discontinued, until at least two years alter a new one has been in operation, otherwise the continuity of the register will be irreparably destroyed. Both the old and the new ones must be registered at the same time, and the results recorded for comparison. 3. Level. The funnel of a rain-gauge must bo set quite level, and so firmly fixed that it will remain so, in spite of any gale of wind or ordinary circumstances. Its correctness in this respect should be tested from time to time. 4. Height. The funnel of gauges newly placed should be one foot above grass. In- formation respecting height above sea level may be obtained from G. J. Symons, Esq., 64, Camden Square, N.W., London. 5. Smt. If the funnel of a japanned gauge become so oxidised as to retain the rain .. in its pores, or threatens to become rusty, it should have a coat of gas tar or japan black, or a fresh funnel of zinc or copper should be provided. 6. Float Gauges. If the measuring rod is detached from the float it should never be left in the gauge ; if it is attached to the float it should be pegged or tied down, and only allowed to rise tD its proper position at the time of reading. To allow for the weight of the float and rod these gauges are generally so constructed as to show O only when a small amount of water is left in them. Care must always be taken to set the rod to the zero orO. 7. Can and Sottle Gauges. The measuring glass should always be held upright. The reading is to be taken midway between the two apparent surfaces of the water. 8. Date of Entry. The amount measured at 9 a.m. on any day is to be set against the previous one, because the amount measured at 9 a.m. of, say, the 17th, contains the fall during fifteen hours of the 16th, and only nine hours of the 17th. (The rule has been ap- proved by the meteorological societies of Eng- land and Scotland, cannot be altered, and is particularly commended to the notice of observers.) 9. Mode of Entry. If less than one tenth (•10) has fallen, the cipher must always be prefixed; thus, if the measure is full up to the seventh line, it must be entered as '07 — that is, no inches, no tenths, and seven hundredths. For the sake of clearness it has been found necessary to lay down an invariable rule that there shall always be two figures to the right of the decimal point. If there be only one figure, as in the case of one tenth of an inch (usually written '!), a cipher must be added, making it '10. Neglect of this rule causes much inconvenience. All columns should be cast tioiee — once up and once down — so as to avoid the same error being made twice. When there is no rain a line should be drawn ratlier than a cipher inserted. 10. Caution. The amount should always be written down before the water is thrown away. 11. Small Quantities. The unit of mea- surement being '01, observers whose gauges are sufficiently delicate to show less than that are, if the amount is under '005, to throw it away ; if it is -005 to '010 inclusive, they are not to enter it as '01. RAISINS— U ASH 1423 12. Abneace. Every obsn-ver should train some one as an osaiatant ; but where this is not possible, instructions should be given that the f^HUf^e should be emptied at 9 a.m. on tlie 1st of the month, and the water bottled, la- Iwlled, and tightly corked, to await the observer's return. 13. Heaiin Raint. When very heavy rains occur it is desirable to measure immediately on their termination ; and it will be found a safe plan, after measuring, to return the water to the gau;;e, so tbat the moruing registration will not bo interfered with. Of course, it there is the slightest doubt as to the gauge holding all the falls it must be emptied, the amount being previously written dowa. 1 1. Snaiu. In snow three methods may be adopted; it is well to try them all: — (1) Melt what is caught in the funnel by adding to the snow a previously ascertained quantity of warm water, and then deducting this quan- tity from the total measurement, enter the residue as rain, (2) Select a place where the snow has not drifted, invert the funnel, and, turning it round, lift and melt what is en- closed. (3) Measure with a rule the averaj;e depth of snow, and take one twelfth us the equivalent of water. Some observers uso in snowy weather a cylinder of the same diameter lis the rain-gauge, and of considerable depth. If the wind is at all rough all the snow is blown out of a flat-funnelled rain-gauge. 15. Overflow. It would seem needless to laiition observers on this head, but as a recent I'ureign table contains six instances in one day, ill which gauges were allowed to run over, it ii evidently necessary that British observers should be on the alert. It is not desirable to purchase any new gauge of wliich the capacity is loss than four inches. 16. Second Oanges. It is often desirable that observers should have two gauges, and chat one of them should be capable of holding eight inches of ruin. One of the gauges should he registered daily, the other weekly or monthly, as preferred, but always on the Ist of each month. By this means a thorough cheek is kept on accidental errors in the entries, which is not the Ciise if both are read daily. 17. Dew and Fog. Smnll amounts of water are at times deposited in rain-gauges by fog and dew. They should be added to the amount of rainfall, because (1) " they tend to water the earth and nourish the streams," and not for that reason only, but (2) because in many cases the rain-gauges can only be visited monthly, and it would then obviously he impossible to separate the yield ot snow, rain, &o. ; therefore, for the sake of uniformity, all must he taken together. 18. Doubtful Entries. Whenever there is the least doubt respecting the accuracy of any observation, the entry should be marked with a P, and the reason stated for its being placed there. Obs. The height at wliich the rain-gange is elevated from the ground is a matter of considerable moment. Thus, one observer found the fall of rain at York for twelve months (1833-1834) to be — at a height of 213 feet from the ground, 14-96 inches; at 44 feet, 19'85 inches ; and ou the ground, 25'71 inches. Later experimentalists have confirmed this curious fact. Thus, Colonel Warde found the following to be the relative rainfall at different periods for the four years extending from 1864 to 1867 : Inches. On a level with the ground . 107 At a height of 2 inches . .1-05 „ 6 ., . . 1 01 1 foct . . 1-00 „ 2 feet . . 0-99 3 „ . . 0-98 5 „ . . 0-96 10 „ . . 095 20 „ . . 0-94 Ono of the causes that have been assigned for this singular phenomenon has been — the greater exposure in elevated situa- tions of the rain to dispersive action of the wind, a surmise which derives some support from the circumstance, that when a rain-gauge is placed on a building, tiic roof of which is Hat, of large area, and with few, if any, chim- neys to distub the air currents, an amount of ruin is collected equalling that obtained on the surface of the ground. EAI'SINS. Sgn. Dried okapes ; Uvx (U. P.). VVM sioOAT*:, UvA (Ph. L ), Uva; pass.b (Ph. E. & D.), L. " The prepared fruit of Vitis vinifera" (hmn.) — Ph. L. The grapes are allowed to ripen and dry on the vine. After being plucked and cleaneil, they are dipped, fur a few seconds, into a boiling lye of wood ashes and quicklime at 12^ nr 15^^ Baume, to every 4 galls, of which a handful of culinary salt and a pint of salad oil lias been added ; they are then exposed for 12 m- 14 days in the sun to dry ; they arc, lastly, carefully garbled, and packed for exportation. Tlie sweet, fleshy kinds of grapes are those selected for the above treatment ; and, in general, their stalks are cut about one half through, or a ring of bark is rem'U'ed, to hasten their maturation. Raisins are nutritious, cooling, antiseptic, and, in general, laxative ; the latter to a greater extent than the fresh fruit. There are many varieties found in commerce. Their uses as a dessert and culinary fruit, and in the manu- facture of wine, d to the madder bath, to vary the shades of colour. Decoction of fustic, weld, logwood, quercitron, &c., are often thus emploxed, the mordants being modified accordingly. By adding bran to the madder bath the colour is said to be rendered much lighter, and of a more agreeable tint. RED GUM. A slight eruptive disease of infancy, occasioned by teething, and, less Ire- queutlv, by irritation from rimgh flannel worn next to the .«kin. See SlEOPHnLUS. KED LAV'ENDEE. See Timctueb of Lavendeb (Compound). KED LIQ'UOR. The crude solution of ace- tate or sulpho-acetate of alumina employed in calico printing. It is generally prepared by mixing crude sulphate of alumina with about an equal weight of crude pyrolignite of lime, both being in the state of solution. RED PIG'MENTS. The preparation of the principal red pigments are described under clieir respective names. The following list includes most of the reds in use : — Arme'nian Bole. 5y». Bole Abmenian ; Boms Abmeniji, L, Formerly imported from Armenia, Portugal, Tuscany, &c. ; now gene- rally made by grinding together a mixture of whiting, red oxide of iron, and red ochre, in nearly equal proportions. Bed, Brown. A factitious mixture of red oxide of iron and red ochre, in variable pro- portions. 1428 EEDUCTION— RE FRIG ERATION Car'miue. Caimina'ted Lake. Bed Chrome. Si/n. Dicheomate of iBir, Red cheomate of l. ; Plumbi noHEOMAB, P. CHEOMUS BXIBEUM, L. Frep. 1. Boil pure carbonate of lead with chromate of potassa, in excess, until it assumes a proper colour; then wash it well with pure water, and dry it in the shade. 2. Boil neutral chromate of lead with a little water of ammonia or lime water. 3. (Liebig and Woiiler.) Fuse saltpetre at a low red beat in a Hessian crucible, and throw in chromate of lead (pure chrome yel- low), by small portions at a time, as long as a strong ebullition follows upon each addition of the pigment, observing to stir the mixture frequently with a glass rod ; after repose for a minute or two, pour off the fluid part, and, as soon as the solid residuum is cold, wash it with water, and dry it by n gentle heat. Obs. Great care must be taken, in conduct- ing the last process, not to employ too much heat, nor to allow the saline matter to stand long over the newly formed chrome-red, as the colour is thus apt to change to a brown or orange. When well managed the product has a crystalline texture, and so beautiful a red colour that it vies with native cinnabar. The liquid poured from the crucible is reserved for manufacturing chrome yellow. Red, In'dian. Syn. PtTEPiB ochee ; Ochea PUEPUEEA Peesioa, T ebea Pbesica, L. This is a native production, brought from Ormus. A factitious article is prepared by calcining a mixture of colcothar and red ochre. Lakes (Various). Red, Light. From yellow ochre, by careful calcination. It works well with both oil and water, and produces an admirable flesh- colour by admixture with pure white. All the ochres, both red and y«llow, are darkened by heat. Red Ov'ange. Syn. Sandix. Obtained from white lead by calcinatim. Very bright. Keal'gar. Bisulphide of arsenic. Red Bole. See Aemenian and Veketian BOLE, (Ochres.) Bed Chalk. A clay iron ore, much used for pencils and crayons, and, when ground, also for paints. Red Lead. Syn. Minium. The finest red lead is prepared by exposing ground and elu- triated massicott, or dross of lead, in shallow iron trays (about 12 inches square, and about 4 or 5 inches deep), piled up on the hearth of a reverberatory furnace, to a heat of about 600 to 650° i'ahr., with occasional stirring, until it acquires the proper colour. The fur- nace employed for the preparation of massicot during the day usually possesses sufficient residuary heat during the night for this pro- cess, by which fuel is saved. Lead for the above purpose should be qiiite free from copper and iron. Red Ofchie. A natural product abounding on the Mendip hills. Red Or'pimeut. Syn. Red aesenic. Ter- sulphide of arsenic. Red Vene'tian. Syn. BoLrs Veneta, L. A species of ochre, brought from Italy, Rose Fiuk. This is whiting coloured with a decoction of Brazil wood to which a little pearlash has been added. A very pretty colour, but it does not stand. It is always kept in a damp state. The colour may be varied by substituting alum for pearlash, or by the addi- tion of a little spirits of tin. Vermil'ion. (See under that word.) REDUCTION. Syn. REVlviFlfcATioif. A term in its fullest sense applied to any opera- tion by which a substance is restored to its neutral state ; but now generally restricted, in chemistry, to the abstraction of oxygen, and hence frequently termed deoxidation or deoxidisement. This change is operated by either heating the substance in contact with carbon or hydrogen, or in exposing it to the action of some other body having a pow- erful affinity for oxygen. See Potassium, &c, REFI"1HNG. A term employed in com- mercial chemistry and metallurgy synony- mously with purification. The separation of the precious metals from those of less value, as in the operation of parting, constitutes the business of the ' refiner,' See Gold, Siltee, &c, REFRACTION (of Light). The deviation of a ray of light from its original path on entering a medium of a different density or power. For the practical application of this property, see Gems. REFRI"G£RANIS. Medicines or agents which tend to lessen the animal temperature without causing any marked diminution of sensibility or nervous energy. Among inter- nal relrigerants cold water, weak acidulous drinks, and saline aperients, are those which are probably the best known and the most useful. Among external refrigerants are cold water, evaporating lotions, weak solutions of subacetate of lead, &c, REFRIGERA'TION. The abatement of heat; the act or operation of cooling. Among the purposes to which refrigeratory processes are applied in the arts, the principal are — the condensation of vapours — the cooling of liquids — the congelation of water, and — the production of extreme degrees of cold in chemi- cal operations. The first of these is referred to under the heads Distilxation, Still, &c. , and the second under Woet. It is, therefore, only necessary to notice here the third and fourth applications of cold, artificially pro- duced, above referred to. The refrigeratory processes at present em- ployed depend upon the greater capacity for heat which the same body possesses as its density lessens, or its attenuation increases; as exhibited in the sudden liquefaction of solids. refrigeration'. 1429 the rapid evnpnration of liqnids, and tlie almost inetantaneoy tlioroughly steaming it. By this method, it is said, the loss of nitrogenous matter is prevented, and the grain coni-eqnently suffers no diminution of nutritive power, as in the case of boiling. 1436 RICINOLEIC ACID— RICKETS Fig. 1. Fig. 2. Microscopic appearance of Mice. Fig. 1 — Transverse section of the husk of rice. Fxo. 2 — A.ppenrance of husk as seen ia a transparent meclium of gt^cerin and ^um : a. Siliceous granules arrariged in longituilinal and transverse ridges, perforated by openinga — stomata, some having liaira over them. b c. Transverse and longitudinal, bntile, rouifh-edtred fibres, d, A Hue membrane of transverse angular cells; these overlie a very delicate membrane of large cells, e. . %Mm& ai{6 ^Q O Q Microscopic iippearance of ground rice-flour. EICINO'LEIC ACID. A variety of oleic i generally confined to chiltlhood, characterised acid discovered in saponified castor oil. by a lnrge head, prominent foreliead, protruded EICK'ETS. Syn. Rachitis, L. A disease, breast bone, flattened ribs, tumid belly, ema- RINGWORM— ROB 1437 elated limbs, and great gen»ral debility. The bono6, more particularly those of the spine and legs, become distorted, and exhibit a deficiency of earth V mutter ; the stools are frequent and loose, a slow fever succeeds, with cough, pain- ful and dilRcult respiration, and, unless the child ruUii's, atrophy is confirmed, and death eu»ut/s. When recovery takes place there is always more or less deformity left. The common causes of rickets are bad nurs- ing, exposure to damp and cold, and insuffi- cient nutrition, arising from the use of white bread containing alum, or any uf the per- nicious compounds vended nnder the niimi> of ' PAUINACEOUa FOOD,' ' INFANTS' F.,' ' PATENT F.,' &c. Rickets, like caries of the bones, is a diseusG which is scarcely known amongst in- fanta whose pap is made of pure wheaten bread, and whose mothers or nurses consume tlie same themselves. The treatment of rickets depends more on proper domestic management than on direct medication. Careful nursing, warm dry cloth- ing, thorough ventilation, moderate exercise, and, above all, a light nutritious mixed diet abounding in nitrogenous mutter and the phosphates, will do much to elfect a cure. To these may be added the administration of the milder chalybeate tonics, bark, or quinine, with occasional doses ot some mild aperient, as phosphate of soda, or, when there is diarrhoea, of rhubarb or some other tonic purge. The administration of small doses of phosphate of lime or of dilute phosphoric acid, frequently repeated, or, still better, the daily use of jelly made of pure ivory or bone shavings, will often effect wonders in tliose cases in which the bones are implicated from an apparent defi- ciency of e«rthy matter. See BuEiD, Faeina, NUBSING, &c. EING'WORM. Si/n. Scald-head; Pok- Bioo, L. The common ringworm, the pob- BIGO SCUTULATA of medical writers, is a disease that appears in circular patches of little pustules, which afterwards form scabs, leaving a red pimply surface, and destroying the bulbs of tile hair in its progress. It spreads rapidly, and is very infectious, often running through a whole school. It chiefly affects the neck, forehead, and scalp of weakly children, and frequently iirises without any apparent cause, but, in general, may be traced to uncleanuess, or contact with parties suffering from the disease. The treatment of ringworm consists in shavin;; the part, and keeping it clean with i-oap and water, at the same time that an occasional mild saline aperient is administered, and a light, nutritious diet, of which the red meat and ripe fruits should form a portion, be rigorously adhered to. When the scabbing commeucus, dressings of tar ointment, or of the ointment of nitrate or red oxide of mercury, or a mixture of equal parts of the first and either the second or third, should be applied, in each case diluting the mixture with suffi- cient lard to adapt it to the state of irritability of the part. During this treiitment the head should be covered with an ordinary nightcap, or some simple bandage, and not enveloped in a bladder or oil-skin case, as ia commonly the practice, since the complete exclusion of at- mospheric air tends to aggravate the disease. EI"PEiriNG. See Bbbwing, Malt li- (JlTOBS, Wine, 4c. EOAST'IKG. Alexis Soyer recommends, "as an invariable rule," that " all dark meats, such as beef and mutton, should be put down to a sharp fire for at least fifteen minutes, until the outside has acquired a coating of osmazome, or condensed gravy, and then removed back, and allowed to cook gently. Lamb, veal, and pork, if young and tender, should be done at a moderate fire. Veal should even be covered with paper. " Very rich meat, if covered with paper, does not require basting. Fowls, Ac, should be placed close to the fire, to set the skin, and in about ten minutes rubbed over with a small piece of butter, pressed in n spoon. Meats, whilst roasting, should be dredged with flour, just at the time when the gnivy begins to appear; the flour absorbs It, and forms a coating which prevents any more coming out. Hares and small game should be treated in the same manner." Under ordinary circumstances as to the fire, and the distance between it and the joint, beef, mutton, and veal, take about i hour per lb. in roasting. Lamb, poultry, and smiM game, require only 12 to 14 minutes per lb,; whilst veal takes fully 15 minutes, and pork takes from i hour to 20 minutes, as they must always be well done. The flesh of old animals requires more eouking than the Hesh of young ones ; and Inferior, tough, and bony parts thau the prime joints and pieces. Roasting is not an economical method of cooking pieces of meat abounding in bone or tendinous matter, since the nutritious portion of these is either destroyed or rendered inso- luble by the heat employed. Thus, the raw bones from a joint are capable of affording a rich and excellent basin of soup, higlily nutri- tious; whilst the bones from a corresponding joint which has been rousted are nearly worth- less when so treated. The same applies with even greater force to the gristly and tendinous portions. A dry heat either destroys them or converts them into a horny substance, unfit for food ; whilst by boiling they are trans- formed into a highly succulent and nutritious article of food, besides affording excellent soup or jelly. Hence the policy of 'boning' meat before roasting or baking it ; or, at all events, of removing the bony portion which would be most exposed to the action of the fire. See Bone and Jkixt. EOB. Syn. ROOB. A term, derived from the Arabic, formerly applied to the inspissated juice of ripe fruit, mixed with honey or sugar to the consistence of a conserve of thin 1438 ROCK— ROT estraot. Rob of elder-berries (eldeb eobj KOOB sAMBirci), juniper berries (juniper rob ; BOOB JtJifiPEBi), mulberries (mclbeeet hob ; hoob diamoeum), and walnuts (walnut eob ; EOOB dtacaeyon), witb a few others, are still found in some of the foreign Pharmacopoeias. SOCE. The popular name of a sweetmeat formed of sugar boiled to a candy, and then poured upon aa oiled slab, and allowed to cool in the lump. It is variously flavoured. £OCK CRTS'IAL. Native crystallised silica. See Quartz. KOCE OIL. See Petroleum. SOCK SOAP. A native silicate of alumina ; used for crayons, and for washing cloth. SOCKETS. (In pyrotechny.) Prep. The CASES. — These are made of stout cartridge paper, rolled on a mould and pasted, and then throttled a little below the mouth, like the neck of a phial. The diameter should be ex- actly equal to that of a leaden ball of the same weight, and the length should be equal to 3J times the external diameter. Above the spindle there must he one interior diameter of composition driven solid. They are filled with the following mixtures, tightly driven in, and when intended for flight (sk¥-eookets), they are 'garnished,' and affixed to willow rods to direct their course. The COMPOSITION. — 1. (Marsh.) — a. For 2-oz. rockets. Fi ora nitre, 54i parts ; sulphur, 18 parts ; charcoal, 27i pirts ; all in fine p iwder, and passed through lawn. > 6. For 4-oz. do. From nitre, 64 parts; sulphur, 16 parts ; charcoal, 20 parts ; as the last. c. For Jib. to 1-lb. do. From nitre, 62f parts; sulphur, 15i parts; charcoal, 214 parts. 2. (Ruggieri.) — a. For rockets of |-inch diameter. From nitre, 16 parts; charcoal, 7 parts ; sulphur, 4 parts. b. For |- to 1 J -inch rockets, use 1 part more of nitre. V. For If-inch rockets, use 2 parts more of nitre. d. By using 1 part less of charcoal and adding respectively 3, 4, and 5 parts of fine steel filings, the above are converted into ' Brilliant fires.' e. By tlie substitution of coarse cast-iron borings for filings, and a further omission of 2 parts of charcoal from each, the latter are con- verted into ' Chinese pire.' Hand-eookets and ground-rockets are usually loaded with nothing but very fine meal gunpowder and iron or zinc filings or borings. After bet-eockets and watee-eockets are charged, a piece of clay is driven in, through which a hole is pierced, and the ' head ' or 'garniture' filled with stars, and a little corn- powder is then applied. See Fibeb, Stars, and PrEOTEOHNT. KOLliS. A variety of fancy bread, gene- rally in the form of email semi-cylindrical cakes, prepared by the bakers, and intended to be eaten hot for breakfast. They differ from ordinary fine or French bread, as it is called, chiefly in containing more water. Some are wetted up witb milk and water, and are hence called ' milk rolls.' EOLL (Wine). Prep. Soak a French roll or sponge-biscuit in raisin, marsala, or sherry wine, surround it by a custard or cream thick- ened with eggs, and add some spice and orna- ments. BOOT. '8i/n. Radix, L. That part of a plant which imbibes its nourishment from the soil or medium in which it grows. In popular language, bulbs, corms, tubers, &c., are im- properly inclnded under this term. KO"FIN£SS. See Mali liquors and Wines. KHYPOPH'AGON. Prep. From yellow soap, sliced, 1 oz. ; soft soap (finest), 3 oz. ; melt them by the heat of hot water, then allow them to cool a little, and stir in of oil of cloves, 4 dr. ; essence of ambergris, 10 drops. It is kept a month before sale. Ust;d for shaving. EOSE. 8yn. Rosa, L. The typical genus of the natural order Rosacea. It includes numerous species greatly prized as garden plants. Rose, Cabbage. Syn. Hundred-leaved rose; RoS^ OKNTIFOLIJB PETALA (B. P.), Rosa cbntifolia (Ph. L. & E.), L. "The fresh petals " (Ph. L.) of this species are used in medicine. Odorous and slightly astringent and laxative. See Waters and Syrup. Eose, Dog. The Rosa canina, or wild briar. See Hips. Eose, French. Syn. Red eose; RosiE UALLIC^ PETALA (B.P.), RoSA GALLIOA (Ph. L. E. & D.), L. " The fresh and dried unex- panded petals" (Ph. L.) of this species are officinal. The white claws of the petals are removed before drying them. Uses, ^e. The red rose is an elegant astringent and tonic, and, as such, is used as the basis of several pharmaceutical prepara- tions. See Confection, Honeys, Infusion, and Syrup. SOSE'IIAEY. Syn. Rosmarinus (Ph. L. E. & D.) The flowering tops of Rosmarinus officinalis (Linn.), or the common rosemary of our gardens, are officinal in the Ph. E. & D. ; as is also the oil (oleum rosmarini) in the B. P. and Ph. L. The odour of both is refresh- ing, and they are reputed carminative, em- menagogue, and neurotic. The dried leaves are occasionally used by the hysterical and hypochondriacal as a substitute for China tea. The oil is an ingredient in Hungary water, and is much used in various cosmetic compounds, under the presumption of its encouraging the growth of hair and improving its quaiitv. EOSE PINK. See Red piqments. EO'SIN. See Resin. EOSY-DEOP. See AcNB. EOT. Syn. Greatkot, Htdeophio e., ROT— EUBIDIUM 1439 Shekf b., Wet b. A disease peculiar to abeep, produced by the prescace in the liver of the DUtoma hepalica, a parasite commonly known under the name of "a fluke." Rot prevails during very wet or rainy sensons. The leading tymptoms are loss of Hesh and vivacity; the lipH and tongue look vivid, and the eyes sad and glassy; the pelt comes off on the slightest pull ; the breath is fetid, and the urine highly coloured and scanty ; and there is either black purging or obstinate costive- ness. The treatment consists in a change to a dry warm elevated situation, and a dry diet^ consisting of oats, barley meal, tail-wheat, Ac, to which some turnips, carrots, or man- f[e\ wurzel may be added, with a liberal supply of common salt, and a few grains of sulphur, daily. These last two substances form the active ingredients in Flesh's ' Patent Resto- rative.' See Meat, Disease of. BOT (in Timber). See Dbx bot. BOTA'TION (of Crops). The rotation or succession of crops is absolutely necessary for the successful and economical cultivation of the soils. Crops have been divided by agri- culturists into exhausting crops, restoring crops, and cleaning crops. The most exhaust- ing crops are usually considered to be those of com, but all those that are allowed to ripen tlieir seed iind which arc carried off the ground are also exhausting, but in different degrees. Even clover, tiires, and grass out green are considered as exhausting, but in a less degree than those that are allowed to ripen. Re- st' >riiig crops are such as are allowed to decay upon tiie ground, or are consumed upon it by douiestic animals. Cleaning crops are such lie are grown in drills, and undergo the usual operations of weeding, hoeing, &e. ; the ma- j'lrity of thes^e may also bo regarded as ex- hausting crops. An exhausting crop should iilwaysbe followed by a restoring or a cleaninff crop; or, where possible, by both combined. Crops should also succeed each other in such a way that the soil may not be exhausted of any one particular kind of nutriment. This is heat effected by so rotating the crops that plants which are nearly allied should not suc- ceed each other on the same soil, or, at all events, not more than once. See Aqbicdl- TUBE, Soils, &c. ROTTEN STONE. See Tbipoli. ROUGE. Syn. Toilet kocoe; Rougb VEGETAL, Rouse d'Espaone, Fr. Prep. Wiish safflowcr (any quantity) until the water comes off colourle>8; dry and pulverise it, and digest the powder in a weak solution of crystallised carbonate of soda; then place some fine cotton-wool at the bottom of a porcelain or glass vessel, pour the filtered tinctorial solution on this, and throw down the colouring matter, by gradually adding lemon juice or wbite-winc vinegar, until it ceases to produce a precipitate ; next woiili the prepared cotton in pure cold water, and dissolve out the colour with a fresh solution of soda; to the new solution add a quantity of finely powdered talc or French chalk, proportionate to the intended quality of rouge; mix well, and pre- cipitate with lemon juice, as before; lastly, collect the powder, dry it with great care, with as little heat as possible, and triturate it with a very small quantity of oil of olives, to render it smooth and adhesive. Obs. According to the best authorities, this is the only article which will brighten a lady's complexion without injuring the skin. The relative fineness and proportion of talc employed determines the quality of the rouge. It is applied by means of a camel-hair pencil, a small ' powder puff,' or a hare's foot. It is also employed under the form of ' pnmmade ' and 'crepons.' The last of these consist of pieces of white woollen crape, upon which the colouring matter of the carthamus has been precipitated, instead of upon the talc, noticed above. The following articles also pass under the name of rouge, and are used for the purposes named after each i — Bonge, Brown-red. Jeweller's rouge. Bonge, Chinese Card. This is said to be u 'carUuimate of soda;' it is colourless when applied, but, being decomposed by the acid se- cretions of the skin, acquires a most beautiful rose-like tint. (U'Sbaughnessy.) Boage, Jeweller's. Sesquioxide of iron pre- pareil by calcination. Used to polish gold,&c. Bouge, Liquid. The red liquid left from the preparation of carmine ; or a solution of car- mine in weak carbonate of potash water, or of pure rouge in alcohol acidulated with acetic acid. Bonge, Indienne. The terra persica, or Indian red ; imported from Orinuz. Bouge de Frusse. Light red or burnt yellow ochre. See Red pigments. Bonge, Spanish Lady's. This is cotton wool which has been repeatedly wetted with an ammoniaial solution of carmine, and dried. It is applied like 'ronge crepons.' Bonge d'Athenes, Vert. Syn. Pube bouge. See Caethamine. BOUGH'ENING. See \Vi>-es. BUBEFA"CIENTS. Syn. Rubepacientia, L. Substances or agents which, when applied for a certain time to the skin, occasion a red- ness and increase of heat, without blistering. They act as counter-irritants. Mustard, pow- dered ginger (both ma<1e into a paste with water), hartshorn and oil, and ether and spirit of wine (when their evaporation is prevented), are familiar examples of this class of reme- dies. BUBE'OLA. See Measles. BUBIA'CIN. An orange-coloured substance, obtained (rom madder. BUBID'IUM. [Eng., L.] A metal belong- ing to the alkaline group discovered by Bunsen and KirchbofE by means of spectrum analysis. It is found in many mineral waters associated with caesium. 1440 RUBY— BUST EU'BY. See Gems and Pastes. EUB. Syn. ViVTM. FOWA, RuTA (Ph. L. & E.), L. " The leaf Ruta graveolena." (Ph. L.) A powerful antispasmodic, diuretic, and stimulant. It is also reputed nervine and em- menagogiie. The fresh leaves are powerfully acrid, and even vesicant ; but they Tjecome milder in drying. — Dose. Of the powder, 15 to 30 gr., twice or thrice daily ; in hysteria, flatulent colic, &c. See Infdsion and Oils (Volatile). EUM. Syn. Spieitus .Iamaoiehsis, Spi- ElTns SACCEABi, L. An ardent spirit ob- tained by distillation from the fermented skimmings of the sugar-boilers (syrnp scum), the draiuings of the sugnr-pots and hogsheads (molasses), the washings of the boilers and other vessels, together with sufficient recent cane juice or wort, prepared by mashing the crushed cane, to impart the necessary flavour. The sweet liquor before fermentation com- monly contains from 12 to X6% of saccharine, and every ten gallons yield from one to two gallons of rum. The average strength of rum, as imported into this country, is about 20 o.P. Like all other spirits, it is colourless when it issues from the still, but owing to the taste of the consumer the distiller is compelled to colour it before it leaves his premises. Ohs. Rum is imported from the West In- dies. The best comes from Jamaica, and is hence distinguished by that name. Leeward Island rum is less esteemed. The duty on rum is 10s. 2d. per proof-gallon if imported direct from any of the British Colonies (Colo- nial rum), but 10*. hd. if from any other part of the world (foreign rum). The consumption of rum has long been declining in England ; its place being chiefly supplied by gin. Rum owes its flavour to a volatile oil and butyric acid, a fact which the wary chemist has availed himself of in the manufacture of a butyric compound (essence of rum) for the especial purpose of enabling the spirit dealer to manufacture a factitious rum from malt or molasses spirit. In Jamaica it is usual to put sliced pine apples into the puncheons con- taining the finer qualities of rum, which is then termed pine-apple mm. See Alcohol, Spibit, &c. RUM, BAY, E Rother's Formula for. According to an American authority, true bay rum is made from Fimenta acris {Myrica acris, Schwartz; Myrtus acris, Willd.), and not from Laurus nobilis, as commonly supposed; the method of its dis- tillation not being known outside the West Indies, it has been customary to make it extemporaneously with the oil of bay distilled from the leaves of the former plant. This preparation is inferior in fragrance, however, to the genuine article. The following formula of R. Rother is said to give very good results. Take of oil of b.ayberry, 1 fl. oz.; Jamaica rum, 1 pint ; strong alcoliol, 4 pints j water, 3 pints. Mix the rum, alcohol, and water, then add the oil; mix and filter. EUPEET'S DEOPS. These are made by letting drops of melted glass fall into cold water. By this means they assume an oval form, with a tail or neck resembling a retort. They possess this tingular property that, if a small portion of the tail is broken off, the whole bursts into powder with an explosion, and a considerable shock is communicated to the hand. EUPIA. This is an affection of the skin attended by the formation on it of vesicles, that develop into ulcers which copiously dis- charge a fonl, unhealthy, and reddish matter. After a time this matter hardens and forms a thick incrustation over the sores. The best treatment is to put the patient upon a generous diet, including wine, and to administer iodide of potassium with sarsa- parilla or quinine. The scabs should be poul- ticed. EXJP'TUEE. See Suboeey. RUSKS. Prep. From 4 eggs ; new milk and warm water, of each \ pint; melted but- ter and sugar, of each i lb. ; yeast, 3 table- spoonfuls ; beat well together with as much flour, added gradually, as will make a very light paste ; let it rise before the fire for half an hour, then add a little more flour, form into small loaves or cakes 5 or 6 inches wide, and flatten them ; bake these moderately, and, when cold, cut them into slices of the size of rusks, and put them into the oven to brown a little. A nice tea-cake when hot, or with caraways, to eat cold. Plain busks are made by simply cutting loaves of bread into slices, and baking them in a slow oven to the proper colour. EUS'ffiA. An arsenical iron pyrites, found in Galatia, which, when reduced to powder, and mixed with half its weight of quicklime, is used by the Turkish ladies to make their * PSILOTHEONS,' Or Compounds to remove super- fluous hair. See Depilatoet. RUST. Syn. RuBiQO, L. The coating or film of oxide or carbonate which forms on the surface of several of the metals when exposed to a moist atmosphere; more particularly, that which forms on iron or steel (eekbi hy- BEATE ; HYDEATED, SESQDIOXIDB OF lEON ; EEREUaO, PEEEI EUBIGO). To prevent iron or steel goods rusting, it is merely necessary to preserve them from damp or moisture. In the shops, small articles in steel are, commonly, either varnished or en- closed in quick-lime finely pulverised; large articles are generally protected with a coating of plumbago, or of boiled oil, or some cheap varnish, applied to them, previously gently heated. Surgical instruments are frequently slightly smeared with a little strong mercurial ointment, with the same intention. Spots of rust may be removed from the sur- face of polished iron or steel by rubbing them with a little tripoli or very fine emery made RUTHENIC ACJD— RTE 1441 into a paste with nweot oil ; or, chemically, by H mixture of polisher's putty-pjwdcr with a little oxalic acid, applied with water. When the last is employed, the articles should be afterwards well rinsed in pure water, then wiped dry, »nd finished off with a warm and dry rubber, in order to remove every trace of acid. HUTHENIC ACID. 5y». Ruthknio anht- DBIOB (RiiOj). This may be procured by heating any of the preceding oxides with potassic nicruto. Kutbenio acid is insoluble in water. Enthenic Sesqnioxide. (RujO^) ; occurs in the anhydrous form when the metul is ignited in a current of air. It is the most stable of the baHic oxides of the metal. Alkalies fail to dissolve it. With acids it forms soluble salts of a yellow colour; when, to n solution of these, an alkali is added, a bulky blackish- brown precipitate of the hydra ted oxide, having the composition Ru^OSg, SH^O, is thrown down. There are three chlorides of ruthenium : — RuClj ; RuCls ; and RuClj. EUIHEN'IUM. (Ru. = 104-2.) A metnl dis- covered by Claus, associated with iridium, in the residue from crude platinum, which is insoluble in aqua regia. It forms smnll anguliir mnsneH, with a metallic lustre; is very brittle and infusible; resists the action of acids, but reaililv oxidises when heated in the air. Sp. gr. H to 11-4. In Fremy's process for sepnrating osmium from the residues of platinum ore, ruthenium occurs in a dioxide. By beating this dioxide in a current of oxygen, the metal may be obtained in the form of a powder of dark grey colour. With oxygen, ruthenium forms four com- pounds :—RuO ; RujOa; RnO„; and RuOj. Euthenium Trichloride (RtiClj), which is the most important of the chlorides, may be procured by dissolving the Bcquioxide in hydrochloric acid. The solution beini; evapo- rated, the trichloride occurs as a greenish-blue deliquescent mass, wliicti is soluble in alcohol. Tests. In solutions of the trichh>riile, hydro- gen sulphide gives a brown precipitate of rutheniesesquisulphide, the supernatant liquid being of a bright blue eulour. This reaction i< a very delicate as well as a very character- istic one. Metallic zinc reduces the yellow trichloride to the blue dichloride, the inetiil being after- wards precipitated as a black powder. Pluui- bicaietatcgive-sa purplisli-red pr'CiiiitKte,mer- curie cyanide a blue one, the supernatant liquid beine: also blue. The caustic and carbonated alkalies, throw down a black precipitate of sesqnioxide of ruthenium, which is insoluble in exiess of the precipitant. If the salts of ruthenium are boiled with sodic forniiate or oxalate the solution becomes colourless, hut no precipitate of reduced nietjil takes place. ET£. Syn. Sboale, L. The seed of Kio. 1. — Transverse section of testa, 8ic. x 108. Kio. 2 — CoaU i» iM Horn mthom. x 170. a, Eiternnl ; h, Middle ; c, Internal coat j i, Starch jtrams. x 108. VOL. II. 91 1442 SABADILLA— SACHET Secale cereale, a gramineous plant, the native country of which is undetermined. It is a more certain crop and reqnires less culture and manure than wheat, and is hence largely cultivated in Germany, Russia, and in the northern parts of Europe, where it is exten- sively employed for bread. VVlien roasted it is occasionally used as a sub.stitute for ciifEee. It furnishes an excellent malt for the distilla- tinn of spirit, and is mucli used iu the making of Hollands. Eye bread is very likely to cause diarrhoea iu those unaccustomed to partake of it. By continued use, however, this inconveuience disappears. Bye bread is acid and dark in colour. It is about equal in nutritive power to wheat. It is less abundant than wheat in librin, but richer in casein and albumen. The foregoing plate represents the micro- scopic appearance of rye. Sommer recommends the microscopic exa- mination of rye flour to be conducted as fol- lows : — The flour is placed on a glass slide, and moistened with water ; a single drop of oil of vitriol is added, and a small disc is laid upon it. If, now, it be viewed with a magnifying power of 200, the starch grains of wheat and rye are seen to dissolve in a uniform manner, hut the grains of barley starch, after losing their external coat, break up into a number of polyhedrons before their solution is com- pleted. Eye, Spurred. See EnaoT. SABADIL'LA. iSyn. Ceeadilla, Ckva- DiLiA, Sabadixla U*- P. Ph. E.), L. Tlie dried fruit {Asagreea officinalis). A drastic and dangerous cathartic, occasionMlly used in tapeworm ; and, externally, to destroy pedi- culi, but, even for this purpose, when the scalp has been denuded or ulcerated, it has some- times caused death. It is now used chiefly as a source of verateinb. SA'BLE. The Mustella Zihellina (Linn.), a small quadruped of the uiartin-cat family, found iu Northern Asia. Its fur is remarkable for its fine quality and rich colour, and (or the hairs turning with equal ease in every di- rection. The skins of the rabbit, cat, &c., dressed, painted, and lustred, are sold under the nsme of commok or uoce: sable. SABOTlEEE. [Fr.] An apparatus of pe- culiar construction, employed by tlie French confectioners for making ices. It consists of a pail to contiiin a freezing mixture, and an inner vessel for the creams to be iced. It may be used with a mixture of pounded ice and salt, or any other freezing mixture. The pail and cream vessels being loaded, and closely covered, an alternate rotatory motion is given to the apparatus by means of the handle, for 10 or 15 minutes, care being taken to occa- sionally SCI ape down the frozen portion of the cream from the sides, by means of a wooden spoon. See Ices and Refeigekation. SACCHAE'IC ACID. Syn. Oxalhydeic ACiDf. A compound, resulting from the ac.ion of dilute nitric acid on sugar. SAC CHABINE. The technical name of the uncrystallisahle sugar found in malt-wort. SACCHARINE FESHEIITATIGir. This occurs during the germination and kiln-drying of grain in the operation of malting, and in the mashing of malt in brewing. The sweet- ening of bread during its exposure to heat in the oven is also included under this head by many writers. The substance which most powerfully excites the sugar fermentation was first shown by Payen and Persoz to be a peculiar principle to which they have given the name of ' dias- tase.' This is always present in good malt, and possesses the singular property of con- verting STAECH successively into gum (dex- trin) and sugar, at a temperature ranging between 149° and 168° Fahr. During the action of this substance on starch it is itself decomposed; and when the sugar fermentation ceases it is found to have entirely disappeared. It is the presence of diastase in malt which alone converts the starch of tlie grain into sugar during the operation of mashing with hot water ; and hence the absolute necessity of employing water at the proper temperature, as on this depends the strength and sweetness of the wort, and consequently its fitness for un- dergoing the vinous fermentation, and for making beer. Vegetable albumen and gluten also possess the property of exciting the sac- charine fermentation, but in a considerably inferior degree to diastase. The sugar formed during the germination of seeds containing starch results from the action of diastase, and disappears as soon as the woody fibre (lignin), which has a similar con- stitution, is developed, forming the skeleton of the young plant. (Liebig.) See Bbewing, Diastase, Dextrin, &c. SACCHAEOm'ETEE. An instrument simi- lar in principle to the common spirit hydro- meter, but so weighted and graduated as to adapt it for the indication of the richness of malt-worts in sugar, or saccharine, expressed in pounds per barrel, or the excess of gravity over that of water, the lust being taken at 1000. See Beewino, Syeup, Wobt, &e. SACH'ET. Syn. Saccwlus, L. Sachets (sACcnu) are little bags containing dry sub- stances, used for the external medication of parts, or for communicating agreeable per- fumes to wearing apparel, drawers, furniture, &c. Those belonging to perfumery are com- monly filled with mixtures of (ragrunt vegeta- ble substances, reduced to coarse powder, and differ from those employed for pot pourri chiefly in being used in the dry state. Sac- cnli are now seldom employed in this coun- try in legitimate medicine. See Powdeks (Scented), &c. Sachet, Ammoniacal. Syn. SAccuirs am- MONiACALis. Prep. Equal parts of sal am- moniac and quicklime are mixed, and sprinkled SACK— SAFFRON 1143 between cotton wadding, which is to be quilted in muslin. Sachet, Anodyne. (Qiiinpy.) 8i/n. Sac- OOWSAKODYNCS. Prfp. Cljiimorailes, 1 oz. ; bay berries, 1 oz. ; Iiivender flower, i oz. : hen- bune seiid, 1 dr. ; opium, 1 dr. To be dipped in hot spirits. Sachet, Anti-phthisic. Si/n. Saccdlits anti- pnTursicna. L. Prep. Dissolve of aloes, 1 oz., in strong decoction of fresh rue, i jiint; next fold a piece of soft muslin in eight fold'' large enough to cover the chest and part of the ■tomach ; steep this in tlie decoction, and dry it in the shade ; lastly, place in a small bag, one side of which is formed of scarlet silk or wool, and the other, intended to be worn next the skin, of the finest net or gauze. A cele- brsted domestic remedy fur consumption and aetliina. It is intended to be constantly worn on the che-t. Sachet, Besolr'ent. S^n. MsLTiNa baq ; SACCrLUS BE80LVKNS, L. Prep, 1. (Dr Brcslau.) Iodide of potassium, 1 part ; sal ammoniac, 8 parts ; dry, and reduce Citch si'pii- nitcly to fine powder; mix them, and enclose i oz. to 1 oz. of the mixed powder in a small hag of linen or silk. Used as a resolvent to indolent tumours, especially goitres and scro- fnlous indurations. It should be worn on the part iiigiit and day for some time. The part next the skin should be well pricked with a needle, ami the powder shaken up and read- justed every 2 or 3 days ; and it should be reneweil about once a fortnight. 2. (Trousseau & Ileveil.) Iodide of potas- sium, 1, part; burnt sponge, 4 parts; fine saw- dust, 6 parts ; as before. Sachet, Sponge. St/n. SACCtTLirs sfonoii, CoLLlKB DB MoBAND. Prep. Muriate of ammonia, chloride of radium, burnt sponge, of cich 1 oz. ; mix, sprinkle the powder im a piece of cotton wool, and quilt between muslin, in the form of a cravat. To be worn con- stantly in eoitre or bioucliocele, renewing it every month. Sachet, Stomachic. (Fuller.) Si/n. Sac- CCira. Prep. Alint, 4 dm.; wormwood, thyme, red roses, each 2 drm. ; balastines, angelica mot, caraway seed, nutmeg, mace, cloves, of each 1 drm. Coarsely powder tlie ingredients, and put them into a bag, to be moistoned with hot red wine when applied for flatulence. SACK. (From sec, Fr., dry.) A wine used by our ancestors, supposed by some to have Ixen Rhenish or Canary ; but, with more probability, by others, tn have been dry mountain — vin d'Espagne ; vin sec— (How- ell, • Fr. and Kng. Diet.,' 1650). Fiilstaffi calls it ' sherris sack ' (sherry sack), from Xeres, a sea town of Corduba, where that kind of sack (wine) is made. (Blount.) At a later * In "^li ike*pe ire's ifiy lack whs nrcnaionally adulte- rniod witli II. IIP. ;iii we ItHrii from KiitBtatTa speech lo tlie Dravcr: " You rugae, there's lime in lliis sack." period the term came to be used as a general name for all sweet wines. SAF'FIiOWEK. Si/n. Bastard saffron. Dteb's b. ; Cabthamus, L. The florets of Carlhamut iinctoriut, a plant cultivated in Spain, Egypt, and the Levant. It contains two colouring principles — the one yellow, an. I the other red. The first i< removed by water, and is rejected. The second is easily dissolved out by weak solutions of the carbonated alka- lies, and is again precipitated on the additi.m of an acid. This property is taken advantnfjo of in the manufacture of rou^^e, and in dyeing silk and cotton. The most lively tints of cherry, flame, flesh, orange-re